CN107998025A - A kind of Mongollian Thyme Herb essential oil mosquito-repellent perfume and preparation method - Google Patents
A kind of Mongollian Thyme Herb essential oil mosquito-repellent perfume and preparation method Download PDFInfo
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Abstract
The present invention relates to a kind of Mongollian Thyme Herb essential oil mosquito-repellent perfume and preparation method, include the component of following parts by weight：0.5~5 part of Mongollian Thyme Herb essential oil, 0.1~0.8 part of elsholtzia splendens essential oil, 3~8 parts of Flos Lonicerae extractive solution, 3~8 parts of dandelion Chinese violet extracting solution, 0.1~0.3 part of glycerine, 0.1 0.3 parts of glycerin monostearate.The present invention extracts essential oil, prepares Mongollian Thyme Herb essential oil mosquito-repellent perfume using the free of contamination Mongollian Thyme Herb of green natural as raw material.Using Mongollian Thyme Herb essential oil, elsholtzia splendens essential oil as mosquito repellent active ingredient, active ingredient using honeysuckle as repellent antipruritic, elsholtzia splendens essential oil, dandelion, Chinese violet complex role under, substantially increase Mongollian Thyme Herb essential oil volume repelling effect, the irritation to skin is avoided at the same time, avoid skin dry, while also have and eliminate the clearing heat and detoxicating effect that bite by mosquitos causes red and swollen pain of itching.
Description
Technical field
The present invention relates to a kind of Mongollian Thyme Herb essential oil mosquito-repellent perfume and preparation method, belong to household chemicals technical field.
Background technology
Floral water species currently on the market is various, and the main active of floral water is mostly conventional synthesis culicifuge,
Such as dimethyl phthalate (BAAPE), repefral (DMP), Metadelphene (DEET).But there is studies have shown that dimethyl phthalate and keep away
Mosquito amine has toxic side effect, and in use, people absorb part dimethyl phthalate by alimentary canal, respiratory tract, can not only induce
The diseases such as asthma, long-time service can also carcinogenic, teratogenesis；Metadelphene can cause children's encephalopathic, nettle rash syndrome, allergic reaction,
Blood pressure is low and heartbeat reduces etc..In addition, floral water currently on the market also has a big feature, by adding a large amount of essence, meet
Accreditation of the consumer for smell, causes essence to be excessively used.
Therefore, develop the floral water of natural source, can obvious mosquito repellent and natural aromatic smell, instead of adding in floral water
Metadelphene, dimethyl phthalate and the essence added, meets using the increasingly urgent health of crowd and environmental requirement, promotes floral water innovation hair
Exhibition, is of great practical significance.Now some researches show that various plants extract is according to there is good repelling effect, such as perfume
Thatch oil, nim oil, eucalyptus oil, basil, peppermint oil, caryophyllus oil, lemon oil etc..
In order to reach refrigerant and repellent antipruritic effect, the floral water of existing market usually also adds menthol and salicylic acid,
But menthol and salicylic acid have skin strong and stimulating, while easily make skin hair shaft, therefore, the use of existing floral water is relaxed
Appropriateness has much room for improvement.
Mongollian Thyme Herb Thymus quinquecostatus Celak., also known as palmate meadowsweet, are Labiatae (Labiatae) thyme
Platymiscium, while be also a kind of important medicinal plant, spice berry and lawn plant.With expelling pathogenic wind from the body surface, ventilation analgesic, stops
Cough antihypertensive effect, be mainly used for treat cold headache, cough, pertussis, epigastric pain, indigestion, vomiting and diarrhoea, toothache,
The diseases such as difficulty and pain in micturition, acute gastroenteritis, hypertension, eczema itch, sore, carbuncle and painful swelling.《Zibo book on Chinese herbal medicine》Described in " Mongollian Thyme Herb gives birth to hill,
Gas fragrance, can mosquito repellent ", Shandong it is among the people dried after, light, sootiness, utilize its aromatic odor mosquito repellent.In addition, also use
Its herb dried makees the insect prevention thing of clothes, fur goods and felt, or dry herb is made sachet, be put in wardrobe,
In pillow, with mosquito repellent；But the repelling effect of Mongollian Thyme Herb is weaker than the repelling effect of conventional synthesis culicifuge, auxiliary mosquito repellent can only be done,
Effect is irritating to the skin at the same time, easily makes skin dry, while also do not possess antibacterial and repellent antipruritic function.
The content of the invention
In view of the deficiencies of the prior art, the present invention provides a kind of Mongollian Thyme Herb essential oil mosquito-repellent perfume and preparation method, the present invention
Floral water natural source traditional Metadelphene, dimethyl phthalate and the essence of material substitution, in addition to significant repelling effect, also
With antibacterial and repellent antipruritic effect；Action temperature and, skin irritation is small, after use without dry skin feel, usage comfort
Improve, while its mosquito repellent effectiveness time is grown, and does not contain essence.
Technical scheme is as follows：
A kind of Mongollian Thyme Herb essential oil mosquito-repellent perfume, includes the component of following parts by weight：
0.5~5 part of Mongollian Thyme Herb essential oil, 0.1~0.8 part of elsholtzia splendens essential oil, 3~8 parts of Flos Lonicerae extractive solution, dandelion-purple
3~8 parts of flower Chinese violet extracting solution, 0.1~0.3 part of glycerine, 0.1-0.3 parts of glycerin monostearate.
According to the present invention preferably, Mongollian Thyme Herb essential oil mosquito-repellent perfume, includes the component of following parts by weight：
0.5~4 part of Mongollian Thyme Herb essential oil, 0.3~0.6 part of elsholtzia splendens essential oil, 3~5 parts of Flos Lonicerae extractive solution, dandelion-purple
3~5 parts of flower Chinese violet extracting solution, 0.2~0.3 part of glycerine, 0.2-0.3 parts of glycerin monostearate.
Preferable according to the present invention, the Mongollian Thyme Herb essential oil is steam distillation 3-5h extractions after Mongollian Thyme Herb is soaked
It is made.
Preferable according to the present invention, the elsholtzia splendens essential oil is after will elsholtzia splendens be soaked, and vapor steams
3-5h extractions are evaporated to be made.
Preferable according to the present invention, the Flos Lonicerae extractive solution is that ultrasound carries after Flos Lonicerae extractive solution is soaked
20-30min is taken to be made.
Preferable according to the present invention, the dandelion-Chinese violet extracting solution is to mix dandelion flower, Chinese violet
Afterwards plus boiling 1-3h, filtrate concentration are made.
According to the present invention, a kind of preparation method of Mongollian Thyme Herb essential oil mosquito-repellent perfume, including step：
1) prepared by Mongollian Thyme Herb essential oil：After Mongollian Thyme Herb is soaked, steam distillation 3-5h extraction Mongollian Thyme Herb essential oils；
2) prepared by elsholtzia splendens essential oil：After elsholtzia splendens is soaked, steam distillation 3-5h extraction elsholtzia splendens essences
Oil；
3) Mongollian Thyme Herb essential oil and elsholtzia splendens essential oil are uniformly mixed according to a ratio, obtain Mongollian Thyme Herb-elsholtzia splendens essential oil；
4) prepared by Flos Lonicerae extractive solution：After Flos Lonicerae extractive solution is soaked, ultrasonic extraction 20-30min；
5) prepared by dandelion-Chinese violet extracting solution：After dandelion flower, Chinese violet mixing plus boiling 1-3h, filtrate are dense
Contracting；
6) Flos Lonicerae extractive solution is sufficiently mixed with dandelion-Chinese violet extracting solution by proportioning, obtain honeysuckle-dandelion-
Chinese violet extracting solution；
7) Mongollian Thyme Herb-elsholtzia splendens essential oil, glycerine, glycerin monostearate are added to honeysuckle-dandelion-purple by proportioning
In flower Chinese violet extracting solution, stir evenly, stand, ageing is filling, up to Mongollian Thyme Herb essential oil mosquito-repellent perfume.
Preferable according to the present invention, in step 1) prepared by Mongollian Thyme Herb essential oil, and Mongollian Thyme Herb crushed 40-60 mesh sieves, add Mongollian Thyme Herb
The water of 8-12 times of weight, soaks 1-3h, steam distillation extraction 3-5h, collects distillate, be Mongollian Thyme Herb essential oil.
Preferable according to the present invention, in step 2) prepared by elsholtzia splendens essential oil, and it is thick that elsholtzia splendens is ground into 15-25 purposes
Powder, adds the water of 8-12 times of elsholtzia splendens weight, soaks 1-3h, steam distillation extraction 3-5h, collects distillate, be Haizhou
Elsholtzia cilita essential oil.
Preferable according to the present invention, in step 1), step 2), the vapo(u)rizing temperature of steam distillation is 95-99 DEG C, distillate
24~30h is cooled down at 2~10 DEG C.
Preferable according to the present invention, in step 4) prepared by Flos Lonicerae extractive solution, and honeysuckle is added deionized water immersion 1-
3h, it is 80-150W to be placed in power, and under frequency 30-60KHZ ultrasound conditions, ultrasonic extraction 20-30min, filtering, filtrate is concentrated into
1ml obtains Flos Lonicerae extractive solution equivalent to traditional Chinese medicine honeysuckle 0.5g.
Preferable according to the present invention, in step 5) prepared by dandelion-Chinese violet extracting solution, by dandelion flower, pale reddish brown
Fourth is by weight (1-2)：After the ratio mixing of (1-2), add dandelion flower, the boiling 1-3h of 7-8 times of Chinese violet weight, mistake
Filter, filtrate are concentrated into 1ml equivalent to dandelion-Chinese violet 0.2g, obtain dandelion-Chinese violet extracting solution.
Advantages of the present invention and effect：
1st, the present invention extracts essential oil, prepares Mongollian Thyme Herb essential oil mosquito-repellent perfume using the free of contamination Mongollian Thyme Herb of green natural as raw material.
Due to containing plurality of active ingredients in Mongollian Thyme Herb essential oil, there is lasting fragrant simple and elegant fragrance, the cineole in component contained therein
Have with camphanone to insect and preferably walk quickly and keep away and fumigation action；Linalool has stronger pharmacological activity such as sedation and analgesia, anti-Jiao
Worry, hypnosis, antibacterial, anti-inflammatory, antineoplastic action, in addition, also containing synthesis d-Bomeol, and synthesize d-Bomeol also known as ice
Piece, has the function that to refresh the mind.Therefore floral water made of can not only avoid the addition of essence, suitable for people of all ages, and have
Good mosquito repellent, anti-inflammatory, inducing resuscitation function, have human body any stimulation.
2nd, the present invention using Mongollian Thyme Herb essential oil, elsholtzia splendens essential oil as mosquito repellent active ingredient, using honeysuckle as repellent antipruritic
Active ingredient, elsholtzia splendens essential oil, dandelion, Chinese violet complex role under, substantially increase Mongollian Thyme Herb essential oil volume mosquito repellent
Effect, while the irritation to skin is avoided, avoid skin dry, while also there is elimination bite by mosquitos to cause redness to be itched bitterly
Clearing heat and detoxicating effect.
Embodiment
Technical scheme is described further with reference to embodiment, but protection scope of the present invention is not limited to
This.
Raw material in embodiment is commercially available convenient source unless otherwise specified.
Embodiment 1：
A kind of Mongollian Thyme Herb essential oil mosquito-repellent perfume, component are as follows：
1 part of Mongollian Thyme Herb essential oil, 0.5 part of elsholtzia splendens essential oil, 3 parts of Flos Lonicerae extractive solution, dandelion-Chinese violet extracting solution 3
Part, 0.3 part of glycerine, 0.3 part of glycerin monostearate.
Preparation method, step are as follows：
1) prepared by Mongollian Thyme Herb essential oil
After Mongollian Thyme Herb is ground into 60 mesh fine powders, the water of 10 times of Mongollian Thyme Herb weight is added, 3h is soaked, pours into distilling apparatus, water
3h is extracted in steam distillation, and the vapo(u)rizing temperature of steam distillation is 96 DEG C, collects distillate, is Mongollian Thyme Herb essential oil；Distillate is in 5 DEG C
Lower cooling 24h, it is spare；
2) prepared by elsholtzia splendens essential oil
Elsholtzia splendens is ground into 20 mesh coarse powder, adds the water of 11 times of elsholtzia splendens weight, 3h is soaked, pours into distilling apparatus
In, steam distillation extraction 3h, the vapo(u)rizing temperature of steam distillation is 97 DEG C, collects distillate, is Mongollian Thyme Herb essential oil；Distillate
24h is cooled down at 5 DEG C, it is spare；
3) prepared by Mongollian Thyme Herb-elsholtzia splendens essential oil
Mongollian Thyme Herb essential oil is mixed with elsholtzia splendens essential oil by proportioning and is shaken up, obtains Mongollian Thyme Herb-elsholtzia splendens essential oil；
4) prepared by Flos Lonicerae extractive solution
Honeysuckle is added into deionized water immersion 2h, it is 100W to be placed in power, and under frequency 40KHZ ultrasound conditions, ultrasound carries
20min is taken, is filtered, filtrate is concentrated into 1ml equivalent to traditional Chinese medicine honeysuckle 0.5g, obtains Flos Lonicerae extractive solution.
5) prepared by dandelion-Chinese violet extracting solution
By dandelion flower, Chinese violet by weight 1:1 ratio mixing, adds 7 times of amount deionized waters and decocts 1h, filter
Cross, filtrate is concentrated into 1ml equivalent to dandelion-Chinese violet medicinal material 0.2g, spare；
6) prepared by honeysuckle-dandelion-Chinese violet extracting solution
Flos Lonicerae extractive solution is mixed with dandelion-Chinese violet extracting solution by proportioning, is sterilized,
7) prepared by floral water
Mongollian Thyme Herb-elsholtzia splendens essential oil, glycerine, glycerin monostearate are added to honeysuckle-dandelion-Chinese violet to carry
Take in liquid, stir evenly, stand, ageing is filling, up to Mongollian Thyme Herb essential oil mosquito-repellent perfume.
Embodiment 2：
A kind of Mongollian Thyme Herb essential oil mosquito-repellent perfume, component are as follows：
1.5 parts of Mongollian Thyme Herb essential oil, 0.1 part of elsholtzia splendens essential oil, 4 parts of Flos Lonicerae extractive solution, dandelion-Chinese violet extracting solution
4 parts, 0.2 part of glycerine, 0.2 part of glycerin monostearate.
Preparation method is the same as embodiment 1.
Comparative example 1
A kind of Mongollian Thyme Herb essential oil mosquito-repellent perfume, with embodiment 1, difference is component, and Haizhou is replaced with P-Cymene
Elsholtzia cilita essential oil.
Preparation method is the same as embodiment 1.
Comparative example 2
A kind of Mongollian Thyme Herb essential oil mosquito-repellent perfume, component is with embodiment 1, and difference is, it is fragrant which does not include Haizhou
Ru essential oils.
Preparation method is the same as embodiment 1.
Experimental example：
First, repelling effect is tested
The verification of repelling effect
Attack experiment must be carried out to the volunteers and aedes albopictus for participating in experiment, experiment is with reference to GB/ before testing
13917.9-2009 method carries out.Method is：300 test worms are put into the mosquito cage of the long a height of 40cm*30cm*30cm of * wide *,
By the skin of the back of the hand exposure 4cm*4cm of testing crew, remainder stretches into after tightly covering and 2min is placed in mosquito cage, comes to stop
More than 15 persons of the test worm fallen are qualified for attack, and this person and mosquito cage can be used for repellency test.In the aspiration of attack qualification
The both hands back of personnel respectively draws the skin surface of 5cm*5cm, and a hand presses 1.5 μ lcm-2Dosage uniformly smear respectively it is real
The floral water of a 1-2 and comparative example 1-2, the skin of exposure 4cm*4cm therein are applied, another hand also exposes the skin of 4cm*4cm
Skin, smears commercially available floral water and is tightly covered as control, remainder.2h after daubing medicament, attack qualification is stretched into by hand
2min in mosquito cage, observation, which whether there is mosquito, is come to suck blood, and later 1h is tested 1 time, as long as there is 1 mosquito to come to suck blood to be judged to repellent
Agent fails, and records the effective protecting time of Mongollian Thyme Herb essential oil mosquito-repellent perfume and Liushen toilet water, and test effect see the table below 1.
Scattering ratio/%=(control aedes albopictus number-processing aedes albopictus number)/control aedes albopictus number * 100
1 scattering ratio of table and mosquito repellent time
| Project | Scattering ratio % | Repelling effect (time) |
| Embodiment 1 | 98.58 | 10.2 |
| Embodiment 2 | 96.76 | 8.4 |
| Comparative example 1 | 67.84 | 5.2 |
| Comparative example 2 | 62.13 | 4.8 |
| Control group | 82.78 | 6.7 |
The results show that the Mongollian Thyme Herb essential oil mosquito-repellent perfume of the present invention has stronger repelling effect, to the repellent of aedes albopictus
Rate is more than 96.76%.Comparative example 1 replaces elsholtzia splendens essential oil with P-Cymene, and comparative example 2 is to remove elsholtzia splendens essence
The dosage of oil but increase Mongollian Thyme Herb essential oil, comparative example 1 and 2 groups of volunteers, which test display, imitates the avoidance effect and mosquito repellent of aedes albopictus
Fruit is decreased significantly compared with embodiment 1 and embodiment 2, and the increase of floral water elsholtzia splendens essential oil of the invention is to Mongollian Thyme Herb essential oil
Repelling effect has castering action, has synergistic function, and have significant repelling effect；In embodiment 1 and embodiment 2
In, floral water prepared by embodiment 1 has stronger repelling effect.
2nd, lasting fragrance is tested
Using normal 200 subjects of sense organ as object on probation, 4 groups are randomly divided into, every group of 50 people, smear the skins such as hand, foot
Skin exposed section, continuous one month, respectively evaluates fragrance after 4,8,12h.According to lasting more than 12h persons, 10 points are obtained；Hold
Continuous 8-12h person, obtains 8 points；Continue 4-8h person, obtain 6 points；Continue 4h and following person, obtain 4 points, carry out assigning a point evaluation.It the results are shown in Table 2.
The 2 lasting fragrance time of table
| Project | Lasting fragrance |
| Embodiment 1 | 9.4 |
| Embodiment 2 | 8.6 |
| Comparative example 1 | 7.9 |
| Comparative example 2 | 6.3 |
The result shows that：The lasting fragrance of embodiment 1 and embodiment 2 and degree of recognition in 200 subjects is higher.
3rd, anti-microbial property test
Using Escherichia coli, staphylococcus aureus agent as strain, anti-microbial property survey is carried out to sample using concussion flask method
Examination, the anti-microbial property of sample are evaluated by bacteriostasis rate, and testing result is shown in Table 3.
The anti-microbial property test result of 3 finished products of table
| Project | Escherichia coli bacteriostasis rate % | Staphylococcus aureus bacteriostasis rate % |
| Embodiment 1 | 94 | 91 |
| Embodiment 2 | 87 | 90 |
| Comparative example 1 | 72 | 68 |
| Comparative example 2 | 57 | 59 |
| Control group (Long Liqi) | 71 | 64 |
As seen from the above table, finished product of the present invention is equal to Escherichia coli, staphylococcus aureus compared with common commercially available floral water
There is notable fungistatic effect.
4th, repellent antipruritic effect
Using 200 bite by mosquitos volunteers as research object, using parallel control as principle, 5 groups, every group 40 are randomly divided into
People, respectively implements 1,2 group, contrasts 1,2 group and control group (Long Liqi floral water).After bite by mosquitos skin, floral water is taken to apply
Locate in bite by mosquitos is red and swollen, smear dosage to cover red and swollen area to spend, observe and record the repellent antipruritic curative effect in 3min and
Action number of cases.Wherein curative effect judging standard：With red, swollen, hot, pain, itching rapidly disappears to be effective；Red, swollen, hot, pain, disappearance of itching are
Generally；Red, swollen, hot, pain, itching does not mitigate or aggravates to be invalid.
4 repellent antipruritic effect of table
| Project | Repellent antipruritic curative effect | Action number of cases |
| Embodiment 1 | Effective 33 effective 6 invalid 1 | 39 |
| Embodiment 2 | Effective 31 effective 9 invalid 0 | 40 |
| Comparative example 1 | Effective 26 effective 8 invalid 6 | 34 |
| Comparative example 2 | Effective 21 effective 10 invalid 9 | 31 |
| Control group | Effective 24 effective 12 invalid 4 | 36 |
The result shows that the floral water containing Mongollian Thyme Herb essential oil of the invention can substantially eliminate as caused by bite by mosquitos it is red, swollen,
Heat, pain, the symptom such as itch, and embodiment 1 and embodiment 2 are superior to control group；And the repellent antipruritic of comparative example 1 and comparative example 2
Effect is below control group.Illustrate that there is synergistic make between each components Component of floral water containing Mongollian Thyme Herb essential oil in the present invention
With repellent antipruritic effect can be significantly increased.
Claims (10)
1. a kind of Mongollian Thyme Herb essential oil mosquito-repellent perfume, includes the component of following parts by weight：
0.5~5 part of Mongollian Thyme Herb essential oil, 0.1~0.8 part of elsholtzia splendens essential oil, 3~8 parts of Flos Lonicerae extractive solution, dandelion-pale reddish brownly
3~8 parts of fourth extracting solution, 0.1~0.3 part of glycerine, 0.1-0.3 parts of glycerin monostearate.
2. Mongollian Thyme Herb essential oil mosquito-repellent perfume according to claim 1, it is characterised in that include the component of following parts by weight：
0.5~4 part of Mongollian Thyme Herb essential oil, 0.3~0.6 part of elsholtzia splendens essential oil, 3~5 parts of Flos Lonicerae extractive solution, dandelion-pale reddish brownly
3~5 parts of fourth extracting solution, 0.2~0.3 part of glycerine, 0.2-0.3 parts of glycerin monostearate.
3. Mongollian Thyme Herb essential oil mosquito-repellent perfume according to claim 1, it is characterised in that the Mongollian Thyme Herb essential oil is by Mongollian Thyme Herb
After soaking, steam distillation 3-5h extractions are made；The elsholtzia splendens essential oil is after will elsholtzia splendens be soaked,
Steam distillation 3-5h extractions are made.
4. Mongollian Thyme Herb essential oil mosquito-repellent perfume according to claim 1, it is characterised in that the Flos Lonicerae extractive solution be by
After Flos Lonicerae extractive solution is soaked, ultrasonic extraction 20-30min is made；The dandelion-Chinese violet extracting solution is by Pu
After public English flower, Chinese violet mixing plus boiling 1-3h, filtrate concentration are made.
5. the preparation method of the Mongollian Thyme Herb essential oil mosquito-repellent perfume described in claim 1, including step：
1) prepared by Mongollian Thyme Herb essential oil：After Mongollian Thyme Herb is soaked, steam distillation 3-5h extraction Mongollian Thyme Herb essential oils；
2) prepared by elsholtzia splendens essential oil：After elsholtzia splendens is soaked, steam distillation 3-5h extraction elsholtzia splendens essential oils；
3) Mongollian Thyme Herb essential oil and elsholtzia splendens essential oil are uniformly mixed according to a ratio, obtain Mongollian Thyme Herb-elsholtzia splendens essential oil；
4) prepared by Flos Lonicerae extractive solution：After Flos Lonicerae extractive solution is soaked, ultrasonic extraction 20-30min；
5) prepared by dandelion-Chinese violet extracting solution：After dandelion flower, Chinese violet mixing plus boiling 1-3h, filtrate concentrate；
6) Flos Lonicerae extractive solution is sufficiently mixed with dandelion-Chinese violet extracting solution by proportioning, obtains honeysuckle-dandelion-pale reddish brown
Chinese violet extracting solution；
7) by proportioning by Mongollian Thyme Herb-elsholtzia splendens essential oil, glycerine, glycerin monostearate with being added to honeysuckle-dandelion-pale reddish brown
In fourth extracting solution, stir evenly, stand, ageing is filling, up to Mongollian Thyme Herb essential oil mosquito-repellent perfume.
6. the preparation method of Mongollian Thyme Herb essential oil mosquito-repellent perfume according to claim 5, it is characterised in that Mongollian Thyme Herb in step 1)
Prepared by essential oil, Mongollian Thyme Herb crushed 40-60 mesh sieves, add the water of 8-12 times of Mongollian Thyme Herb weight, soaks 1-3h, steam distillation extraction
3-5h, collects distillate, is Mongollian Thyme Herb essential oil.
7. the preparation method of Mongollian Thyme Herb essential oil mosquito-repellent perfume according to claim 5, it is characterised in that Haizhou in step 2)
Prepared by Elsholtzia cilita essential oil, elsholtzia splendens is ground into the coarse powder of 15-25 mesh, adds the water of 8-12 times of elsholtzia splendens weight, soaks 1-
3h, steam distillation extraction 3-5h, collects distillate, is elsholtzia splendens essential oil.
8. the preparation method of the Mongollian Thyme Herb essential oil mosquito-repellent perfume according to claim 6 or 7, it is characterised in that step 1), step
It is rapid 2) in, the vapo(u)rizing temperature of steam distillation is 95-99 DEG C, and distillate cools down 24~30h at 2~10 DEG C.
9. the preparation method of Mongollian Thyme Herb essential oil mosquito-repellent perfume according to claim 5, it is characterised in that gold and silver in step 4)
Prepared by flower extracting solution, honeysuckle is added deionized water immersion 1-3h, it is 80-150W to be placed in power, and frequency 30-60KHZ is ultrasonic
Under the conditions of, ultrasonic extraction 20-30min, is filtered, and filtrate is concentrated into 1ml equivalent to traditional Chinese medicine honeysuckle 0.5g, obtains honeysuckle extraction
Liquid.
10. the preparation method of Mongollian Thyme Herb essential oil mosquito-repellent perfume according to claim 5, it is characterised in that Pu in step 5)
Prepared by public English-Chinese violet extracting solution, by dandelion flower, Chinese violet by weight (1-2)：After the ratio mixing of (1-2), add
The boiling 1-3h of dandelion flower, 7-8 times of Chinese violet weight, filtering, filtrate are concentrated into 1ml equivalent to dandelion-Chinese violet
0.2g, obtains dandelion-Chinese violet extracting solution.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109055054A (en) * | 2018-10-11 | 2018-12-21 | 山东大学齐鲁医院 | A kind of mosquito-expelling and antipruritic handmade soap and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103704277A (en) * | 2013-11-26 | 2014-04-09 | 延安常泰药业有限责任公司 | Application of thymus quinquecostatus volatile oil to prepare culicifuge |
| CN105616237A (en) * | 2014-10-31 | 2016-06-01 | 郁丁丁 | Floral water |
| CN106727166A (en) * | 2017-03-14 | 2017-05-31 | 张立源 | A kind of repellent antipruritic floral water |
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2017
- 2017-12-20 CN CN201711387656.3A patent/CN107998025B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103704277A (en) * | 2013-11-26 | 2014-04-09 | 延安常泰药业有限责任公司 | Application of thymus quinquecostatus volatile oil to prepare culicifuge |
| CN105616237A (en) * | 2014-10-31 | 2016-06-01 | 郁丁丁 | Floral water |
| CN106727166A (en) * | 2017-03-14 | 2017-05-31 | 张立源 | A kind of repellent antipruritic floral water |
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| 张云: "四种植物精油对蚊虫的熏杀活性及酯酶活性的影响", 《中国生物防治学报》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109055054A (en) * | 2018-10-11 | 2018-12-21 | 山东大学齐鲁医院 | A kind of mosquito-expelling and antipruritic handmade soap and preparation method thereof |
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