CN107117867A - A kind of SiO2Grey dawn textured man-made stone diamond stone sheet material and its production technology - Google Patents
A kind of SiO2Grey dawn textured man-made stone diamond stone sheet material and its production technology Download PDFInfo
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- CN107117867A CN107117867A CN201710358729.XA CN201710358729A CN107117867A CN 107117867 A CN107117867 A CN 107117867A CN 201710358729 A CN201710358729 A CN 201710358729A CN 107117867 A CN107117867 A CN 107117867A
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B26/00—Compositions of mortars, concrete or artificial stone, containing only organic binders, e.g. polymer or resin concrete
- C04B26/02—Macromolecular compounds
- C04B26/10—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C04B26/18—Polyesters; Polycarbonates
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B26/00—Compositions of mortars, concrete or artificial stone, containing only organic binders, e.g. polymer or resin concrete
- C04B26/02—Macromolecular compounds
- C04B26/04—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C04B26/06—Acrylates
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B26/00—Compositions of mortars, concrete or artificial stone, containing only organic binders, e.g. polymer or resin concrete
- C04B26/02—Macromolecular compounds
- C04B26/10—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C04B26/12—Condensation polymers of aldehydes or ketones
- C04B26/122—Phenol-formaldehyde condensation polymers
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B26/00—Compositions of mortars, concrete or artificial stone, containing only organic binders, e.g. polymer or resin concrete
- C04B26/02—Macromolecular compounds
- C04B26/10—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C04B26/14—Polyepoxides
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B26/00—Compositions of mortars, concrete or artificial stone, containing only organic binders, e.g. polymer or resin concrete
- C04B26/02—Macromolecular compounds
- C04B26/10—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C04B26/16—Polyurethanes
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/54—Substitutes for natural stone, artistic materials or the like
- C04B2111/542—Artificial natural stone
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/80—Optical properties, e.g. transparency or reflexibility
- C04B2111/82—Coloured materials
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
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Abstract
A kind of SiO of the present invention2Grey dawn textured man-made stone diamond stone sheet material and its production technology, including the 1. mesh quartz sand of major ingredient 40 70,70 100 mesh quartzs, 600 mesh ultrawhite silica flours, 325 mesh silica flours；2. the mesh quartz sand of auxiliary material 40 70,70 100 mesh quartzs, 600 mesh ultrawhite silica flours, 325 mesh silica flours；3. A colors gas phase SiO2, B color gas phases SiO2, C color gas phases SiO2；4. D mixture of colours mill base；5. colored pigment；Silane coupler；Unsaturated polyester resin；Curing agent；The artificial quartz in lump that the present invention makes is handsome in appearance, and pattern is distinct, and color is unique, and decorative pattern forms uniqueness；The species and style of artificial quartz in lump are enriched similar to a kind of fish maw shape decorative pattern, the decorative pattern of arbitrariness can be made by mould of different shapes；By producing dislocation combination, production efficiency is high, effectively reduces the fraction defective of product, can mass production.
Description
Technical field
The invention belongs to quartz technical field, specifically, it is related to a kind of SiO2Grey dawn textured man-made stone diamond stone plate
Material and its production technology.
Background technology
In building decoration field, stone material with its it is attractive in appearance, graceful, ornamental strong the features such as turned into primary decoration material it
One.All the time, natural marble figue it is abundant, naturally, because its natural decorative effect, texture and by extensive use, but
Due to there is resource-constrained, there is aberration in large area paving and different degrees of radioactivity is exceeded, and hardness is low, and easy scratching etc. is asked
Topic, limits its comprehensive development to a certain extent.
Artificial quartz in lump be by quartz sand powder be main stuffing, using unsaturated polyester resin as adhesive, in vacuum shape
The Novel stone that high pressure is compressing under condition, shape under middle temperature state, it is a kind of "dead" pollution, the repeatable ring utilized
Guarantor, green building material and ornament materials.
Although artificial quartz in lump rich color is gorgeous, radiationless, wear-resisting, pressure-resistant, anti scuffing, anticorrosive, anti-aging, antiseepage
Thoroughly, but be due to without marmorean native texture and color, artificial quartz in lump class is cannot get big raising.It is domestic at present
The outer diamond plate for having imitating natural marble, but color is relatively stiff, and texture is unnatural.Meanwhile, pattern type artificial quartz in lump
Due to complex process, low production efficiency, and sheet material, the color in pressing process is easily interpenetrated sheet material, and fraction defective is high, from
And causing the supply of material few, price is high.
Therefore, it is necessary to carry out upgrading or technological transformation to existing production technology.
The content of the invention
Instant invention overcomes shortcoming of the prior art, there is provided a kind of SiO with natural marble stone material texture2Fish maw
Spend line artificial quartz stone plate and its production technology in vain, good product performance, production efficiency is high, and qualification rate is high.
In order to solve the above-mentioned technical problem, the present invention is achieved by the following technical solutions：
A kind of SiO2Grey dawn textured man-made stone diamond stone sheet material, including major ingredient 1. major ingredient 40-70 mesh quartz sand, 70-100 mesh
Quartz, 600 mesh ultrawhite silica flours, 325 mesh silica flours, unsaturated polyester resin, colored pigment；
2. auxiliary material 40-70 mesh quartz sand, 70-100 mesh quartz, 600 mesh ultrawhite silica flours, 325 mesh silica flours, unsaturation
Polyester resin, colored pigment；
3. A colors gas phase SiO2Compound, B color gas phases SiO2Compound, C color gas phases SiO2Compound；
4. D mixture of colours mill base；
5. silane coupler；Curing agent；
Further, a kind of SiO2Grey dawn textured man-made stone diamond stone sheet material, it is characterised in that according to parts by weight, institute
State 1. 10-15 parts of major ingredient 40-70 mesh quartz sand, 20-25 parts of 70-100 mesh quartzs, 600 1-5 parts of mesh ultrawhite silica flours, 325 mesh
10-20 parts of silica flour, 0.2 part of colored pigment, 5-10 parts of unsaturated-resin；
2. 5-10 parts of auxiliary material 40-70 mesh quartz sand, 10-15 parts of 70-100 mesh quartzs, 600 mesh ultrawhite silica flour 0.5-2
Part, 5-10 parts of 325 mesh silica flour, 0.05 part of colored pigment, 2-5 parts of unsaturated-resin；
3. A colors gas phase SiO20.1-0.2 parts of compound (0.05 part of colored pigment), B color gas phases SiO2Compound 0.05-0.1
Part (0.05 part of colored pigment), C color gas phases SiO20.05-0.1 parts of compound (0.15 part of colored pigment)；
4. 0.1-0.2 parts of D mixture of colours mill base
5. silane coupler 0.05-0.15 parts；0.05-0.15 parts of curing agent
Further, a kind of SiO2Grey dawn textured man-made stone diamond stone sheet material, it is characterised in that：The unsaturated polyester (UP)
Resin can also be the one or more in epoxy resin, phenolic resin, acrylic resin and polyurethane resin.
Further, a kind of SiO2Grey dawn textured man-made stone diamond stone sheet material, it is characterised in that：The colored pigment and
Mix the one or more that mill base is inorganic pigment or organic pigment or mill base.
Further, a kind of SiO2Grey dawn textured man-made stone diamond stone sheet material, it is characterised in that：The inorganic pigment is
The inorganic pigments such as titanium white, medium chrome yellow, iron oxide yellow, iron oxide red, barba hispanica, cadmium red, cadmium yellow, carbon black, iron oxide black, the organic pigment is bright red
Powder, azophosphine, dark green or phthalocyanine blue, the mill base are white slurry, black wash, bright red slurry, dark green slurry or phthalocyanine blue slurry.
Further, a kind of SiO2Grey dawn textured man-made stone diamond stone sheet material, it is characterised in that：The curing agent was
Aoxidize (2 ethyl hexanoic acid) tert-butyl ester, methyl ethyl ketone peroxide, peroxidized t-butyl perbenzoate, dibenzoyl peroxide and fat many
One or more in first amine.
Further, a kind of SiO2Grey dawn textured man-made stone diamond stone sheet material, it is characterised in that：The silane coupler
For γ-methacryloxypropyl trimethoxy silane, γ-(2,3- the third oxygen of epoxy) propyl trimethoxy silicane, N- β (ammonia
Ethyl)-γ-aminopropyltriethoxy dimethoxysilane, N- (β-aminoethyl)-gamma-aminopropyl-triethoxy-silane, N- β (ammonia second
Base)-γ-aminopropyltrimethoxysilane, anilinomethyl triethoxysilane, gamma-aminopropyl-triethoxy-silane, vinyl three
One or more in Ethoxysilane, vinyltrimethoxy silane and γ-chloropropyl triethoxysilane.
Compared with prior art, the beneficial effects of the invention are as follows：
A kind of SiO of the present invention2Grey dawn textured man-made stone diamond stone sheet material and its production technology, that makes is artificial
Quartz is handsome in appearance, and pattern is distinct, and color is unique, enriches the species and style of artificial quartz in lump, while production efficiency is high,
The fraction defective of product is effectively reduced, can mass production.
Embodiment
The preferred embodiments of the present invention are illustrated below, it will be appreciated that preferred embodiment described herein is only used
In the description and interpretation present invention, it is not intended to limit the present invention.
The present invention, a kind of SiO2Grey dawn textured man-made stone diamond stone sheet material, including the following raw material：According to parts by weight：1. lead
Expect 13.5 parts of 40-70 mesh quartz sand, 21.5 parts of 70-100 mesh quartz, 600 1.5 parts of mesh ultrawhite silica flours, 325 mesh silica flours 15
Part, 8.8 parts of unsaturated polyester resin, 0.2 part of colored pigment；
2. 7.8 parts of auxiliary material 40-70 mesh quartz sand, 11 parts of 70-100 mesh quartz, 600 1 part of mesh ultrawhite silica flours, 325 mesh
8 parts of silica flour, 4.5 parts of unsaturated polyester resin, 0.05 part of colored pigment；
3. A colors gas phase SiO25.5 parts of compound (0.05 part of colored pigment), B color gas phases SiO20.5 part of (coloured face of compound
0.05 part of material), C color gas phases SiO20.5 part of compound (0.15 part of colored pigment)；
4. 0.2 part of D mixture of colours mill base；
5. 0.1 part of silane coupler；0.1 part of curing agent；
A kind of SiO2The production technology of grey dawn textured man-made stone diamond stone sheet material, comprises the following steps：
(1) each material each component is weighed according to formula；
(2) stir：The quartz sand, silica flour, silane coupler that step (1) is 1. weighed to major ingredient are stirred in double planetary
It is pre-mixed in bucket；The curing agent mixed, decoration colored pigment and unsaturated polyester resin are poured into double planetary agitator
It is middle to be mixed, then add silica flour and mixed.15~55Hz of stirring frequency, 180~600s of mixing time；
2. the quartz sand, silica flour, silane coupler for step (1) being weighed into auxiliary material are premixed in double planetary agitator
Close；The curing agent mixed, decoration colored pigment and unsaturated polyester resin are poured into and mixed in double planetary agitator
Close, then add silica flour and mixed.15~55Hz of stirring frequency, 180~600s of mixing time；
3. the major ingredient 1. and 2. mixed and auxiliary material are pre-mixed in double planetary agitator；
4. weigh 1/3 it is 3. mixed expect in double planetary agitator, add A color gas phases SiO2Compound carries out low speed and stirred
Mix to uniform；
5. compound will be 4. stirred in double planetary agitator, add B color gas phases SiO2Compound and C color gas phases SiO2
Compound continues to stir, untill multi-level color occurs in stirring material.
(3) cloth：1：SiO is got out in advance2Grey dawn pattern mould is put into charge car, then by the thing 3. mixed
Material feeding beater is further broken up, into material distributing machine in cloth, cloth should flood SiO2Grey dawn pattern mould；2. start pre-
The press material good to cloth carries out precompressed；3. charge car is lifted, SiO2Grey dawn pattern mould lifts and feed separation；4. will 5.
Mixing gained compound is filled into SiO2Grey dawn pattern mould is hollowed out in lines, D mixture of colours mill bases is poured 5. mixed
Compound in, institute leach-color slurry should be into line style；
(4) suppress：After cloth is completed, repressed vibration equipment is compressing under -0.1Mpa vacuum condition, pressure
50~200t, 30~55Hz of vibration frequency, 60~600s of time；
(5) heat cure：After vibration compacting, into curing apparatus, solidify at a temperature of 80~130 DEG C, hardening time
For 30~180 minutes；
(6) after the completion of solidifying, room temperature it is to be cooled completely after enter the fixed thickness of sheet material thicknessing machine, then set by water mill polishing
It is standby to be polished.
Finally it should be noted that：The preferred embodiments of the present invention are these are only, are not intended to limit the invention, although
The present invention is described in detail with reference to embodiment, for those skilled in the art, it still can be to foregoing
Technical scheme described in each embodiment is modified, or to which part technical characteristic carry out equivalent substitution, but it is all
Within the spirit and principles in the present invention, any modification, equivalent substitution and improvements made etc. should be included in the protection of the present invention
Within the scope of.
Claims (8)
1. a kind of SiO2Grey dawn textured man-made stone diamond stone sheet material, it is characterised in that：Including 1. major ingredient 40-70 mesh quartz sand, 70-
100 mesh quartzs, 600 mesh ultrawhite silica flours, 325 mesh silica flours, unsaturated polyester resin, colored pigment；
2. auxiliary material 40-70 mesh quartz sand, 70-100 mesh quartz, 600 mesh ultrawhite silica flours, 325 mesh silica flours, unsaturated polyester (UP)
Resin, colored pigment；
3. A colors gas phase SiO2Compound, B color gas phases SiO2Compound, C color gas phases SiO2Compound；
4. D mixture of colours mill base；
5. silane coupler；Curing agent.
2. a kind of SiO according to claim 12Grey dawn textured man-made stone diamond stone sheet material, it is characterised in that according to parts by weight,
1. 10-15 parts of the major ingredient 40-70 mesh quartz sands, 20-25 parts of 70-100 mesh quartzs, 600 1-5 parts of mesh ultrawhite silica flours, 325
10-20 parts of mesh silica flour, 0.2 part of colored pigment, 5-10 parts of unsaturated-resin；
2. 5-10 parts of auxiliary material 40-70 mesh quartz sand, 10-15 parts of 70-100 mesh quartzs, 600 0.5-2 parts of mesh ultrawhite silica flours,
325 5-10 parts of mesh silica flours, 0.05 part of colored pigment, 2-5 parts of unsaturated-resin；
3. A colors gas phase SiO20.1-0.2 parts of compound (0.05 part of colored pigment), B color gas phases SiO20.05-0.1 parts of compound
(0.05 part of colored pigment), C color gas phases SiO20.05-0.1 parts of compound (0.15 part of colored pigment)；
4. 0.1-0.2 parts of D mixture of colours mill base
5. silane coupler 0.05-0.15 parts；0.05-0.15 parts of curing agent.
3. a kind of SiO according to claim 12Grey dawn textured man-made stone diamond stone sheet material, it is characterised in that：The unsaturation
Polyester resin can also be the one or more in epoxy resin, phenolic resin, acrylic resin and polyurethane resin.
4. a kind of SiO according to claim 12Grey dawn textured man-made stone diamond stone sheet material, it is characterised in that：The coloured face
Material and the one or more that mixing mill base is inorganic pigment or organic pigment or mill base.
5. a kind of SiO according to claim 42Grey dawn textured man-made stone diamond stone sheet material, it is characterised in that：The inorganic face
Expect for titanium white, medium chrome yellow, iron oxide yellow, iron oxide red, barba hispanica, cadmium red, cadmium yellow, carbon black or iron oxide black, the organic pigment is pigment scarlet powder, azo
Yellow, dark green or phthalocyanine blue, the mill base are white slurry, black wash, bright red slurry, dark green slurry or phthalocyanine blue slurry.
6. a kind of SiO according to claim 12Grey dawn textured man-made stone diamond stone sheet material, it is characterised in that：The curing agent
For peroxidating (2 ethyl hexanoic acid) tert-butyl ester, methyl ethyl ketone peroxide, peroxidized t-butyl perbenzoate, dibenzoyl peroxide and fat
One or more in fat polyamine.
7. a kind of SiO according to claim 12Grey dawn textured man-made stone diamond stone sheet material, it is characterised in that：The silane is even
Connection agent is γ-methacryloxypropyl trimethoxy silane, γ-(2,3- the third oxygen of epoxy) propyl trimethoxy silicane, N- β
(aminoethyl)-γ-aminopropyltriethoxy dimethoxysilane, N- (β-aminoethyl)-gamma-aminopropyl-triethoxy-silane, N- β (ammonia
Ethyl)-γ-aminopropyltrimethoxysilane, anilinomethyl triethoxysilane, gamma-aminopropyl-triethoxy-silane, vinyl
One or more in triethoxysilane, vinyltrimethoxy silane and γ-chloropropyl triethoxysilane.
8. a kind of SiO according to claim 12The production technology of grey dawn textured man-made stone diamond stone sheet material, it is characterised in that：
Comprise the following steps：
(1) each material each component is weighed according to formula；
(2) stir：1. step (1) is weighed into the quartz sand, silica flour, silane coupler of major ingredient in double planetary agitator
Premixing；The curing agent mixed, decoration colored pigment and unsaturated polyester resin are poured into and entered in double planetary agitator
Row mixing, then adds silica flour and is mixed, 15~55Hz of stirring frequency, 180~600s of mixing time；
2. the quartz sand, silica flour, silane coupler for step (1) being weighed into auxiliary material are pre-mixed in double planetary agitator；
The curing agent mixed, decoration colored pigment and unsaturated polyester resin are poured into and mixed in double planetary agitator,
Then add silica flour to be mixed, 15~55Hz of stirring frequency, 180~600s of mixing time；
3. the major ingredient 1. and 2. mixed and auxiliary material are pre-mixed in double planetary agitator；
4. weigh 1/3 it is 3. mixed expect in double planetary agitator, add A color gas phases SiO2Compound carries out stirring at low speed extremely
Uniformly；
5. compound will be 4. stirred in double planetary agitator, add B color gas phases SiO2Compound and C color gas phases SiO2Mixing
Material continues to stir, untill multi-level color occurs in stirring material.
(3) cloth：1：SiO is got out in advance2Grey dawn pattern mould is put into charge car, is then sent the material 3. mixed
Enter beater further to break up, into material distributing machine in cloth, cloth should flood SiO2Grey dawn pattern mould；2. start preformer
The material good to cloth carries out precompressed；3. charge car is lifted, SiO2Grey dawn pattern mould lifts and feed separation；4. will 5. it mix
Gained compound is filled into SiO2Grey dawn pattern mould is hollowed out in lines, D mixture of colours mill bases is poured 5. mixed mixed
Close in material, institute's leach-color slurry should be into line style；
(4) suppress：After cloth is completed, repressed vibration equipment is compressing under -0.1Mpa vacuum condition, and pressure 50~
200t, 30~55Hz of vibration frequency, 60~600s of time；
(5) heat cure：After vibration compacting, into curing apparatus, solidify at a temperature of 80~130 DEG C, hardening time is 30
~180 minutes；
(6) after the completion of solidifying, the room temperature completely rear sheet material thicknessing machine that enters to be cooled determines thickness, then enters by water mill polissoir
Row polishing.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111574110A (en) * | 2020-03-24 | 2020-08-25 | 肇庆威泰石英石有限公司 | Antique wood grain quartz stone plate and preparation method thereof |
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| CN104478299A (en) * | 2014-11-21 | 2015-04-01 | 广东中旗新材料科技有限公司 | Double-pattern artificial quartz stone plate and production process thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111574110A (en) * | 2020-03-24 | 2020-08-25 | 肇庆威泰石英石有限公司 | Antique wood grain quartz stone plate and preparation method thereof |
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Address after: 528518 No. 112 Mingcheng Second Road, Gaoming District, Foshan City, Guangdong Province Applicant after: Guangdong Zhongqi New Materials Co., Ltd. Address before: 528518 No. 112 Mingcheng Second Road, Gaoming District, Foshan City, Guangdong Province Applicant before: Guangdong Banner New Material Technology Co., Ltd. |
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Application publication date: 20170901 |