CN107129192A - A kind of wood grain type textured man-made stone diamond stone sheet material and its production technology - Google Patents
A kind of wood grain type textured man-made stone diamond stone sheet material and its production technology Download PDFInfo
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- CN107129192A CN107129192A CN201710357321.0A CN201710357321A CN107129192A CN 107129192 A CN107129192 A CN 107129192A CN 201710357321 A CN201710357321 A CN 201710357321A CN 107129192 A CN107129192 A CN 107129192A
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Classifications
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B26/00—Compositions of mortars, concrete or artificial stone, containing only organic binders, e.g. polymer or resin concrete
- C04B26/02—Macromolecular compounds
- C04B26/10—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C04B26/18—Polyesters; Polycarbonates
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B7/00—Mixing; Kneading
- B29B7/002—Methods
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C67/00—Shaping techniques not covered by groups B29C39/00 - B29C65/00, B29C70/00 or B29C73/00
- B29C67/24—Shaping techniques not covered by groups B29C39/00 - B29C65/00, B29C70/00 or B29C73/00 characterised by the choice of material
- B29C67/242—Moulding mineral aggregates bonded with resin, e.g. resin concrete
- B29C67/243—Moulding mineral aggregates bonded with resin, e.g. resin concrete for making articles of definite length
- B29C67/244—Moulding mineral aggregates bonded with resin, e.g. resin concrete for making articles of definite length by vibrating the composition before or during moulding
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29L—INDEXING SCHEME ASSOCIATED WITH SUBCLASS B29C, RELATING TO PARTICULAR ARTICLES
- B29L2007/00—Flat articles, e.g. films or sheets
- B29L2007/002—Panels; Plates; Sheets
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/54—Substitutes for natural stone, artistic materials or the like
- C04B2111/542—Artificial natural stone
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- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Ceramic Engineering (AREA)
- Mechanical Engineering (AREA)
- Structural Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Finishing Walls (AREA)
Abstract
A kind of wood grain type textured man-made stone diamond stone sheet material of the present invention and its production technology, including major ingredient A colors, decorative pattern material B colors, the raw material of major ingredient A colors include 0.075~2mm particulate materials, 0.005~0.045mm silica flours;Colored pigment;Silane coupler;Unsaturated polyester resin;Curing agent;The component and proportioning of decorative pattern material B colors be:Inorganic pigment;Or inorganic pigment, 0.045~0.212mm silica flours;Wherein, particulate material is quartz particles or glass particle, or the artificial quartz in lump that two kinds of mixture is made is handsome in appearance; pattern is distinct, and color is unique, enriches the species and style of artificial quartz in lump; production efficiency is high simultaneously, effectively reduces the fraction defective of product, can mass production.
Description
Technical field
The invention belongs to quartz technical field, specifically, be related to a kind of wood grain type textured man-made stone diamond stone sheet material and
Its production technology.
Background technology
In building decoration field, stone material with its it is attractive in appearance, graceful, ornamental strong the features such as turned into primary decoration material it
One.All the time, natural marble figue it is abundant, naturally, because its natural decorative effect, texture and by extensive use, but
Due to there is resource-constrained, there is aberration in large area paving and different degrees of radioactivity is exceeded, and hardness is low, and easy scratching etc. is asked
Topic, limits its comprehensive development to a certain extent.
Artificial quartz in lump be by quartz sand powder be main stuffing, using unsaturated polyester resin as adhesive, in vacuum shape
The Novel stone that high pressure is compressing under condition, shape under middle temperature state, it is a kind of "dead" pollution, the repeatable ring utilized
Guarantor, green building material and ornament materials.
Although artificial quartz in lump rich color is gorgeous, radiationless, wear-resisting, pressure-resistant, anti scuffing, anticorrosive, anti-aging, antiseepage
Thoroughly, but be due to without marmorean native texture and color, artificial quartz in lump class is cannot get big raising.It is domestic at present
The outer diamond plate for having imitating natural marble, but color is relatively stiff, and texture is unnatural.Meanwhile, pattern type artificial quartz in lump
Due to complex process, low production efficiency, and sheet material, the color in pressing process is easily interpenetrated sheet material, and fraction defective is high, from
And causing the supply of material few, price is high.
Wood grain type artificial quartz stone checkered plate has imitated the texture of wood, allows non-renewable or higher price wood
Line skin texture material is achieved above in stone material by new technology;Therefore, it is necessary to existing production technology carry out upgrading or
Technological transformation.
The content of the invention
Instant invention overcomes shortcoming of the prior art, there is provided a kind of wood grain type decorative pattern people with natural stone texture
Quartzite slate and its production technology are made, good product performance, production efficiency is high, and qualification rate is high.
In order to solve the above-mentioned technical problem, the present invention is achieved by the following technical solutions:
A kind of wood grain type textured man-made stone diamond stone sheet material, including major ingredient A colors, decorative pattern material B colors,
The raw material of the major ingredient A colors includes 0.075~2mm particulate materials, 0.005~0.045mm silica flours, coloured face
Material, silane coupler, unsaturated polyester resin, curing agent;
The component and proportioning of decorative pattern material B colors be:Inorganic pigment;Or inorganic pigment, 0.045~0.212mm silica flours;
Wherein, particulate material is quartz particles or glass particle, or two kinds of mixture.
Further, the major ingredient A colors are 98~99.8 parts of total material, and decorative pattern material B colors are 0.1~2 part of total material.
Further, the major ingredient A colors include according to percentage by weight:0.075~5mm particulate materials 55%~65%;
0.005~0.045mm silica flours 20%~30%;Colored pigment 0.01%~3%;Silane coupler 0.1%~1%;Insatiable hunger
With polyester resin 8%~14%;Curing agent 0.8%~1.4%.
Further, according to percentage by weight, the component and proportioning of the decorative pattern material B colors are:Inorganic pigment 100%;Or nothing
Machine pigment 1%~30%, 0.045~0.212mm silica flours 70%~99%.
Further, the unsaturated polyester resin can also be epoxy resin, phenolic resin, acrylic resin and polyurethane
One or more in resin.
Further, the colored pigment is the one or more of inorganic pigment or organic pigment or mill base.
Further, the inorganic pigment is titanium white, medium chrome yellow, iron oxide yellow, iron oxide red, barba hispanica, cadmium red, cadmium yellow, carbon black, iron oxide black etc.
Inorganic pigment, the organic pigment is the organic pigment such as pigment scarlet powder, azophosphine, dark green and phthalocyanine blue, the mill base is white slurry,
The mill bases such as black wash, bright red slurry, dark green slurry, phthalocyanine blue slurry.
Further, the curing agent is peroxidating (2 ethyl hexanoic acid) tert-butyl ester, methyl ethyl ketone peroxide, perbenzoic acid
One or more in the tert-butyl ester, dibenzoyl peroxide and fat polyamine.
Further, the silane coupler is γ-methacryloxypropyl trimethoxy silane, γ-(2,3- epoxies
Third oxygen) propyl trimethoxy silicane, N- β (aminoethyl)-γ-aminopropyltriethoxy dimethoxysilane, N- (β-aminoethyl)-γ-
Aminopropyl triethoxysilane, N- β (aminoethyl)-γ-aminopropyltrimethoxysilane, anilinomethyl triethoxysilane, γ-
Aminopropyl triethoxysilane, VTES, vinyltrimethoxy silane and γ-chloropropyl triethoxy silicon
One or more in alkane.
A kind of production technology of wood grain type textured man-made stone diamond stone sheet material, comprises the following steps:
(1) each material each component is weighed according to formula;
(2) stir:1. particulate material, the silane coupler of major ingredient A colors step (1) weighed are stirred in double planetary
It is pre-mixed in bucket;The curing agent mixed, decoration colored pigment and unsaturated polyester resin are poured into double planetary agitator
It is middle to be mixed, then add silica flour and mixed, 15~55Hz of stirring frequency, 180~600s of mixing time;
2. decorative pattern material B colorants rub material by manually sieving uniformly;
(3) distributing mode:1st, first Wood-grain mould is put into charge car, then the A being stirred by automatic distributing handlebar expects
Cloth is being put well inside Wood-grain mould;2nd, whole Wood-grain mould is filled up;3. by the jacking system of charge car wood grain mould
Tool is mentioned out of charge car;4th, Wood-grain mould texture blank space is sprayed onto the color patterned material of B are had been prepared for by dry powder spray gun;5、
A is expected to insert the region for having sprayed dry powder;
(4) suppress:After cloth is completed, repressed vibration equipment is compressing under -0.1Mpa vacuum condition, pressure
50~200t, 30~55Hz of vibration frequency, 60~600s of time;
(5) heat cure:After vibration compacting, into curing apparatus, solidify at a temperature of 80~130 DEG C, hardening time
For 30~180 minutes;
(6) after the completion of solidifying, room temperature it is to be cooled completely after enter the fixed thickness of sheet material thicknessing machine, then set by water mill polishing
It is standby to be polished.
The production technology of another wood grain type textured man-made stone diamond stone sheet material, comprises the following steps:
(1) each material each component is weighed according to formula;
(2) stir:1. particulate material, the silane coupler of major ingredient A colors step (1) weighed are stirred in double planetary
It is pre-mixed in bucket;The curing agent mixed, decoration colored pigment and unsaturated polyester resin are poured into double planetary agitator
It is middle to be mixed, then add silica flour and mixed, 15~55Hz of stirring frequency, 180~600s of mixing time;
2. decorative pattern material B colorants rub material by manually sieving uniformly;
(3) distributing mode:1st, the color patterned material of B being stirred, input is automatic to drench inside stock tank;2nd, automatic cloth is started
The A being stirred is expected uniform by being arrived under charge car above the belt of charge car by truck;3rd, automatic pouring slurry valve is opened, is mixed up
Pulp flow;4th, by the lasting walking of automatic distributing car, the dry and wet slurry colour band of showering curtain type, 5, pass through automatic distributing car are formed
Walking ready-made straight line wood grain slurry be covered with whole cloth it is framed in;
(4) suppress:After cloth is completed, repressed vibration equipment is compressing under -0.1Mpa vacuum condition, pressure
50~200t, 30~55Hz of vibration frequency, 60~600s of time;
(5) heat cure:After vibration compacting, into curing apparatus, solidify at a temperature of 80~130 DEG C, hardening time
For 30~180 minutes;
(6) after the completion of solidifying, room temperature it is to be cooled completely after enter the fixed thickness of sheet material thicknessing machine, then set by water mill polishing
It is standby to be polished.
Compared with prior art, the beneficial effects of the invention are as follows:
A kind of wood grain type textured man-made stone diamond stone sheet material of the present invention and its production technology, the synthetic quartz made
Stone is handsome in appearance, and pattern is distinct, and color is unique, the species and style of artificial quartz in lump is enriched, while production efficiency is high, effectively
The fraction defective of product is reduced, can mass production.
Embodiment
The preferred embodiments of the present invention are illustrated below, it will be appreciated that preferred embodiment described herein is only used
In the description and interpretation present invention, it is not intended to limit the present invention.
Embodiment 1:
A kind of wood grain type textured man-made stone diamond stone sheet material of the present invention, including major ingredient A colors, decorative pattern material B colors.
Major ingredient A colors include according to percentage by weight:0.075~5mm particulate materials 63%;0.005~0.045mm silica flours
26%;Colored pigment 1.5%;Silane coupler 0.6%;Unsaturated polyester resin 8%;Curing agent 0.9%.
According to percentage by weight, the component and proportioning of decorative pattern material B colors are:Inorganic pigment 100%;Or inorganic pigment 25%,
0.045~0.212mm silica flours 75%;
Wherein, particulate material is quartz particles or glass particle, or two kinds of mixture.
Major ingredient A colors are 99 parts of total material, and decorative pattern material B colors are 1 part of total material.
Unsaturated polyester resin can also be one in epoxy resin, phenolic resin, acrylic resin and polyurethane resin
Plant or a variety of.
Colored pigment is the one or more of inorganic pigment or organic pigment or mill base.
Inorganic pigment is titanium white, medium chrome yellow, iron oxide yellow, iron oxide red or iron oxide black, and organic pigment is pigment scarlet powder, dark green or phthalocyanine
Indigo plant, mill base is white slurry, black wash, bright red slurry, dark green slurry or phthalocyanine blue slurry.
Curing agent is peroxidating (2 ethyl hexanoic acid) tert-butyl ester, methyl ethyl ketone peroxide, peroxidized t-butyl perbenzoate, peroxide
Change the one or more in dibenzoyl and fat polyamine.
Silane coupler is γ-methacryloxypropyl trimethoxy silane, γ-(2,3- the third oxygen of epoxy) propyl group three
Methoxy silane, N- β (aminoethyl)-γ-aminopropyltriethoxy dimethoxysilane, the ethoxy of N- (β-aminoethyl)-γ-aminopropyl three
Base silane, N- β (aminoethyl)-γ-aminopropyltrimethoxysilane, anilinomethyl triethoxysilane, the ethoxy of γ-aminopropyl three
Base silane, VTES, vinyltrimethoxy silane and one kind in γ-chloropropyl triethoxysilane or
It is a variety of.
A kind of production technology of wood grain type textured man-made stone diamond stone sheet material, comprises the following steps:
(1) each material each component is weighed according to formula;
(2) stir:1. particulate material, the silane coupler of major ingredient A colors step (1) weighed are stirred in double planetary
It is pre-mixed in bucket;The curing agent mixed, decoration colored pigment and unsaturated polyester resin are poured into double planetary agitator
It is middle to be mixed, then add silica flour and mixed.15~55Hz of stirring frequency, 180~600s of mixing time;
2. decorative pattern material B colorants rub material by manually sieving uniformly;
(3) distributing mode:1st, first Wood-grain mould is put into charge car, then the A being stirred by automatic distributing handlebar expects
Cloth is being put well inside Wood-grain mould;2nd, whole Wood-grain mould is filled up;3. by the jacking system of charge car wood grain mould
Tool is mentioned out of charge car;4th, Wood-grain mould texture blank space is sprayed onto the color patterned material of B are had been prepared for by dry powder spray gun;5、
A is expected to insert the region for having sprayed dry powder;
(4) suppress:After cloth is completed, repressed vibration equipment is compressing under -0.1Mpa vacuum condition, pressure
50~200t, 30~55Hz of vibration frequency, 60~600s of time;
(5) heat cure:After vibration compacting, into curing apparatus, solidify at a temperature of 80~130 DEG C, hardening time
For 30~180 minutes;
(6) after the completion of solidifying, room temperature it is to be cooled completely after enter the fixed thickness of sheet material thicknessing machine, then set by water mill polishing
It is standby to be polished.
Embodiment 2:
The present embodiment and the technical scheme of embodiment 1 are essentially identical, and something in common is repeated no more, and its difference is:
Distributing mode:1st, the color patterned material of B being stirred, input is automatic to drench inside stock tank;2nd, automatic distributing is started
The A material that handlebar is stirred are uniform by being arrived under charge car above the belt of charge car;3rd, automatic pouring slurry valve is opened, is mixed up out
Starch flow;4th, by the lasting walking of automatic distributing car, the dry and wet slurry colour band of showering curtain type, 5, pass through automatic distributing car are formed
It is framed interior that ready-made straight line wood grain slurry is covered with whole cloth by walking;
Finally it should be noted that:The preferred embodiments of the present invention are these are only, are not intended to limit the invention, although
The present invention is described in detail with reference to embodiment, for those skilled in the art, it still can be to foregoing
Technical scheme described in each embodiment is modified, or to which part technical characteristic carry out equivalent substitution, but it is all
Within the spirit and principles in the present invention, any modification, equivalent substitution and improvements made etc. should be included in the protection of the present invention
Within the scope of.
Claims (10)
1. a kind of wood grain type textured man-made stone diamond stone sheet material, it is characterised in that:Including major ingredient A colors, decorative pattern material B colors,
The raw material of the major ingredient A colors includes 0.075~2mm particulate materials, 0.005~0.045mm silica flours, colored pigment, silicon
Alkane coupling agent, unsaturated polyester resin, curing agent;
The component and proportioning of decorative pattern material B colors be:Inorganic pigment;Or inorganic pigment, 0.045~0.212mm silica flours;
Wherein, particulate material is quartz particles or glass particle, or two kinds of mixture.
2. a kind of wood grain type textured man-made stone diamond stone sheet material according to claim 1, it is characterised in that:The major ingredient A colors are
98~99.8 parts of total material, decorative pattern material B colors are 0.1~2 part of total material.
3. a kind of wood grain type textured man-made stone diamond stone sheet material according to claim 1, it is characterised in that:The major ingredient A colors are pressed
Include according to percentage by weight:0.075~5mm particulate materials 55%~65%;0.005~0.045mm silica flours 20%~30%;
Colored pigment 0.01%~3%;Silane coupler 0.1%~1%;Unsaturated polyester resin 8%~14%;Curing agent 0.8%
~1.4%.
4. a kind of wood grain type textured man-made stone diamond stone sheet material according to claim 1, it is characterised in that:According to weight percent
Than the component and proportioning of the decorative pattern material B colors are:Inorganic pigment 100%;Or inorganic pigment 1%~30%, 0.045~
0.212mm silica flours 70%~99%.
5. a kind of wood grain type textured man-made stone diamond stone sheet material according to claim 1, it is characterised in that:The unsaturated polyester (UP)
Resin can also be the one or more in epoxy resin, phenolic resin, acrylic resin and polyurethane resin.
6. a kind of wood grain type textured man-made stone diamond stone sheet material according to claim 1, it is characterised in that:The colored pigment is
The one or more of inorganic pigment or organic pigment or mill base.
7. a kind of wood grain type textured man-made stone diamond stone sheet material according to claim 6, it is characterised in that:The curing agent was
Aoxidize (2 ethyl hexanoic acid) tert-butyl ester, methyl ethyl ketone peroxide, peroxidized t-butyl perbenzoate, dibenzoyl peroxide and fat many
One or more in first amine.
8. a kind of wood grain type textured man-made stone diamond stone sheet material according to claim 6, it is characterised in that:The silane coupler
For γ-methacryloxypropyl trimethoxy silane, γ-(2,3- the third oxygen of epoxy) propyl trimethoxy silicane, N- β (ammonia
Ethyl)-γ-aminopropyltriethoxy dimethoxysilane, N- (β-aminoethyl)-gamma-aminopropyl-triethoxy-silane, N- β (ammonia second
Base)-γ-aminopropyltrimethoxysilane, anilinomethyl triethoxysilane, gamma-aminopropyl-triethoxy-silane, vinyl three
One or more in Ethoxysilane, vinyltrimethoxy silane and γ-chloropropyl triethoxysilane.
9. a kind of production technology of wood grain type textured man-made stone diamond stone sheet material according to claim 1, it is characterised in that:Including
Following steps:
(1) each material each component is weighed according to formula;
(2) stir:1. the particulate materials of major ingredient A colors step (1) weighed, silane coupler are in double planetary agitator
Premixing;The curing agent mixed, decoration colored pigment and unsaturated polyester resin are poured into and entered in double planetary agitator
Row mixing, then adds silica flour and is mixed, 15~55Hz of stirring frequency, 180~600s of mixing time;
2. decorative pattern material B colorants rub material by manually sieving uniformly;
(3) distributing mode:1st, first Wood-grain mould is put into charge car, then the A material cloth being stirred by automatic distributing handlebar exists
Put well inside Wood-grain mould;2nd, whole Wood-grain mould is filled up;3. by the jacking system of charge car Wood-grain mould from
Mention in charge car;4th, Wood-grain mould texture blank space is sprayed onto the color patterned material of B are had been prepared for by dry powder spray gun;5th, A
Material inserts the region for having sprayed dry powder;
(4) suppress:After cloth is completed, repressed vibration equipment is compressing under -0.1Mpa vacuum condition, and pressure 50~
200t, 30~55Hz of vibration frequency, 60~600s of time;
(5) heat cure:After vibration compacting, into curing apparatus, solidify at a temperature of 80~130 DEG C, hardening time is 30
~180 minutes;
(6) after the completion of solidifying, the room temperature completely rear sheet material thicknessing machine that enters to be cooled determines thickness, then enters by water mill polissoir
Row polishing.
10. a kind of production technology of wood grain type textured man-made stone diamond stone sheet material according to claim 1, it is characterised in that:Bag
Include following steps:
(1) each material each component is weighed according to formula;
(2) stir:1. the particulate materials of major ingredient A colors step (1) weighed, silane coupler are in double planetary agitator
Premixing;The curing agent mixed, decoration colored pigment and unsaturated polyester resin are poured into and entered in double planetary agitator
Row mixing, then adds silica flour and is mixed, 15~55Hz of stirring frequency, 180~600s of mixing time;
2. decorative pattern material B colorants rub material by manually sieving uniformly;
(3) distributing mode:1st, the color patterned material of B being stirred, input is automatic to drench inside stock tank;2nd, automatic distributing car is started
The A material being stirred is uniform by being arrived under charge car above the belt of charge car;3rd, automatic pouring slurry valve is opened, pulp is mixed up
Flow;4th, by the lasting walking of automatic distributing car, the dry and wet slurry colour band of showering curtain type, 5, the row by automatic distributing car are formed
Walk ready-made straight line wood grain slurry be covered with whole cloth it is framed in;
(4) suppress:After cloth is completed, repressed vibration equipment is compressing under -0.1Mpa vacuum condition, and pressure 50~
200t, 30~55Hz of vibration frequency, 60~600s of time;
(5) heat cure:After vibration compacting, into curing apparatus, solidify at a temperature of 80~130 DEG C, hardening time is 30
~180 minutes;
(6) after the completion of solidifying, the room temperature completely rear sheet material thicknessing machine that enters to be cooled determines thickness, then enters by water mill polissoir
Row polishing.
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CN111574110A (en) * | 2020-03-24 | 2020-08-25 | 肇庆威泰石英石有限公司 | Antique wood grain quartz stone plate and preparation method thereof |
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CN108726917A (en) * | 2018-07-05 | 2018-11-02 | 珠海市盛西源机电设备有限公司 | Artificial stone marbling entity plane materiel |
CN109664395A (en) * | 2019-01-15 | 2019-04-23 | 苏州科逸住宅设备股份有限公司 | Quartzite slate of imitation marble and preparation method thereof |
CN111574110A (en) * | 2020-03-24 | 2020-08-25 | 肇庆威泰石英石有限公司 | Antique wood grain quartz stone plate and preparation method thereof |
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