CN104478299A - Double-pattern artificial quartz stone plate and production process thereof - Google Patents
Double-pattern artificial quartz stone plate and production process thereof Download PDFInfo
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- CN104478299A CN104478299A CN201410676107.8A CN201410676107A CN104478299A CN 104478299 A CN104478299 A CN 104478299A CN 201410676107 A CN201410676107 A CN 201410676107A CN 104478299 A CN104478299 A CN 104478299A
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Abstract
The invention discloses a double-pattern artificial quartz stone plate comprising a main material (with the color A), a pattern material (with the color B) and a pattern material (with the color C), wherein the raw materials of the main material (with the color A) include 0.075-5mm granular raw materials, 0.005-0.063mm quartz powder, colored pigment, a silane coupling agent, unsaturated polyester resin and a curing agent; the pattern material (with the color B) and a pattern material (with the color C) respectively comprise the components according to a certain ratio: 0.075-0.5mm quartz particles, 0.005-0.063mm quartz powder, colored pigment and a silane coupling agent, wherein the granular raw materials are quartz particles or glass particles and mixtures of the quartz particles and the glass particles. By using the double-pattern artificial quartz stone plate and a production process thereof, the production efficiency is high, meanwhile, the unqualified product rate is effectively reduced, the colors are separated from each other, and the mass production can be realized.
Description
Technical field
The present invention relates to a kind of artificial quartz stone plate, specifically, relate to a kind of honeysuckle line artificial quartz stone plate and production technique thereof.
Background technology
Artificial quartz in lump is main stuffing by quartz sand powder, using unsaturated polyester resin as tackiness agent, the Novel stone formalized vibrate press forming, middle temperature state under vacuum condition under, it is a kind of no radioactivity pollute, the environmental protection that can reuse, green building material and finishing material.
At first, quartzite is only applied on the higher cabinet table surface of effects on surface requirement, furniture table-board, laboratory operation platform.Along with Economic development and market are ripe further, the every field such as domestic and international more ground, metope, furniture bring into use quartzite, such as various large hotel, mansion, landmark, and quartzite just progressively becomes the substitute products of lithotome.
Domestic conventional quartz stone product is at first based on monochrome, and along with the development in market, plain quarz stone can not meet the esthetic requirement of the continuous renewal in market, the diamond plate of nearly 2 years existing imitated natural granites, but color is relatively stiff, and texture is nature not.Meanwhile, pattern type quartzite slate is due to complex process, and production efficiency is low, and sheet material color in pressing process easily interpenetrates, and fraction defective is high, thus causes the supply of material few, and price is high.
Therefore, be necessary to carry out upgrading or technological transformation to existing production technique.
Summary of the invention
Instant invention overcomes shortcoming of the prior art, provide a kind of honeysuckle line artificial quartz stone plate and the production technique thereof with natural stone texture, good product performance, production efficiency is high, and qualification rate is high.
In order to solve the problems of the technologies described above, the present invention is achieved by the following technical solutions:
A kind of honeysuckle line artificial quartz stone plate, comprises major ingredient A look, decorative pattern material B look and decorative pattern material C look,
The raw material of described major ingredient A look comprises 0.075 ~ 5mm particulate material, 0.005 ~ 0.063mm silica powder; Colored pigment; Silane coupling agent; Unsaturated polyester resin; Solidifying agent;
Component and the proportioning of decorative pattern material B look and decorative pattern material C look are: 0.075 ~ 0.5mm quartz particles; 0.005 ~ 0.063mm silica powder; Colored pigment; Silane coupling agent;
Wherein, particulate material is quartz particles or glass particle, or the mixture of two kinds.
Further, described major ingredient A look is 98-99.8 part of total material, and decorative pattern material B look is 0.1-1 part of total material, and decorative pattern material C look is 0.1-1 part of total material.
Further, described major ingredient A look comprises according to weight percent: 0.075 ~ 5mm particulate material 55% ~ 65%; 0.005 ~ 0.063mm silica powder 20%-30%; Decoration colored pigment 0.01%-10%; Silane coupling agent 0.1%-1%; Unsaturated polyester resin 8%-12%; Solidifying agent 0.8%-1.2%.
Further, according to weight percent, component and the proportioning of described decorative pattern material B look and decorative pattern material C look are: 0.075 ~ 0.5mm quartz particles 75% ~ 90%, 0.005 ~ 0.063mm silica powder 5%-20%; Colored pigment 0.01%-15%; Silane coupling agent 0.1%-1%.
Further, described colored pigment is one or more of mineral dye or pigment dyestuff.
Further, described mineral dye is titanium white, medium chrome yellow medium yellow, iron oxide yellow, iron oxide red or red lead.
Further, described pigment dyestuff is red, phthalein viridescent and phthalocyanine blue.
Further, described solidifying agent is one or more in peroxidation (2 ethyl hexanoic acid) tert-butyl ester, methylethyl ketone peroxide, peroxidized t-butyl perbenzoate, dibenzoyl peroxide and fat polyamine.
Further, described silane coupling agent is one or more in γ-methacryloxypropyl trimethoxy silane, γ-(2,3-epoxy third oxygen) propyl trimethoxy silicane, N-β (aminoethyl)-γ-aminopropyltriethoxy dimethoxysilane, N-(β-aminoethyl)-γ-aminopropyl triethoxysilane, N-β (aminoethyl)-γ-aminopropyltrimethoxysilane, anilinomethyl triethoxysilane, γ-aminopropyl triethoxysilane, vinyltriethoxysilane, vinyltrimethoxy silane and γ-chloropropyl triethoxysilane.
A production technique for honeysuckle line artificial quartz stone plate, comprises the following steps:
(1) each material each component is taken according to formula;
(2) stir: the quartz particles of the major ingredient A look 1. step 1 taken, glass particle, silane coupling agent, silica powder pre-mixing in double planetary agitation vat; The unsaturated polyester resin being mixed with solidifying agent and decoration colored pigment is poured in double planetary agitation vat and mixes.Stirring frequency 15-55Hz, churning time 180-600s;
2. decorative pattern material B colorant, decorative pattern material C colorant manually rub material evenly;
3. spread by color patterned for B material in the A material mixed, low frequency is uniformly mixed; Sprinkled by color patterned for C material, low frequency is uniformly mixed again, and obtains final compound.Stirring frequency 5-15Hz, churning time 5-60S;
(4) cloth: batch mixing is sent in charge car by distributing belt, then by charge car batch mixing is evenly arranged framed with cloth in;
(4) suppress: after cloth completes, repressed vibration equipment compression moulding under the vacuum condition of-0.1Mpa, pressure 50-100t, vibrational frequency 30-55Hz, time 180-600s;
(5) thermofixation: after vibration compacting, enter curing apparatus, solidify at the temperature of 80-120 DEG C, set time is for being 60 ~ 90 minutes;
(6) after having solidified, normal temperature place to be cooled completely after to enter sheet material thicknessing machine fixed thick, then carry out polishing through 20 water mill polissoirs.
Compared with prior art, the invention has the beneficial effects as follows:
A kind of honeysuckle line artificial quartz stone plate of the present invention and production technique thereof, production efficiency is high, and effectively reduce the fraction defective of product, color is separated from each other simultaneously, can mass production.
Embodiment
Below the preferred embodiments of the present invention are described, should be appreciated that preferred embodiment described herein is only for instruction and explanation of the present invention, is not intended to limit the present invention.
Embodiment 1:
A kind of honeysuckle line artificial quartz stone plate described in the present embodiment, comprises major ingredient A look, decorative pattern material B look and decorative pattern material C look,
Major ingredient A look is 99 parts of total material, and decorative pattern material B look is 0.5 part of total material, and decorative pattern material C look is 0.5 part of total material,
Major ingredient A look comprises according to weight percent: 0.075 ~ 5mm particulate material 60%; 0.005 ~ 0.063mm silica powder 25%; Decoration colored pigment 5%; Silane coupling agent 0.5%; Unsaturated polyester resin 8.5%; Solidifying agent 1%;
Wherein, particulate material is quartz particles.
According to weight percent, component and the proportioning of decorative pattern material B look and decorative pattern material C look are: 0.075 ~ 0.5mm quartz particles 80%, 0.005 ~ 0.063mm silica powder 10%; Colored pigment 9.5%; Silane coupling agent 0.5%.
Colored pigment is mineral dye, and mineral dye is iron oxide red.
Solidifying agent is peroxidation (2 ethyl hexanoic acid) tert-butyl ester.
Silane coupling agent is N-(β-aminoethyl)-γ-aminopropyl triethoxysilane.
A production technique for honeysuckle line artificial quartz stone plate, comprises the following steps:
(1) each material each component is taken according to formula;
(2) stir: the quartz particles of the major ingredient A look 1. step 1 taken, glass particle, silane coupling agent, silica powder pre-mixing in double planetary agitation vat; The unsaturated polyester resin being mixed with solidifying agent and decoration colored pigment is poured in double planetary agitation vat and mixes, stirring frequency 15-55Hz, churning time 180-600s;
2. decorative pattern material B colorant, decorative pattern material C colorant manually rub material evenly;
3. spread by color patterned for B material in the A material mixed, low frequency is uniformly mixed; Sprinkled by color patterned for C material, low frequency is uniformly mixed again, and obtains final compound, stirring frequency 5-15Hz, churning time 5-60S;
(5) cloth: batch mixing is sent in charge car by distributing belt, then by charge car batch mixing is evenly arranged framed with cloth in;
(4) suppress: after cloth completes, repressed vibration equipment compression moulding under the vacuum condition of-0.1Mpa, pressure 50-100t, vibrational frequency 30-55Hz, time 180-600s;
(5) thermofixation: after vibration compacting, enter curing apparatus, solidify at the temperature of 80-120 DEG C, set time is for being 60 ~ 90 minutes;
(6) after having solidified, normal temperature place to be cooled completely after to enter sheet material thicknessing machine fixed thick, then carry out polishing through 20 water mill polissoirs.
Embodiment 2:
A kind of honeysuckle line artificial quartz stone plate described in the present embodiment, comprises major ingredient A look, decorative pattern material B look and decorative pattern material C look,
Major ingredient A look is 98-99.8 part of total material, and decorative pattern material B look is 0.1-1 part of total material, and decorative pattern material C look is 0.1-1 part of total material;
Major ingredient A look comprises according to weight percent: 0.075 ~ 5mm particulate material 58%; 0.005 ~ 0.063mm silica powder 24%; Decoration colored pigment 8%; Silane coupling agent 0.8%; Unsaturated polyester resin 8.3%; Solidifying agent 0.9%;
Wherein, particulate material is quartz particles or glass particle, or the mixture of two kinds.
Further, according to weight percent, component and the proportioning of decorative pattern material B look and decorative pattern material C look are: 0.075 ~ 0.5mm quartz particles 85%%, 0.005 ~ 0.063mm silica powder 7%; Colored pigment 7.7%; Silane coupling agent 0.3%.
Colored pigment is pigment dyestuff, and pigment dyestuff is phthalocyanine blue.
Solidifying agent is fat polyamine.
Silane coupling agent is in γ-chloropropyl triethoxysilane.
Last it is noted that these are only the preferred embodiments of the present invention; be not limited to the present invention; although with reference to embodiment to invention has been detailed description; for a person skilled in the art; it still can be modified to the technical scheme described in foregoing embodiments; or equivalent replacement is carried out to wherein portion of techniques feature; but it is within the spirit and principles in the present invention all; any amendment of doing, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.
Claims (10)
1. a honeysuckle line artificial quartz stone plate, is characterized in that: comprise major ingredient A look, decorative pattern material B look and decorative pattern material C look,
The raw material of described major ingredient A look comprises 0.075 ~ 5mm particulate material, 0.005 ~ 0.063mm silica powder; Colored pigment; Silane coupling agent; Unsaturated polyester resin; Solidifying agent;
Component and the proportioning of decorative pattern material B look and decorative pattern material C look are: 0.075 ~ 0.5mm quartz particles; 0.005 ~ 0.063mm silica powder; Colored pigment; Silane coupling agent;
Wherein, particulate material is quartz particles or glass particle, or the mixture of two kinds.
2. a kind of honeysuckle line artificial quartz stone plate according to claim 1, is characterized in that: described major ingredient A look is 98-99.8 part of total material, and decorative pattern material B look is 0.1-1 part of total material, and decorative pattern material C look is 0.1-1 part of total material.
3. a kind of honeysuckle line artificial quartz stone plate according to claim 2, is characterized in that: described major ingredient A look comprises according to weight percent: 0.075 ~ 5mm particulate material 55% ~ 65%; 0.005 ~ 0.063mm silica powder 20%-30%; Decoration colored pigment 0.01%-10%; Silane coupling agent 0.1%-1%; Unsaturated polyester resin 8%-12%; Solidifying agent 0.8%-1.2%.
4. a kind of honeysuckle line artificial quartz stone plate according to claim 2, it is characterized in that: according to weight percent, component and the proportioning of described decorative pattern material B look and decorative pattern material C look are: 0.075 ~ 0.5mm quartz particles 75% ~ 90%, 0.005 ~ 0.063mm silica powder 5%-20%; Colored pigment 0.01%-15%; Silane coupling agent 0.1%-1%.
5. a kind of honeysuckle line artificial quartz stone plate according to claim 1, is characterized in that: described colored pigment is one or more of mineral dye or pigment dyestuff.
6. a kind of honeysuckle line artificial quartz stone plate according to claim 5, is characterized in that: described mineral dye is titanium white, medium chrome yellow medium yellow, iron oxide yellow, iron oxide red or red lead.
7. a kind of honeysuckle line artificial quartz stone plate according to claim 5, is characterized in that: described pigment dyestuff is red, the dark green and phthalocyanine blue of phthalein.
8. a kind of honeysuckle line artificial quartz stone plate according to claim 1, is characterized in that: described solidifying agent is one or more in peroxidation (2 ethyl hexanoic acid) tert-butyl ester, methylethyl ketone peroxide, peroxidized t-butyl perbenzoate, dibenzoyl peroxide and fat polyamine.
9. a kind of honeysuckle line artificial quartz stone plate according to claim 1, it is characterized in that: described silane coupling agent is γ-methacryloxypropyl trimethoxy silane, γ-(2, 3-epoxy third oxygen) propyl trimethoxy silicane, N-β (aminoethyl)-γ-aminopropyltriethoxy dimethoxysilane, N-(β-aminoethyl)-γ-aminopropyl triethoxysilane, N-β (aminoethyl)-γ-aminopropyltrimethoxysilane, anilinomethyl triethoxysilane, γ-aminopropyl triethoxysilane, vinyltriethoxysilane, one or more in vinyltrimethoxy silane and γ-chloropropyl triethoxysilane.
10. the production technique of a kind of honeysuckle line artificial quartz stone plate according to claim 1, is characterized in that: comprise the following steps:
(1) each material each component is taken according to formula;
(2) stir: the quartz particles of the major ingredient A look 1. step 1 taken, glass particle, silane coupling agent, silica powder pre-mixing in double planetary agitation vat; The unsaturated polyester resin being mixed with solidifying agent and decoration colored pigment is poured in double planetary agitation vat and mixes, stirring frequency 15-55Hz, churning time 180-600s;
2. decorative pattern material B colorant, decorative pattern material C colorant manually rub material evenly;
3. spread by color patterned for B material in the A material mixed, low frequency is uniformly mixed; Sprinkled by color patterned for C material, low frequency is uniformly mixed again, and obtains final compound, stirring frequency 5-15Hz, churning time 5-60S;
(3) cloth: batch mixing is sent in charge car by distributing belt, then by charge car batch mixing is evenly arranged framed with cloth in;
(4) suppress: after cloth completes, repressed vibration equipment compression moulding under the vacuum condition of-0.1Mpa, pressure 50-100t, vibrational frequency 30-55Hz, time 180-600s;
(5) thermofixation: after vibration compacting, enter curing apparatus, solidify at the temperature of 80-120 DEG C, set time is for being 60 ~ 90 minutes;
(6) after having solidified, normal temperature place to be cooled completely after to enter sheet material thicknessing machine fixed thick, then carry out polishing through 20 water mill polissoirs.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105801003A (en) * | 2016-03-14 | 2016-07-27 | 广东中旗新材料科技有限公司 | Compound-color artificial quartz quartzite board having flowability and production process thereof |
| CN105801000A (en) * | 2016-03-14 | 2016-07-27 | 广东中旗新材料科技有限公司 | Bulk pattern artificial quartz stone plate and production process thereof |
| CN105801013A (en) * | 2016-02-19 | 2016-07-27 | 山东源根化学技术研发有限公司 | Self-cleaning anti-haze outdoor artificial quartz stone plate and preparation method thereof |
| CN105819740A (en) * | 2016-03-14 | 2016-08-03 | 广东中旗新材料科技有限公司 | Self-enhanced ceramic cold glaze and preparation method thereof |
| CN105819747A (en) * | 2016-03-14 | 2016-08-03 | 广东中旗新材料科技有限公司 | Artificial quartz stone sheet material with linear patterns and production technology thereof |
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| CN105801013A (en) * | 2016-02-19 | 2016-07-27 | 山东源根化学技术研发有限公司 | Self-cleaning anti-haze outdoor artificial quartz stone plate and preparation method thereof |
| CN105801003A (en) * | 2016-03-14 | 2016-07-27 | 广东中旗新材料科技有限公司 | Compound-color artificial quartz quartzite board having flowability and production process thereof |
| CN105801000A (en) * | 2016-03-14 | 2016-07-27 | 广东中旗新材料科技有限公司 | Bulk pattern artificial quartz stone plate and production process thereof |
| CN105819740A (en) * | 2016-03-14 | 2016-08-03 | 广东中旗新材料科技有限公司 | Self-enhanced ceramic cold glaze and preparation method thereof |
| CN105819747A (en) * | 2016-03-14 | 2016-08-03 | 广东中旗新材料科技有限公司 | Artificial quartz stone sheet material with linear patterns and production technology thereof |
| CN106927729A (en) * | 2017-01-26 | 2017-07-07 | 佛山市高明区新意新石业有限公司 | The quartzite slate preparation method and its product of a kind of imitation marble |
| CN106927729B (en) * | 2017-01-26 | 2019-05-17 | 佛山市高明区新意新石业有限公司 | A kind of the quartzite slate preparation method and its product of imitation marble |
| CN106915921A (en) * | 2017-03-22 | 2017-07-04 | 佛山市蓝瑞欧特信息服务有限公司 | A kind of fire retardant man-made quartzite slate and preparation method thereof |
| CN106977135A (en) * | 2017-05-19 | 2017-07-25 | 广东中旗新材料科技有限公司 | A kind of end-of-dayglass artificial quartz stone plate and preparation method thereof |
| CN107117867A (en) * | 2017-05-19 | 2017-09-01 | 广东中旗新材料科技有限公司 | A kind of SiO2Grey dawn textured man-made stone diamond stone sheet material and its production technology |
| CN107117868A (en) * | 2017-05-19 | 2017-09-01 | 广东中旗新材料科技有限公司 | A kind of SiO2 grey dawns textured man-made stone diamond stone sheet material and preparation method thereof |
| CN107117865A (en) * | 2017-05-19 | 2017-09-01 | 广东中旗新材料科技有限公司 | A kind of double-colored fine grained artificial quartz stone plate and its production technology |
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