CN106943327A - A kind of bletilla striata toothpaste and preparation method thereof - Google Patents
A kind of bletilla striata toothpaste and preparation method thereof Download PDFInfo
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- CN106943327A CN106943327A CN201710210977.XA CN201710210977A CN106943327A CN 106943327 A CN106943327 A CN 106943327A CN 201710210977 A CN201710210977 A CN 201710210977A CN 106943327 A CN106943327 A CN 106943327A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
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Abstract
The present invention relates to technical field of traditional Chinese medicines, especially a kind of bletilla striata toothpaste and preparation method thereof, using the bletilla striata, toothpaste matrix, Chinese medicine composition as raw material, according to rational proportioning, bletilla striata toothpaste is prepared into reference to the adjustment of preparation technology parameter, the function except disclosure satisfy that daily cleaning tooth, also there is sterilized, anti-inflammatory, after long-term use, the generation of the diseases such as teeth whitening, light, and the anti-treating dental ulcer of energy, periodontitis is enabled to.
Description
Technical field
The invention belongs to technical field of toothpaste, especially a kind of bletilla striata toothpaste and preparation method thereof.
Background technology
With continuing to develop for society, the daily contacts of people, contact are frequent, the problem of oral health in, it is neat clean
White tooth is a part for people's look Chinese medicine, more and more of interest by people, and oral cavity is used as gastral
Initial point, plays a part of Chinese medicine in food digestion, with the intake to food, chews, swallows and the work(such as speech, expression
Can, therefore oral cavity turns into the important barrier together of human body, can prevent the intrusion of extraneous pathogenic microorganism, it is ensured that health.
The bletilla striata is herbaceos perennial, is most one of monoid of economic worth in temperate zone Terrestrial orchid section plant, also
It is one of conventional Chinese medicine of China, its main component contains the materials such as mannosan, starch, volatile oil, pharmaceutically has
Astringing to arrest bleeding, clearing heat and promoting diuresis, effect of detumescence and promoting granulation.
At present, the toothpaste species that in the market is sold is more, and effect is more single, such as Patent No. CN200610147512.6
A kind of disclosed fresh ginger toothpaste, is added to toothpaste using ginger of squeezing the juice and plays killing helicobacter pylori effect, for another example Patent No.
CN201210375804.0 discloses a kind of snakegourd toothpaste, and bactericidal action is played using addition fruit-rind of Chinese trichosanthes extract solution.
The content of the invention
In order to solve above-mentioned technical problem present in prior art, the present invention provides a kind of bletilla striata toothpaste.
It is achieved particular by following technical scheme：
The present invention provides a kind of bletilla striata toothpaste, and raw material is in parts by weight：5~12 parts of the bletilla striata, 80~90 parts of toothpaste matrix,
1~3 part of Chinese medicine composition.
Further preferred raw material is 8 parts of the bletilla striata, 86 parts of toothpaste matrix, 2 parts of Chinese medicine composition in parts by weight.
It is a further object to provide the preparation method of the bletilla striata toothpaste, comprise the following steps：
(1) bletilla striata is handled：After the bletilla striata is cleaned, temperature is put into soak 1~3h in 30~35 DEG C of clear water, 100 are ground into
~200 mesh, are dried to adequate moisture, and are put into extraction in extractor, obtain bletilla striata extract, standby；
(2) mix：Bletilla striata extract in step (1), Chinese medicine composition are mixed be put into stirring 3 in de-airing mixer~
5min, mixing speed is 50~100r/min, adds toothpaste matrix, continues to stir 10~15min, obtains lotion；
(3) by after the sterilized processing of lotion in step (2), packed with composite soft tube.
The raw material of the Chinese medicine composition is 12~18 parts of the tuber of dwarf lilyturf, 12~16 parts of the leaf of bamboo, peppermint 14~18 in parts by weight
Part, 12~16 parts of chrysanthemum, 5~8 parts of pseudo-ginseng, 3~7 parts of the fruit of Rangoon creeper, 4~8 parts of purslane.
100~200 mesh are ground into after the tuber of dwarf lilyturf, the leaf of bamboo, peppermint, chrysanthemum, pseudo-ginseng, the fruit of Rangoon creeper and purslane mixing,
It is 15~25% to dry to moisture, then with ultrasonication.
The raw material of the toothpaste matrix is 30~35 parts of rubbing agent, 15~20 parts of excipient, NMF 30 in parts by weight
~40 parts, 2~3 parts of thickener, 0.7~1.2 part of essence, 2~4 parts of foaming agent, 0.5~1.3 part of sweetener
The extraction conditions of the bletilla striata are in the step (1)：Ethanol is digestion agent, and Extracting temperature is 26.4 DEG C, extraction time
For 45min, extract 3 times.
It is that adequate moisture refers to that moisture is 20~30% in the step (1).
The beneficial effect of the present invention
The present invention addition bletilla striata, using functions such as anti-inflammatory sterilization, astringing to arrest bleeding, clearing heat and promoting diuresis, the detumescence and promoting granulations of the bletilla striata, leads to
Regulation and control bletilla striata Extraction technique is crossed, and then make it that the active principle in the bletilla striata is able to maximized utilization, and then improves the bletilla striata
Utilization rate, and be added to according to suitable dosage in the composition of toothpaste, assign toothpaste multi-efficiency.
Toothpaste matrix is added in the present invention, as the bletilla striata and the carrier of Chinese medicine composition, and by regulating and controlling in toothpaste matrix
Each group distribution ratio so that each component in raw material can be fully miscible, so lotion become fine and smooth, compacted, light,
Distribution of color is uniform, further improves the quality of lotion.
The present invention is raw material by using the bletilla striata, toothpaste matrix, Chinese medicine composition, according to rational proportioning, with reference to preparation
The adjustment of technological parameter is prepared into bletilla striata toothpaste, the function except disclosure satisfy that daily cleaning tooth, also with sterilized, anti-inflammatory
Effect, after long-term use, enables to the generation of the diseases such as teeth whitening, light, and the anti-treating dental ulcer of energy, periodontitis.
Embodiment
The invention will be further described with reference to embodiments：
Embodiment 1
Formula：Bletilla striata 5kg, toothpaste matrix 80kg, Chinese medicine composition 1kg；
Preparation method：(1) bletilla striata is handled：After the bletilla striata is cleaned, temperature is put into soak 1h in 30 DEG C of clear water, is ground into
100 mesh, are dried to adequate moisture, and are put into extraction in extractor, obtain bletilla striata extract, standby；
(2) mix：Bletilla striata extract, Chinese medicine composition in step (1) are mixed to be put into de-airing mixer and stir 3min,
Mixing speed is 50r/min, adds toothpaste matrix, continues to stir 10min, obtains lotion；
(3) by after the sterilized processing of lotion in step (2), packed with composite soft tube.
The raw material of the Chinese medicine composition in parts by weight for tuber of dwarf lilyturf 12kg, leaf of bamboo 12kg, peppermint 14kg, chrysanthemum 12kg,
Pseudo-ginseng 5kg, fruit of Rangoon creeper 3kg, purslane 4kg.
100 mesh are ground into after the tuber of dwarf lilyturf, the leaf of bamboo, peppermint, chrysanthemum, pseudo-ginseng, the fruit of Rangoon creeper and purslane mixing, are dried extremely
Moisture is 15%, then with ultrasonication.
The raw material of the toothpaste matrix is rubbing agent 30kg, excipient 15kg, NMF 30kg, thickener in parts by weight
2kg, essence 0.7kg, foaming agent 2kg, sweetener 1.3kg.
The extraction conditions of the bletilla striata are in the step (1)：Ethanol is digestion agent, and Extracting temperature is 26.4 DEG C, extraction time
For 45min, extract 3 times.
It is that adequate moisture refers to that moisture is 20% in the step (1).
Embodiment 2
Formula：Bletilla striata 12kg, toothpaste matrix 90kg, Chinese medicine composition 3kg；
Preparation method：(1) bletilla striata is handled：After the bletilla striata is cleaned, temperature is put into soak 3h in 35 DEG C of clear water, is ground into
200 mesh, are dried to adequate moisture, and are put into extraction in extractor, obtain bletilla striata extract, standby；
(2) mix：Bletilla striata extract, Chinese medicine composition in step (1) are mixed to be put into de-airing mixer and stir 5min,
Mixing speed is 100r/min, adds toothpaste matrix, continues to stir 15min, obtains lotion；
(3) by after the sterilized processing of lotion in step (2), packed with composite soft tube.
The raw material of the Chinese medicine composition in parts by weight for tuber of dwarf lilyturf 18kg, leaf of bamboo 16kg, peppermint 18kg, chrysanthemum 16kg,
Pseudo-ginseng 8kg, fruit of Rangoon creeper 7kg, purslane 8kg.
200 mesh are ground into after the tuber of dwarf lilyturf, the leaf of bamboo, peppermint, chrysanthemum, pseudo-ginseng, the fruit of Rangoon creeper and purslane mixing, are dried extremely
Moisture is 25%, then with ultrasonication.
The raw material of the toothpaste matrix is rubbing agent 35kg, excipient 20kg, NMF 40kg, thickener in parts by weight
3kg, essence 1.2kg, foaming agent 4kg, sweetener 0.5kg.
The extraction conditions of the bletilla striata are in the step (1)：Ethanol is digestion agent, and Extracting temperature is 26.4 DEG C, extraction time
For 45min, extract 3 times.
It is that adequate moisture refers to that moisture is 30% in the step (1).
Embodiment 3
Formula：Bletilla striata 8kg, toothpaste matrix 86kg, Chinese medicine composition 2kg；
Preparation method：(1) bletilla striata is handled：After the bletilla striata is cleaned, temperature is put into soak 2h in 32 DEG C of clear water, is ground into
160 mesh, are dried to adequate moisture, and are put into extraction in extractor, obtain bletilla striata extract, standby；
(2) mix：Bletilla striata extract, Chinese medicine composition in step (1) are mixed to be put into de-airing mixer and stir 4min,
Mixing speed is 80r/min, adds toothpaste matrix, continues to stir 12min, obtains lotion；
(3) by after the sterilized processing of lotion in step (2), packed with composite soft tube.
The raw material of the Chinese medicine composition in parts by weight for tuber of dwarf lilyturf 17kg, leaf of bamboo 12kg, peppermint 15kg, chrysanthemum 15kg,
Pseudo-ginseng 7kg, fruit of Rangoon creeper 6kg, purslane 6kg.
180 mesh are ground into after the tuber of dwarf lilyturf, the leaf of bamboo, peppermint, chrysanthemum, pseudo-ginseng, the fruit of Rangoon creeper and purslane mixing, are dried extremely
Moisture is 20%, then with ultrasonication.
The raw material of the toothpaste matrix is rubbing agent 30kg, excipient 18kg, NMF 35kg, thickener in parts by weight
2kg, essence 1kg, foaming agent 3kg, sweetener 1kg.
The extraction conditions of the bletilla striata are in the step (1)：Ethanol is digestion agent, and Extracting temperature is 26.4 DEG C, extraction time
For 45min, extract 3 times.
It is that adequate moisture refers to that moisture is 25% in the step (1).
Embodiment 4
Formula：Bletilla striata 10kg, toothpaste matrix 82kg, Chinese medicine composition 1.5kg；
Preparation method：(1) bletilla striata is handled：After the bletilla striata is cleaned, temperature is put into soak 3h in 33 DEG C of clear water, is ground into
120 mesh, are dried to adequate moisture, and are put into extraction in extractor, obtain bletilla striata extract, standby；
(2) mix：Bletilla striata extract, Chinese medicine composition in step (1) are mixed to be put into de-airing mixer and stir 5min,
Mixing speed is 60r/min, adds toothpaste matrix, continues to stir 12min, obtains lotion；
(3) by after the sterilized processing of lotion in step (2), packed with composite soft tube.
The raw material of the Chinese medicine composition in parts by weight for tuber of dwarf lilyturf 18kg, leaf of bamboo 12kg, peppermint 18kg, chrysanthemum 12kg,
Pseudo-ginseng 5kg, fruit of Rangoon creeper 3kg, purslane 8kg.
180 mesh are ground into after the tuber of dwarf lilyturf, the leaf of bamboo, peppermint, chrysanthemum, pseudo-ginseng, the fruit of Rangoon creeper and purslane mixing, are dried extremely
Moisture is 23%, then with ultrasonication.
The raw material of the toothpaste matrix is rubbing agent 35kg, excipient 15kg, NMF 30kg, thickener in parts by weight
2kg, essence 1kg, foaming agent 2.5kg, sweetener 1.2kg.
The extraction conditions of the bletilla striata are in the step (1)：Ethanol is digestion agent, and Extracting temperature is 26.4 DEG C, extraction time
For 45min, extract 3 times.
It is that adequate moisture refers to that moisture is 24% in the step (1).
Embodiment 5
Formula：Bletilla striata 8kg, toothpaste matrix 86kg, Chinese medicine composition 2.5kg；
Preparation method：(1) bletilla striata is handled：After the bletilla striata is cleaned, temperature is put into soak 2h in 34 DEG C of clear water, is ground into
140 mesh, are dried to adequate moisture, and are put into extraction in extractor, obtain bletilla striata extract, standby；
(2) mix：Bletilla striata extract, Chinese medicine composition in step (1) are mixed to be put into de-airing mixer and stir 4min,
Mixing speed is 80r/min, adds toothpaste matrix, continues to stir 15min, obtains lotion；
(3) by after the sterilized processing of lotion in step (2), packed with composite soft tube.
The raw material of the Chinese medicine composition in parts by weight for tuber of dwarf lilyturf 12kg, leaf of bamboo 12kg, peppermint 18kg, chrysanthemum 16kg,
Pseudo-ginseng 5kg, fruit of Rangoon creeper 3kg, purslane 8kg.
180 mesh are ground into after the tuber of dwarf lilyturf, the leaf of bamboo, peppermint, chrysanthemum, pseudo-ginseng, the fruit of Rangoon creeper and purslane mixing, are dried extremely
Moisture is 18%, then with ultrasonication.
The raw material of the toothpaste matrix is rubbing agent 33kg, excipient 17kg, NMF 36kg, thickener in parts by weight
3kg, essence 0.9kg, foaming agent 3kg, sweetener 0.8kg.
The extraction conditions of the bletilla striata are in the step (1)：Ethanol is digestion agent, and Extracting temperature is 26.4 DEG C, extraction time
For 45min, extract 3 times.
It is that adequate moisture refers to that moisture is 25% in the step (1).
Embodiment 6
Formula：Bletilla striata 12kg, toothpaste matrix 80kg, Chinese medicine composition 3kg；
Preparation method：(1) bletilla striata is handled：After the bletilla striata is cleaned, temperature is put into soak 2h in 30 DEG C of clear water, is ground into
150 mesh, are dried to adequate moisture, and are put into extraction in extractor, obtain bletilla striata extract, standby；
(2) mix：Bletilla striata extract, Chinese medicine composition in step (1) are mixed to be put into de-airing mixer and stir 5min,
Mixing speed is 50r/min, adds toothpaste matrix, continues to stir 10min, obtains lotion；
(3) by after the sterilized processing of lotion in step (2), packed with composite soft tube.
The raw material of the Chinese medicine composition in parts by weight for tuber of dwarf lilyturf 17kg, leaf of bamboo 15kg, peppermint 16kg, chrysanthemum 14kg,
Pseudo-ginseng 7kg, fruit of Rangoon creeper 4kg, purslane 5kg.
170 mesh are ground into after the tuber of dwarf lilyturf, the leaf of bamboo, peppermint, chrysanthemum, pseudo-ginseng, the fruit of Rangoon creeper and purslane mixing, are dried extremely
Moisture is 23%, then with ultrasonication.
The raw material of the toothpaste matrix is rubbing agent 32kg, excipient 16kg, NMF 32kg, thickener in parts by weight
3kg, essence 1kg, foaming agent 3kg, sweetener 1.2kg
The extraction conditions of the bletilla striata are in the step (1)：Ethanol is digestion agent, and Extracting temperature is 26.4 DEG C, extraction time
For 45min, extract 3 times.
It is that adequate moisture refers to that moisture is 29% in the step (1).
Test example 1
Clinical test suffers from canker sore patient for totally 140, is randomly divided into 7 groups, every group of 20 people, embodiment uses the present invention
Bletilla striata toothpaste prepared by scheme, control group uses snakegourd toothpaste prepared by patent CN201210375804.0, uses sooner or later daily,
By the observation of two weeks by a definite date, as a result as shown above, using bletilla striata ointment effect of the present invention due to control group, wherein to implement
Bletilla striata toothpaste curative effect prepared by the scheme of example 3 is the most notable.
Claims (8)
1. a kind of toothpaste of the bletilla striata, it is characterised in that raw material is in parts by weight：5~12 parts of the bletilla striata, toothpaste matrix 80~90
Part, 1~3 part of Chinese medicine composition.
2. bletilla striata toothpaste as claimed in claim 1, it is characterised in that the raw material is 8 parts of the bletilla striata, toothpaste matrix in parts by weight
86 parts, 2 parts of Chinese medicine composition.
3. bletilla striata toothpaste as claimed in claim 1, it is characterised in that the raw material of the Chinese medicine composition is the tuber of dwarf lilyturf in parts by weight
12~18 parts, 12~16 parts of the leaf of bamboo, 14~18 parts of peppermint, 12~16 parts of chrysanthemum, 5~8 parts of pseudo-ginseng, 3~7 parts of the fruit of Rangoon creeper, dent
4~8 parts of amaranth.
4. bletilla striata toothpaste as claimed in claim 3, it is characterised in that the tuber of dwarf lilyturf, the leaf of bamboo, peppermint, chrysanthemum, pseudo-ginseng, the fruit of Rangoon creeper
And it is ground into 100~200 mesh after purslane mixing, it is 15~25% to dry to moisture, then with ultrasonication.
5. bletilla striata toothpaste as claimed in claim 1, it is characterised in that the raw material of the toothpaste matrix is rubbing agent in parts by weight
30~35 parts, 15~20 parts of excipient, 30~40 parts of NMF, 2~3 parts of thickener, 0.7~1.2 part of essence, foaming agent 2~4
Part, 0.5~1.3 part of sweetener.
6. the preparation method of bletilla striata toothpaste as described in any one of Claims 1 to 5, it is characterised in that comprise the following steps：
(1) bletilla striata is handled：After the bletilla striata is cleaned, temperature is put into soak 1~3h in 30~35 DEG C of clear water, 100~200 are ground into
Mesh, is dried to adequate moisture, and is put into extraction in extractor, obtains bletilla striata extract, standby；
(2) mix：Bletilla striata extract, Chinese medicine composition in step (1) are mixed and are put into 3~5min of stirring in de-airing mixer,
Mixing speed is 50~100r/min, adds toothpaste matrix, continues to stir 10~15min, obtains lotion；
(3) by after the sterilized processing of lotion in step (2), packed with composite soft tube.
7. the preparation method of bletilla striata toothpaste as claimed in claim 6, it is characterised in that the extraction bar of the bletilla striata in the step (1)
Part is：Ethanol is digestion agent, and Extracting temperature is 26.4 DEG C, and extraction time is 45min, is extracted 3 times.
8. the preparation method of bletilla striata toothpaste as claimed in claim 6, it is characterised in that be that adequate moisture is in the step (1)
It is 20~30% to refer to moisture.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710210977.XA CN106943327A (en) | 2017-03-31 | 2017-03-31 | A kind of bletilla striata toothpaste and preparation method thereof |
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| CN201710210977.XA CN106943327A (en) | 2017-03-31 | 2017-03-31 | A kind of bletilla striata toothpaste and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107837225A (en) * | 2017-11-20 | 2018-03-27 | 王建林 | A kind of honey nutrition mothproof toothpaste and preparation method thereof |
| CN107982314A (en) * | 2017-12-16 | 2018-05-04 | 陈延琼 | A kind of herbal composite of medicated toothpaste and preparation method thereof |
| CN108295023A (en) * | 2018-04-12 | 2018-07-20 | 绵阳师范学院 | A kind of Chinese medicinal toothpaste and preparation method thereof |
| CN109528608A (en) * | 2018-12-13 | 2019-03-29 | 北京方诣生物医药有限公司 | A kind of oral cavity bacteriostatic composition |
| CN109864943A (en) * | 2019-04-03 | 2019-06-11 | 黄山峰源生物科技有限公司 | A kind of preparation method and application of bletilla striata polyphenol |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104666153A (en) * | 2013-11-30 | 2015-06-03 | 刘志方 | Antibacterial and antiphlogistic health care mouth wash with honeysuckle flower as main material |
| CN104997701A (en) * | 2015-08-17 | 2015-10-28 | 杭州华胄科技有限公司 | Oral care product containing bletilla striata alcohol extract and having anti-Hp (helicobacter pylori) efficacy |
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2017
- 2017-03-31 CN CN201710210977.XA patent/CN106943327A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104666153A (en) * | 2013-11-30 | 2015-06-03 | 刘志方 | Antibacterial and antiphlogistic health care mouth wash with honeysuckle flower as main material |
| CN104997701A (en) * | 2015-08-17 | 2015-10-28 | 杭州华胄科技有限公司 | Oral care product containing bletilla striata alcohol extract and having anti-Hp (helicobacter pylori) efficacy |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107837225A (en) * | 2017-11-20 | 2018-03-27 | 王建林 | A kind of honey nutrition mothproof toothpaste and preparation method thereof |
| CN107982314A (en) * | 2017-12-16 | 2018-05-04 | 陈延琼 | A kind of herbal composite of medicated toothpaste and preparation method thereof |
| CN108295023A (en) * | 2018-04-12 | 2018-07-20 | 绵阳师范学院 | A kind of Chinese medicinal toothpaste and preparation method thereof |
| CN108295023B (en) * | 2018-04-12 | 2021-05-04 | 绵阳师范学院 | Traditional Chinese medicine toothpaste and preparation method thereof |
| CN109528608A (en) * | 2018-12-13 | 2019-03-29 | 北京方诣生物医药有限公司 | A kind of oral cavity bacteriostatic composition |
| CN109864943A (en) * | 2019-04-03 | 2019-06-11 | 黄山峰源生物科技有限公司 | A kind of preparation method and application of bletilla striata polyphenol |
| CN109864943B (en) * | 2019-04-03 | 2021-07-30 | 黄山峰源生物科技有限公司 | Preparation method and application of bletilla striata polyphenol |
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Application publication date: 20170714 |
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