CN1066152C - 制备n－膦酰基甲基甘氨酸的方法 - Google Patents

制备n－膦酰基甲基甘氨酸的方法 Download PDF

Info

Publication number
CN1066152C
CN1066152C CN96193655A CN96193655A CN1066152C CN 1066152 C CN1066152 C CN 1066152C CN 96193655 A CN96193655 A CN 96193655A CN 96193655 A CN96193655 A CN 96193655A CN 1066152 C CN1066152 C CN 1066152C
Authority
CN
China
Prior art keywords
pmida
pmg
activated carbon
hydrogen peroxide
norit
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN96193655A
Other languages
English (en)
Chinese (zh)
Other versions
CN1183100A (zh
Inventor
中野国雄
平山征男
佐山修二
大桥直彦
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sankyo Co Ltd
Original Assignee
Sankyo Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sankyo Co Ltd filed Critical Sankyo Co Ltd
Publication of CN1183100A publication Critical patent/CN1183100A/zh
Application granted granted Critical
Publication of CN1066152C publication Critical patent/CN1066152C/zh
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
    • C07F9/40—Esters thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
    • C07F9/3804—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)] not used, see subgroups
    • C07F9/3808—Acyclic saturated acids which can have further substituents on alkyl
    • C07F9/3813—N-Phosphonomethylglycine; Salts or complexes thereof

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
CN96193655A 1995-03-07 1996-03-07 制备n－膦酰基甲基甘氨酸的方法 Expired - Fee Related CN1066152C (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP46005/1995 1995-03-07
JP46005/95 1995-03-07
JP4600595 1995-03-07

Publications (2)

Publication Number Publication Date
CN1183100A CN1183100A (zh) 1998-05-27
CN1066152C true CN1066152C (zh) 2001-05-23

Family

ID=12734963

Family Applications (1)

Application Number Title Priority Date Filing Date
CN96193655A Expired - Fee Related CN1066152C (zh) 1995-03-07 1996-03-07 制备n－膦酰基甲基甘氨酸的方法

Country Status (5)

Country Link
KR (1) KR19980702708A (cg-RX-API-DMAC7.html)
CN (1) CN1066152C (cg-RX-API-DMAC7.html)
AU (1) AU4889396A (cg-RX-API-DMAC7.html)
TW (1) TW322481B (cg-RX-API-DMAC7.html)
WO (1) WO1996027602A1 (cg-RX-API-DMAC7.html)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5962729A (en) * 1998-05-14 1999-10-05 Calgon Carbon Corporation Method for the manufacture of N-phosphonomethylglycine from N-phosphonomethyliminodiacetic acid using a catalytic carbon
ES2195929T3 (es) 1999-07-23 2003-12-16 Basf Ag Procedimiento para la obtencion de glifosatos o de una sal de los mismos.
DE19938622C2 (de) * 1999-08-14 2002-10-02 Sueddeutsche Kalkstickstoff Verfahren zur Herstellung von N-(Phosphonomethyl)glycin
CA2409745A1 (en) * 2000-05-22 2001-12-06 Monsanto Technology, Llc Reaction systems for making n-(phosphonomethyl)glycine compounds
CN101311183B (zh) * 2000-05-22 2011-08-31 孟山都技术有限责任公司 制备n-(膦酰基甲基)甘氨酸化合物的反应系统
CN1301259C (zh) * 2004-01-16 2007-02-21 广东琪田农药化工有限公司 由双甘膦制备草甘膦的方法
CN104585228B (zh) * 2005-03-04 2017-05-24 孟山都技术公司 减轻用除草剂草甘膦制剂处理的草甘膦耐受性转基因棉花植物内的坏死
CN101092429B (zh) * 2006-06-23 2010-08-11 北京紫光英力化工技术有限公司 一种催化氧化法制备草甘膦的方法
CN101092428B (zh) * 2006-06-23 2011-04-06 北京紫光英力化工技术有限公司 一种双甘膦空气氧化制备草甘膦的新工艺
CN101508701B (zh) * 2008-12-10 2012-09-05 上海泰禾(集团)有限公司 一种活性碳作催化剂氧气氧化双甘膦制备草甘膦的方法
JP5815506B2 (ja) 2010-03-31 2015-11-17 クラレケミカル株式会社 活性炭及びその用途
KR101246278B1 (ko) * 2012-09-18 2013-03-22 주식회사 천보 이미노디아세트산의 합성방법
CN104829649A (zh) * 2015-05-05 2015-08-12 安徽省益农化工有限公司 采用双甘膦为原料生产草甘膦的方法

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3969398A (en) * 1974-05-01 1976-07-13 Monsanto Company Process for producing N-phosphonomethyl glycine
EP0088180A1 (en) * 1982-03-08 1983-09-14 Geshuri Laboratories Ltd. N-phosphonomethylglycine derivatives
EP0162035A2 (en) * 1984-05-10 1985-11-21 Monsanto Company Process for the selective production of secondary and primary amines
EP0980334A2 (en) * 1997-05-09 2000-02-23 The Procter & Gamble Company Flexible, collapsible, self-supporting storage bags and containers

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IL66137A (en) * 1982-06-25 1986-03-31 Geshuri Lab Ltd Process for producing n-phosphonomethylglycine isopropyl amine salt and herbicidal compositions prepared therewith
ZA853525B (en) * 1984-05-10 1986-06-25 Monsanto Co Oxidation catalyst

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3969398A (en) * 1974-05-01 1976-07-13 Monsanto Company Process for producing N-phosphonomethyl glycine
EP0088180A1 (en) * 1982-03-08 1983-09-14 Geshuri Laboratories Ltd. N-phosphonomethylglycine derivatives
EP0162035A2 (en) * 1984-05-10 1985-11-21 Monsanto Company Process for the selective production of secondary and primary amines
EP0980334A2 (en) * 1997-05-09 2000-02-23 The Procter & Gamble Company Flexible, collapsible, self-supporting storage bags and containers

Also Published As

Publication number Publication date
HK1017360A1 (en) 1999-11-19
KR19980702708A (ko) 1998-08-05
WO1996027602A1 (en) 1996-09-12
TW322481B (cg-RX-API-DMAC7.html) 1997-12-11
CN1183100A (zh) 1998-05-27
AU4889396A (en) 1996-09-23

Similar Documents

Publication Publication Date Title
CN1066152C (zh) 制备n－膦酰基甲基甘氨酸的方法
CN1286788C (zh) 2,2,2－三氟乙醇的制造方法
CN1293944C (zh) 烯烃氢氰化用的镍/磷配体催化剂的制备方法
CN1301210C (zh) 非危险溴化试剂的制备
CN1675159A (zh) 制备酸式甲酸盐的方法和设备及所述甲酸盐的应用
CN100343259C (zh) 制备3－丙烯基头孢菌素dmf溶剂化物的方法
CN1055693C (zh) 生物可利用的结晶形式头孢呋辛酯
CN1088269A (zh) 回收铑的方法
CN87106482A (zh) 苯甲酸衍生物的制备方法
CN1151155A (zh) 用基于铱和碘化物的可溶性催化剂制备羧酸或相应酯的方法
CN1926125A (zh) 环状碳酸酯类的制造方法
US5948938A (en) Process for preparing N-phosphonomethylglycine
CN1195763C (zh) 制备n－膦酰甲基甘氨酸的方法
CN1070195C (zh) 制备有机磷酯化合物的方法
CN1239507C (zh) N－膦酰基甲基甘氨酸的制备方法
JP3719756B2 (ja) Ｎ−ホスホノメチルグリシンの製造方法
CN1715268A (zh) 双硫醇衍生物的制备方法
CN1681758A (zh) 制备4－烷基苯酚的方法
CN1080265C (zh) 7－烷氧烷基－1,2,4－三唑并[1,5－a]嘧啶衍生物的制备方法
CN1209138A (zh) 9,11β－环氧甾族化合物的制备方法
CN1430613A (zh) 制备2－氯－5－氯甲基－1,3－噻唑的方法
CN1289457C (zh) 3,3－二甲基－2－甲酰基环丙烷羧酸衍生物的制造方法
CN101065387A (zh) 含磷酰胆碱基的化合物及其制备方法
CN1220687C (zh) 制备2－氰基亚氨基－1,3－噻唑烷的方法
NZ561684A (en) An improved process for the purification of perindopril

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
C19 Lapse of patent right due to non-payment of the annual fee
CF01 Termination of patent right due to non-payment of annual fee