CN106422407A - Method for purifying and extracting spices - Google Patents
Method for purifying and extracting spices Download PDFInfo
- Publication number
- CN106422407A CN106422407A CN201611005447.3A CN201611005447A CN106422407A CN 106422407 A CN106422407 A CN 106422407A CN 201611005447 A CN201611005447 A CN 201611005447A CN 106422407 A CN106422407 A CN 106422407A
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- China
- Prior art keywords
- extracting
- bittern material
- extraction
- spices
- main tank
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
Abstract
The invention discloses a method for purifying and extracting spices. The method particularly comprises the following steps: (1) extracting and concentrating the spices: adding water to the spices and then placing the spices added with water to an extracting tank, wherein the mass ratio of water to the spices is 8: 1, sealing and heating the extracting tank, wherein the heating temperature is 100 DEG C, carrying out decoction on the spices, then adding water to the spices for two times, wherein the adding amounts of water are respectively 7 and 6 times of the mass of the spices, and continuously carrying out the decoction according to the method; (2) collecting aromatic oil; (3) further concentrating brine: further concentrating the brine prepared in the step (1) in a concentrator, controlling the temperature at 70 to 80 DEG C, controlling the vacuum degree of the concentrator at 0.07MPa and the concentration time for 30 to 60 minutes, wherein the density of the concentrated brine at the temperature of 60 DEG C is 1.2kg/m<3>. The method for purifying and extracting the spices disclosed by the invention is simple in technological process, beneficial to industrial production, and capable of fully purifying and extracting materials in the spices, so that spiced foods with higher quality can be made.
Description
Technical field
The present invention is a kind of purification extracting process, the purification extracting process of especially a kind of bittern material.
Background technology
Pot-stewed meat or fowl is the common name of cool food dish in cookery, is each department home cooking that what's frequently heard can be repeated in detail.Bittern material is to make pot-stewed meat or fowl
Flavoring agent, generally refer to make salt Chinese medicine spice.Bittern material has a strong fragranced, the smell of removable raw-food material,
Function with the fragrance increasing food.Processing method common in the market is all bittern material to be placed on to add water in halogen pot just boil
Make salt, and without purification extraction, different bittern material formula can make the salt of different flavor.This salt can not
Fully absorb the purification of bittern material.
Content of the invention
For above-mentioned the deficiencies in the prior art, the invention provides a kind of purification extracting process of bittern material.
For achieving the above object, the technical solution used in the present invention is：A kind of purification extracting process of bittern material, concrete steps
It is：
(1) extraction of bittern material concentrates：Bittern material is added water to be put in extraction pot, and the mass ratio of water and bittern material is 8：1, to carrying
Tank is taken to carry out sealing, heat, heating-up temperature is 100 DEG C, and bittern material is decocted, decocting time is 30-60 minute, decocts process
In be stirred continuously, and adopt recirculated water, water is extracted out from the lower end of extraction pot, is recycled to upper end and flows down.After decocting time arrives, by halogen
Material filters, and water is released from extraction pot bottom；Then add water twice again in bittern material, quality is respectively 7 times and 6 of bittern material quality
Times, continue to decoct according to above-mentioned method.
(2) collect aromatic oil：During the decocting of bittern material, the aromatic oil in bittern material can evaporate, and is filled by collecting
Put and aromatic oil is collected.
(3) concentration further of salt：The salt that step (1) is obtained further is concentrated in concentrator, temperature
Degree controls at 70-80 DEG C, and in 0.07MPa, concentration time is 30-60 minute to the vacuum degree control of concentrator.Salt after concentration
It is 1.2kg/m in 60 DEG C of density3.
A kind of extraction pot, including duplex strainer, extracts main tank, oil water separator, cooler, horizontal condenser, foam
Catcher and duplex strainer, the main tank top of described extraction is end socket, described end socket is provided with foam catcher and external-open is thrown
Material hole, the entrance point of described oil water separator with extraction main pot sidewall above be connected, the port of export of described oil water separator with cold
But device entrance connects, and the outlet of described cooler is connected with horizontal condenser entrance, and aerofluxuss are passed through in described horizontal condenser outlet
Pipe is connected with foam catcher, and the main pot bottom of described extraction is provided with steam feeder and ash gate, and described duplex strainer leads to
Cross discharge nozzle and be connected with extracting main pot bottom.
Preferably, the described side wall extracting main tank is provided with ash gate and opens cylinder, and described ash gate opens cylinder head
Connected by cylinder saddle, it is inner cylinder body that described ash gate opens cylinder middle section, described inner cylinder body upper and lower side is provided with chuck, institute
State ash gate unlatching cylinder bottom to be connected with extracting main pot bottom by conduit, the main tank wall of described extraction is provided with insulation
Layer, is provided with warming plate between described heat-insulation layer, and the main tank lower inside of described extraction is provided with drainage screen, below drainage screen
It is provided with steam distributor, the side wall of the main tank of described extraction is additionally provided with tank body ear mount, air inlet pipe, and described tank body ear mount is located at and carries
Take above the side wall of main tank, described air inlet pipe is located at the middle part extracting main tank, and described air inlet pipe is provided with ring flange.
Preferably, described end socket is provided with scope section.
Preferably, it is provided with regarding cylinder on main tank connected discharge nozzle with extracting in duplex strainer.
Present invention process flow process is simple, beneficial to industrialized production, can sufficiently purify the material extracting in bittern material, makes
Go out the higher pot-stewed meat or fowl of quality.
Brief description
Fig. 1 is the structural representation of extraction pot of the present invention.
Fig. 2 is the structural representation of extraction pot upper end.
In figure：1- air inlet pipe, the 2- main tank of extraction, 3- oil water separator, 4- cooler, 5- horizontal condenser, 6- foam are caught
Storage, 7- external-open batching hole, 8- duplex strainer, 9- divide depending on cylinder, 10- discharge nozzle, 11- drainage conduit, 12- ash gate, 13- steam
Cloth device, 14- scope section, 15- ash gate open cylinder, 16- drainage screen, 17- steam feeder, 18- end socket, 19- ear mount,
20- ring flange.
Specific embodiment
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clear, complete
Site preparation description is it is clear that described embodiment is only a part of embodiment of the present invention, rather than whole embodiments.It is based on
Embodiment in the present invention, it is every other that those of ordinary skill in the art are obtained under the premise of not making creative work
Embodiment, broadly falls into the scope of protection of the invention.
A kind of purification extracting process of bittern material, comprises the concrete steps that：
(1) extraction of bittern material concentrates：Take 100kg bittern material, plus the water of 800kg is put in extraction pot, and extraction pot is carried out
Sealing, heating, heating-up temperature is 100 DEG C, bittern material is decocted, decocting time is 50 minutes, is stirred continuously during decocting,
And adopting recirculated water, water is extracted out from the lower end of extraction pot, is recycled to upper end and flows down.After decocting time arrives, bittern material is filtered, water from
Extract pot bottom to release；Then add water twice again in bittern material, quality is respectively 700kg and continues according to the above-mentioned side of 600kg
Method decocts.
(2) collect aromatic oil：During the decocting of bittern material, the aromatic oil in bittern material can evaporate, and is filled by collecting
Put and aromatic oil is collected.
(3) concentration further of salt：In concentrator, (Wenzhou City's imperial examinations light industry and machinery have the salt that step (1) is obtained
The SJN-2-2000 dual-effect concentrator of limit company) in further concentrated, temperature control at 70 DEG C, the vacuum of concentrator
Control in 0.07MPa, concentration time is 45 minutes, finally obtains the salt of 800kg, the salt after concentration in 60 DEG C of density is
1.2kg/m3.
As shown in Figure 1：A kind of extraction pot, including duplex strainer 8, extracts main tank 2, oil water separator 3, cooler 4, crouches
Formula condenser 5, foam catcher 6 and duplex strainer 8, main tank 2 top of described extraction is end socket 18, is provided with end socket 18
Foam catcher 6, external-open batching hole 7 and scope section 14, can observe, by scope section 14, the feelings extracted within main tank 2
Condition, the entrance point of described oil water separator 3 with extract main tank 2 side wall above be connected, the port of export of described oil water separator 3 with cold
But device 4 entrance connects, and the outlet of described cooler 4 is connected with horizontal condenser 5 entrance, and aerofluxuss are passed through in horizontal condenser 5 outlet
Pipe is connected with foam catcher 6, and main tank 2 bottom of described extraction is provided with steam feeder 17 and ash gate 12, described duplex mistake
Filter 8 passes through discharge nozzle 10 and is connected with extracting main tank 2 bottom.
The side wall extracting main tank 2 is provided with ash gate and opens cylinder 15, ash gate is opened cylinder 15 top and passed through cylinder
Bearing connects, and middle part is inner cylinder body, and inner cylinder body upper and lower side is provided with chuck, opens cylinder 15 bottom in ash gate and passes through conduit
It is connected with extracting main tank 2 bottom, on extracting main tank 2 outer wall, is provided with heat-insulation layer, be responsible for wall contacts in heat-insulation layer with extracting
Place be provided with warming plate, extract main tank 2 lower inside be provided with drainage screen 16, the mesh quality of drainage screen 6 and precision
Height, preferably laser boring drainage screen, there is corrosion-resistant coating, with bittern material, corrosion phenomenon will not occur.Filter effect can be ensured, and
Bittern material quality can not be destroyed；It is provided with steam distributor 13 below drainage screen 16, by steam distributor 13, steam heat is flow to
Uniformly guiding, it is ensured that steam hot-fluid is equally distributed entering drainage screen 16, is uniform to bittern material heating, is not in row
Temperature contrast.It is additionally provided with tank body ear mount 19 in the side wall extracting main tank 2, air inlet pipe 1, wherein tank body ear mount 19 are located at extracts master
Above the side wall of tank 2, air inlet pipe 1 is located at the middle part extracting main tank 2, and described air inlet pipe 1 is provided with ring flange 20.
It is provided with regarding cylinder 9 with extracting on the discharge nozzle 10 that main tank 2 is connected in duplex strainer 8, the material depending on cylinder 9 is preferably
Boron glass, boron glass is high temperature resistant, anti-high pressure, by can be observed how the situation of expects pipe 10 regarding cylinder 9.
The bittern material and water needing processing is poured into from external-open batching hole 7, closes external-open batching hole 7 and drainage screen 16, bittern material
People drop under gravity on the drainage screen 16 extracting within main tank 2, bittern material is piled up on drainage screen 16, starts
Steam feeder 17, the hot-fluid that steam feeder 17 provides uniformly flows to drainage screen 16 through steam distributor 13, in hot-fluid
In the presence of a part of bittern material saltwater brine start to evaporate, one is condensed with inwall attachment, with the continuation of hot-fluid, condensation more
Come more, fall to falling after rise above drainage screen 16 finally along inwall, a part enters oil water separator 3 along pipeline,
Oil water separator 3 occurs to separate, and so that aromatic oil is separated with vapor, at this moment the aromatic oil isolated is reclaimed, then remain
The port of export that the gasification aromatic oil that remaining part is divided enters oil water separator 3 with air-flow enters cooler 4 along pipeline, in cooler
In 4, the aromatic oil of gasification is lowered the temperature, realize to fragrant oil recovery, due to air-flow continuous action, will not be complete in cooler 4
Full aromatic oil is reclaimed, remainder enters horizontal condenser 5 from cooler 4 port of export along pipeline, by horizontal cold
Condenser 5 reclaims to gasification aromatic oil again, due to can significantly provide condensation recovering effect by dual cold filtration,
The mixing liquid (aromatic oil and water, containing a small amount of vapor) entering horizontal condenser 5 is caught along discharge duct entrance foam
Storage 6, mixing liquid tangentially enters along wall from the upper part of tank, for the helical movement downwards by the constraint of wall, inertia from
Under mental power function, heavy being thrown to wall and separated with air-flow of quality, then drop down onto tank bottoms along wall, finally enter the main tank 2 of extraction
Inside, forms recirculated water, and the gas after separating is for the helical movement from bottom to top near central shaft, finally arranges from top exit
Go out gas.
After opening drainage screen 16, the saltwater brine after steaming and decocting passes through drainage screen 16 to enter in discharge nozzle 10 and enters duplex strainer 8,
Realize the separating-purifying to saltwater brine in the presence of filter bag, drainage conduit 11 from duplex strainer 8 for the salt discharge it is not necessary to
Filtering residue takes out from filter bag, using duplex strainer 8 benefit be can simultaneously using it is also possible to be used alone one of,
Another is as standby or maintenance.
After the completion of reaction, steam off feeder 17, opens bat gate opening cylinder, reduces the gas extracting in main tank 2
Pressure, after air pressure drops to normal value, opens ash gate 12, bittern material filtering residue is disposed.
Claims (5)
1. a kind of purification extracting process of bittern material, comprises the concrete steps that：
(1) extraction of bittern material concentrates：Bittern material is added water to be put in extraction pot, and the mass ratio of water and bittern material is 8：1, to extraction pot
Carry out sealing, heat, heating-up temperature is 100 DEG C, and bittern material is decocted, decocting time is 30-60 minute, during decocting not
Disconnected stirring, and adopt recirculated water, water is extracted out from the lower end of extraction pot, is recycled to upper end and flows down.After decocting time arrives, by bittern material mistake
Filter, water is released from extraction pot bottom；Then add water twice again in bittern material, quality is respectively 7 times and 6 times of bittern material quality, continues
Continue and decoct according to above-mentioned method；
(2) collect aromatic oil：During the decocting of bittern material, the aromatic oil in bittern material can evaporate, will by collection device
Aromatic oil collects；
(3) concentration further of salt：The salt that step (1) is obtained further is concentrated in concentrator, temperature control
At 70-80 DEG C, in 0.07MPa, concentration time is 30-60 minute to the vacuum degree control of concentrator to system.Salt after concentration is 60
DEG C density be 1.2kg/m3.
2. as claimed in claim 1 a kind of bittern material purification extracting process it is characterised in that：Described extraction pot includes duplex
Filter, extracts main tank, oil water separator, cooler, horizontal condenser, foam catcher and duplex strainer, described extraction
Main tank top is end socket, and described end socket is provided with foam catcher and external-open batching hole, the entrance point of described oil water separator
It is connected above main pot sidewall with extracting, the port of export of described oil water separator is connected with cooler entrance, the going out of described cooler
Mouth is connected with horizontal condenser entrance, and described horizontal condenser outlet is connected with foam catcher by exhaustor, described extraction
Main pot bottom is provided with steam feeder and ash gate, and described duplex strainer passes through discharge nozzle and is connected with extracting main pot bottom.
3. as claimed in claim 2 a kind of bittern material purification extracting process it is characterised in that：The described side wall extracting main tank sets
It is equipped with ash gate and opens cylinder, described ash gate is opened cylinder head and connected by cylinder saddle, and described ash gate opens cylinder
Middle part is inner cylinder body, and described inner cylinder body upper and lower side is provided with chuck, and described ash gate is opened cylinder bottom and passed through conduit and extraction
Main pot bottom connects, and the main tank wall of described extraction is provided with heat-insulation layer, is provided with warming plate between described heat-insulation layer, described carries
Take main tank lower inside to be provided with drainage screen, be provided with steam distributor below drainage screen, the side wall of the main tank of described extraction
It is additionally provided with tank body ear mount, air inlet pipe, described tank body ear mount is located above the side wall extracting main tank, described air inlet pipe is located to be extracted
The middle part of main tank, described air inlet pipe is provided with ring flange.
4. as claimed in claim 2 a kind of bittern material purification extracting process it is characterised in that：It is provided with visor on described end socket
Part.
5. as claimed in claim 2 a kind of bittern material purification extracting process it is characterised in that：Lead with extracting in duplex strainer
It is provided with regarding cylinder on tank connected discharge nozzle.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611005447.3A CN106422407A (en) | 2016-11-15 | 2016-11-15 | Method for purifying and extracting spices |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611005447.3A CN106422407A (en) | 2016-11-15 | 2016-11-15 | Method for purifying and extracting spices |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106422407A true CN106422407A (en) | 2017-02-22 |
Family
ID=58208636
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611005447.3A Pending CN106422407A (en) | 2016-11-15 | 2016-11-15 | Method for purifying and extracting spices |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106422407A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107047819A (en) * | 2017-02-27 | 2017-08-18 | 四川星麻哥食品有限公司 | It is a kind of that the equipment that flavour and fragrance substance produces flavored oils is extracted from spice |
| CN110180213A (en) * | 2019-06-26 | 2019-08-30 | 重庆真本味食品有限公司 | A kind of spice extraction enrichment facility |
| CN111449226A (en) * | 2020-04-11 | 2020-07-28 | 重庆真本味食品有限公司 | Process for purifying and extracting brine material |
| CN113201402A (en) * | 2021-04-22 | 2021-08-03 | 江西思派思香料化工有限公司 | Process and equipment for preparing spice by distillation method |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107047819A (en) * | 2017-02-27 | 2017-08-18 | 四川星麻哥食品有限公司 | It is a kind of that the equipment that flavour and fragrance substance produces flavored oils is extracted from spice |
| CN110180213A (en) * | 2019-06-26 | 2019-08-30 | 重庆真本味食品有限公司 | A kind of spice extraction enrichment facility |
| CN111449226A (en) * | 2020-04-11 | 2020-07-28 | 重庆真本味食品有限公司 | Process for purifying and extracting brine material |
| CN113201402A (en) * | 2021-04-22 | 2021-08-03 | 江西思派思香料化工有限公司 | Process and equipment for preparing spice by distillation method |
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Application publication date: 20170222 |
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