CN205948410U - Naringin crystallization treatment tank - Google Patents
Naringin crystallization treatment tank Download PDFInfo
- Publication number
- CN205948410U CN205948410U CN201620732296.0U CN201620732296U CN205948410U CN 205948410 U CN205948410 U CN 205948410U CN 201620732296 U CN201620732296 U CN 201620732296U CN 205948410 U CN205948410 U CN 205948410U
- Authority
- CN
- China
- Prior art keywords
- tank body
- manhole
- filter screen
- pneumatic door
- naringin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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Abstract
The utility model provides a naringin crystallization treatment tank, characterized by advances discharge gate, shower, manhole, sight glass, exhaust -valve, gas -phase pipe, steel lining net, business turn over material nest of tubes one -tenth by the jar body, temperature detect ware, cooling jacket, steam heating pipe, filter screen, pneumatic door, liquid. The jar body has cooling jacket for totally enclosed nonrust steel can, is close to the bottom and locates to be equipped with efficient steam heating pipe. The temperature detect ware is equipped with in the middle part trompil of the jar body. Jar bottom be pneumatic door, and the bottom connects into that discharging pipe to liquid advances the discharge gate, and pneumatic door pan kou locates to be equipped with removable filter screen. The top is equipped with the shower in jar. Jar upper portion is equipped with the manhole. The glass sight glass is equipped with at the manhole middle part. The tank deck is equipped with the exhaust -valve. The jar is equipped with gas -phase pipe. The beneficial effects of the utility model are that: simple structure is reasonable, and is multiple functional, and it can carry out each item operations such as filtration, crystallization, suction filtration, concentration, heavy crystal of naringin production, reduces intensity of labour, improves production efficiency.
Description
Technical field
This utility model is related to a kind of natural extract purification apparatus, specifically a kind of naringin crystal refining tank.
Background technology
At present, the production of natural plant extracts naringin need to be through raw material pulverizing, steaming and decocting extraction, filtration, crystallization, centrifugal drying
Dry, recrystallization, the again operation such as centrifuge dripping, drying, the equipment that wherein crystal refining process uses just has flame filter press, knot
Brilliant settling tank, board-like centrifuge, mobile pump, heating for dissolving tank etc., using equipment more, operating procedure is numerous and diverse, low production efficiency
Under, and because intermediate link is excessive, process time is partially long, it is possible to create pollution or microbial reproduction, impact product quality and health
Safety.
Content of the invention
This utility model is that in the production for current natural plant extracts naringin, crystal refining process uses equipment
More, operating procedure is numerous and diverse, production efficiency is low, and because intermediate link is excessive, process time is partially long, it is possible to create pollution or micro-
Biological self reproducing, the deficiency of impact product quality and safe and sanitary, a kind of naringin crystal refining tank is provided.
A kind of this utility model naringin crystal refining tank mainly employs the design of integration function, incorporates filtration, adds
The functions such as heat, cooling, crystallization, concentration, sucking filtration, recrystallization, it is achieved thereby that the efficient crystallization of naringin refines produce.
Technical solution of the present utility model is：A kind of naringin crystal refining tank is by tank body, hygrosensor, cooling
Chuck, steam-heating pipe, filter screen, pneumatic door, liquid feed inlet and outlet, shower, manhole, visor, exhaust-valve, gas phase pipe, steel lining
Net, feed and exhaust tube composition.Tank body is hermetic stainless cylinder of steel, with cooling jacket, equipped with efficient steam at bottom
It is characterised in that the perforate of steam-heating pipe bottom, Pericarpium Citri grandiss glycosidal crystalline will not block steam vent to heating tube.In the middle part of tank body, perforate is equipped with temperature
Degree detector, for monitoring temperature in tank.Tank base is pneumatic door, and pneumatic door is discoid, and pneumatic door bottom taps into discharging
To liquid feed inlet and outlet, equipped with filter screen at pneumatic door Pan Kou, filter screen all has support steel lining net it is characterised in that filter screen is to pipe up and down
Exchangeable, can change as needed at any time, and specification is 200-300 mesh, can filter off the solid impurity in extracting solution when can feed,
Crystallize and naringin crystal during complete heel row mother solution, can be prevented to run off, and the water carried secretly in crystallization can be extracted when discharging opening connects vacuum
Point, reach the effect of sucking filtration.In tank body, top is provided with shower, it is characterized in that having spray apertures below shower, spray apertures
Orientation angle ordered distribution, during spray, the big I of the cooperation water yield covers most of region in tank, reaches effective drip washing, can distinguish
It is sprayed using tap water and pure water, spray can effectively remove the mother solution of residual in crystallization when crystallizing sucking filtration, improve knot
Brilliant purity.Jar top is provided with manhole, for the turnover of personnel when overhauling, and throws in nucleus from there when crystallization is difficult.People
Equipped with glass visor in the middle part of hole, for observing situation in tank.Tank deck is provided with exhaust-valve, for controlling the air pressure in tank.On tank body
Portion is provided with gas phase pipe, connects condenser and vacuum system, collects for gas phase when concentrating and vacuum takes out material.
The beneficial effects of the utility model are：Simple and reasonable, multiple functional, it can carry out the mistake of naringin production
The operations such as filter, crystallization, sucking filtration, concentration, recrystallization, reduce labor intensity, improve production efficiency.
Brief description
Fig. 1 is a kind of cut-away view of naringin crystal refining tank.
In figure, 1, tank body；2nd, hygrosensor；3rd, cooling jacket；4th, steam-heating pipe；5th, filter screen；6th, pneumatic door；7th, liquid
Body feed inlet and outlet；8th, shower；9th, manhole；10th, visor；11st, exhaust-valve；12nd, gas phase pipe；15th, feed and exhaust tube.
Fig. 2 is a kind of tank bottoms cut-away view of naringin crystal refining tank.
In figure, 13, steel lining net；5th, filter screen；14th, seal washer；15th, feed and exhaust tube.
A kind of shower upward view of Fig. 3 naringin crystal refining tank.
In figure, 16, spray apertures；8th, shower.
Specific embodiment
Below, describe embodiment of the present utility model with reference to the accompanying drawings in detail.
As shown in Figure 1, 2, 3, a kind of naringin crystal refining tank, is by by tank body（1）, hygrosensor（2）, cooling folder
Set（3）, steam-heating pipe（4）, filter screen（5）, pneumatic door（6）, liquid feed inlet and outlet（7）, shower（8）, manhole（9）, visor
（10）, exhaust-valve（11）, gas phase pipe（12）, steel lining net（13）, feed and exhaust tube（15）Composition.Tank body（1）For hermetic stainless
Cylinder of steel, with cooling jacket（3）, equipped with efficient steam-heating pipe at bottom（4）It is characterised in that steam-heating pipe
（4）Bottom perforate, Pericarpium Citri grandiss glycosidal crystalline will not block steam vent.In the middle part of tank body, perforate is equipped with hygrosensor（2）, for monitoring in tank
Temperature.Jar bottom is pneumatic door（6）, pneumatic door（6）For discoid, pneumatic door（6）Bottom taps into discharge nozzle（15）To liquid
Feed inlet and outlet（7）, pneumatic door（6）Equipped with replaceable filter screen at Pan Kou（5）, filter screen（5）All there is support steel lining net up and down（13）, its
It is characterised by filter screen（5）For exchangeable, can change at any time as needed, specification is 200-300 mesh, can filter off extraction during charging
Solid impurity in liquid, can prevent naringin crystal to run off, and work as discharging opening when crystallizing complete heel row mother solution（7）Connecing can during vacuum
Extract the moisture carried secretly in crystallization, reach the effect of sucking filtration.Tank body（1）Top is provided with shower（8）, it is characterized in that shower
（8）Lower section has spray apertures（16）, spray apertures（16）Orientation angle ordered distribution, during spray, the big I of the cooperation water yield covers
In tank, most of region, reaches effective drip washing, can be sprayed using tap water and pure water respectively, the spray when crystallizing sucking filtration
The mother solution of residual in crystallization can effectively be removed, improve crystallization purity.Tank（1）Top is provided with manhole（9）, for people when overhauling
The turnover of member, and throw in nucleus from there when crystallization is difficult.Manhole（9）Middle part is equipped with glass visor（10）, for observing tank
Interior situation.Tank body（1）Top is provided with exhaust-valve（11）, for controlling tank body（1）Interior air pressure.Tank body（1）It is provided with gas phase pipe
（12）, connect condenser and vacuum system, collect for gas phase when concentrating and vacuum takes out material.
During work, close pneumatic bottom door（6）And all valves, gas phase pipe（12）Connection vacuum system, tank body (1) forms one
Fixed vacuum, from liquid feed inlet and outlet (7) extracting high-temperature Fructus Citri grandiss fruit extracting solution（Temperature>80℃）, observe charging from visor (10)
Amount, when inlet amount reaches requirement, closing liquid feed inlet and outlet (7), disconnect the bonding in vacuum of gas phase pipe (12), open exhaust-valve
(11), open the inlet/outlet valve of cooling jacket (3), extracting solution temperature drop, begin with crystallization and separate out, observe knot from visor (10)
Brilliant situation, after 24-36 hour, crystallize completely, closes cooling jacket (3) Inlet and outlet water valve, the cooling water in emptying chuck.Open
Waste liquor after liquid feed inlet and outlet (7) discharge crystallization, purpose product naringin crystal is intercepted by tank bottoms replaceable filter screen (5)
Stay in tank.After waste liquor drains, liquid feed inlet and outlet (7) connects vacuum system, extracts the waste liquor carried secretly in crystallization, sprays simultaneously
Shower pipe (8) accesses pure water and is sprayed, and crystallization is carried out with sufficient filtering and washing roguing.Sucking filtration finishes rear closing liquid turnover
Material mouth（7）, add appropriate pure water from shower (8), the steam valve opening steam-heating pipe (4) is heated, by temperature
Degree detector（2）Observe and control temperature in tank, Pericarpium Citri grandiss glycosidal crystalline is heated dissolving, from visor（10）Observe dissolving situation.Crystallize
After CL, steam off valve, open cooling jacket（3）Cooling water turnover valve, feed liquid is lowered the temperature, temperature drop
Naringin crystallizes precipitation again afterwards.After recrystallization is complete, as above discharges waste liquor filtering and washing, obtain the half-dried Fructus Citri grandiss of high-purity
Skin glycoside product（To be dried）, open pneumatic bottom door (6), hopper receives the product after recrystallization.
When finding that crystallization is difficult, manhole (9) can be opened and put into appropriate nucleus（Naringin crystal）.
When feed concentration is low, close exhaust-valve (11), gas phase pipe (12) connects vacuum system, open steam-heating pipe
(4) steam valve, carries out heating in vacuum concentration, reclaims and use after the moisture of evaporation is condensed.Observe in tank from visor (10)
Liquid level judges concentrating degree.Lower the temperature again after the completion of concentration and crystallized.
Claims (1)
1. a kind of naringin crystal refining tank, is characterized in that by tank body（1）, hygrosensor（2）, cooling jacket（3）, steam adds
Heat pipe（4）, filter screen（5）, pneumatic door（6）, liquid feed inlet and outlet（7）, shower（8）, manhole（9）, visor（10）, exhaust-valve
（11）, gas phase pipe（12）, steel lining net（13）, feed and exhaust tube（15）Composition；Tank body（1）For hermetic stainless cylinder of steel, with cold
But chuck（3）, equipped with efficient steam-heating pipe at bottom（4）, steam-heating pipe（4）Bottom perforate；Open in the middle part of tank body
Hole is equipped with hygrosensor（2）；Tank body（1）Bottom is pneumatic door（6）, pneumatic door（6）For discoid, bottom taps into discharge nozzle
（15）To liquid feed inlet and outlet（7）, pneumatic door（6）Equipped with removable filter screen at Pan Kou（5）, removable filter screen（5）Up and down
All there is support steel lining net（13）, filter screen（5）For exchangeable, specification is 200-300 mesh；Tank body（1）Top is provided with shower
（8）, shower（8）Lower section has spray apertures（16）, spray apertures（16）Orientation angle ordered distribution；Tank body（1）Top is provided with
Manhole（9）；Manhole（9）Middle part is equipped with glass visor（10）；Tank body（1）Top is provided with exhaust-valve（11）；Tank body（1）It is provided with gas phase
Pipe（12）, connect condenser and vacuum system.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620732296.0U CN205948410U (en) | 2016-07-13 | 2016-07-13 | Naringin crystallization treatment tank |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620732296.0U CN205948410U (en) | 2016-07-13 | 2016-07-13 | Naringin crystallization treatment tank |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205948410U true CN205948410U (en) | 2017-02-15 |
Family
ID=57970403
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620732296.0U Expired - Fee Related CN205948410U (en) | 2016-07-13 | 2016-07-13 | Naringin crystallization treatment tank |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205948410U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108325263A (en) * | 2018-02-06 | 2018-07-27 | 浙江亚光科技股份有限公司 | Suction filtration tank |
| CN112169741A (en) * | 2020-11-16 | 2021-01-05 | 杭州重力脚轮科技有限公司 | Polyurethane stirring reaction kettle |
-
2016
- 2016-07-13 CN CN201620732296.0U patent/CN205948410U/en not_active Expired - Fee Related
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108325263A (en) * | 2018-02-06 | 2018-07-27 | 浙江亚光科技股份有限公司 | Suction filtration tank |
| CN112169741A (en) * | 2020-11-16 | 2021-01-05 | 杭州重力脚轮科技有限公司 | Polyurethane stirring reaction kettle |
| CN112169741B (en) * | 2020-11-16 | 2022-03-22 | 杭州重力脚轮科技有限公司 | Polyurethane stirring reaction kettle |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170215 Termination date: 20170713 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |