CN111449226A - Process for purifying and extracting brine material - Google Patents
Process for purifying and extracting brine material Download PDFInfo
- Publication number
- CN111449226A CN111449226A CN202010281997.8A CN202010281997A CN111449226A CN 111449226 A CN111449226 A CN 111449226A CN 202010281997 A CN202010281997 A CN 202010281997A CN 111449226 A CN111449226 A CN 111449226A
- Authority
- CN
- China
- Prior art keywords
- halogen
- heating
- standing
- materials
- halogen material
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000463 material Substances 0.000 title claims abstract description 105
- 238000000034 method Methods 0.000 title claims abstract description 24
- 239000012267 brine Substances 0.000 title abstract description 23
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 title abstract description 23
- 229910052736 halogen Inorganic materials 0.000 claims abstract description 81
- 150000002367 halogens Chemical class 0.000 claims abstract description 81
- 238000010438 heat treatment Methods 0.000 claims abstract description 35
- 238000002156 mixing Methods 0.000 claims abstract description 14
- 239000012535 impurity Substances 0.000 claims abstract description 12
- 238000000605 extraction Methods 0.000 claims abstract description 11
- 238000001914 filtration Methods 0.000 claims abstract description 11
- 238000002425 crystallisation Methods 0.000 claims abstract description 9
- 230000008025 crystallization Effects 0.000 claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 6
- 238000003756 stirring Methods 0.000 claims abstract description 5
- 230000017525 heat dissipation Effects 0.000 claims abstract description 4
- 239000002994 raw material Substances 0.000 claims description 6
- 239000013078 crystal Substances 0.000 claims description 5
- 238000005516 engineering process Methods 0.000 claims description 5
- 235000013305 food Nutrition 0.000 claims description 4
- 238000000926 separation method Methods 0.000 claims description 4
- 230000008014 freezing Effects 0.000 claims description 3
- 238000007710 freezing Methods 0.000 claims description 3
- 238000012360 testing method Methods 0.000 claims description 3
- 238000011076 safety test Methods 0.000 claims description 2
- 238000000746 purification Methods 0.000 abstract description 5
- 238000002360 preparation method Methods 0.000 abstract description 2
- 241001131796 Botaurus stellaris Species 0.000 description 3
- 239000003205 fragrance Substances 0.000 description 3
- 238000012986 modification Methods 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- 235000015090 marinades Nutrition 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 235000011194 food seasoning agent Nutrition 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 230000035943 smell Effects 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/10—Natural spices, flavouring agents or condiments; Extracts thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/10—Natural spices, flavouring agents or condiments; Extracts thereof
- A23L27/11—Natural spices, flavouring agents or condiments; Extracts thereof obtained by solvent extraction
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Extraction Or Liquid Replacement (AREA)
Abstract
The invention discloses a process for purifying and extracting halogen materials, which comprises the steps of preparing halogen materials, wherein the preparation process comprises the steps of centrifugal mixing, heating and purifying, standing and extracting and crystallizing, the centrifugal mixing adopts a centrifugal machine to mix the halogen materials, the standing and extracting adopts a separating funnel to stand and extract, the halogen materials are heated to 50-75 ℃, after the heating is finished, filtering impurities in the brine material through multiple filter screens to obtain the brine material without impurities, heating and purifying the brine material, heating the brine material by adopting a boiler with better heat dissipation capacity, stirring continuously during heating, stopping heating when the water in the brine material is reduced to below 50%, filtering for the second time, standing and extracting the brine material, pouring the brine material into a separating funnel, standing, in the standing process, extracting the halogen material, and crystallizing and separating out the halogen material after the halogen material is placed to room temperature; the invention has the advantages of excellent halogen material purification, halogen material extraction and crystallization.
Description
Technical Field
The invention relates to the technical field of halogen materials, in particular to a process for purifying and extracting halogen materials.
Background
The marinade is a seasoning for preparing marinade, generally refers to a traditional Chinese medicine spice for preparing brine, has strong fragrance, can remove fishy and mutton smells of food raw materials, and has the function of increasing the fragrance of food.
The marinating method is characterized in that the marinating materials are placed in a marinating pot and boiled with water to prepare brine, the brine is not purified and extracted, different marinating material formulas can be prepared into brine with different fragrance types, the brine cannot completely absorb the purification of the marinating materials, the safety is not high, oil and the like in the marinating materials cannot be separated, and the brine is not convenient to store.
Disclosure of Invention
The invention aims to overcome the defects of the prior art, provides a process for purifying and extracting halogen materials, has the advantages of excellent halogen material purification, halogen material extraction and crystallization separation, and solves the problems in the prior art.
In order to achieve the purpose, the invention provides the following technical scheme: a process for purifying and extracting halogen materials, wherein the raw materials are halogen materials, and the preparation process comprises the steps of centrifugal mixing, heating and purifying, standing and extracting and crystallizing and separating out respectively;
the centrifugal mixing adopts a centrifuge to mix the halogen material, and the standing extraction adopts a separating funnel to perform standing extraction;
the processing technology is as follows:
(1) heating the halogen material to 50-75 ℃, and filtering impurities in the halogen material through multiple filter screens after heating to obtain the halogen material without impurities;
(2) centrifuging and mixing the raw materials in the step (1), placing the halogen materials in the step (1) in a centrifuge, testing the temperature of the halogen materials before centrifuging, centrifuging when the temperature of the halogen materials is between 40 and 75 ℃, wherein the centrifuging time is 10 to 20 minutes, and obtaining the mixed halogen materials after the centrifuging is finished;
(3) heating and purifying the step (2), heating by adopting a boiler with good heat dissipation capacity, continuously stirring in the heating process, stopping heating when the water in the halogen material is reduced to below 50%, and filtering for the second time;
(4) standing and extracting the halogen material in the step (3), pouring the halogen material into a separating funnel, standing, and extracting the halogen material in the standing process;
(5) standing the halogen material in the step (4) to room temperature, crystallizing and separating out, putting the halogen material into a tank body, refrigerating and crystallizing, and crystallizing and separating out when the halogen material reaches a freezing point;
(6) and (5) taking out the crystals, and heating to obtain the purified and extracted halogen material.
Preferably, the heating temperature of the (3) is 60-80 ℃.
Preferably, all of the components used pass food safety tests.
Preferably, the halogen material is a halogen material which can be normally used.
The parts not involved in the invention are the same as or can be realized by the prior art.
Compared with the prior art, the invention has the following beneficial effects:
1: the purification and extraction processing technology of the brine material filters impurities in the brine material through multi-layer filtration, prevents the impurities in the brine material from appearing, increases the mixing degree of the brine material by adopting a centrifugal machine to mix the brine material, ensures that the brine material cannot be mixed unevenly, and heats the brine material through a boiler so as to purify the brine material;
2: a process for purifying and extracting bittern includes such steps as separating oil from bittern by separating funnel, refrigerating to separate out crystal, purifying again and refining.
Detailed Description
The present invention will be further described with reference to specific embodiments, which will become apparent from the following description, but are intended to be exemplary only, and not limiting as to the scope of the invention, it will be understood by those skilled in the art that changes in detail and modifications of form and detail may be made therein without departing from the spirit and scope of the invention, and that such changes and modifications are within the scope of the invention.
Example 1
A process for purifying and extracting bittern includes such steps as centrifugal mixing, heating for purifying, laying aside for extracting and crystallizing out.
The centrifugal mixing adopts a centrifuge to mix the halogen material, and the standing extraction adopts a separating funnel to perform standing extraction;
the processing technology is as follows:
(1) heating the halogen material to 50-75 ℃, and filtering impurities in the halogen material through multiple filter screens after heating to obtain the halogen material without impurities;
(2) centrifuging and mixing the raw materials in the step (1), placing the halogen materials in the step (1) in a centrifuge, testing the temperature of the halogen materials before centrifuging, centrifuging when the temperature of the halogen materials is between 40 and 75 ℃, wherein the centrifuging time is 10 to 20 minutes, and obtaining the mixed halogen materials after the centrifuging is finished;
(3) heating and purifying the step (2), heating by adopting a boiler with good heat dissipation capacity, continuously stirring in the heating process, stopping heating when the water in the halogen material is reduced to below 50%, and filtering for the second time;
(4) standing and extracting the halogen material in the step (3), pouring the halogen material into a separating funnel, standing, and extracting the halogen material in the standing process;
(5) standing the halogen material in the step (4) to room temperature, crystallizing and separating out, putting the halogen material into a tank body, refrigerating and crystallizing, and crystallizing and separating out when the halogen material reaches a freezing point;
(6) and (5) taking out the crystals, and heating to obtain the purified and extracted halogen material.
According to the steps, the purification and extraction of the halogen materials are guaranteed.
In summary, the following steps: the invention relates to a process for purifying and extracting halogen materials, which comprises the steps of heating the halogen materials to 50-75 ℃ at the beginning, carrying out multiple filtration through a filter screen, preventing impurities in the halogen materials from appearing, influencing the taste of the halogen materials, placing the filtered halogen materials into a centrifuge, centrifuging for 15 minutes at 40-75 ℃ to ensure that the temperature of the halogen materials is between 40-75 ℃ so as to ensure the mixing of the halogen materials, carrying out heating and purifying after the mixing is finished, stirring in the purifying process, carrying out secondary filtration after the water in the halogen materials is reduced to below 50%, standing and extracting to separate oil, placing the halogen materials to room temperature after the extraction is finished, refrigerating, carrying out crystallization separation when the crystallization point is reached, taking out the crystallization after the crystallization separation is finished, storing the crystallization, heating for use when the crystallization is required, reducing the oil content of the halogen materials through the steps, the taste is mixed best, and impurities are reduced, so that the taste of the marinating material is guaranteed, the marinating material can be used at any time, and the crystals are melted to be used when the marinating material is needed.
While there have been shown and described what are at present considered to be the fundamental principles of the invention and its essential features and advantages, it will be understood by those skilled in the art that the invention is not limited by the embodiments described above, which are merely illustrative of the principles of the invention, but that various changes and modifications may be made therein without departing from the spirit and scope of the invention as defined by the appended claims and their equivalents.
Claims (5)
1. A process for purifying and extracting halogen materials is characterized in that: the raw material is a halogen material, wherein the processing technology comprises centrifugal mixing, heating and purifying, standing and extracting and crystallization and separation respectively;
the centrifugal mixing adopts a centrifugal machine to mix the halogen materials, and the standing extraction adopts a separating funnel to perform standing extraction.
2. The process of claim 1, wherein the process comprises the steps of: the processing technology comprises the following steps:
(1) heating the halogen material to 50-75 ℃, and filtering impurities in the halogen material through multiple filter screens after heating to obtain the halogen material without impurities;
(2) centrifuging and mixing the raw materials in the step (1), placing the halogen materials in the step (1) in a centrifuge, testing the temperature of the halogen materials before centrifuging, centrifuging when the temperature of the halogen materials is between 40 and 75 ℃, wherein the centrifuging time is 10 to 20 minutes, and obtaining the mixed halogen materials after the centrifuging is finished;
(3) heating and purifying the step (2), heating by adopting a boiler with good heat dissipation capacity, continuously stirring in the heating process, stopping heating when the water in the halogen material is reduced to below 50%, and filtering for the second time;
(4) standing and extracting the halogen material in the step (3), pouring the halogen material into a separating funnel, standing, and extracting the halogen material in the standing process;
(5) standing the halogen material in the step (4) to room temperature, crystallizing and separating out, putting the halogen material into a tank body, refrigerating and crystallizing, and crystallizing and separating out when the halogen material reaches a freezing point;
(6) and (5) taking out the crystals, and heating to obtain the purified and extracted halogen material.
3. The process of claim 2, wherein the process comprises the steps of: the heating temperature of the step (3) is 60-80 ℃.
4. The process of claim 2, wherein the process comprises the steps of: all of the components used pass food safety tests.
5. The process of claim 2, wherein the process comprises the steps of: the halogen material is a halogen material which can be normally used.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010281997.8A CN111449226A (en) | 2020-04-11 | 2020-04-11 | Process for purifying and extracting brine material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010281997.8A CN111449226A (en) | 2020-04-11 | 2020-04-11 | Process for purifying and extracting brine material |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN111449226A true CN111449226A (en) | 2020-07-28 |
Family
ID=71670697
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202010281997.8A Pending CN111449226A (en) | 2020-04-11 | 2020-04-11 | Process for purifying and extracting brine material |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN111449226A (en) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106422407A (en) * | 2016-11-15 | 2017-02-22 | 重庆市梁平张鸭子食品有限公司 | Method for purifying and extracting spices |
| CN110180213A (en) * | 2019-06-26 | 2019-08-30 | 重庆真本味食品有限公司 | A kind of spice extraction enrichment facility |
-
2020
- 2020-04-11 CN CN202010281997.8A patent/CN111449226A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106422407A (en) * | 2016-11-15 | 2017-02-22 | 重庆市梁平张鸭子食品有限公司 | Method for purifying and extracting spices |
| CN110180213A (en) * | 2019-06-26 | 2019-08-30 | 重庆真本味食品有限公司 | A kind of spice extraction enrichment facility |
Non-Patent Citations (2)
| Title |
|---|
| 陈苍林: "卤水", 《江苏调味副食品》 * |
| 鲁肇元，等: "复合调味料及其产品开发", 《中国酿造》 * |
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| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20200728 |
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| RJ01 | Rejection of invention patent application after publication |