CN113201402A - Process and equipment for preparing spice by distillation method - Google Patents

Process and equipment for preparing spice by distillation method Download PDF

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Publication number
CN113201402A
CN113201402A CN202110434653.0A CN202110434653A CN113201402A CN 113201402 A CN113201402 A CN 113201402A CN 202110434653 A CN202110434653 A CN 202110434653A CN 113201402 A CN113201402 A CN 113201402A
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CN
China
Prior art keywords
demister
tank
extraction
extraction tank
groove
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
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CN202110434653.0A
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Chinese (zh)
Inventor
李祥林
傅厚明
许小勇
王建军
李群伟
祝汉平
傅娟娟
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jiangxi Spice Chemical Industrial Co ltd
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Jiangxi Spice Chemical Industrial Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by Jiangxi Spice Chemical Industrial Co ltd filed Critical Jiangxi Spice Chemical Industrial Co ltd
Priority to CN202110434653.0A priority Critical patent/CN113201402A/en
Publication of CN113201402A publication Critical patent/CN113201402A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials
    • C11B9/027Recovery of volatiles by distillation or stripping

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Extraction Or Liquid Replacement (AREA)

Abstract

The invention discloses a process and equipment for preparing spice by a distillation method, and the process and equipment comprise an extraction tank, a condenser, a cooler, an end enclosure, an oil-water separator, a filter, an extraction pump and a demister, wherein the demister is arranged at the top of the extraction tank, the condenser is respectively connected with the demister and the cooler, the oil-water separator is respectively connected with the cooler and the extraction tank, and the filter is respectively connected with the extraction tank and the extraction pump; the invention has the beneficial effects that: the designed stabilizing mechanism is beneficial to stably installing the demister and the extracting tank through the fastening piece, so that the installing efficiency of the demister is improved; the clamping groove, the protrusion, the positioning block and the positioning groove are matched through the designed positioning mechanism, so that the fastening positioning of the second connecting part and the first connecting part is increased, and the fastening of the second connecting part and the first connecting part is more efficient; through the maintenance mechanism who designs, it is more high-efficient to overhaul equipment to take out the maintenance instrument of placing in overhauing the box, has improved the efficiency that the equipment overhauld and maintained.

Description

Process and equipment for preparing spice by distillation method
Technical Field
The invention belongs to the technical field of spice preparation, and particularly relates to a process and equipment for preparing spice by a distillation method.
Background
When preparing the spice, a multifunctional extraction tank is commonly used; the multifunctional extraction tank is a common leaching extraction device, the device can extract spices in a normal pressure, micro-pressure, water decoction, warm leaching, hot reflux and forced circulation percolation extraction mode, and the device is widely applied to the fields of biological pharmacy, health food, functional beverage and daily chemical industry; has the advantages of high efficiency, high equipment utilization rate and convenient operation.
The existing equipment for preparing the spice by the distillation method has the following defects in use:
1. when the first connecting part of the oil-water separator is connected with the second connecting part of the seal head, the connecting holes are not convenient to align, and the fastening efficiency of the first connecting part and the second connecting part is reduced;
2. the demister is connected with the extracting tank through a plurality of bolts, so that time and labor are wasted, and the efficiency of connecting the demister with the extracting tank is reduced.
Disclosure of Invention
The invention aims to provide a process and equipment for preparing spices by a distillation method, which aims to solve the problem that when a first connecting part of an oil-water separator and a second connecting part of a seal head in the background technology are connected, the connecting holes are inconvenient to align, and the fastening efficiency of the first connecting part and the second connecting part is reduced; the demister is connected with the extracting tank through a plurality of bolts, so that time and labor are wasted, and the efficiency problem of connection of the demister and the extracting tank is reduced.
In order to achieve the purpose, the invention provides the following technical scheme: the device for preparing the spice by the distillation method comprises an extraction tank, a condenser, a cooler, an end socket, an oil-water separator, a filter, an extraction pump and a demister, wherein the demister is arranged at the top of the extraction tank, the condenser is respectively connected with the demister and the cooler, the oil-water separator is respectively connected with the cooler and the extraction tank, the filter is respectively connected with the extraction tank and the extraction pump, the demister and the extraction tank are provided with a stabilizing mechanism, the stabilizing mechanism comprises a fastener, a first screw hole and a second screw hole, the fastener is respectively connected with the extraction tank and the demister, and the surface of the fastener is provided with the first screw hole and the second screw hole; the bottom of head is provided with the second connecting portion, oil water separator's top is provided with first connecting portion, be provided with positioning mechanism on second connecting portion and the first connecting portion, positioning mechanism includes draw-in groove, locating piece, constant head tank and arch, the bottom of second connecting portion is provided with the locating piece, and the bottom of locating piece has seted up the draw-in groove, the top of first connecting portion seted up with locating piece assorted constant head tank, the inside of constant head tank be provided with the arch of draw-in groove block.
As a preferred technical scheme of the present invention, the locking groove is a trapezoidal groove, and the protrusion is of a trapezoidal structure.
As a preferable technical scheme of the present invention, the surfaces of the second connecting portion and the first connecting portion are both provided with connecting holes, and the connecting holes are matched.
In a preferred embodiment of the present invention, the fastening member and the demister are fixed by screws, and the fastening member and the extraction tank are fixed by screws.
The invention further comprises a bottom frame for supporting the extraction pump, wherein a protective cover is hinged to the front surface of the bottom frame, and an overhauling mechanism is arranged inside the bottom frame.
As a preferable technical scheme, the maintenance mechanism comprises a maintenance box, a sliding block and a sliding groove, the maintenance box is arranged inside the bottom frame, the sliding block is arranged at the bottom of the maintenance box, the sliding groove matched with the sliding block is formed in the inner bottom of the bottom frame, and maintenance tools are stored in the maintenance box.
As a preferable technical scheme of the invention, the sliding block is of a cuboid structure, and the sliding groove is a U-shaped groove.
The invention also discloses a manufacturing process of the equipment for preparing the spice by the distillation method, which comprises the following steps:
the method comprises the following steps: the screw penetrates through the first screw hole and is driven into the demister, a new screw is picked up, the new screw penetrates through the second screw hole and is driven into the extraction tank, and the demister and the extraction tank are stably installed;
step two: putting the crushed spice raw materials into an extraction tank through a feeding port, adding an aqueous solution into the extraction tank, and soaking;
step three: soaking the perfume raw materials, introducing steam into the jacket of the extraction tank, heating, and extracting effective components of the perfume;
step four: cooling the tank body by introducing cooling water into the jacket of the extraction tank, opening the feed liquid discharge valve after the tank body is cooled, discharging the feed liquid, transferring the feed liquid into a filter for filtering, and extracting the filtered spice by an extraction pump;
step five: opening a discharge valve at the bottom of the extraction tank, discharging the spice residues in the tank body, and cleaning the tank body.
Compared with the prior art, the invention has the beneficial effects that:
(1) the designed stabilizing mechanism is beneficial to stably installing the demister and the extracting tank through the fastening piece, so that the installing efficiency of the demister is improved;
(2) the clamping groove, the protrusion, the positioning block and the positioning groove are matched through the designed positioning mechanism, so that the fastening positioning of the second connecting part and the first connecting part is increased, and the fastening of the second connecting part and the first connecting part is more efficient;
(3) through the maintenance mechanism who designs, it is more high-efficient to overhaul equipment to take out the maintenance instrument of placing in overhauing the box, has improved the efficiency that the equipment overhauld and maintained.
Drawings
FIG. 1 is a schematic structural view of the present invention;
FIG. 2 is an enlarged view of the region G of FIG. 1 according to the present invention;
FIG. 3 is an enlarged view of the N region of FIG. 1 according to the present invention;
FIG. 4 is an enlarged view of area E of FIG. 1 according to the present invention;
FIG. 5 is a perspective view of the fastener of the present invention;
in the figure: 1. an extraction tank; 2. a condenser; 3. a cooler; 4. a second connecting portion; 5. a first connection portion; 6. sealing the end; 7. an oil-water separator; 8. a filter; 9. an extraction pump; 10. a protective cover; 11. overhauling the box; 12. a chassis; 13. a card slot; 14. positioning blocks; 15. positioning a groove; 16. a protrusion; 17. a slider; 18. a chute; 19. a demister; 20. a fastener; 21. a first screw hole; 22. a second screw hole.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1, fig. 2, fig. 3, fig. 4 and fig. 5, the present invention provides a technical solution: an apparatus for preparing spice by distillation method comprises an extraction tank 1, a condenser 2, a cooler 3, a seal head 6, an oil-water separator 7, a filter 8, an extraction pump 9 and a demister 19, wherein the condenser 2 is used for condensing steam, the cooler 3 cools condensate, the oil-water separator 7 is used for separating oil from cooled recovery liquid, the demister 19 is used for eliminating foam generated in the spice preparation process, the top of the extraction tank 1 is provided with the demister 19, the condenser 2 is respectively connected with the demister 19 and the cooler 3, the oil-water separator 7 is respectively connected with the cooler 3 and the extraction tank 1, the filter 8 is respectively connected with the extraction tank 1 and the extraction pump 9, the demister 19 and the extraction tank 1 are provided with stabilizing mechanisms, each stabilizing mechanism comprises a fastener 20, a first screw hole 21 and a second screw hole 22, the fastener 20 is respectively connected with the extraction tank 1 and the demister 19, the surface of the fastening piece 20 is provided with a first screw hole 21 and a second screw hole 22, which is beneficial to stably mounting the demister 19 and the extraction tank 1 through the fastening piece 20, and the mounting efficiency of the demister 19 is improved; the bottom of the seal head 6 is provided with a second connecting part 4, the top of the oil-water separator 7 is provided with a first connecting part 5, the second connecting part 4 and the first connecting part 5 are provided with a positioning mechanism, the positioning mechanism comprises a clamping groove 13, a positioning block 14, a positioning groove 15 and a bulge 16, the bottom of the second connecting part 4 is provided with the positioning block 14, the bottom of the positioning block 14 is provided with the clamping groove 13, the top of the first connecting part 5 is provided with the positioning groove 15 matched with the positioning block 14, the bulge 16 clamped with the clamping groove 13 is arranged inside the positioning groove 15, when in use, a positioning block 14 at the bottom of the second connecting part 4 is inserted into a positioning groove 15 arranged at the top of the first connecting part 5, and the protrusion 16 is inserted into the slot 13, and the fastening positioning of the second connecting part 4 and the first connecting part 5 is increased by the matching of the slot 13, the protrusion 16, the positioning block 14 and the positioning groove 15, so that the fastening of the second connecting part 4 and the first connecting part 5 is more efficient.
In this embodiment, preferably, the locking groove 13 is a trapezoidal groove, and the protrusion 16 is a trapezoidal structure, so as to facilitate the locking between the trapezoidal protrusion 16 and the trapezoidal locking groove 13.
In this embodiment, preferably, the surfaces of the second connecting portion 4 and the first connecting portion 5 are both provided with connecting holes and matched with the connecting holes, so that bolts can pass through the connecting holes to fasten the second connecting portion 4 and the first connecting portion 5.
In this embodiment, it is preferable that the fastening member 20 and the demister 19 are fixed by screws, and the fastening member 20 and the extraction tank 1 are fixed by screws, which helps to fix the demister 19 and the extraction tank 1 firmly by the fastening member 20.
In this embodiment, preferably, the device further comprises a bottom frame 12 supporting the extraction pump 9, a protective cover 10 is hinged to the front surface of the bottom frame 12, an overhaul mechanism is arranged inside the bottom frame 12, the overhaul mechanism comprises an overhaul box 11, a sliding block 17 and a sliding groove 18, the overhaul box 11 is arranged inside the bottom frame 12, the sliding block 17 is arranged at the bottom of the overhaul box 11, the sliding groove 18 matched with the sliding block 17 is formed in the inner bottom of the bottom frame 12, an overhaul tool is stored in the overhaul box 11, when the device needs to be overhauled and maintained, the protective cover 10 is opened, the overhaul box 11 is pulled outwards to expose the overhaul box 11, the overhaul tool placed in the overhaul box 11 is taken out to overhaul the device, and therefore the overhaul and maintenance efficiency is improved; after the overhaul is finished, the overhaul tool is placed back into the overhaul box 11, the overhaul box 11 is pushed into the bottom frame 12, and the protective cover 10 is covered.
In this embodiment, preferably, the sliding block 17 is a rectangular parallelepiped structure, and the sliding groove 18 is a "U" shaped groove, so that the rectangular parallelepiped sliding block 17 can slide along the "U" shaped sliding groove 18.
A manufacturing process of equipment for preparing spice by a distillation method comprises the following steps:
the method comprises the following steps: a screw is driven into the demister 19 through the first screw hole 21, a new screw is picked up, and the new screw is driven into the extraction tank 1 through the second screw hole 22, so that the demister 19 and the extraction tank 1 are stably installed;
step two: putting the crushed spice raw materials into an extraction tank 1 through a feeding port, adding an aqueous solution into the tank, and soaking;
step three: soaking the perfume raw materials, introducing steam into the jacket of the extraction tank 1, and heating to extract effective components of the perfume;
step four: cooling the tank body by introducing cooling water into the jacket of the extraction tank 1, opening the feed liquid discharge valve after the tank body is cooled, discharging the feed liquid, transferring the feed liquid into a filter 8 for filtering, and extracting the filtered spice by an extraction pump 9;
step five: opening a discharge valve at the bottom of the extraction tank 1, discharging the spice residues in the tank body, and cleaning the tank body.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (8)

1. The utility model provides an equipment of distillation method preparation spices, is including extracting jar (1), condenser (2), cooler (3), head (6), oil water separator (7), filter (8), extraction pump (9), demister (19), the top of extracting jar (1) is provided with demister (19), condenser (2) are connected with demister (19) and cooler (3) respectively, oil water separator (7) are connected with cooler (3) and extraction jar (1) respectively, filter (8) respectively with extract jar (1) and extract pump (9) and be connected its characterized in that: the demister (19) and the extraction tank (1) are provided with stabilizing mechanisms, each stabilizing mechanism comprises a fastening piece (20), a first screw hole (21) and a second screw hole (22), the fastening pieces (20) are respectively connected with the extraction tank (1) and the demister (19), and the surfaces of the fastening pieces (20) are provided with the first screw holes (21) and the second screw holes (22); the bottom of head (6) is provided with second connecting portion (4), the top of oil water separator (7) is provided with first connecting portion (5), be provided with positioning mechanism on second connecting portion (4) and first connecting portion (5), positioning mechanism includes draw-in groove (13), locating piece (14), constant head tank (15) and arch (16), the bottom of second connecting portion (4) is provided with locating piece (14), and the bottom of locating piece (14) has seted up draw-in groove (13), constant head tank (15) with locating piece (14) assorted has been seted up at the top of first connecting portion (5), the inside of constant head tank (15) is provided with arch (16) with draw-in groove (13) block.
2. An apparatus for preparing a fragrance by distillation according to claim 1, wherein: the clamping groove (13) is a trapezoidal groove, and the protrusion (16) is of a trapezoidal structure.
3. An apparatus for preparing a fragrance by distillation according to claim 1, wherein: and the surfaces of the second connecting part (4) and the first connecting part (5) are provided with connecting holes which are matched with each other.
4. An apparatus for preparing a fragrance by distillation according to claim 1, wherein: the fastener (20) and the demister (19) are fixed through screws, and the fastener (20) and the extraction tank (1) are fixed through screws.
5. An apparatus for preparing a fragrance by distillation according to claim 1, wherein: still including supporting chassis (12) of extraction pump (9), the front surface of chassis (12) articulates there is protective cover (10), the inside of chassis (12) is provided with overhauls the mechanism.
6. An apparatus for preparing a fragrance by distillation according to claim 5, wherein: the maintenance mechanism is including overhauing box (11), slider (17) and spout (18), the inside of chassis (12) is arranged in maintenance box (11), and the bottom of overhauing box (11) is provided with slider (17), the interior bottom of chassis (12) seted up with slider (17) assorted spout (18), the maintenance instrument has been put in maintenance box (11).
7. An apparatus for the preparation of a fragrance by distillation according to claim 6, characterized in that: the slide block (17) is of a cuboid structure, and the sliding groove (18) is a U-shaped groove.
8. The process for manufacturing a device for preparing a perfume by distillation according to any one of claims 1 to 7, wherein: the manufacturing process comprises the following steps:
the method comprises the following steps: a screw is driven into the demister (19) through the first screw hole (21), a new screw is picked up, the new screw is driven into the extraction tank (1) through the second screw hole (22), and the demister (19) and the extraction tank (1) are stably installed;
step two: putting the crushed spice raw materials into an extraction tank (1) through a feeding port, adding an aqueous solution into the tank, and soaking;
step three: after the spice raw materials are soaked, steam is introduced into a jacket of the extraction tank (1) and heated to extract effective ingredients of the spice;
step four: cooling water is introduced into a jacket of the extraction tank (1) to cool the tank body, after the tank body is cooled, a feed liquid discharge valve is opened, feed liquid is discharged, the feed liquid is transferred to a filter (8) for filtering, and the filtered spice is extracted through an extraction pump (9);
step five: opening a discharge valve at the bottom of the extraction tank (1), discharging the spice slag in the tank body, and cleaning the tank body.
CN202110434653.0A 2021-04-22 2021-04-22 Process and equipment for preparing spice by distillation method Pending CN113201402A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202110434653.0A CN113201402A (en) 2021-04-22 2021-04-22 Process and equipment for preparing spice by distillation method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202110434653.0A CN113201402A (en) 2021-04-22 2021-04-22 Process and equipment for preparing spice by distillation method

Publications (1)

Publication Number Publication Date
CN113201402A true CN113201402A (en) 2021-08-03

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CN202110434653.0A Pending CN113201402A (en) 2021-04-22 2021-04-22 Process and equipment for preparing spice by distillation method

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Application publication date: 20210803