CN1563311A - Technique for extracting rhodamine oil - Google Patents
Technique for extracting rhodamine oil Download PDFInfo
- Publication number
- CN1563311A CN1563311A CN 200410029668 CN200410029668A CN1563311A CN 1563311 A CN1563311 A CN 1563311A CN 200410029668 CN200410029668 CN 200410029668 CN 200410029668 A CN200410029668 A CN 200410029668A CN 1563311 A CN1563311 A CN 1563311A
- Authority
- CN
- China
- Prior art keywords
- rose
- fast
- oil
- retort
- open type
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 title description 6
- PYWVYCXTNDRMGF-UHFFFAOYSA-N rhodamine B Chemical compound [Cl-].C=12C=CC(=[N+](CC)CC)C=C2OC2=CC(N(CC)CC)=CC=C2C=1C1=CC=CC=C1C(O)=O PYWVYCXTNDRMGF-UHFFFAOYSA-N 0.000 title 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 27
- 241000220317 Rosa Species 0.000 claims abstract description 20
- 238000004821 distillation Methods 0.000 claims abstract description 13
- 238000001816 cooling Methods 0.000 claims abstract description 8
- 238000000926 separation method Methods 0.000 claims abstract description 8
- 241000628997 Flos Species 0.000 claims description 13
- 238000000605 extraction Methods 0.000 claims description 11
- 238000003756 stirring Methods 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 3
- 239000000284 extract Substances 0.000 abstract description 6
- 238000010438 heat treatment Methods 0.000 abstract description 6
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 239000003921 oil Substances 0.000 description 14
- 235000019198 oils Nutrition 0.000 description 13
- 239000010666 rose oil Substances 0.000 description 9
- 235000019719 rose oil Nutrition 0.000 description 9
- 239000007788 liquid Substances 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 239000000341 volatile oil Substances 0.000 description 4
- 238000004939 coking Methods 0.000 description 2
- 238000009833 condensation Methods 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 210000002700 urine Anatomy 0.000 description 1
Landscapes
- Fats And Perfumes (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
A process for preparing extract oil of rose includes placing rose flower and water into distillation tank, connecting steam into jacket of distillation tank, heating and agitating the tank carrying out secondary distillation for steam produced in the tank and then condensing and cooling it, obtaining extract oil of rose by carrying out the second stage of oil-water separation.
Description
[technical field]
What the present invention relates to is a kind of extraction process of Chinese medicinal materials, and what be specifically related to is a kind of Rose extracts essential oil technology.
[background technology]
In the prior art, Rose extracts essential oil technology is Rose and water to be presented in the inferior pyramidal retort directly water is heated, and the steam after the heating separates obtaining Flos Rosae Rugosae quintessence oil then by the shell-and tube condenser condensation by water-and-oil separator.This extraction process is owing to adopt the retort of going up inferior pyramidal, and directly feed retort with dry steam and heat, residue after distillation finishes, can only be with manually in the lateral hole of retort, excavating, Rose is attached on the heating pipe because the coking phenomenon that high temperature produced, clean very difficult, very time-consuming, owing to adopt dry steam not through separating and purifying, in the thermal process reactor of whole static state, thermal source in the steam and impurity have directly damaged composition and the character of Rose, make the rose oil muddiness that distills out contain smell of urine flavor again, still residual stain in the oil has influenced the quality of rose oil, and shell-and tube condenser of this process using cools off, make the gas-liquid that has rose oil enter condenser and can not get cooling off completely, cause the loss of rose oil gas-liquid, adopt a table oil water separator to separate simultaneously, make profit can not get separating fully, directly influenced the output and the purity of rose oil.How to make the rose oil of extraction keep original character of Rose and composition, and make that its transparency is good, quality and output height, be that those skilled in the art want to solve and an insoluble difficult problem always.
[summary of the invention]
In view of problems of the prior art, the object of the present invention is to provide a kind of character and composition that makes rose oil keep reason, improve the extraction process of quality, output and the purity of rose oil product.For achieving the above object, the present invention takes following scheme to finish: the extraction process of this Flos Rosae Rugosae quintessence oil, it is characterized in that Rose and water mixing are inserted in the fast-open type retort, then steam is fed in the chuck of fast-open type retort, heat while stirring in the fast-open type retort with whipping appts, the steam that produces in the fast-open type retort is through behind the second distillation of distillation column, by condenser condenses, water cooler cooling, carry out secondary oily water separation again, obtain Flos Rosae Rugosae quintessence oil at last.Described fast-open type retort is pneumatic open and close type retort; Described condenser and water cooler are rolled plate.
The present invention feeds steam in the chuck of retort and heats, because heating-surface area is big, rate of heating is fast, after Rose in the retort and water are heated, under the stirring of whipping appts, thermal response is carried out under dynamic situation, can not make the Rose in the retort produce coking phenomenon, and can not have influence on Rose intrinsic quality, keep original fragrance of Rose and transparency; Adopt the retort of pneumatic open and close type, distillation test residue can disposablely be discharged, save time very much, and it is convenient to clean, adopt board-like condenser, condensation area is big, easy cleaning, with condensed gas-liquid again through supercooler, it is fully cooled off, can not run off, adopt secondary oily water separation simultaneously, oil is thoroughly separated with water, improved the output and the purity of Flos Rosae Rugosae quintessence oil.Adopt the extraction process of theme of the present invention, will bring positive economic benefit for the producer that extracts Flos Rosae Rugosae quintessence oil.
[description of drawings]
The present invention has following accompanying drawing:
Fig. 1 is a process flow sheet of the present invention.
[embodiment]
Accompanying drawing has been represented implementation of processes process of the present invention, further describes each relevant details of embodiment below more in conjunction with the accompanying drawings.The extraction process of this Flos Rosae Rugosae quintessence oil, at first be that Rose and water mixing are inserted in the fast-open type retort, then steam is fed in the chuck of fast-open type retort, heat while stirring in the fast-open type retort with whipping appts, the steam that produces in the fast-open type retort is through behind the second distillation of distillation column, by condenser condenses, water cooler cooling, carry out secondary oily water separation again, obtain the Flos Rosae Rugosae quintessence oil product at last; In heat-processed, temperature should be controlled at 100～120 ℃; Be back to again in retort and the distillation column through the water after the secondary separation; Described fast-open type retort is pneumatic open and close type retort; The retort of described pneumatic open and close type is to be provided with cylinder and connecting rod in the outside of tank body, described cylinder is by hinged-support and rod hinge connection, to the retort distillation test residue, as long as press pneumatically operated switch, the capping of discharge port is opened fully, with the disposable discharge of residue, save time very much, and clean conveniently; Described condenser and water cooler are rolled plate; Described rolled plate condenser and water cooler are the cooling tubes that adopts rolled plate in condenser and water cooler; After the cooling of this two-stage, make the gas-liquid cooling fully, can not run off, and provide good basis for the oily water separation of subsequent processing; Because the special proportion of rose oil in order fully to collect the Rose essential oil, so adopt secondary oily water separation, makes oil thoroughly separate with water, has improved the output and the purity of Flos Rosae Rugosae quintessence oil; Equipment in the technology of the present invention all adopts the fine stainless material, and not to Rose and water direct heating, and the chuck of heating source at retort carried out, can not have influence on original character of Rose and composition, kept original fragrance of Rose and transparency.According to the Rose essential oil that the present invention extracts, quality, constant and based on very high purity compared with prior art, have outstanding substantive distinguishing features and obvious improvement.
Claims (3)
1, a kind of extraction process of Flos Rosae Rugosae quintessence oil, it is characterized in that Rose and water mixing are inserted in the fast-open type retort, then steam is fed in the chuck of fast-open type retort, heat while stirring in the fast-open type retort with whipping appts, the steam that produces in the fast-open type retort is through behind the second distillation of distillation column, by condenser condenses, water cooler cooling, carry out secondary oily water separation again, obtain the Flos Rosae Rugosae quintessence oil product at last.
2, the extraction process of Flos Rosae Rugosae quintessence oil according to claim 1 is characterized in that described fast-open type retort is pneumatic open and close type retort.
3, the extraction process of Flos Rosae Rugosae quintessence oil according to claim 1 is characterized in that described condenser and water cooler are rolled plate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200410029668 CN1232622C (en) | 2004-03-31 | 2004-03-31 | Technique for extracting rhodamine oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200410029668 CN1232622C (en) | 2004-03-31 | 2004-03-31 | Technique for extracting rhodamine oil |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1563311A true CN1563311A (en) | 2005-01-12 |
| CN1232622C CN1232622C (en) | 2005-12-21 |
Family
ID=34480970
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200410029668 Expired - Fee Related CN1232622C (en) | 2004-03-31 | 2004-03-31 | Technique for extracting rhodamine oil |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1232622C (en) |
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101721338B (en) * | 2009-11-20 | 2012-08-22 | 甘肃农业大学 | Cosmetic containing Rosa setate X R. rugosa water |
| CN102952644A (en) * | 2012-12-06 | 2013-03-06 | 广西京桂香料有限公司 | Device for extracting natural cinnamon oil |
| CN103146487A (en) * | 2013-04-08 | 2013-06-12 | 云南绿宝香精香料股份有限公司 | Water steam distillation device with duplex effects of extraction and separation |
| CN103740469A (en) * | 2014-02-07 | 2014-04-23 | 郭永来 | Steam distillation aromatic essential oil device |
| CN103897807A (en) * | 2014-04-24 | 2014-07-02 | 四川银谷玫瑰科技有限公司 | Method for extracting rose essential oil |
| CN105001973A (en) * | 2015-07-21 | 2015-10-28 | 广西壮族自治区林业科学研究院 | Comprehensive processing equipment for dry ginger slices and ginger oil |
| CN105199833A (en) * | 2015-07-21 | 2015-12-30 | 广西大学 | Comprehensive processing method of dried ginger slices and ginger oil |
| CN108467792A (en) * | 2018-05-17 | 2018-08-31 | 无锡市鹅湖玫瑰园艺文化有限公司 | Rosa Damascana extraction element |
| CN108998244A (en) * | 2018-08-08 | 2018-12-14 | 甘肃瑰隆生物科技有限公司 | Rose ethereal oil extraction element |
| CN109749852A (en) * | 2019-03-13 | 2019-05-14 | 甘肃瑰隆生物科技有限公司 | The conveying charging process of rose in a kind of Rosa Damascana extraction process |
| CN111763571A (en) * | 2020-07-08 | 2020-10-13 | 湖北瑞晟生物有限责任公司 | Rose essential oil draws uses quick distillation plant |
| CN112500931A (en) * | 2020-11-28 | 2021-03-16 | 盐城拉芬化妆品有限公司 | Preparation method of plant essential oil of acne-removing whitening skin care product |
-
2004
- 2004-03-31 CN CN 200410029668 patent/CN1232622C/en not_active Expired - Fee Related
Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101721338B (en) * | 2009-11-20 | 2012-08-22 | 甘肃农业大学 | Cosmetic containing Rosa setate X R. rugosa water |
| CN102952644A (en) * | 2012-12-06 | 2013-03-06 | 广西京桂香料有限公司 | Device for extracting natural cinnamon oil |
| CN103146487A (en) * | 2013-04-08 | 2013-06-12 | 云南绿宝香精香料股份有限公司 | Water steam distillation device with duplex effects of extraction and separation |
| CN103740469A (en) * | 2014-02-07 | 2014-04-23 | 郭永来 | Steam distillation aromatic essential oil device |
| CN103740469B (en) * | 2014-02-07 | 2015-04-08 | 郭永来 | Steam distillation aromatic essential oil device |
| CN103897807A (en) * | 2014-04-24 | 2014-07-02 | 四川银谷玫瑰科技有限公司 | Method for extracting rose essential oil |
| CN105001973A (en) * | 2015-07-21 | 2015-10-28 | 广西壮族自治区林业科学研究院 | Comprehensive processing equipment for dry ginger slices and ginger oil |
| CN105199833A (en) * | 2015-07-21 | 2015-12-30 | 广西大学 | Comprehensive processing method of dried ginger slices and ginger oil |
| CN108467792A (en) * | 2018-05-17 | 2018-08-31 | 无锡市鹅湖玫瑰园艺文化有限公司 | Rosa Damascana extraction element |
| CN108998244A (en) * | 2018-08-08 | 2018-12-14 | 甘肃瑰隆生物科技有限公司 | Rose ethereal oil extraction element |
| CN109749852A (en) * | 2019-03-13 | 2019-05-14 | 甘肃瑰隆生物科技有限公司 | The conveying charging process of rose in a kind of Rosa Damascana extraction process |
| CN111763571A (en) * | 2020-07-08 | 2020-10-13 | 湖北瑞晟生物有限责任公司 | Rose essential oil draws uses quick distillation plant |
| CN112500931A (en) * | 2020-11-28 | 2021-03-16 | 盐城拉芬化妆品有限公司 | Preparation method of plant essential oil of acne-removing whitening skin care product |
| CN112500931B (en) * | 2020-11-28 | 2021-09-21 | 上海丽舒丹医药科技有限公司 | Preparation method of plant essential oil of acne-removing whitening skin care product |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1232622C (en) | 2005-12-21 |
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| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| ASS | Succession or assignment of patent right |
Owner name: ZHEJIANG KAIDI PHARMACEUTICAL CHEMICAL MACHINERY C Free format text: FORMER OWNER: QIU YUNBIAO Effective date: 20110830 Free format text: FORMER OWNER: GAO YANTING |
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| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20110830 Address after: 325200 No. 7 Yaohua Road, eighteen industrial districts, Zhejiang, Ruian Patentee after: Zhejiang KAIDI Pharmaceutical Chemical Machinery Co., Ltd. Address before: 325200 Taiping stone 19, Anyang Town, Zhejiang, Ruian Co-patentee before: Gao Yanting Patentee before: Qiu Yunbiao |
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| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20051221 Termination date: 20130331 |