CN1232622C - Technique for extracting rhodamine oil - Google Patents
Technique for extracting rhodamine oil Download PDFInfo
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- CN1232622C CN1232622C CN 200410029668 CN200410029668A CN1232622C CN 1232622 C CN1232622 C CN 1232622C CN 200410029668 CN200410029668 CN 200410029668 CN 200410029668 A CN200410029668 A CN 200410029668A CN 1232622 C CN1232622 C CN 1232622C
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- rose
- water
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Abstract
The present invention discloses a technology for extracting rose essence oil, which is characterized in that rose flowers and water are mixed and placed in a quickly-opened distillation tank; then steam is led in a jacket of the quickly-opened distillation tank, and the rose flowers and the water are stirred and heated in the quickly-opened distillation tank by a stirring device; after steam generated in the quickly-opened distillation tank is twice distilled by a distillation column, and the steam is condensed by a condenser and cooled by a cooler; secondary water-oil separating is carried out; finally the rose essence oil is obtained. In the present invention, the steam is led in the jacket of the distillation tank to be heated. Because of large heating area and high heating speed, after the rose flowers and the water in the distillation tank are heated, heating reaction is carried out in a dynamic state under the condition that the rose flowers and the water are stirred by the stirring device. Thus, the internal quality of the rose flowers is not influenced, and the original properties and the transparence of the rose flowers are preserved. After secondary water-oil separating is adopted, oil and water are thoroughly separated from each other. Thereby, the quality, the output and the purity of the rose essence oil are increased.
Description
[technical field]
What the present invention relates to is a kind of extracting method of Chinese medicinal materials, and what be specifically related to is a kind of Rose extracts essential oil method.
[background technology]
In the prior art, Rose extracts essential oil method is Rose and water to be presented in the inferior pyramidal retort directly water is heated, and the steam after the heating separates obtaining Flos Rosae Rugosae quintessence oil then by the shell-and tube condenser condensation by water-and-oil separator.This extracting method is owing to adopted the retort of last inferior pyramidal, and directly feed retort with dry steam and heat, residue after distillation finishes, can only be with manually in the lateral hole of retort, excavating, Rose is attached on the heating pipe because the coking phenomenon that high temperature produced, clean very difficult, very time-consuming, owing to adopt dry steam not through separating and purifying, in the thermal process reactor of whole static state, thermal source in the steam and impurity have directly damaged composition and the character of Rose, make the rose oil muddiness that distills out contain smell of urine flavor again, still residual stain in the oil has influenced the quality of rose oil, and this method adopts a shell-and tube condenser to cool off, make the gas-liquid that has rose oil enter condenser and can not get cooling off completely, cause the loss of rose oil gas-liquid, adopt simultaneously a table oil water separator carry out he from, make profit can not get separating fully, directly influenced the output and the purity of rose oil.How to make the rose oil of extraction keep original character of Rose and composition, and make that its transparency is good, quality and output height, be that those skilled in the art want to solve and an insoluble difficult problem always.
[summary of the invention]
In view of problems of the prior art, the object of the present invention is to provide a kind of rose oil that makes to keep original character and composition, improve the extracting method of quality, output and the purity of rose oil product.For achieving the above object, the present invention takes following scheme to finish: the extracting method of this Flos Rosae Rugosae quintessence oil, it is characterized in that Rose and water mixing are inserted in the pneumatic open and close type retort, then steam is fed in the chuck of pneumatic open and close type retort, heat while stirring in pneumatic open and close type retort with whipping appts, the steam that produces in the pneumatic open and close type retort is through behind the second distillation of distillation column, pass through condenser condenses, the water cooler cooling, carry out secondary oily water separation again, obtain Flos Rosae Rugosae quintessence oil at last, described pneumatic open and close type retort is to be provided with cylinder and connecting rod in the outside of tank body, and described cylinder and connecting rod are by hinged-support and rod hinge connection, to the retort distillation test residue, press pneumatically operated switch, the capping of discharge port is opened fully, and with the disposable discharge of residue, described condenser and water cooler are rolled plate.
The present invention feeds steam in the chuck of retort and heats, because heating-surface area is big, rate of heating is fast, after Rose in the retort and water are heated, under the stirring of whipping appts, thermal response is carried out under dynamical state, can not make the Rose in the retort produce coking phenomenon, and can not have influence on Rose intrinsic quality, keep original fragrance of Rose and transparency; Adopt the retort of pneumatic open and close type, distillation test residue can disposablely be discharged, save time very much, and it is convenient to clean, adopt board-like condenser, condensation area is big, easy cleaning, with condensed gas-liquid again through supercooler, it is fully cooled off, can not run off, adopt secondary oily water separation simultaneously, oil is thoroughly separated with water, improved the output and the purity of Flos Rosae Rugosae quintessence oil.Adopt the extracting method of theme of the present invention, will bring positive economic benefit for the producer that extracts Flos Rosae Rugosae quintessence oil.
[description of drawings]
The present invention has following accompanying drawing:
Fig. 1 is a schema of the present invention.
[embodiment]
Accompanying drawing has been represented the implementation process of the inventive method, further describes each relevant details of embodiment below more in conjunction with the accompanying drawings.The extracting method of this Flos Rosae Rugosae quintessence oil, at first be that Rose and water mixing are inserted in the pneumatic open and close type retort, then steam is fed in the chuck of pneumatic open and close type retort, heat while stirring in pneumatic open and close type retort with whipping appts, the steam that produces in the pneumatic open and close type retort is through behind the second distillation of distillation column, by condenser condenses, water cooler cooling, carry out secondary oily water separation again, obtain the Flos Rosae Rugosae quintessence oil product at last; In heat-processed, temperature should be controlled at 100～120 ℃; Be back to again in retort and the distillation column through the water after the secondary separation; The retort of described pneumatic open and close type is to be provided with cylinder and connecting rod in the outside of tank body, described cylinder is by hinged-support and rod hinge connection, to the retort distillation test residue, as long as press pneumatically operated switch, the capping of discharge port is opened fully, with the disposable discharge of residue, save time very much, and clean conveniently; Described condenser and water cooler are rolled plate; Described rolled plate condenser and water cooler are the cooling tubes that adopts rolled plate in condenser and water cooler; After the cooling of this two-stage, make the gas-liquid cooling fully, can not run off, and provide good basis for the oily water separation of subsequent processing; Because the special proportion of rose oil in order fully to collect the Rose essential oil, so adopt secondary oily water separation, makes oil thoroughly separate with water, has improved the output and the purity of Flos Rosae Rugosae quintessence oil; Equipment in the inventive method all adopts the fine stainless material, and not to Rose and water direct heating, and heating source is carried out in the chuck of retort, can not have influence on original character of Rose and composition, kept original fragrance of Rose and transparency.According to the Rose essential oil that the present invention extracts, quality, output and based on very high purity compared with prior art, have outstanding substantive distinguishing features and obvious improvement.
Claims (1)
1, a kind of extracting method of Flos Rosae Rugosae quintessence oil, it is characterized in that Rose and water mixing are inserted in the pneumatic open and close type retort, then steam is fed in the chuck of pneumatic open and close type retort, heat while stirring in pneumatic open and close type retort with whipping appts, the steam that produces in the pneumatic open and close type retort is through behind the second distillation of distillation column, condenser condenses and water cooler cooling by rolled plate, carry out secondary oily water separation again, obtain the Flos Rosae Rugosae quintessence oil product at last, described pneumatic open and close type retort is to be provided with cylinder and connecting rod in the outside of tank body, described cylinder is by hinged-support and rod hinge connection, to the retort distillation test residue, press pneumatically operated switch, the capping of discharge port is opened fully, with the disposable discharge of residue.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200410029668 CN1232622C (en) | 2004-03-31 | 2004-03-31 | Technique for extracting rhodamine oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200410029668 CN1232622C (en) | 2004-03-31 | 2004-03-31 | Technique for extracting rhodamine oil |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1563311A CN1563311A (en) | 2005-01-12 |
| CN1232622C true CN1232622C (en) | 2005-12-21 |
Family
ID=34480970
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200410029668 Expired - Fee Related CN1232622C (en) | 2004-03-31 | 2004-03-31 | Technique for extracting rhodamine oil |
Country Status (1)
| Country | Link |
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| CN (1) | CN1232622C (en) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101721338B (en) * | 2009-11-20 | 2012-08-22 | 甘肃农业大学 | Cosmetic containing Rosa setate X R. rugosa water |
| CN102952644B (en) * | 2012-12-06 | 2014-04-23 | 广西京桂香料有限公司 | Device for extracting natural cinnamon oil |
| CN103146487B (en) * | 2013-04-08 | 2014-07-30 | 云南绿宝香精香料股份有限公司 | Water steam distillation device with duplex effects of extraction and separation |
| CN103740469B (en) * | 2014-02-07 | 2015-04-08 | 郭永来 | Steam distillation aromatic essential oil device |
| CN103897807B (en) * | 2014-04-24 | 2016-02-17 | 银谷玫瑰科技有限公司 | A kind of extracting method of Flos Rosae Rugosae quintessence oil |
| CN105199833B (en) * | 2015-07-21 | 2019-02-05 | 广西大学 | A kind of method for comprehensive processing of dried ginger slice and ginger oil |
| CN105001973B (en) * | 2015-07-21 | 2019-02-12 | 广西壮族自治区林业科学研究院 | A kind of consolidating processing equipment of dried ginger slice and ginger oil |
| CN108467792A (en) * | 2018-05-17 | 2018-08-31 | 无锡市鹅湖玫瑰园艺文化有限公司 | Rosa Damascana extraction element |
| CN108998244A (en) * | 2018-08-08 | 2018-12-14 | 甘肃瑰隆生物科技有限公司 | Rose ethereal oil extraction element |
| CN109749852A (en) * | 2019-03-13 | 2019-05-14 | 甘肃瑰隆生物科技有限公司 | The conveying charging process of rose in a kind of Rosa Damascana extraction process |
| CN111763571A (en) * | 2020-07-08 | 2020-10-13 | 湖北瑞晟生物有限责任公司 | Rose essential oil draws uses quick distillation plant |
| CN112500931B (en) * | 2020-11-28 | 2021-09-21 | 上海丽舒丹医药科技有限公司 | Preparation method of plant essential oil of acne-removing whitening skin care product |
-
2004
- 2004-03-31 CN CN 200410029668 patent/CN1232622C/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CN1563311A (en) | 2005-01-12 |
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| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
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| ASS | Succession or assignment of patent right |
Owner name: ZHEJIANG KAIDI PHARMACEUTICAL CHEMICAL MACHINERY C Free format text: FORMER OWNER: QIU YUNBIAO Effective date: 20110830 Free format text: FORMER OWNER: GAO YANTING |
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| C41 | Transfer of patent application or patent right or utility model | ||
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Effective date of registration: 20110830 Address after: 325200 No. 7 Yaohua Road, eighteen industrial districts, Zhejiang, Ruian Patentee after: Zhejiang KAIDI Pharmaceutical Chemical Machinery Co., Ltd. Address before: 325200 Taiping stone 19, Anyang Town, Zhejiang, Ruian Co-patentee before: Gao Yanting Patentee before: Qiu Yunbiao |
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| C17 | Cessation of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20051221 Termination date: 20130331 |