CN101343594A - Preparation method for rose hip or seed oil - Google Patents
Preparation method for rose hip or seed oil Download PDFInfo
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- CN101343594A CN101343594A CNA2007100527490A CN200710052749A CN101343594A CN 101343594 A CN101343594 A CN 101343594A CN A2007100527490 A CNA2007100527490 A CN A2007100527490A CN 200710052749 A CN200710052749 A CN 200710052749A CN 101343594 A CN101343594 A CN 101343594A
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Abstract
The invention relates to a preparation method for rose fruit or rose seed oil, which comprises the main procedures: sorting and removing coarse rose fruit, crushing the rose fruit, removing husks, then breaking rose seeds into particles and heating the particles in a frying pan up to 40 DEG C to 60 DEG C to separate out the rose oil through one to three levels of squeezing, as well as separating out ester gum and phospholipid from the rose oil; and maintaining the purity of the rose oil through filtration, storage and purification.
Description
Technical field
The present invention relates to a kind of extractive technique of natural rose spices, the preparation method of specifically a kind of Rose hips or seed oil belongs to the crude vegetal preparing technical field.
Background technology
Natural rose seed oil Rosa davurica pall, claims thorn rose rose, wild rose, rose hip again at (vegetable formal name) Rosa davurica Rosa bella.
Natural rose oil is plant base oil and the Clean products that refines from the wild rose seed.It is 100% fully natural green skin care good product.The wild rose seed is through squeezing, concise method, inclusion-free, effective.
Similar products like is arranged abroad.Be called Rosehip seed oil rose-seed oil.External rose oil is from Rosehip moschata and Rosa rubiginosa, obtains in Rosa canina and the seed.The foreign language title is referred to as Rosehip seed oil, Chinese rose-seed oil.Wild rose seed oil is fatty oil or fixed oil, mainly is the ester class of Fatty Alcohol(C12-C14 and C12-C18).Wild rose seed oil is a kind of effective natural phant treated oil because the boiling point height so be suitable for cosmetic industry most, also is one of senior raw material rare in the cosmetic industry, and rose-seed oil can be used in food, medicine, healthcare products and makeup.
Though rose oil is a kind of rare senior plant perfume, can be widely used in food, medicine, healthcare products and makeup, but will be extracting in Rose, Rose hips or the rose seed, need to realize through complicated Technology, constantly study through people,, found the certain methods of refining Rose hips or seed, conclude and get up roughly to have three kinds, the one, distillation method; The 2nd, milling process; The 3rd, solvent extration.Distillation method is to take low-temperature distillation to obtain rose oil after rose Rose hips or the rose seed pulverization process; Milling process is that the rose seed is handled, and pulverizes and squeeze the acquisition rose oil; Solvent extration is that the rose seed is dissolved in the solvent, is obtaining rose oil through fractionation by distillation.Aforesaid method has been brought into play certain active effect at extraction rose flowers and fruits or seed oil method, but still there is deficiency in aforesaid method, distillation, milling process can not be removed the detrimental impurity in the rose oil, raw oil oil is highly seasoned, in many cases, owing to steam high temperature can make rose oil in some compositions decompose the quality that reduces rose oil, solvent extration needs the high density solvent, rose seed dissolved time in the high density solvent is long to the unsaturated fatty acids in the rose oil, linolic acid, vitamin-E produces certain destruction, the poor product quality of producing is difficult to treat each other and squeezes into the international market.
Summary of the invention
The objective of the invention is to prepare the problem that exists in the rose oil technology at above-mentioned Rose hips or rose seed, new preparation method in one is proposed, this method can extract Rose hips or rose-seed oil in low temperature pressing, and not with an organic solvent, the whole course of processing is to carry out at low temperatures, overcome Rose hips or oxidation of rose-seed oil composition and degraded effectively, the rose oil composition is not destroyed, make the production technology collection squeezing of rose, extraction, be located away from one, the phase transition process that does not have material, easy to operate, pollution-free, no toxin, energy efficient, the oil yield of its Rose hips or rose seed reaches more than 95%.
The preparation method of Rose hips of the present invention or rose-seed oil: 1, the preparation method of a kind of Rose hips or seed oil purifies four steps and finishes by fragmentation, squeezing, vacuum filtration, separation storage: it is characterized in that:
Operation mainly comprises:
(1) with pulverizer with the Rose hips fragmentation, remove shell, then the rose seed is broken into particulate state, in frying pan, heat in 40--60 ℃, 60 ℃ that are kept at in the following container;
(2) three grades of squeezings through one, two, three squeezing, are isolated rose oil;
(3) filter, residue is known in vacuum filtration, keeps the purity of oil;
(4) separate, store purification, separate glue fat and phosphatide in the rose oil;
The preparation method of a kind of Rose hips of the present invention or seed oil is characterized in that: a preceding operation steps of sorting for removing impurities, the fruit or rose seed, carpopodium, sand and the dust contaminant removal that will soon go bad of also comprising of operation (1);
The preparation method of a kind of Rose hips of the present invention or seed oil is characterized in that: operation (2) is preceding also to comprise an operation: in frying pan, heat 40--60 ℃ with interior 60 ℃ of being kept at in the following container.
The preparation method of a kind of Rose hips of the present invention or seed oil is characterized in that: also comprise an operation after the operation (5): rose oil is carried out aquation, and temperature is controlled at 85-90 ℃, separates plastic emitting fat and phosphatide with whizzer; Or adopting the plate filter filter at low temperature, temperature is controlled at 10-20 ℃, exerts pressure 0.02 kilogram, from filter, isolate rose oil slowly.
The preparation method of a kind of Rose hips of the present invention or seed oil is characterized in that: rose oil is stored purification, and temperature is controlled at below 30-35 ℃.
After adopting above-mentioned preparation method, the present invention keeps the purity of oil because through steps of sorting for removing impurities, squeezing, filtration, residue is known in vacuum filtration, and through aquation, separates plastic emitting fat and phosphatide with whizzer; Rose oil is stored purification, from Rose hips or seed, prepare high-quality rose oil.
Description of drawings
Below with reference to the accompanying drawings, in conjunction with the embodiments the present invention is further described:
Fig. 1 is the flow process chart of the embodiment of the invention.
Embodiment
As of the present invention shown in Figure 1, a kind of Rose hips that the present invention discloses or the preparation method of seed oil comprise that mainly fragmentation, squeezing, vacuum filtration, separation, storage purify four operations.
At first steps of sorting for removing impurities, be about to rotten fruit or rose seed, carpopodium, sand and dust contaminant removal; With the Rose hips fragmentation, remove shell with pulverizer, then the rose seed is broken into particulate state, heat in frying pan in 40--60 ℃, 60 ℃ that are kept at in the following container; Through the squeezing of first road, from Rose hips or seed, extract 50% rose oil; Then carry out the squeezing of second road, extract 35% Rose hips or seed oil; Then carry out the squeezing of the 3rd road again, extract Rose hips or the seed oil of 10-15%.Rose oil is carried out aquation, and temperature is controlled at 85-90 ℃, separates plastic emitting fat and phosphatide with whizzer; Or adopting the plate filter filter at low temperature, temperature is controlled at 10-20 ℃, exerts pressure 0.02 kilogram, from filter, isolate Rose hips or seed oil slowly.After isolating the removal of impurities of rose oil usefulness filter cloth, use highly dense filter paper filtering again, store purification then, from Rose hips or seed, prepare high-quality Rose hips or seed oil.
Processed oil sent in Beijing's prevention and control of diseases detect, detected result sees Table 1
Table 1 Rose hips of the present invention or the analysis of seed oil main component
The present invention enters to store to filtration from go into to squeeze out Rose hips or seed oil and purifies, adopt sealing-duct to carry the pollution of avoiding rose oil, rose edible vegetable oil and essential oil are provided with transport pipe separately, manage storage tank and do not use with, and the assurance oil storage is preserved in 20-30 ℃ constant temperature.
Claims (5)
1, the preparation method of a kind of Rose hips or seed oil finishes by steps of sorting for removing impurities, fragmentation, squeezing, vacuum filtration, five steps of separation, it is characterized in that:
Operation mainly comprises:
(1) with pulverizer with the Rose hips fragmentation, remove shell, then the rose seed is broken into particulate state, in frying pan, heat in 40--60 ℃, 60 ℃ that are kept at in the following container;
(2) three grades of squeezings through one, two, three squeezing, are isolated rose oil;
(3) filter, residue is known in vacuum filtration, keeps the purity of oil;
(4) separate, separate glue fat and phosphatide in the rose oil;
(5) storing purification is.
2, the preparation method of a kind of Rose hips according to claim 1 or seed oil is characterized in that: a preceding operation steps of sorting for removing impurities, the fruit or rose seed, carpopodium, sand and the dust contaminant removal that will soon go bad of also comprising of operation (1).
3, the preparation method of a kind of Rose hips according to claim 1 or seed oil is characterized in that: operation (2) is preceding also to comprise an operation: in frying pan, heat 40--60 ℃ with interior 60 ℃ of being kept at in the following container.
4, the preparation method of a kind of Rose hips according to claim 1 or seed oil is characterized in that: also comprise an operation after the operation (5): rose oil is carried out aquation filter, temperature is controlled at 85-90 ℃, separates plastic emitting fat and phosphatide; Or the employing filter at low temperature, temperature is controlled at 10-20 ℃, and plate filter filters, and the 0.02-0.03 kilogram of exerting pressure is isolated rose oil slowly from filter.
5, the preparation method of a kind of Rose hips according to claim 4 or seed oil is characterized in that: rose oil is stored purification, and temperature is controlled at below 30-35 ℃.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2007100527490A CN101343594A (en) | 2007-07-14 | 2007-07-14 | Preparation method for rose hip or seed oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2007100527490A CN101343594A (en) | 2007-07-14 | 2007-07-14 | Preparation method for rose hip or seed oil |
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| Publication Number | Publication Date |
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| CN101343594A true CN101343594A (en) | 2009-01-14 |
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| Application Number | Title | Priority Date | Filing Date |
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| CNA2007100527490A Pending CN101343594A (en) | 2007-07-14 | 2007-07-14 | Preparation method for rose hip or seed oil |
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| CN (1) | CN101343594A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102492541A (en) * | 2011-12-13 | 2012-06-13 | 九三粮油工业集团有限公司 | Method for extracting rose hip oil by supercritical carbon dioxide |
| CN108026475A (en) * | 2015-08-05 | 2018-05-11 | 伊森舍创新有限责任公司 | The system and method for extracting essential oil |
| CN109010133A (en) * | 2018-09-10 | 2018-12-18 | 深圳市仙迪化妆品有限公司 | A kind of molten rose berry extract of oil and application |
| CN109125168A (en) * | 2018-09-10 | 2019-01-04 | 深圳市仙迪化妆品有限公司 | A kind of fructus rosae extracting solution and the preparation method and application thereof |
-
2007
- 2007-07-14 CN CNA2007100527490A patent/CN101343594A/en active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102492541A (en) * | 2011-12-13 | 2012-06-13 | 九三粮油工业集团有限公司 | Method for extracting rose hip oil by supercritical carbon dioxide |
| CN108026475A (en) * | 2015-08-05 | 2018-05-11 | 伊森舍创新有限责任公司 | The system and method for extracting essential oil |
| CN109010133A (en) * | 2018-09-10 | 2018-12-18 | 深圳市仙迪化妆品有限公司 | A kind of molten rose berry extract of oil and application |
| CN109125168A (en) * | 2018-09-10 | 2019-01-04 | 深圳市仙迪化妆品有限公司 | A kind of fructus rosae extracting solution and the preparation method and application thereof |
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Open date: 20090114 |