CN101343594A - Preparation method for rose hip or seed oil - Google Patents
Preparation method for rose hip or seed oil Download PDFInfo
- Publication number
- CN101343594A CN101343594A CNA2007100527490A CN200710052749A CN101343594A CN 101343594 A CN101343594 A CN 101343594A CN A2007100527490 A CNA2007100527490 A CN A2007100527490A CN 200710052749 A CN200710052749 A CN 200710052749A CN 101343594 A CN101343594 A CN 101343594A
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- rose
- oil
- seed
- preparation
- seed oil
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- 241000220317 Rosa Species 0.000 title claims abstract description 58
- 235000015112 vegetable and seed oil Nutrition 0.000 title claims abstract description 27
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 235000019719 rose oil Nutrition 0.000 claims abstract description 31
- 239000010666 rose oil Substances 0.000 claims abstract description 31
- 235000013399 edible fruits Nutrition 0.000 claims abstract description 7
- 238000000746 purification Methods 0.000 claims abstract description 7
- 239000003921 oil Substances 0.000 claims description 15
- 235000019198 oils Nutrition 0.000 claims description 15
- 239000012535 impurity Substances 0.000 claims description 7
- 238000013467 fragmentation Methods 0.000 claims description 6
- 238000006062 fragmentation reaction Methods 0.000 claims description 6
- 238000003828 vacuum filtration Methods 0.000 claims description 6
- 239000000356 contaminant Substances 0.000 claims description 3
- 239000000428 dust Substances 0.000 claims description 3
- 239000004576 sand Substances 0.000 claims description 3
- 238000000926 separation method Methods 0.000 claims description 3
- 239000003292 glue Substances 0.000 claims description 2
- 238000000034 method Methods 0.000 abstract description 13
- 238000003860 storage Methods 0.000 abstract description 5
- 238000001914 filtration Methods 0.000 abstract description 4
- 239000002245 particle Substances 0.000 abstract 2
- 235000010985 glycerol esters of wood rosin Nutrition 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000010903 husk Substances 0.000 abstract 1
- 150000003904 phospholipids Chemical class 0.000 abstract 1
- 239000002904 solvent Substances 0.000 description 6
- 241000109365 Rosa arkansana Species 0.000 description 5
- 235000005066 Rosa arkansana Nutrition 0.000 description 5
- 238000004821 distillation Methods 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 238000003801 milling Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 235000013932 Rosa davurica Nutrition 0.000 description 2
- 241000675183 Rosa davurica Species 0.000 description 2
- 239000002537 cosmetic Substances 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- OYHQOLUKZRVURQ-HZJYTTRNSA-N Linoleic acid Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(O)=O OYHQOLUKZRVURQ-HZJYTTRNSA-N 0.000 description 1
- 235000016607 Rosa bella Nutrition 0.000 description 1
- 241000914162 Rosa bella Species 0.000 description 1
- 235000000539 Rosa canina Nutrition 0.000 description 1
- 240000008530 Rosa canina Species 0.000 description 1
- 235000000542 Rosa eglanteria Nutrition 0.000 description 1
- 244000181066 Rosa eglanteria Species 0.000 description 1
- 229930003427 Vitamin E Natural products 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 239000002199 base oil Substances 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 239000008157 edible vegetable oil Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 150000002191 fatty alcohols Chemical class 0.000 description 1
- 239000010685 fatty oil Substances 0.000 description 1
- 238000005194 fractionation Methods 0.000 description 1
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 1
- 229960004232 linoleic acid Drugs 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000000346 nonvolatile oil Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 239000003053 toxin Substances 0.000 description 1
- 231100000765 toxin Toxicity 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- 238000005292 vacuum distillation Methods 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
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- Fats And Perfumes (AREA)
- Edible Oils And Fats (AREA)
Abstract
The invention relates to a preparation method for rose fruit or rose seed oil, which comprises the main procedures: sorting and removing coarse rose fruit, crushing the rose fruit, removing husks, then breaking rose seeds into particles and heating the particles in a frying pan up to 40 DEG C to 60 DEG C to separate out the rose oil through one to three levels of squeezing, as well as separating out ester gum and phospholipid from the rose oil; and maintaining the purity of the rose oil through filtration, storage and purification.
Description
Technical field
The present invention relates to a kind of extractive technique of natural rose spices, the preparation method of specifically a kind of Rose hips or seed oil belongs to the crude vegetal preparing technical field.
Background technology
Natural rose seed oil Rosa davurica pall, claims thorn rose rose, wild rose, rose hip again at (vegetable formal name) Rosa davurica Rosa bella.
Natural rose oil is plant base oil and the Clean products that refines from the wild rose seed.It is 100% fully natural green skin care good product.The wild rose seed is through squeezing, concise method, inclusion-free, effective.
Similar products like is arranged abroad.Be called Rosehip seed oil rose-seed oil.External rose oil is from Rosehip moschata and Rosa rubiginosa, obtains in Rosa canina and the seed.The foreign language title is referred to as Rosehip seed oil, Chinese rose-seed oil.Wild rose seed oil is fatty oil or fixed oil, mainly is the ester class of Fatty Alcohol(C12-C14 and C12-C18).Wild rose seed oil is a kind of effective natural phant treated oil because the boiling point height so be suitable for cosmetic industry most, also is one of senior raw material rare in the cosmetic industry, and rose-seed oil can be used in food, medicine, healthcare products and makeup.
Though rose oil is a kind of rare senior plant perfume, can be widely used in food, medicine, healthcare products and makeup, but will be extracting in Rose, Rose hips or the rose seed, need to realize through complicated Technology, constantly study through people,, found the certain methods of refining Rose hips or seed, conclude and get up roughly to have three kinds, the one, distillation method; The 2nd, milling process; The 3rd, solvent extration.Distillation method is to take low-temperature distillation to obtain rose oil after rose Rose hips or the rose seed pulverization process; Milling process is that the rose seed is handled, and pulverizes and squeeze the acquisition rose oil; Solvent extration is that the rose seed is dissolved in the solvent, is obtaining rose oil through fractionation by distillation.Aforesaid method has been brought into play certain active effect at extraction rose flowers and fruits or seed oil method, but still there is deficiency in aforesaid method, distillation, milling process can not be removed the detrimental impurity in the rose oil, raw oil oil is highly seasoned, in many cases, owing to steam high temperature can make rose oil in some compositions decompose the quality that reduces rose oil, solvent extration needs the high density solvent, rose seed dissolved time in the high density solvent is long to the unsaturated fatty acids in the rose oil, linolic acid, vitamin-E produces certain destruction, the poor product quality of producing is difficult to treat each other and squeezes into the international market.
Summary of the invention
The objective of the invention is to prepare the problem that exists in the rose oil technology at above-mentioned Rose hips or rose seed, new preparation method in one is proposed, this method can extract Rose hips or rose-seed oil in low temperature pressing, and not with an organic solvent, the whole course of processing is to carry out at low temperatures, overcome Rose hips or oxidation of rose-seed oil composition and degraded effectively, the rose oil composition is not destroyed, make the production technology collection squeezing of rose, extraction, be located away from one, the phase transition process that does not have material, easy to operate, pollution-free, no toxin, energy efficient, the oil yield of its Rose hips or rose seed reaches more than 95%.
The preparation method of Rose hips of the present invention or rose-seed oil: 1, the preparation method of a kind of Rose hips or seed oil purifies four steps and finishes by fragmentation, squeezing, vacuum filtration, separation storage: it is characterized in that:
Operation mainly comprises:
(1) with pulverizer with the Rose hips fragmentation, remove shell, then the rose seed is broken into particulate state, in frying pan, heat in 40--60 ℃, 60 ℃ that are kept at in the following container;
(2) three grades of squeezings through one, two, three squeezing, are isolated rose oil;
(3) filter, residue is known in vacuum filtration, keeps the purity of oil;
(4) separate, store purification, separate glue fat and phosphatide in the rose oil;
The preparation method of a kind of Rose hips of the present invention or seed oil is characterized in that: a preceding operation steps of sorting for removing impurities, the fruit or rose seed, carpopodium, sand and the dust contaminant removal that will soon go bad of also comprising of operation (1);
The preparation method of a kind of Rose hips of the present invention or seed oil is characterized in that: operation (2) is preceding also to comprise an operation: in frying pan, heat 40--60 ℃ with interior 60 ℃ of being kept at in the following container.
The preparation method of a kind of Rose hips of the present invention or seed oil is characterized in that: also comprise an operation after the operation (5): rose oil is carried out aquation, and temperature is controlled at 85-90 ℃, separates plastic emitting fat and phosphatide with whizzer; Or adopting the plate filter filter at low temperature, temperature is controlled at 10-20 ℃, exerts pressure 0.02 kilogram, from filter, isolate rose oil slowly.
The preparation method of a kind of Rose hips of the present invention or seed oil is characterized in that: rose oil is stored purification, and temperature is controlled at below 30-35 ℃.
After adopting above-mentioned preparation method, the present invention keeps the purity of oil because through steps of sorting for removing impurities, squeezing, filtration, residue is known in vacuum filtration, and through aquation, separates plastic emitting fat and phosphatide with whizzer; Rose oil is stored purification, from Rose hips or seed, prepare high-quality rose oil.
Description of drawings
Below with reference to the accompanying drawings, in conjunction with the embodiments the present invention is further described:
Fig. 1 is the flow process chart of the embodiment of the invention.
Embodiment
As of the present invention shown in Figure 1, a kind of Rose hips that the present invention discloses or the preparation method of seed oil comprise that mainly fragmentation, squeezing, vacuum filtration, separation, storage purify four operations.
At first steps of sorting for removing impurities, be about to rotten fruit or rose seed, carpopodium, sand and dust contaminant removal; With the Rose hips fragmentation, remove shell with pulverizer, then the rose seed is broken into particulate state, heat in frying pan in 40--60 ℃, 60 ℃ that are kept at in the following container; Through the squeezing of first road, from Rose hips or seed, extract 50% rose oil; Then carry out the squeezing of second road, extract 35% Rose hips or seed oil; Then carry out the squeezing of the 3rd road again, extract Rose hips or the seed oil of 10-15%.Rose oil is carried out aquation, and temperature is controlled at 85-90 ℃, separates plastic emitting fat and phosphatide with whizzer; Or adopting the plate filter filter at low temperature, temperature is controlled at 10-20 ℃, exerts pressure 0.02 kilogram, from filter, isolate Rose hips or seed oil slowly.After isolating the removal of impurities of rose oil usefulness filter cloth, use highly dense filter paper filtering again, store purification then, from Rose hips or seed, prepare high-quality Rose hips or seed oil.
Processed oil sent in Beijing's prevention and control of diseases detect, detected result sees Table 1
Table 1 Rose hips of the present invention or the analysis of seed oil main component
The present invention enters to store to filtration from go into to squeeze out Rose hips or seed oil and purifies, adopt sealing-duct to carry the pollution of avoiding rose oil, rose edible vegetable oil and essential oil are provided with transport pipe separately, manage storage tank and do not use with, and the assurance oil storage is preserved in 20-30 ℃ constant temperature.
Claims (5)
1, the preparation method of a kind of Rose hips or seed oil finishes by steps of sorting for removing impurities, fragmentation, squeezing, vacuum filtration, five steps of separation, it is characterized in that:
Operation mainly comprises:
(1) with pulverizer with the Rose hips fragmentation, remove shell, then the rose seed is broken into particulate state, in frying pan, heat in 40--60 ℃, 60 ℃ that are kept at in the following container;
(2) three grades of squeezings through one, two, three squeezing, are isolated rose oil;
(3) filter, residue is known in vacuum filtration, keeps the purity of oil;
(4) separate, separate glue fat and phosphatide in the rose oil;
(5) storing purification is.
2, the preparation method of a kind of Rose hips according to claim 1 or seed oil is characterized in that: a preceding operation steps of sorting for removing impurities, the fruit or rose seed, carpopodium, sand and the dust contaminant removal that will soon go bad of also comprising of operation (1).
3, the preparation method of a kind of Rose hips according to claim 1 or seed oil is characterized in that: operation (2) is preceding also to comprise an operation: in frying pan, heat 40--60 ℃ with interior 60 ℃ of being kept at in the following container.
4, the preparation method of a kind of Rose hips according to claim 1 or seed oil is characterized in that: also comprise an operation after the operation (5): rose oil is carried out aquation filter, temperature is controlled at 85-90 ℃, separates plastic emitting fat and phosphatide; Or the employing filter at low temperature, temperature is controlled at 10-20 ℃, and plate filter filters, and the 0.02-0.03 kilogram of exerting pressure is isolated rose oil slowly from filter.
5, the preparation method of a kind of Rose hips according to claim 4 or seed oil is characterized in that: rose oil is stored purification, and temperature is controlled at below 30-35 ℃.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2007100527490A CN101343594A (en) | 2007-07-14 | 2007-07-14 | Preparation method for rose hip or seed oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2007100527490A CN101343594A (en) | 2007-07-14 | 2007-07-14 | Preparation method for rose hip or seed oil |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN101343594A true CN101343594A (en) | 2009-01-14 |
Family
ID=40245709
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNA2007100527490A Pending CN101343594A (en) | 2007-07-14 | 2007-07-14 | Preparation method for rose hip or seed oil |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN101343594A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102492541A (en) * | 2011-12-13 | 2012-06-13 | 九三粮油工业集团有限公司 | Method for extracting rose hip oil by supercritical carbon dioxide |
| CN108026475A (en) * | 2015-08-05 | 2018-05-11 | 伊森舍创新有限责任公司 | The system and method for extracting essential oil |
| CN109010133A (en) * | 2018-09-10 | 2018-12-18 | 深圳市仙迪化妆品有限公司 | A kind of molten rose berry extract of oil and application |
| CN109125168A (en) * | 2018-09-10 | 2019-01-04 | 深圳市仙迪化妆品有限公司 | A kind of fructus rosae extracting solution and the preparation method and application thereof |
-
2007
- 2007-07-14 CN CNA2007100527490A patent/CN101343594A/en active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102492541A (en) * | 2011-12-13 | 2012-06-13 | 九三粮油工业集团有限公司 | Method for extracting rose hip oil by supercritical carbon dioxide |
| CN108026475A (en) * | 2015-08-05 | 2018-05-11 | 伊森舍创新有限责任公司 | The system and method for extracting essential oil |
| CN109010133A (en) * | 2018-09-10 | 2018-12-18 | 深圳市仙迪化妆品有限公司 | A kind of molten rose berry extract of oil and application |
| CN109125168A (en) * | 2018-09-10 | 2019-01-04 | 深圳市仙迪化妆品有限公司 | A kind of fructus rosae extracting solution and the preparation method and application thereof |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Open date: 20090114 |