CN109010133A - A kind of molten rose berry extract of oil and application - Google Patents
A kind of molten rose berry extract of oil and application Download PDFInfo
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- CN109010133A CN109010133A CN201811050009.8A CN201811050009A CN109010133A CN 109010133 A CN109010133 A CN 109010133A CN 201811050009 A CN201811050009 A CN 201811050009A CN 109010133 A CN109010133 A CN 109010133A
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- 239000000284 extract Substances 0.000 title claims abstract description 52
- 241000036312 Juniperus coahuilensis Species 0.000 title claims abstract description 40
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000000463 material Substances 0.000 claims abstract description 20
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 15
- 239000001569 carbon dioxide Substances 0.000 claims abstract description 11
- 229910002092 carbon dioxide Inorganic materials 0.000 claims abstract description 11
- 238000001035 drying Methods 0.000 claims abstract description 9
- 238000000194 supercritical-fluid extraction Methods 0.000 claims abstract description 9
- 230000002087 whitening effect Effects 0.000 claims abstract description 9
- 239000002537 cosmetic Substances 0.000 claims abstract description 8
- 239000000843 powder Substances 0.000 claims abstract description 8
- 235000016709 nutrition Nutrition 0.000 claims abstract description 4
- 238000000605 extraction Methods 0.000 claims description 32
- 235000013399 edible fruits Nutrition 0.000 claims description 21
- 241000220317 Rosa Species 0.000 claims description 16
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 15
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 14
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 8
- 235000019441 ethanol Nutrition 0.000 claims description 4
- 239000003963 antioxidant agent Substances 0.000 claims description 3
- 230000003078 antioxidant effect Effects 0.000 claims description 3
- 238000000926 separation method Methods 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- 235000021028 berry Nutrition 0.000 claims 1
- 229910052799 carbon Inorganic materials 0.000 claims 1
- 239000000203 mixture Substances 0.000 abstract description 8
- 206010020751 Hypersensitivity Diseases 0.000 abstract description 3
- 208000026935 allergic disease Diseases 0.000 abstract description 3
- 230000007815 allergy Effects 0.000 abstract description 3
- 238000002360 preparation method Methods 0.000 abstract 1
- 239000003921 oil Substances 0.000 description 25
- 239000002994 raw material Substances 0.000 description 10
- 238000000034 method Methods 0.000 description 8
- GCNLQHANGFOQKY-UHFFFAOYSA-N [C+4].[O-2].[O-2].[Ti+4] Chemical compound [C+4].[O-2].[O-2].[Ti+4] GCNLQHANGFOQKY-UHFFFAOYSA-N 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 5
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 4
- 238000001291 vacuum drying Methods 0.000 description 4
- CWVRJTMFETXNAD-FWCWNIRPSA-N 3-O-Caffeoylquinic acid Natural products O[C@H]1[C@@H](O)C[C@@](O)(C(O)=O)C[C@H]1OC(=O)\C=C\C1=CC=C(O)C(O)=C1 CWVRJTMFETXNAD-FWCWNIRPSA-N 0.000 description 2
- PZIRUHCJZBGLDY-UHFFFAOYSA-N Caffeoylquinic acid Natural products CC(CCC(=O)C(C)C1C(=O)CC2C3CC(O)C4CC(O)CCC4(C)C3CCC12C)C(=O)O PZIRUHCJZBGLDY-UHFFFAOYSA-N 0.000 description 2
- SWRFKGRMQVLMKA-JIZJWZDPSA-N Casuarictin Chemical compound OC1=C(O)C(O)=CC(C(=O)O[C@H]2[C@@H]3OC(=O)C4=CC(O)=C(O)C(O)=C4C4=C(O)C(O)=C(O)C=C4C(=O)O[C@H]3[C@@H]3OC(=O)C4=CC(O)=C(O)C(O)=C4C4=C(O)C(O)=C(O)C=C4C(=O)OC[C@H]3O2)=C1 SWRFKGRMQVLMKA-JIZJWZDPSA-N 0.000 description 2
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 description 2
- CWVRJTMFETXNAD-KLZCAUPSSA-N Neochlorogenin-saeure Natural products O[C@H]1C[C@@](O)(C[C@@H](OC(=O)C=Cc2ccc(O)c(O)c2)[C@@H]1O)C(=O)O CWVRJTMFETXNAD-KLZCAUPSSA-N 0.000 description 2
- 244000050053 Rosa multiflora Species 0.000 description 2
- 235000000656 Rosa multiflora Nutrition 0.000 description 2
- 235000000659 Rosa rugosa Nutrition 0.000 description 2
- 229930003268 Vitamin C Natural products 0.000 description 2
- 235000006708 antioxidants Nutrition 0.000 description 2
- CWVRJTMFETXNAD-JUHZACGLSA-N chlorogenic acid Chemical compound O[C@@H]1[C@H](O)C[C@@](O)(C(O)=O)C[C@H]1OC(=O)\C=C\C1=CC=C(O)C(O)=C1 CWVRJTMFETXNAD-JUHZACGLSA-N 0.000 description 2
- 229940074393 chlorogenic acid Drugs 0.000 description 2
- FFQSDFBBSXGVKF-KHSQJDLVSA-N chlorogenic acid Natural products O[C@@H]1C[C@](O)(C[C@@H](CC(=O)C=Cc2ccc(O)c(O)c2)[C@@H]1O)C(=O)O FFQSDFBBSXGVKF-KHSQJDLVSA-N 0.000 description 2
- 235000001368 chlorogenic acid Nutrition 0.000 description 2
- BMRSEYFENKXDIS-KLZCAUPSSA-N cis-3-O-p-coumaroylquinic acid Natural products O[C@H]1C[C@@](O)(C[C@@H](OC(=O)C=Cc2ccc(O)cc2)[C@@H]1O)C(=O)O BMRSEYFENKXDIS-KLZCAUPSSA-N 0.000 description 2
- 239000001963 growth medium Substances 0.000 description 2
- 241000411851 herbal medicine Species 0.000 description 2
- 239000002480 mineral oil Substances 0.000 description 2
- 235000010446 mineral oil Nutrition 0.000 description 2
- 235000019154 vitamin C Nutrition 0.000 description 2
- 239000011718 vitamin C Substances 0.000 description 2
- 201000004384 Alopecia Diseases 0.000 description 1
- 108091003079 Bovine Serum Albumin Proteins 0.000 description 1
- 229920001408 Casuarictin Polymers 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 241000195955 Equisetum hyemale Species 0.000 description 1
- 240000006240 Linum usitatissimum Species 0.000 description 1
- 235000004431 Linum usitatissimum Nutrition 0.000 description 1
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 description 1
- 208000025865 Ulcer Diseases 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 238000004176 ammonification Methods 0.000 description 1
- 239000003242 anti bacterial agent Substances 0.000 description 1
- 229940088710 antibiotic agent Drugs 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- SWXVUIWOUIDPGS-UHFFFAOYSA-N diacetone alcohol Natural products CC(=O)CC(C)(C)O SWXVUIWOUIDPGS-UHFFFAOYSA-N 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000003628 erosive effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000012091 fetal bovine serum Substances 0.000 description 1
- 229930003944 flavone Natural products 0.000 description 1
- 150000002213 flavones Chemical class 0.000 description 1
- 235000011949 flavones Nutrition 0.000 description 1
- 235000021022 fresh fruits Nutrition 0.000 description 1
- SWRFKGRMQVLMKA-UHFFFAOYSA-N galloyl-bis-HHDP glucose Natural products OC1=C(O)C(O)=CC(C(=O)OC2C3OC(=O)C4=CC(O)=C(O)C(O)=C4C4=C(O)C(O)=C(O)C=C4C(=O)OC3C3OC(=O)C4=CC(O)=C(O)C(O)=C4C4=C(O)C(O)=C(O)C=C4C(=O)OCC3O2)=C1 SWRFKGRMQVLMKA-UHFFFAOYSA-N 0.000 description 1
- 230000003676 hair loss Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000003211 malignant effect Effects 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 1
- 210000003205 muscle Anatomy 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 150000008442 polyphenolic compounds Chemical class 0.000 description 1
- 235000013824 polyphenols Nutrition 0.000 description 1
- 239000010667 rosehip oil Substances 0.000 description 1
- 238000010186 staining Methods 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 235000002906 tartaric acid Nutrition 0.000 description 1
- 239000011975 tartaric acid Substances 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 231100000397 ulcer Toxicity 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- 235000019871 vegetable fat Nutrition 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 210000003905 vulva Anatomy 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/10—General cosmetic use
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Veterinary Medicine (AREA)
- Dermatology (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Medicines Containing Plant Substances (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention discloses a kind of molten rose berry extract of oil and applications, are related to cosmetic technical field.The extract is mainly made by following steps: fresh fructus rosae being taken to be dried in vacuo；Mixture after drying is ground into powder；Smashed material is put into extractor；Finally carry out carbon dioxide supercritical extraction, the isolated molten rose berry extract of oil.The rose berry extract obtained by carbon dioxide supercritical extraction can be applied in the preparation of cosmetics, and can be used as the whitening nutritional agents in cosmetics, great whitening effect, and safely and effectively, be not easy allergy.
Description
Technical field
The present invention relates to cosmetic technical field, a kind of molten rose berry extract of oil and application are referred in particular to.
Background technique
Fructus rosae is rose.The vegetable fat being process by the fruit of fructus rosae, referred to as rose hip oil.Rose
Fruit has the appellation of " king of vitamin C ".Through every 6810 milligrams of content of hectogram fresh fruit edible part VC of detection or more, up to
8300 milligrams, occuping is " hat of the earth fruit " first of all veterinary antibiotics." this is through meeting original " cynarrhodion also known as battalion are real,
Sour temperature, it is nontoxic.Curing mainly ulcer malignant sore, knot meat falls muscle, lose sore hot gas, the erosion of vulva not recover, sharp joint.Japanese rose branchlet master in " China's book on Chinese herbal medicine "
Control clearing heat for detumescence, baldness and boil.Japanese rose leaf cures mainly subdhing swelling and detoxicating, sore and toxic in " dictionary of medicinal plant " and " China's book on Chinese herbal medicine ".
Mainly contain chlorogenic acid (chlorogenic acid), horse-tail tan pavilion (casuarictin).Contain flax in rosaceous fruit
The substances such as acid, flavones, these are all the ingredients extremely beneficial to human body.
Summary of the invention
The technical problems to be solved by the present invention are: how to obtain a new molten rose berry extract of oil and be applied.
In order to solve the above-mentioned technical problem, the invention discloses a kind of molten rose berry extracts of oil, specifically by the following method
It is made:
S1 is dry, and fresh fructus rosae material vacuum is dry, makes water content 5-8%；
S2 is crushed, and dried fructus rosae is crushed to 20-60 mesh；
S3 feeds intake, and the fructus rosae material crushed is put into extractor；
S4 extraction, carries out carbon dioxide supercritical extraction, the isolated molten rose berry extract of oil.
Further, in the drying steps, fructus rosae used includes the fruit of fructus rosae, rose fruit seed, fructus rosae leaf
With fructus rosae flower.
Further, in the drying steps, fruit, rose fruit seed, fructus rosae leaf and the fructus rosae flower of the fructus rosae
The weight content of any one material is less than or equal to 85%.
Further, in the drying steps, drying temperature is lower than 70 DEG C, is higher than -10 DEG C；In the pulverising step, powder
Broken temperature is lower than 70 DEG C, is higher than -10 DEG C.
It further, further include the investment auxiliary extraction agent into extractor in the material addition step.
Further, in the material addition step, auxiliary extraction agent used be one of acetone, ethyl alcohol, ethyl acetate or
It is a variety of.
Further, in the material addition step, the input fructus rosae material relative extractive tank volume accounting crushed
For 60-80%, input auxiliary extraction agent relative extractive tank volume accounting is 5-10%.
Further, in the extraction step, extraction temperature is less than or equal to 60 DEG C, is more than or equal to -10 DEG C, pressure 25-
35MPa, extraction time 3-5h, carbon dioxide flow 200-300kg/h.
Further, in the extraction step, separation includes the first knockout drum and the second knockout drum, the first knockout drum temperature
Lower than 70 DEG C, it is higher than -10 DEG C, pressure 7-20MPa, the second knockout drum temperature is lower than 50 DEG C, is higher than -10 DEG C, pressure 1-
6MPa。
In addition, also disclosing the application of the molten rose berry extract of oil, specially the molten rose berry extract of oil is answered
Whitening nutritional agents and/or antioxidant for cosmetics.
The molten rose berry extract of oil that the present invention obtains, wherein complicated component, nutriment enrich, including
1) in the molten rose berry extract of oil natural unsaturated fatty acid content in 15.5-47%；
2) in the molten rose berry extract of oil natural polyphenol content in 5.5-15%；
3) in the molten rose berry extract of oil natural oil-soluble vitamins content in 5.5-15%；
4) in the molten rose berry extract of oil tartaric acid content in 0.5-5%；
5) in the molten rose berry extract of oil Vitamin C content in 1.5-5%.
The molten rose berry extract of oil that the present invention obtains, can be used for the whitening nutritional agents of cosmetics, can also be used as
The antioxidant of cosmetic.Great whitening effect, and safely and effectively, it is not easy allergy.
Specific embodiment
To explain the technical content, the achieved purpose and the effect of the present invention in detail, it is explained in detail below in conjunction with embodiment.
Implement 1
A kind of molten rose berry extract of oil, is obtained by following manufacture craft:
1) dry: fruit, rose fruit seed, fructus rosae leaf and the fructus rosae flower of fresh fructus rosae being taken to carry out at 70 DEG C or less
Vacuum drying, so that the moisture weight content of final raw material is 8%, and the weight percent of four kinds of raw materials is respectively 25%；
2) crush: by it is above-mentioned it is dried after raw mixture be ground into -40 mesh powder of 30 mesh, and crushing process
In, temperature is maintained at 38 DEG C；
3) it feeds intake: the fructus rosae material crushed is put into extractor, feeding intake and accounting for entire extractor volume ratio is 80%,
Ethyl acetate can also be added as auxiliary extraction agent simultaneously, and its volume accounting is 5%；
4) extract: carbon dioxide supercritical extraction, in the step, extraction temperature is 60 DEG C, pressure 35MPa, titanium dioxide
Carbon flow is 300kg/h, extraction time 3.5h；And when separating, the first knockout drum temperature is 50 DEG C, pressure 20MPa；Second
Knockout drum temperature is 45 DEG C, pressure 1-6MPa；Oily molten rose extract is obtained from first outlet.
Implement 2
A kind of molten rose berry extract of oil, is obtained by following manufacture craft:
1) dry: to take fruit, rose fruit seed, fructus rosae leaf and the fructus rosae flower of fresh fructus rosae to carry out at 60 DEG C true
Sky is dry so that the moisture weight content of final raw material is 7%, and the weight percent of four kinds of raw materials be respectively 30%,
30%, 20%, 20%；
2) crush: by it is above-mentioned it is dried after raw mixture be ground into -30 mesh powder of 20 mesh, and crushing process
In, temperature is maintained at 40 DEG C；
3) it feeds intake: the fructus rosae material crushed is put into extractor, feeding intake and accounting for entire extractor volume ratio is 75%,
Acetone can also be added as auxiliary extraction agent simultaneously, and its volume accounting is 6%；
4) extract: carbon dioxide supercritical extraction, in the step, extraction temperature is 57 DEG C, pressure 32MPa, titanium dioxide
Carbon flow is 270kg/h, extraction time 3h；And when separating, the first knockout drum temperature is 65 DEG C, pressure 17MPa；Second point
It is 47 DEG C from tank temperature degree, pressure 1-6MPa；Oily molten rose extract is obtained from first outlet.
Implement 3
A kind of molten rose berry extract of oil, is obtained by following manufacture craft:
1) dry: fruit, rose fruit seed, fructus rosae leaf and the fructus rosae flower of fresh fructus rosae being taken to carry out at 50 DEG C or less
Vacuum drying, so that the moisture weight content of final raw material is 6%, and the weight percent of four kinds of raw materials is respectively
35%, 35%, 15%, 15%；
2) crush: by it is above-mentioned it is dried after raw mixture be ground into -40 mesh powder of 30 mesh, and crushing process
In, temperature is maintained at 45 DEG C；
3) it feeds intake: the fructus rosae material crushed is put into extractor, feeding intake and accounting for entire extractor volume ratio is 70%,
Ethyl acetate and acetone can also be added as auxiliary extraction agent simultaneously, and its volume accounting is 7%；
4) extract: carbon dioxide supercritical extraction, in the step, extraction temperature is 55 DEG C, pressure 30MPa, titanium dioxide
Carbon flow is 250kg/h, extraction time 4h；And when separating, the first knockout drum temperature is 60 DEG C, pressure 15MPa；Second point
It is 43 DEG C from tank temperature degree, pressure 1-6MPa；Oily molten rose extract is obtained from first outlet.
Implement 4
A kind of molten rose berry extract of oil, is obtained by following manufacture craft:
1) dry: fruit, rose fruit seed, fructus rosae leaf and the fructus rosae flower of fresh fructus rosae being taken to carry out at 45 DEG C or less
Vacuum drying, so that the moisture weight content of final raw material is 6%, and the weight percent of four kinds of raw materials is respectively
10%, 80%, 5%, 5%；
2) crush: by it is above-mentioned it is dried after raw mixture be ground into -50 mesh powder of 40 mesh, and crushing process
In, temperature is maintained at 50 DEG C；
3) it feeds intake: the fructus rosae material crushed is put into extractor, feeding intake and accounting for entire extractor volume ratio is 65%,
Ethyl alcohol can also be added as auxiliary extraction agent simultaneously, and its volume accounting is 8%；
4) extract: carbon dioxide supercritical extraction, in the step, extraction temperature is 53 DEG C, pressure 28MPa, titanium dioxide
Carbon flow is 220kg/h, extraction time 4.5h；And when separating, the first knockout drum temperature is 55 DEG C, pressure 13MPa；Second
Knockout drum temperature is 40 DEG C, pressure 1-6MPa；Oily molten rose extract is obtained from first outlet.
Implement 5
A kind of molten rose berry extract of oil, is obtained by following manufacture craft:
1) dry: fruit, rose fruit seed, fructus rosae leaf and the fructus rosae flower of fresh fructus rosae being taken to carry out at -5 DEG C or less
Vacuum drying, so that the moisture weight content of final raw material is 5%, and the weight percent of four kinds of raw materials is respectively
85%, 5%, 5%, 5%；
2) crush: by it is above-mentioned it is dried after raw mixture be ground into -60 mesh powder of 50 mesh, and crushing process
In, temperature is maintained at -5 DEG C；
3) it feeds intake: the fructus rosae material crushed is put into extractor, feeding intake and accounting for entire extractor volume ratio is 60%,
Ethyl acetate, acetone and ethyl alcohol can also be added collectively as auxiliary extraction agent simultaneously, and its volume accounting is 10%；
4) extract: carbon dioxide supercritical extraction, in the step, extraction temperature is -10 DEG C, pressure 25MPa, titanium dioxide
Carbon flow is 200kg/h, extraction time 5h；And when separating, the first knockout drum temperature is -5 DEG C, pressure 10MPa；Second point
It is -5 DEG C from tank temperature degree, pressure 1-6MPa；Oily molten rose extract is obtained from first outlet.
Experimental example 1
Experimental subjects: 200 bright normal experimenters, male 100, are randomly divided into two groups by female 100.
Experimental method: weight accounting is mixed for the 2.5% molten rose berry extract of present invention oil and 97.5% White Mineral Oil
It closes, while 2.5% quinhydrones being mixed with 97.5% White Mineral Oil.Two kinds of mixtures will be formed by respectively to wherein one group reality
It tests object and carries out whitening test, use 60 days in total.
Experimental result: the mixture of oil-containing molten rose berry extract and quinhydrones, stimulation rate are respectively 0 people, 81 people, allergy rate
Respectively 0 people, 32 people, whitening effective average time are respectively 21 days, 28 days.
It can obtain from the experimental example, the molten great whitening effect of rose berry extract of oil of the invention, and safely and effectively, be not easy
It is quick.
Experimental example 2
Experimental subjects: fetal bovine serum culture medium culture B-16 cell is used, and is divided into same two groups, to subsequent experimental
It is used.
Test method: the molten rose berry extract of oil of the invention is taken into the appropriate culture medium for being added thereto one group
In, and using it as experimental group.Meanwhile another group without any processing and be blank group.By experimental group and blank group same
Under the conditions of cultivate 5 days after, two groups of cell is fixed with formaldehyde, then with the cma staining of ammonification.
Experimental result: can be obtained, the cell to live by observation, and due to the presence of the molten rose berry extract of oil, experimental group does not have
There is dyeing, and blank group is then obviously colored.Therefore it can illustrate that the molten rose berry extract of oil has white-skinned face function to cell.
The above description is only an embodiment of the present invention, is not intended to limit the scope of the invention, all to utilize this hair
Equivalent transformation made by bright description is applied directly or indirectly in other relevant technical fields, and is similarly included in
In scope of patent protection of the invention.
Claims (10)
1. a kind of molten rose berry extract of oil, which is characterized in that comprise the following steps:
S1 is dry, and fresh fructus rosae material vacuum is dry, makes water content 5-8%；
S2 is crushed, and dried fructus rosae is crushed to 20-60 mesh；
S3 feeds intake, and the fructus rosae material crushed is put into extractor；
S4 extraction, carries out carbon dioxide supercritical extraction, the isolated molten rose berry extract of oil.
2. the molten rose berry extract of oil as described in claim 1, it is characterised in that: in the drying steps, fructus rosae used
Fruit, rose fruit seed, fructus rosae leaf and fructus rosae flower including fructus rosae.
3. the molten rose berry extract of oil as claimed in claim 2, it is characterised in that: in the drying steps, the fructus rosae
Fruit, rose fruit seed, fructus rosae leaf and fructus rosae flower any one material weight content be less than or equal to 85%.
4. the molten rose berry extract of oil as described in claim 1, it is characterised in that: in the drying steps, drying temperature is low
In 70 DEG C, it is higher than -10 DEG C；In the pulverising step, crushes temperature and be lower than 70 DEG C, be higher than -10 DEG C.
5. the molten rose berry extract of oil as described in claim 1, it is characterised in that: further include to extraction in the material addition step
Take investment auxiliary extraction agent in tank.
6. the molten rose berry extract of oil as claimed in claim 5, it is characterised in that: in the material addition step, auxiliary extraction used
Taking agent is one of acetone, ethyl alcohol, ethyl acetate or a variety of.
7. the molten rose berry extract of oil as claimed in claim 5, it is characterised in that: in the material addition step, input powder
Broken good fructus rosae material relative extractive tank volume accounting is 60-80%, input auxiliary extraction agent relative extractive tank volume
Accounting is 5-10%.
8. the molten rose berry extract of oil as described in claim 1, it is characterised in that: in the extraction step, extraction temperature is small
In being equal to 60 DEG C, it is more than or equal to -10 DEG C, pressure 25-35MPa, extraction time 3-5h, carbon dioxide flow 200-
300kg/h。
9. the molten rose berry extract of oil as claimed in claim 8, it is characterised in that: in the extraction step, separation includes the
One knockout drum and the second knockout drum, the first knockout drum temperature are lower than 70 DEG C, are higher than -10 DEG C, pressure 7-20MPa, the second separation
Tank temperature degree is lower than 50 DEG C, is higher than -10 DEG C, pressure 1-6MPa.
10. such as the application of the molten rose berry extract of the described in any item oil of claim 1-9, it is characterised in that: by the molten rose of oil
Berry extract is applied to the whitening nutritional agents and/or antioxidant of cosmetics.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201811050009.8A CN109010133A (en) | 2018-09-10 | 2018-09-10 | A kind of molten rose berry extract of oil and application |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201811050009.8A CN109010133A (en) | 2018-09-10 | 2018-09-10 | A kind of molten rose berry extract of oil and application |
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| CN109010133A true CN109010133A (en) | 2018-12-18 |
Family
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| Application Number | Title | Priority Date | Filing Date |
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| CN201811050009.8A Pending CN109010133A (en) | 2018-09-10 | 2018-09-10 | A kind of molten rose berry extract of oil and application |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111903978A (en) * | 2020-07-02 | 2020-11-10 | 太阳树（厦门）生物工程有限公司 | Production method of rose hip extract containing VC |
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| CN102492541A (en) * | 2011-12-13 | 2012-06-13 | 九三粮油工业集团有限公司 | Method for extracting rose hip oil by supercritical carbon dioxide |
| CN107233233A (en) * | 2017-07-29 | 2017-10-10 | 深圳市仙迪化妆品有限公司 | A kind of cosmetic composition containing rose hip oil and preparation method thereof |
| CN108342251A (en) * | 2018-05-08 | 2018-07-31 | 深圳市仙迪化妆品有限公司 | One seed pod oil and the preparation method and application thereof |
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| CN101343594A (en) * | 2007-07-14 | 2009-01-14 | 周志忠 | Preparation method for rose hip or seed oil |
| CN102492541A (en) * | 2011-12-13 | 2012-06-13 | 九三粮油工业集团有限公司 | Method for extracting rose hip oil by supercritical carbon dioxide |
| CN107233233A (en) * | 2017-07-29 | 2017-10-10 | 深圳市仙迪化妆品有限公司 | A kind of cosmetic composition containing rose hip oil and preparation method thereof |
| CN108342251A (en) * | 2018-05-08 | 2018-07-31 | 深圳市仙迪化妆品有限公司 | One seed pod oil and the preparation method and application thereof |
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Address after: 518000, room five, floor 192, 501 Chongqing Road, Heping community, Fuyong street, Baoan District, Guangdong, Shenzhen Applicant after: Shenzhen Xiandi Cosmetics Co., Ltd Address before: 518000, room five, floor 192, 501 Chongqing Road, Heping community, Fuyong street, Baoan District, Guangdong, Shenzhen Applicant before: SHENZHEN SANDA COSMETICS Co.,Ltd. |
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