CN108998244A - Rose ethereal oil extraction element - Google Patents
Rose ethereal oil extraction element Download PDFInfo
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- CN108998244A CN108998244A CN201810898776.8A CN201810898776A CN108998244A CN 108998244 A CN108998244 A CN 108998244A CN 201810898776 A CN201810898776 A CN 201810898776A CN 108998244 A CN108998244 A CN 108998244A
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- pipe
- tank body
- alembic
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- oil
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- 239000000341 volatile oil Substances 0.000 title claims abstract description 42
- 238000000605 extraction Methods 0.000 title claims abstract description 36
- 241000220317 Rosa Species 0.000 title claims abstract description 31
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 122
- 239000003921 oil Substances 0.000 claims abstract description 78
- 238000004821 distillation Methods 0.000 claims abstract description 58
- 230000014759 maintenance of location Effects 0.000 claims abstract description 25
- 239000012153 distilled water Substances 0.000 claims abstract description 20
- 238000003860 storage Methods 0.000 claims abstract description 19
- 238000010438 heat treatment Methods 0.000 claims description 26
- 239000000463 material Substances 0.000 claims description 19
- 239000000945 filler Substances 0.000 claims description 18
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 17
- 229910052802 copper Inorganic materials 0.000 claims description 17
- 239000010949 copper Substances 0.000 claims description 17
- 238000011049 filling Methods 0.000 claims description 15
- 238000003780 insertion Methods 0.000 claims description 13
- 230000037431 insertion Effects 0.000 claims description 13
- 230000000694 effects Effects 0.000 claims description 12
- NJPPVKZQTLUDBO-UHFFFAOYSA-N novaluron Chemical compound C1=C(Cl)C(OC(F)(F)C(OC(F)(F)F)F)=CC=C1NC(=O)NC(=O)C1=C(F)C=CC=C1F NJPPVKZQTLUDBO-UHFFFAOYSA-N 0.000 claims description 12
- 238000005452 bending Methods 0.000 claims description 11
- 230000007246 mechanism Effects 0.000 claims description 10
- 239000011229 interlayer Substances 0.000 claims description 8
- 238000007789 sealing Methods 0.000 claims description 7
- 239000010425 asbestos Substances 0.000 claims description 5
- 229910052895 riebeckite Inorganic materials 0.000 claims description 5
- 238000009413 insulation Methods 0.000 claims description 4
- 230000008901 benefit Effects 0.000 abstract description 14
- 239000002699 waste material Substances 0.000 abstract description 7
- 239000000284 extract Substances 0.000 abstract description 2
- 235000019198 oils Nutrition 0.000 description 56
- 238000000034 method Methods 0.000 description 14
- 125000003118 aryl group Chemical group 0.000 description 9
- 230000006872 improvement Effects 0.000 description 9
- 239000010410 layer Substances 0.000 description 9
- 239000000126 substance Substances 0.000 description 9
- 238000009833 condensation Methods 0.000 description 8
- 230000005494 condensation Effects 0.000 description 8
- 238000000926 separation method Methods 0.000 description 7
- 238000005520 cutting process Methods 0.000 description 6
- 238000009826 distribution Methods 0.000 description 6
- 235000019476 oil-water mixture Nutrition 0.000 description 6
- 230000008569 process Effects 0.000 description 6
- 238000005194 fractionation Methods 0.000 description 5
- 238000010586 diagram Methods 0.000 description 4
- 230000006870 function Effects 0.000 description 4
- 230000001105 regulatory effect Effects 0.000 description 4
- 230000000630 rising effect Effects 0.000 description 4
- 241000196324 Embryophyta Species 0.000 description 3
- 230000009471 action Effects 0.000 description 3
- 230000002411 adverse Effects 0.000 description 3
- 230000004888 barrier function Effects 0.000 description 3
- 238000001704 evaporation Methods 0.000 description 3
- 238000011017 operating method Methods 0.000 description 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- 239000004519 grease Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 230000009711 regulatory function Effects 0.000 description 2
- 238000012546 transfer Methods 0.000 description 2
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 238000004508 fractional distillation Methods 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 238000001802 infusion Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000005192 partition Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 238000001256 steam distillation Methods 0.000 description 1
- 238000010025 steaming Methods 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
- B01D17/02—Separation of non-miscible liquids
- B01D17/0208—Separation of non-miscible liquids by sedimentation
- B01D17/0214—Separation of non-miscible liquids by sedimentation with removal of one of the phases
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The invention belongs to essential oil extracting device fields, it is especially rose ethereal oil extraction element, including alembic, the top of alembic is equipped with retention pipe, the bottom end for retaining pipe side is equipped with distillation column, the end of retention pipe, which is respectively embedded into, to be arranged in alembic and distillation column, and alembic and distillation column are connected to retention pipe, the top of distillation column is equipped with condenser pipe, the middle position of condenser pipe is equipped with condenser, the side of condenser pipe bottom end is equipped with cooler, cooler and distillation column are connected to condenser pipe, the adjacent side of cooler is equipped with level-one oil water separator, one end of level-one oil water separator is equipped with second level oil water separator, the bottom of second level oil water separator is equipped with filter pipe, the end of filter pipe is nested with collecting pipe, second level oil water separator and collecting pipe are connected to filter pipe, the side of collecting pipe is equipped with distilled water storage pool, with essence Oil extract purity quality is excellent, avoids water resource waste phenomenon, using it is simple and easy the advantages that.
Description
Technical field
The invention belongs to essential oil extracting device fields, are especially rose ethereal oil extraction element.
Background technique
Essential oil extraction refers to extracts essential oil from plant.Common essential oil extracting process has steam distillation, freezing pressure
Contracting method (squeezing method), chemical solvent extraction, grease partition method (rouge suction method), carbon dioxide extraction method and infusion method.Wherein steam
The method of evaporating is the extraction most common method of aromatic essential oil, and 95% aromatic essential oil is to be extracted by the way of distillation and obtained, therefore,
Obtain rose ethereal oil, it is necessary to have corresponding extraction element.
It is found by retrieval, a kind of essential oil extracting device of the disclosure of the invention of patent No. CN104271720A, structure packet
Include: container is configured to accommodate oil-containing material；Extraction of essential oil receiver is contained in the container；Condenser, have with
The outlet pairing of receiver fluid type and that the steam containing essential oil distributed by oil-containing material is positioned to receive relative to container；
And at least one microwave reflection structural body, it is associated at least one of the container, the receiver, the condenser.The dress
Sufficiently small overall dimensions can be had assembling the device in the inside of standard size kitchen microwave ovens by setting.
However, the analysis found that, existing rose ethereal oil extraction element has the following disadvantages；First, extraction of essential oil
Purity it is to be improved；Second, there are certain water resource waste phenomenons；Third, inconvenient for use.
Summary of the invention
Therefore, in order to solve above-mentioned deficiency, the present invention provides rose ethereal oil extraction element herein, has extraction of essential oil pure
Spend best in quality, avoid water resource waste phenomenon, using it is simple and easy the advantages that.
The invention is realized in this way construction rose ethereal oil extraction element, including alembic, the top of alembic are equipped with
The bottom end of retention pipe, retention pipe side is equipped with distillation column, and the end for retaining pipe is respectively embedded into setting and works as in alembic and distillation column
In, and alembic and distillation column are connected to retention pipe, the top of distillation column is equipped with condenser pipe, and the middle position of condenser pipe is equipped with
The side of condenser, condenser pipe bottom end is equipped with cooler, and cooler and distillation column are connected to condenser pipe, and the adjacent side of cooler is set
There is level-one oil water separator, one end of level-one oil water separator is equipped with second level oil water separator, the bottom of second level oil water separator
Equipped with filter pipe, the end of filter pipe is nested with collecting pipe, and second level oil water separator and collecting pipe are connected to filter pipe, collects
The side of pipe is equipped with distilled water storage pool, and distilled water storage pool is connected to collecting pipe.
Alembic includes outer tank body and inner tank body, and the bottom of outer tank body is equipped with pedestal, and the bottom of pedestal is equipped with support frame, branch
Support is bolted to connection with pedestal, and the bottom end inside outer tank body is equipped with heating cabinet, and the side of heating cabinet is equipped with heating cabinet
Door, heating door are flexibly connected with outer tank body, and the top of heating cabinet is arranged in inner tank body, and inner tank body insertion setting is worked as in outer tank body
In, and be fixedly connected with heating cabinet, and the middle position of outer tank body and inner tank body is filled with asbestos insulation filler, inner tank body bottom
The side at end is equipped with filling door, and the medial surface of filling door is equipped with sealing ring, and sealing ring is bonded fixation with filling door, and filling door and
Outer tank body is flexibly connected, and the side of inner tank body forms the interior tank skin interlayer of hollow out, and the top of inner tank body is equipped with pipe sleeve, and pipe sleeve runs through
Setting is connected in outer tank body, and with inner tank body, and the top of pipe sleeve is equipped with bending retention pipe, and bending retention pipe passes through with pipe sleeve
Bolt is fixedly connected.
Level-one oil water separator includes feeding dish, and the side of feeding dish bottom end is equipped with bottom inlet pipe, bottom inlet pipe
Opposite side is equipped with discharge tube, and the top of discharge tube is equipped with flowline, and the top of flowline, which is equipped with, separates mechanism, separates mechanism and charge
Ware is fixedly connected；Mechanism is separated to be made of handle, movable axis, rocker arm and choke plug, the side of movable axis is equipped with bracket, bracket with
Feeding dish is bolted to connection, and movable axis insertion setting in the bracket, and is flexibly connected with bracket, and rocker arm is arranged in activity
The top of axis, rocker arm are fixedly connected with movable axis, and one end of rocker arm is equipped with handle, and handle is embedding to be set on rocker arm, and with shake
Arm welding, the bottom of handle opposite side are equipped with choke plug, and choke plug insertion is arranged in flowline.
As an improvement of the above technical solution, the top inside inner tank body is equipped with relief valve, and relief valve insertion is arranged in pipe
In set, and it is bolted to connection with pipe sleeve.The release that distillation steam is carried out by the relief valve of setting, due to distilling
Alembic internal temperature is higher in journey, and pressure is larger, therefore can be set by the pressure release threshold value to relief valve to make alembic
Internal pressure reach to a certain degree when pressure release, thus containing rose aromatic substance distillation steam when pressure release into
Enter bending retention pipe to wait for being further processed.
As an improvement of the above technical solution, the side at the top of outer tank body is equipped with quck-opening valve, and quck-opening valve passes through with outer tank body
Bolt is fixedly connected.It to be used for alembic cutting and the flowing of distribution water source by the quck-opening valve of setting, also there is good flow
Regulatory function improves the degree easy to use of this kind of extraction element.
As an improvement of the above technical solution, the inside of interior tank skin interlayer be equipped with copper material filler, copper material filler with it is interior
Tank body fitting is fixed.By the copper material filler of setting, using the excellent heating conduction of copper material, when alembic preheating,
Heat can be quickly transmitted, preheating time is shortened, and when interval starts, is capable of providing good insulating power, makes
It is not easy to lose to obtain distillation operation process heat, effectively improves distilling effect.
As an improvement of the above technical solution, bottom inlet pipe, discharge tube and flowline are connected to feeding dish.By setting
Oil water mixture is added in feeding dish the bottom inlet pipe set, and since oily density is less than water, oil can swim in water
Upper layer, with when rising steadily higher than flowline position of water level in feeding dish, oil is received from oil pipe leakage discharge
Collection blocks flowline if oily layer pulls up handle, transfer choke plug than relatively thin, stops flowline, with
The water body for still having oil to mix can be discharged into second water-oil separating by discharge tube afterwards, discharge tube serves as second level level-one at this time
The inlet tube of oil water separator carries out water-oil separating again, realizes the second-order separation, improves separating effect.
As an improvement of the above technical solution, the inside of flowline is equipped with check valve, and check valve and discharge tube pass through bolt
It is fixedly connected.By the check valve of setting, oil water mixture adverse current is prevented, to level-one level-one oil water separator and second level level-one
Oil water separator plays unidirectional barrier action when linking.
As an improvement of the above technical solution, the middle position of rocker arm and choke plug is equipped with motion bar, and rocker arm and choked flow
Plug is bolted to connection with motion bar.By the rocker arm of setting, when handle position is raised, rocker arm is on movable axis in suitable
Hour hands rotation, the motion bar position of the rocker arm other end is downward at this time, pushes choke plug to block flowline, prevents water quality companion
It is discharged together with oil.
As an improvement of the above technical solution, quck-opening valve is installed, quck-opening valve and alembic pass through spiral shell at the top of alembic
Bolt is fixedly connected.It is mainly used for alembic cutting and the flowing of distribution water source by the quck-opening valve of setting, also there is good flow
Regulatory function improves the degree easy to use of this kind of extraction element.
As an improvement of the above technical solution, the inside of condenser is equipped with helix tube, and helix tube is arranged in the shape of a spiral, and spiral shell
Coil is connected to condenser pipe.By the condenser of setting, alembic is carried out and after distillation column is respectively completed distillation and fractionation
Condensation, helix tube therein extend steam passage path, can preferably form the condensation of steam.
As an improvement of the above technical solution, the side of distilled water storage pool is equipped with return pipe, and alembic and distillation column are equal
It is connected to return pipe.The water filtered out from second level oil water separator is stored by the distilled water storage pool of setting, is being carried out
When alembic distillation and distillation column fractionation operation, the water body that can be used in distilled water storage pool is carried out, so as to subtract
The input cost of few water resource, avoids water resource waste.
The present invention provides rose ethereal oil extraction element by improving herein, has extraction of essential oil purity quality excellent, keeps away
Exempt from water resource waste phenomenon, using it is simple and easy the advantages that, embody are as follows:
Advantage 1: being equipped with quck-opening valve at the top of alembic, quck-opening valve is bolted to connection with alembic.Pass through setting
Quck-opening valve is mainly used for alembic cutting and the flowing of distribution water source, also has good flow regulating function, improves this kind and mention
Take the degree easy to use of device.
Advantage 2: the inside of condenser is equipped with helix tube, and helix tube is arranged in the shape of a spiral, and helix tube is connected to condenser pipe.
By the condenser of setting, carries out alembic and distillation column is respectively completed the condensation after distillation and fractionation, spiral shell therein
Coil extends steam passage path, can preferably form the condensation of steam.
Advantage 3: the side of distilled water storage pool is equipped with return pipe, and alembic and distillation column are connected to return pipe.Pass through
The distilled water storage pool of setting stores the water filtered out from second level oil water separator, is carrying out alembic distillation and distillation column
When being fractionated operation, the water body that can be used in distilled water storage pool is carried out, so as to reduce the input cost of water resource,
Avoid water resource waste.
The present invention has distillation starting preheating quickly, interval starts insulating power by improving alembic provided herein
The advantages that good, distillation operation process heat is not easy to lose, effectively improves distilling effect, easy-to-use, embodies are as follows:
Advantage 1: the top inside inner tank body is equipped with relief valve, and relief valve insertion setting passes through spiral shell in pipe sleeve, and with pipe sleeve
Bolt is fixedly connected.By the relief valve of setting carry out distillation steam release, due in distillation process alembic internal temperature compared with
Height, pressure is larger, therefore can be set by the pressure release threshold value to relief valve reach alembic internal pressure to a certain degree
When pressure release, thus containing rose aromatic substance distillation steam enter when pressure release bending retention pipe wait for
It is further processed.
Advantage 2: the side at the top of outer tank body is equipped with quck-opening valve, and quck-opening valve is bolted to connection with outer tank body.Pass through
The quck-opening valve of setting will be used for alembic cutting and the flowing of distribution water source, also have good flow regulating function, improve this
The degree easy to use of kind extraction element.
Advantage 3: the inside of interior tank skin interlayer is equipped with copper material filler, and copper material filler is bonded fixation with inner tank body.Pass through
The copper material filler of setting can quickly transmit heat when alembic preheating using the excellent heating conduction of copper material,
Shorten preheating time, and when interval starts, good insulating power is capable of providing, so that distillation operation process heat
It is not easy to lose, effectively improve distilling effect.
The present invention is easy to operate with water-oil separating by improving level-one oil water separator provided herein, the second-order separation,
The advantages that good separating effect, embodies are as follows:
Advantage 1: bottom inlet pipe, discharge tube and flowline are connected to feeding dish.By the bottom inlet pipe of setting by grease
Mixture is added in feeding dish, and since oily density is less than water, oil can float layer on the water, with water level in feeding dish
When rising steadily higher than flowline position, oil from oil pipe leakage discharge be collected, if oily layer is than relatively thin
, then handle is pulled up, choke plug is transferred, blocks flowline, stops flowline, then will can still have oil by discharge tube
The water body of matter mixing is discharged into second water-oil separating, and discharge tube serves as the inlet tube of second level level-one oil water separator at this time, then
It is primary to carry out water-oil separating, it realizes the second-order separation, improves separating effect.
Advantage 2: the inside of flowline is equipped with check valve, and check valve is bolted to connection with discharge tube.Pass through setting
Check valve, prevent oil water mixture adverse current, to level-one level-one oil water separator and second level level-one oil water separator linking
When play unidirectional barrier action.
Advantage 3: the middle position of rocker arm and choke plug is equipped with motion bar, and rocker arm and choke plug pass through spiral shell with motion bar
Bolt is fixedly connected.By the rocker arm of setting, when handle position is raised, rocker arm is in rotate clockwise on movable axis, at this time rocker arm
The motion bar position of the other end is downward, and choke plug is pushed to block flowline, and water quality is prevented to be discharged together with oil.
Detailed description of the invention
Fig. 1 is rose ethereal oil extraction element structural schematic diagram of the present invention；
Fig. 2 is the flow diagram of rose ethereal oil extraction element of the present invention；
Fig. 3 is alembic structural schematic diagram of the present invention；
Fig. 4 is the enlarged drawing of alembic of the present invention；
Fig. 5 is level-one oil water separator structural schematic diagram of the present invention；
Fig. 6 is the partial structurtes enlarged drawing of level-one oil water separator of the present invention；
Serial number as shown in the figure: alembic 1, quck-opening valve 2, retention pipe 3, distillation column 4, condenser pipe 5, condenser 6, helix tube 7, level-one
Oil water separator 8, second level oil water separator 9, filter pipe 10, return pipe 11, collecting pipe 12, distilled water storage pool 13, cooler
14, outer tank body 101, inner tank body 102, heating cabinet 103, pedestal 104, support frame 105, heating door 106, filling door 107, open fastly
Valve 108, relief valve 109, pipe sleeve 1010, bending retention pipe 1011, interior tank skin interlayer 1012, copper material filler 1013, asbestos every
Hot filler 1014, bottom inlet pipe 801, feeding dish 802, guard tube 803, check valve 804, separates mechanism at sealing ring 1015
805, flowline 806, bracket 807, handle 808, motion bar 809, rocker arm 8010, movable axis 8011 and choke plug 8012.
Specific embodiment
Below in conjunction with attached drawing, the present invention is described in detail, and technical solution in the embodiment of the present invention carries out clear
Chu is fully described by.
The present invention provides rose ethereal oil extraction element by improving herein, as Figure 1-Figure 2, including alembic 1, it steams
The top for evaporating tank 1 is equipped with retention pipe 3, and the bottom end of retention 3 side of pipe is equipped with distillation column 4, and the end of retention pipe 3 is respectively embedded into setting
In alembic 1 and distillation column 4, and alembic 1 and distillation column 4 are connected to retention pipe 3, and the top of distillation column 4 is equipped with cold
Solidifying pipe 5, the middle position of condenser pipe 5 are equipped with condenser 6, and the side of 5 bottom end of condenser pipe is equipped with cooler 14, cooler 14 and steaming
Fractional distillation column 4 is connected to condenser pipe 5, and the adjacent side of cooler 14 is equipped with level-one oil water separator 8, one end of level-one oil water separator 8
Equipped with second level oil water separator 9, the bottom of second level oil water separator 9 is equipped with filter pipe 10, and the end of filter pipe 10 is nested with receipts
Collector 12, second level oil water separator 9 and collecting pipe 12 are connected to filter pipe 10, and the side of collecting pipe 12 is stored equipped with distilled water
Pond 13, distilled water storage pool 13 are connected to collecting pipe 12.
The top of alembic 1 is equipped with quck-opening valve 2, and quck-opening valve 2 is bolted to connection with alembic 1.Pass through setting
Quck-opening valve 2 be mainly used for alembic 1 cutting and distribution water source flowing, also have good flow regulating function, improve this
The degree easy to use of kind extraction element.
The inside of condenser 6 is equipped with helix tube 7, and helix tube 7 is arranged in the shape of a spiral, and helix tube 7 is connected to condenser pipe 5.
By the condenser 6 of setting, carries out alembic 1 and distillation column 4 is respectively completed the condensation after distillation and fractionation, it is therein
Helix tube 7 extends steam passage path, can preferably form the condensation of steam.
The side of distilled water storage pool 13 is equipped with return pipe 11, and alembic 1 and distillation column 4 are connected to return pipe 11.It is logical
Cross setting distilled water storage pool 13 water filtered out from second level oil water separator 9 is stored, carry out alembic 1 distillation and
When distillation column 4 is fractionated operation, the water body that can be used in distilled water storage pool 13 is carried out, so as to reduce water resource
Input cost avoids water resource waste.
The operating method of rose ethereal oil extraction element: firstly, the part that rose contains aromatic substance is laid on distillation
The bottom of tank 1, and water is added and carries out distillation operation, it, can be by the fragrance of plant memory when hot steam is filled in alembic 1
Derived essential oil is evaporated with water vapour, and is fractionated as water vapour enters distillation column 4 by the retention pipe 3 of top, is mentioned
High DNA purity, then water vapour containing volatile oil enters in the condenser 6 in 5 middle position of condenser pipe, has inside condenser 6
There is the helix tube 7 being arranged in the shape of a spiral, helix tube 7 extends steam passage path, can preferably form the condensation of steam, coagulates
Water body after knot, which enters in cooler 14, to be cooled down, and volatile oil is then layered with water body, swims in since density is less than water
The water surface finally passes through the separation and Extraction rose ethereal oil of level-one oil water separator 8 and second level oil water separator 9, and water body is then from filter
The discharge of water pipe 10 is stored in distilled water storage pool 13, when carrying out the distillation of alembic 1 and distillation column 4 is fractionated operation,
The water body that can be used in distilled water storage pool 13 carries out, and so as to reduce the input cost of water resource, avoids water resource unrestrained
Take.
As Figure 3-Figure 4, alembic includes outer tank body 101 and inner tank body 102, and the bottom of outer tank body 101 is equipped with pedestal
104, the bottom of pedestal 104 is equipped with support frame 105, and support frame 105 is bolted to connection with pedestal 104, in outer tank body 101
The bottom end in portion is equipped with heating cabinet 103, and the side of heating cabinet 103 is equipped with heating door 106, and heating door 106 and outer tank body 101 are living
The top of heating cabinet 103 is arranged in dynamic connection, inner tank body 102, and the insertion of inner tank body 102 is arranged in outer tank body 101, and with add
Hot storehouse 103 is fixedly connected, and the middle position of outer tank body 101 and inner tank body 102 is filled with asbestos insulation filler 1014, inner canister
The side of 102 bottom end of body is equipped with filling door 107, and the medial surface of filling door 107 is equipped with sealing ring 1015, sealing ring 1015 and filling
107 fitting of door is fixed, and filling door 107 is flexibly connected with outer tank body 101, and the side of inner tank body 102 forms the interior tank skin of hollow out
Interlayer 1012, the top of inner tank body 102 are equipped with pipe sleeve 1010, and pipe sleeve 1010, which runs through, to be arranged in outer tank body 101, and and inner canister
Body 102 is connected to, and the top of pipe sleeve 1010 is equipped with bending and retains pipe 1011, and it is solid by bolt that bending retains pipe 1011 and pipe sleeve 1010
Fixed connection.
In the present invention, the top inside inner tank body 102 is equipped with relief valve 109, and the insertion of relief valve 109 is arranged in pipe sleeve 1010
In the middle, and with pipe sleeve 1010 it is bolted to connection.The release that distillation steam is carried out by the relief valve 109 of setting, due to
Alembic internal temperature is higher in distillation process, and pressure is larger, thus can by the pressure release threshold value to relief valve 109 set come
Pressure release when reaching alembic internal pressure to a certain degree, thus containing rose aromatic substance distillation steam in pressure release
When enter bending retention pipe 1011 and wait for being further processed, the side at the top of outer tank body 101 is equipped with quck-opening valve 108,
Quck-opening valve 108 is bolted to connection with outer tank body 101.Alembic cutting is used for by the quck-opening valve 108 of setting and is divided
Water distribution source flow also has good flow regulating function, improves the degree easy to use of this kind of extraction element, interior tank skin folder
The inside of layer 1012 is equipped with copper material filler 1013, and copper material filler 1013 is bonded fixation with inner tank body 102.Pass through the copper of setting
Material filler 1013 can quickly transmit heat when alembic preheating using the excellent heating conduction of copper material, shorten
Preheating time, and when interval starts, it is capable of providing good insulating power, so that distillation operation process heat is not easy
It scatters and disappears, effectively improves distilling effect.
The operating method of alembic 1: firstly, being laid on the part that rose contains aromatic substance from filling door 107
Water pipe is connect, by quck-opening valve 108 according to work by the bottom of inner tank body 102 after closing the sealing of filling door 107 with quck-opening valve 108
Skill requires control to add water in the middle to inner tank body 102, can be by heating equipment or other heating equipments to inner canister in heating cabinet 103
Body 102 is heated, can be by the volatile oil ingredient of plant memory with dampening when hot steam is filled in inner tank body 102
Evaporation of vapours, as 102 internal temperature of inner tank body constantly rises, internal pressure is also risen with it, therefore can be by pressure release
The pressure release threshold value setting of valve 109 is come pressure release when reaching alembic internal pressure to a certain degree, to contain rose
Aromatic substance distillation steam enters bending retention pipe 1011 when pressure release and waits for being further processed, especially interior tank skin
Copper material filler 1013 inside interlayer 1012, can be fast when alembic preheating using the excellent heating conduction of copper material
Speed transmitting heat, shortens preheating time, and when interval starts, asbestos insulation filler 1014 can be cooperated to provide good
Good insulating power effectively improves distilling effect so that distillation operation process heat is not easy to lose.
As shown in Fig. 5-Fig. 6, level-one oil water separator 8 includes feeding dish 802, and the side of 802 bottom end of feeding dish is equipped with bottom
Portion's inlet tube 801, the opposite side of bottom inlet pipe 801 are equipped with discharge tube 3, and the top of discharge tube 3 is equipped with flowline 806, flowline
806 top is equipped with and separates mechanism 805, separates mechanism 805 and is fixedly connected with feeding dish 802；
It separates mechanism 805 to be made of handle 808, movable axis 8011, rocker arm 8010 and choke plug 8012, the side of movable axis 8011
Equipped with bracket 807, bracket 807 is bolted to connection with feeding dish 802, and the insertion of movable axis 8011 is arranged in bracket 807,
And be flexibly connected with bracket 807, the top of movable axis 8011, rocker arm 8010 and the fixed company of movable axis 8011 is arranged in rocker arm 8010
It connecing, one end of rocker arm 8010 is equipped with handle 808, and handle 808 is embedding to be set on rocker arm 8010, and welds with rocker arm 8010,
The bottom of 808 opposite side of handle is equipped with choke plug 8012, and the insertion of choke plug 8012 is arranged in flowline 806.
In the present invention, bottom inlet pipe 801, discharge tube 3 and flowline 806 are connected to feeding dish 802.Pass through setting
Oil water mixture is added in feeding dish 802 bottom inlet pipe 801, and since oily density is less than water, oil can be swum in
Layer waterborne, with when rising steadily higher than 806 position of flowline of water level in feeding dish 802, oil is revealed from oil pipe 6 and is arranged
It is collected out, if oily layer pulls up handle 808 than relatively thin, transfers choke plug 8012, block flowline
806, stop flowline 806, the water body for still having oil to mix can be then discharged into second water-oil separating by discharge tube 3,
Discharge tube 3 serves as the inlet tube 1 of second level level-one oil water separator at this time, carries out water-oil separating again, realizes the second-order separation, mentions
The inside of high separating effect, flowline 806 is equipped with check valve 804, and check valve 804 is bolted to connection with discharge tube 3.It is logical
The check valve 804 for crossing setting prevents oil water mixture adverse current, to level-one level-one oil water separator and second level level-one water-oil separating
Device plays unidirectional barrier action when linking, and the middle position of rocker arm 8010 and choke plug 8012 is equipped with motion bar 809, and
Rocker arm 8010 and choke plug 8012 are bolted to connection with motion bar 809.By the rocker arm 8010 of setting, work as handle
808 positions are raised, and rocker arm 8010 is in rotate clockwise on movable axis 8011, at this time the motion bar 809 of 8010 other end of rocker arm
Position is downward, and choke plug 8012 is pushed to block flowline 806, and water quality is prevented to be discharged together with oil.
The operating method of level-one oil water separator 8: when rose position containing aromatic substance by distillation, fractionation, condensation and
After cooling, the mixture of volatile oil oil and water is obtained, level-one oil water separator is just needed to carry out against two kinds of substances at this time
Oil water mixture is added in feeding dish 802 by the bottom inlet pipe 801 of setting for separation, since oily density is less than water, because
This oil can float layer on the water, with when rising steadily higher than 806 position of flowline of water level in feeding dish 802, oil
Matter is collected from the leakage discharge of oil pipe 6, if oily layer pulls up handle 808, when handle 808 than relatively thin
Set and raise, rocker arm 8010 on movable axis 8011 in rotating clockwise, at this time 809 position of motion bar of 8010 other end of rocker arm to
Under, it pushes choke plug 8012 to block flowline 806, water quality is prevented to be discharged together with oil, stop flowline 806,
The water body for still having oil to mix can be then discharged into second water-oil separating by discharge tube 3, discharge tube 3 serves as second level at this time
The inlet tube 1 of level-one oil water separator carries out water-oil separating again, realizes the second-order separation, improves separating effect.
Claims (10)
1. rose ethereal oil extraction element, including alembic (1), it is characterised in that: the top of the alembic (1) is equipped with retention
It manages (3), the bottom end of the retention pipe (3) side is equipped with distillation column (4), and the end of the retention pipe (3) is respectively embedded into setting and exists
In alembic (1) and distillation column (4), and the alembic (1) and distillation column (4) are connected to retention pipe (3), described
The top of distillation column (4) is equipped with condenser pipe (5), and the middle position of the condenser pipe (5) is equipped with condenser (6), the condenser pipe
(5) side of bottom end is equipped with cooler (14), and the cooler (14) and the distillation column (4) connect with the condenser pipe (5)
Logical, the adjacent side of the cooler (14) is equipped with level-one oil water separator (8), and one end of the level-one oil water separator (8) is equipped with
The bottom of second level oil water separator (9), the second level oil water separator (9) is equipped with filter pipe (10), the filter pipe (10)
End is nested with collecting pipe (12), and the second level oil water separator (9) and collecting pipe (12) are connected to the filter pipe (10),
The side of the collecting pipe (12) is equipped with distilled water storage pool (13), the distilled water storage pool (13) and the collecting pipe (12)
Connection；
Alembic (1) includes outer tank body (101) and inner tank body (102)；The bottom of the outer tank body (101) is equipped with pedestal (104),
The bottom of the pedestal (104) is equipped with support frame (105), and support frame as described above (105) is bolted with the pedestal (104)
Connection, the internal bottom end of the outer tank body (101) are equipped with heating cabinet (103), and the side of the heating cabinet (103) is equipped with heating cabinet
Door (106), the heating door (106) are flexibly connected with the outer tank body (101), and the inner tank body (102) is arranged described
The top of heating cabinet (103), the inner tank body (102) insertion are arranged in outer tank body (101), and with the heating cabinet
(103) it is fixedly connected, and the middle position of the outer tank body (101) and inner tank body (102) is filled with asbestos insulation filler
(1014), the side of inner tank body (102) bottom end is equipped with filling door (107), and the medial surface of the filling door (107) is equipped with close
Seal ring (1015), the sealing ring (1015) are bonded fixation with the filling door (107), and the filling door (107) with it is described
Outer tank body (101) is flexibly connected, and the side of the inner tank body (102) forms the interior tank skin interlayer (1012) of hollow out, the inner canister
The top of body (102) be equipped with pipe sleeve (1010), the pipe sleeve (1010) through be arranged in outer tank body (101), and with it is described
Inner tank body (102) connection, the top of the pipe sleeve (1010) are equipped with bending retention pipe (1011), the bending retention pipe (1011)
It is bolted to connection with the pipe sleeve (1010)；
Level-one oil water separator (8) includes feeding dish (802), and the side of feeding dish (802) bottom end is equipped with bottom inlet pipe
(801), the opposite side of the bottom inlet pipe (801) is equipped with discharge tube (803), and the top of the discharge tube (803) is equipped with fuel-displaced
It manages (806), the top of the flowline (806), which is equipped with, to be separated mechanism (805), described to separate mechanism (805) and the feeding dish
(802) it is fixedly connected；The mechanism (805) that separates is by handle (808), movable axis (8011), rocker arm (8010) and choke plug
(8012) it constitutes, the side of the movable axis (8011) is equipped with bracket (807), the bracket (807) and the feeding dish (802)
Be bolted to connection, the movable axis (8011) insertion is arranged in the bracket (807), and with the bracket (807)
It is flexibly connected, rocker arm (8010) setting is in the top of the movable axis (8011), the rocker arm (8010) and the activity
Axis (8011) is fixedly connected, and one end of the rocker arm (8010) is equipped with handle (808), and the handle (808) is embedding to be set on institute
It states on rocker arm (8010), and is welded with the rocker arm (8010), the bottom of handle (808) opposite side is equipped with choke plug
(8012), choke plug (8012) insertion is arranged in flowline (806).
2. rose ethereal oil extraction element according to claim 1, it is characterised in that: inner tank body (102) inside
Top is equipped with relief valve (109), and the relief valve (109) insertion is arranged in pipe sleeve (1010), and with the pipe sleeve
(1010) it is bolted to connection.
3. rose ethereal oil extraction element according to claim 1, it is characterised in that: at the top of the outer tank body (101)
Side is equipped with quck-opening valve (108), and the quck-opening valve (108) is bolted to connection with the outer tank body (101).
4. rose ethereal oil extraction element according to claim 1, it is characterised in that: the interior tank skin interlayer (1012)
Inside is equipped with copper material filler (1013), and the copper material filler (1013) is bonded fixation with the inner tank body (102).
5. rose ethereal oil extraction element according to claim 1, it is characterised in that: the bottom inlet pipe (801) is put
Water pipe (803) and flowline (806) are connected to the feeding dish (802).
6. rose ethereal oil extraction element according to claim 1, it is characterised in that: the inside of the flowline (806)
Equipped with check valve (804), the check valve (804) is bolted to connection with the discharge tube (803).
7. rose ethereal oil extraction element according to claim 1, it is characterised in that: the rocker arm (8010) and choke plug
(8012) middle position be equipped with motion bar (809), and the rocker arm (8010) and choke plug (8012) with the motion bar
(809) it is bolted to connection.
8. rose ethereal oil extraction element according to claim 1, it is characterised in that: pacify at the top of the alembic (1)
Equipped with quck-opening valve (2), the quck-opening valve (2) is bolted to connection with the alembic (1).
9. rose ethereal oil extraction element according to claim 1, it is characterised in that: the inside of the condenser (6) is set
Have helix tube (7), the helix tube (7) is arranged in the shape of a spiral, and the helix tube (7) is connected to the condenser pipe (5).
10. rose ethereal oil extraction element according to claim 1, it is characterised in that: the distilled water storage pool (13)
Side be equipped with return pipe (11), the alembic (1) and distillation column (4) are connected to the return pipe (11).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810898776.8A CN108998244A (en) | 2018-08-08 | 2018-08-08 | Rose ethereal oil extraction element |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810898776.8A CN108998244A (en) | 2018-08-08 | 2018-08-08 | Rose ethereal oil extraction element |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108998244A true CN108998244A (en) | 2018-12-14 |
Family
ID=64596280
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810898776.8A Pending CN108998244A (en) | 2018-08-08 | 2018-08-08 | Rose ethereal oil extraction element |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108998244A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110467969A (en) * | 2019-07-23 | 2019-11-19 | 广西壮族自治区林业科学研究院 | A kind of process equipment and processing method of jasmine flower concrete production jasmine essential oil |
| CN110835583A (en) * | 2019-11-25 | 2020-02-25 | 温州宏量机械科技有限公司 | Rose essence purification tube body for cosmetics |
| CN112481038A (en) * | 2020-11-30 | 2021-03-12 | 贵州荔波亿隆之家农业科技有限公司 | Shaddock ped essential oil extraction element |
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Application publication date: 20181214 |