CN112481038A - Shaddock ped essential oil extraction element - Google Patents
Shaddock ped essential oil extraction element Download PDFInfo
- Publication number
- CN112481038A CN112481038A CN202011375093.8A CN202011375093A CN112481038A CN 112481038 A CN112481038 A CN 112481038A CN 202011375093 A CN202011375093 A CN 202011375093A CN 112481038 A CN112481038 A CN 112481038A
- Authority
- CN
- China
- Prior art keywords
- separation
- pipe
- pipeline
- tank
- separation tank
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000341 volatile oil Substances 0.000 title claims abstract description 37
- 238000000605 extraction Methods 0.000 title claims abstract description 32
- 244000276331 Citrus maxima Species 0.000 title claims description 23
- 235000001759 Citrus maxima Nutrition 0.000 title claims description 20
- 238000000926 separation method Methods 0.000 claims abstract description 134
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 68
- 238000004821 distillation Methods 0.000 claims abstract description 39
- 238000011084 recovery Methods 0.000 claims description 7
- 238000002156 mixing Methods 0.000 claims description 2
- 238000009833 condensation Methods 0.000 abstract description 18
- 230000005494 condensation Effects 0.000 abstract description 18
- 230000000694 effects Effects 0.000 abstract description 8
- 240000000560 Citrus x paradisi Species 0.000 abstract 2
- 238000000034 method Methods 0.000 description 7
- 239000003921 oil Substances 0.000 description 5
- 239000002699 waste material Substances 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 4
- 238000010992 reflux Methods 0.000 description 4
- 238000011049 filling Methods 0.000 description 3
- 238000000638 solvent extraction Methods 0.000 description 3
- 238000009825 accumulation Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000007599 discharging Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000001256 steam distillation Methods 0.000 description 2
- 206010000060 Abdominal distension Diseases 0.000 description 1
- 206010011224 Cough Diseases 0.000 description 1
- 206010062717 Increased upper airway secretion Diseases 0.000 description 1
- 241001093501 Rutaceae Species 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 208000006673 asthma Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000004134 energy conservation Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 235000012907 honey Nutrition 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 208000026435 phlegm Diseases 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B9/00—Cleaning hollow articles by methods or apparatus specially adapted thereto
- B08B9/08—Cleaning containers, e.g. tanks
- B08B9/0804—Cleaning containers having tubular shape, e.g. casks, barrels, drums
- B08B9/0808—Cleaning containers having tubular shape, e.g. casks, barrels, drums by methods involving the use of tools, e.g. by brushes, scrapers
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Mechanical Engineering (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The invention discloses a pomelo peel essential oil extraction device, which comprises a heater and a distillation tank, wherein the upper end of the distillation tank is connected with the upper end of a condensation pipe through a connecting pipe, the lower end of the condensation pipe is connected with a separation tank, the separation tank is arranged into an upper separation tank and a lower separation tank, the lower end of the upper separation tank is connected with a first return pipeline and a first separation pipeline, the lower end of the lower separation tank is connected with a second return pipeline and a second separation pipeline, the upper separation tank and the lower separation tank are connected through the first separation pipeline, valves are arranged at corresponding positions of partial pipelines, the pomelo peel essential oil extraction device can carry out separation and extraction by arranging the upper separation tank and the lower separation tank, has better extraction effect, can recover a water layer part after primary separation by matching with the return pipeline and a diversion pipeline, can recycle water in the condensation pipe as separation water, has compact structure, small occupied area and high resource utilization rate, the practicability is strong.
Description
Technical Field
The invention relates to the technical field of extraction and separation of essential oil, in particular to a shaddock peel essential oil extraction device.
Background
The pericarpium Citri Grandis is pericarp of Citrus Grandis of Rutaceae, and is bitter and pungent. Warm in nature, has effects of relieving epigastric distention, regulating qi-flowing, resolving food stagnation, eliminating phlegm, relieving cough and asthma, etc. The pericarpium Citri Grandis contains volatile oil, and can be used as raw material for extracting essence and spice. The traditional methods for extracting the shaddock peel essential oil comprise a steam distillation method and a solvent extraction method. The temperature in the extraction process of the steam distillation method is generally controlled to be about 100 ℃, so that important components such as aldehydes and esters in the essential oil are partially lost, and the essential oil quality is reduced due to easy polymerization and deterioration. The solvent extraction method has the disadvantages of bad fragrance, dark color, and poor transparency, and the essential oil has pungent odor due to incomplete removal of extraction solvent.
Chinese patent (publication No. CN 210314167U, bulletin date: 2020.04.14) discloses a green glaze essential oil extraction device, the extraction device adopts an organic solvent extraction method to extract green glaze essential oil, the device realizes an extraction function by arranging a screw press, a standing layering box, an extraction stirring layering box and a distillation machine, and the device has good effects of rapid processing and production due to the assembly line type structural design.
Chinese patent (publication No. CN 203999557U, bulletin day 2014.12.10) discloses a honey pomelo peel essential oil extraction and separation device, which distills and extracts the pomelo peel essential oil by arranging an inner cavity, an external heating cavity, a condensing tank and the like, and has the advantages of simple structure, convenience in acquisition and the like.
Disclosure of Invention
The invention aims to provide a shaddock ped essential oil extraction device to solve the problems in the background technology.
The invention adopts a distillation method to realize the extraction function of essential oil, designs a circulating reflux mechanism to enhance the purification effect, and reasonably uses each production part in a matching way to achieve the effect of energy conservation and utilization.
In order to achieve the purpose, the invention provides the following technical scheme:
a shaddock ped essential oil extraction device comprises a bottom plate, wherein a placing table is arranged on the bottom plate, a heater is arranged on the placing table, a distillation tank is arranged on the heater, a feed inlet and a discharge outlet are respectively formed in the upper end and the lower end of the distillation tank, an unloading centrifugal machine is arranged under the discharge outlet, the upper end of the distillation tank is connected with a condensation pipe through a connecting pipe, the lower end of the condensation pipe is connected with separation tanks, the number of the separation tanks is two, the upper end and the lower end of the separation tanks are the same, the separation tank bodies are fixed on a vertical frame arranged on the bottom plate through trays, the upper separation tank and the lower separation tank are connected through a first separation pipeline, the lower end of the separation tank positioned below is connected with a collection box arranged on the bottom plate through a second separation pipeline, a spiral pipeline is arranged in the condensation pipe in a surrounding manner, and the, the upper end port of the water inlet pipe is connected with the upper end of the water guide pipe, the lower end of the water guide pipe extends into the water supply tank and is connected with a water pump arranged in the water supply tank, a main leading-in pipe and a leading-out pipe are respectively arranged above and below the axis position of the center position in the separation tank, a secondary leading-in pipe is arranged on one side of the main leading-in pipe, a separation pipe is arranged inside the separation tank and on the other side of the main leading-in pipe, an upper observation window and a lower observation window are arranged on the tank wall of the separation tank, the lower end of the upper separation tank is connected with the right end of a first backflow pipeline, the left end of the first backflow pipeline is connected with the tank wall of the distillation tank, a first backflow valve is arranged at the left part of the first backflow pipeline, the middle part of the first backflow pipeline is connected with the upper end of a through-flow pipeline, the lower end of the through-, the lower extreme of below knockout drum links to each other with the right-hand member of second return line, the left end of second return line links to each other with the lower part of through-flow pipeline, and the middle part of second return line is equipped with second return valve, and the upper end of below knockout drum links to each other with the reposition of redundant personnel pipeline right-hand member, the left end of reposition of redundant personnel pipeline links to each other with the right part of first return line, the reposition of redundant personnel pipeline middle part is equipped with reposition of redundant personnel valve.
As a further scheme of the invention: the right-hand member of first return line, the right-hand member of second return line link to each other with the delivery tube of top knockout drum and below knockout drum respectively, the upper and lower end of first separation pipeline links to each other with the main inlet tube upper end of the separator tube lower extreme of top knockout drum and below knockout drum respectively, because first separation pipeline does not match with leading-in pipe pipeline diameter size, is equipped with the allotment and connects and is connected in first separation pipeline and main inlet tube junction, the right-hand member of reposition of redundant personnel pipeline links to each other with the inferior leading-in pipe upper end of below knockout drum, the upper end of second separation pipeline links to each other with the separator tube lower extreme of below knockout drum, the diameter size of first return line, through-flow pipeline is unanimous with the pipeline diameter size of delivery tube, the diameter size of first separation pipeline and second separation pipeline is unanimous with separator tube diameter size.
As a still further scheme of the invention: the lower part of the main introducing pipe extends into the separation tank, the length of the extending part is one half of the height of the separation tank, the upper part of the separation pipe extends into the separation tank, and the length of the extending part is three quarters of the height of the separation tank.
As a still further scheme of the invention: the joint of the through-flow pipeline and the first return pipeline is arranged on the left side of the joint of the diversion pipeline and the first return pipeline.
As a still further scheme of the invention: the two observation windows are respectively arranged on the tank wall at the position of one fourth and three fourths of the height of the separation tank, the upper part of the guide pipe does not extend into the separation tank, and the diameters of the main guide pipe, the separation pipe and the secondary guide pipe are sequentially reduced.
As a still further scheme of the invention: the heater is the inside hollow structure of hemisphere, the internal diameter of heater equals with the retort external diameter, the inside lower surface wall welding of retort has the heat conduction frame.
As a still further scheme of the invention: the condenser pipe is internally and fixedly connected with a flow guide rod through a thin rod, two ends of the flow guide rod are semicircular, the flow guide rod is parallel to the condenser pipe, and the flow guide rod is positioned on a central line inside the condenser pipe.
Compared with the prior art, the invention has the beneficial effects that:
1. this shaddock ped essential oil extraction element carries out the distillation through setting up heater and retort cooperation, has avoided heating inhomogeneous, the problem that the temperature is difficult to the regulation and control when adopting single retort to distill.
2. All parts for distillation, condensation, separation and collection are arranged above the bottom plate, so that the structure is compact, the occupied area is small, and the space utilization rate is high.
3. Two times of separation processing is carried out to essential oil through setting up two upper and lower knockout drums, has reduced and has adopted single separator to separate produced separation insufficient, the separation effect is not good scheduling problem.
4. The water in the condenser pipe can flow into the knockout drum and supply the separation to use as water layer part after the condensation work is accomplished, has effectively practiced thrift the water resource, avoids the water waste.
5. The water layer part separated and treated by the upper separating tank flows back into the distillation tank through the first backflow pipeline, so that the part of the unseparated essential oil contained in the water layer part can be recycled, and resource waste is avoided.
6. Water injected by the water conduit finally reaches the water recovery device through the condensation pipe and the separation tank to be recovered, the separation tank and the inner walls of the pipelines can be cleaned while the water is recovered, the pipelines are prevented from being blocked by scale accumulation, and the self-cleaning degree is high.
Drawings
Fig. 1 is a schematic diagram of the whole structure of a shaddock ped essential oil extraction device.
Fig. 2 is a schematic view of the internal structure of a condenser tube of the shaddock ped essential oil extraction device.
Fig. 3 is a schematic diagram of the internal structure of a separation tank of the shaddock ped essential oil extraction device.
FIG. 4 is a schematic view of the internal structure of the heater and distillation tank of the device for extracting essential oil from pericarpium Citri Grandis.
Wherein: a bottom plate-1, a placing table-2, a heater-3, a distillation tank-4, a charging port-5, a control panel-6, a discharging port-7, a discharging centrifuge-8, a vertical frame-9, a water supply tank-10, a collecting tank-11, a connecting pipe-12, a condensing pipe-13, a water guide pipe-14, a main guide pipe-15, a separation tank-16, an observation window-17, a tray-18, a water recovery device-19, a guide rod-20, a water inlet pipe-21, a spiral pipeline-22, a water outlet pipe-23, a secondary guide pipe-24, a separation pipe-25, a separation cavity-26, a guide pipe-27, a first return pipeline-28, a second return pipeline-29, a through-flow pipeline-30 and a first separation pipeline-31, a shunt pipeline-32, a second separation pipeline-33, a first return valve-34, a stop valve-35, a second return valve-36, a shunt valve-37 and a heat conducting frame-38.
Detailed Description
It should be noted that the embodiments and features of the embodiments may be combined with each other without conflict.
In the description of the present invention, it is to be understood that the terms "center", "longitudinal", "lateral", "up", "down", "front", "back", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", and the like, indicate orientations or positional relationships based on those shown in the drawings, and are used only for convenience in describing the present invention and for simplicity in description, and do not indicate or imply that the referenced devices or elements must have a particular orientation, be constructed and operated in a particular orientation, and thus, are not to be construed as limiting the present invention. Furthermore, the terms "first", "second", etc. are used for descriptive purposes only and are not to be construed as indicating or implying relative importance or implicitly indicating the number of technical features indicated. Thus, a feature defined as "first," "second," etc. may explicitly or implicitly include one or more of that feature. In the description of the present invention, "a plurality" means two or more unless otherwise specified.
In the description of the present invention, it should be noted that, unless otherwise explicitly specified or limited, the terms "mounted," "connected," and "connected" are to be construed broadly, e.g., as meaning either a fixed connection, a removable connection, or an integral connection; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meaning of the above terms in the present invention can be understood by those of ordinary skill in the art through specific situations.
The present invention will be described in detail below with reference to the embodiments with reference to the attached drawings.
Example one
Referring to fig. 1-4, a shaddock ped essential oil extraction device comprises a bottom plate 1, a placing table 2 is arranged on the bottom plate 1, a heater 3 is arranged on the placing table 2, a distillation tank 4 is arranged on the heater 3, a feed inlet 5 and a discharge outlet 7 are respectively arranged at the upper end and the lower end of the distillation tank 4, a discharge centrifuge 8 is arranged under the discharge outlet 7, the upper end of the distillation tank 4 is connected with a condenser pipe 13 through a connecting pipe 12, the lower end of the condenser pipe 13 is connected with separating tanks 16, the number of the separating tanks 16 is two, the separating tanks 16 are the same from top to bottom, the tank bodies of the separating tanks 16 are fixed on a vertical frame 9 arranged on the bottom plate 1 through trays 18, the upper and the lower separating tanks 16 are connected through first separating pipelines 31, the lower ends of the separating tanks 16 positioned below are connected with a collecting box 11 arranged on the bottom plate 1 through second separating pipelines 33, a spiral pipeline 22 is arranged around the interior of the condensation pipe 13, the lower end and the lower end of the spiral pipeline 22 are respectively connected with a water inlet pipe 21 and a water outlet pipe 23, the upper end port of the water inlet pipe 21 is connected with the upper end of the water conduit 14, the lower end of the water conduit 14 extends into the water supply tank 10 and is connected with a water pump arranged in the water supply tank 10, a main leading-in pipe 15 and a leading-out pipe 27 are respectively arranged above and below the axis position of the central position in the separation tank 16, a secondary leading-in pipe 24 is arranged on one side of the main leading-in pipe 15, a separation pipe 25 is arranged inside the separation tank 16 and on the other side of the main leading-in pipe 15, two identical observation windows 17 are arranged on the tank wall of the separation tank 16, the lower end of the upper separation tank 16 is connected with the right end of a first backflow pipeline 28, the left end of the first backflow pipeline 28 is connected with the tank wall of the distillation tank 4, a first backflow, the middle part of the first backflow pipeline 28 is connected with the upper end of the through-flow pipeline 30, the lower end of the through-flow pipeline 30 is connected with the water recovery device 19 arranged on the bottom plate 1, the middle part of the through-flow pipeline 30 is provided with a stop valve 35, the lower end of the lower separation tank 16 is connected with the right end of the second backflow pipeline 29, the left end of the second backflow pipeline 29 is connected with the lower part of the through-flow pipeline 30, the middle part of the second backflow pipeline 29 is provided with a second backflow valve 36, the upper end of the lower separation tank 16 is connected with the right end of the diversion pipeline 32, the left end of the diversion pipeline 32 is connected with the right part of the first backflow pipeline 28, and the middle part of the diversion pipeline 32 is provided with a diversion valve 37.
Specifically, the right end of the first return pipeline 28 and the right end of the second return pipeline 29 are respectively connected with the delivery pipes 27 of the upper separation tank 16 and the lower separation tank 16, the upper and lower ends of the first separating duct 31 are connected to the lower end of the separating pipe 25 of the upper separating tank 16 and the upper end of the main introducing pipe 15 of the lower separating tank 16, respectively, and since the first separating duct 31 is not matched in diameter size with the introducing pipe, a blending joint is arranged at the joint of the first separation pipeline 31 and the main inlet pipe 15 and is connected, the right end of the branch pipe 32 is connected to the upper end of the secondary introduction pipe 24 of the lower separation tank 16, the upper end of the second separation conduit 33 is connected to the lower end of the separation pipe 25 of the lower separation tank 16, the first return duct 28 and the through-flow duct 30 have a diameter size corresponding to the duct diameter size of the delivery duct 27, the first 31 and second 33 separation ducts have a diameter size corresponding to the diameter size of the separation tube 25.
Preferably, the connection between the vent pipe 30 and the first return pipe 28 is disposed at the left side of the connection between the branch pipe 32 and the first return pipe 28, so that the liquid after the first separation can be prevented from flowing into the vent pipe 30 first and causing waste.
Further, the lower portion of the main introduction pipe 15 protrudes into the separation tank 16, and the length of the protruding portion is one half of the height of the separation tank 16, and the upper portion of the separation pipe 25 protrudes into the separation tank 16, and the length of the protruding portion is three quarters of the height of the separation tank 16.
Preferably, the two observation windows 17 are respectively arranged on the tank wall at the position of one fourth and three quarters of the height of the separation tank 16, the upper part of the delivery pipe 27 does not extend into the separation tank 16, and the pipeline diameter sizes of the main inlet pipe 15, the delivery pipe 27, the separation pipe 25 and the secondary inlet pipe 24 are reduced in sequence.
Preferably, the heater 3 is a hemispherical inner hollow structure, the inner diameter of the heater 3 is equal to the outer diameter of the distillation retort 4, the heat conduction frame 38 is welded on the lower surface wall inside the distillation retort 4, when the lower part of the distillation retort 4 is embedded inside the heater 3, when the distillation retort 4 is heated by the heater 3, the distillation retort 4 can be heated more uniformly at a heating speed.
Before use, the first reflux valve 34, the first reflux valve 35 and the second reflux valve 36 are closed, the shunt valve 37 is opened, the water pump is opened, the water conduit 14 starts to fill water into the condenser pipe 13, the water in the condenser pipe 13 flows into the lower separation tank 16 through the upper separation tank 16, when the water level in the lower separation tank 16 is about one fourth of the height of the separation tank 16, the water filling is stopped, the shunt valve 37 is closed, when the device is used, the treated pomelo peel is filled into the distillation tank 4 through the material inlet, after a proper amount of water is added, the heater 3 is opened through the control panel 6, the heater 3 starts to heat the distillation tank 4, the gas containing essential oil after distillation enters the condenser pipe 13 through the connecting pipe 12, flows into the upper separation tank 16 after condensation treatment, simultaneously, the water pump is opened to adjust the water filling speed for slow water filling, at the moment, the water in the condenser pipe 13 gradually enters and is stored in the upper separation tank 16, gradually raising the water level in the upper separation tank 16, according to the principle of oil-water separation, leading the oil layer above to reach the upper end of the separation pipe 25, observing the internal condition of the separation tank 16 through the observation window 17, opening the first return valve 34 after the oil layer is almost separated, leading the separated water layer part in the upper separation tank 16 to flow into the distillation tank 4 and continue distillation treatment, closing the first return valve 34 after the water in the first return pipeline 28 is exhausted, continuing water injection through the water guide pipe 14, repeating the distillation and separation operation, stopping distillation when the oil layer part in the lower separation tank 16 reaches the position which is half of the height of the separation tank 16, opening the shunt valve 37, starting separation treatment of the oil layer part in the lower separation tank 16 and separating the oil layer part into the collection tank 11 through the separation pipe 25, opening the stop valve 35 and the second return valve 36 after separation is finished, the water layer is partially flowed into the water recovery device 19 to realize the recovery treatment.
Example two
Referring to fig. 2, on the basis of embodiment 1, although the extraction separation and the cyclic resource utilization can be performed well, the condensation pipe 13 has both condensation and diversion functions, and the diversion effect on the steam is low, which affects the subsequent separation work, and therefore, the diversion rod 20 is fixedly connected inside the condensation pipe 13 through a thin rod.
Furthermore, both ends of the flow guide rod 20 are semicircular, the flow guide rod 20 and the condenser pipe 13 are parallel to each other, and the flow guide rod 20 is located on the central line inside the condenser pipe 13.
Thus, the gas generated after distillation is condensed in the condensation pipe 13, the spiral pipe 22 is arranged at the periphery of the flow guide rod 20, and the gas condensed and liquefied flows downwards along the flow guide rod 20 and finally flows into the main inlet pipe 15.
To sum up, the shaddock ped essential oil extraction device is provided with the heater 3 to be matched with the distillation retort 4 for distillation, so that the problems of uneven heating and difficult temperature regulation during distillation by adopting a single distillation retort 4 are solved, all components for distillation, condensation, separation and collection are arranged above the bottom plate 1, the structure is compact, the occupied area is small, the space utilization rate is high, essential oil is separated by arranging the upper separation tank 16 and the lower separation tank 16, the problems of insufficient separation, poor separation effect and the like caused by separation by a single separation device are solved, a water layer part separated by the upper separation tank 16 flows back into the distillation retort 4 through the first backflow pipeline 28, so that the part of the essential oil part which is not separated can be recycled, the resource waste is avoided, and water in the condensation pipe 13 can flow into the separation tank 16 for separation after the condensation work is completed, effectively practiced thrift the water resource, avoided the water waste, the water that is injected into by leading water pipe 14 reachs water recovery unit 19 through condenser pipe 13, knockout drum 16 at last and retrieves, also can wash knockout drum 16 and each pipeline inner wall when retrieving, avoids miscellaneous dirt accumulation to block up the pipeline, and overall device resource utilization is high, and the practicality is strong.
Although the preferred embodiments of the present patent have been described in detail, the present patent is not limited to the above embodiments, and various changes can be made without departing from the spirit of the present patent within the knowledge of those skilled in the art.
Claims (7)
1. The utility model provides a shaddock ped essential oil extraction element, includes bottom plate (1), be equipped with on bottom plate (1) and place platform (2), it is equipped with heater (3) on platform (2) to place, be equipped with retort (4) on heater (3), charge door (5) and bin outlet (7) have been opened respectively to the upper and lower end of retort (4), be equipped with discharge centrifuge (8) under bin outlet (7), the upper end of retort (4) is passed through connecting pipe (12) and is linked to each other with condenser pipe (13), the lower extreme of condenser pipe (13) links to each other with knockout drum (16), its characterized in that, the quantity of knockout drum (16) sets up to two the same from top to bottom, knockout drum (16) can body passes through tray (18) and fixes on the perpendicular frame (9) that is equipped with on bottom plate (1), and two knockout drums (16) link to each other through first separation pipeline (31) from top to bottom, the lower end of a separating tank (16) positioned below is connected with a collecting box (11) arranged on the bottom plate (1) through a second separating pipeline (33), a spiral pipeline (22) is arranged in the condensing pipe (13) in a surrounding manner, the lower end and the lower end of the spiral pipeline (22) are respectively connected with a water inlet pipe (21) and a water outlet pipe (23), the upper port of the water inlet pipe (21) is connected with the upper end of a water guide pipe (14), the lower end of the water guide pipe (14) extends into a water supply tank (10) and is connected with a water pump arranged in the water supply tank (10), a main inlet pipe (15) and a guide outlet pipe (27) are respectively arranged above and below the axis position of the center of the inside of the separating tank (16), a secondary inlet pipe (24) is arranged on one side of the main inlet pipe (15), a separating pipe (25) is arranged inside the separating tank (16) and on the other side of the main inlet pipe (15), the wall of the separation tank (16) is provided with an upper observation window and a lower observation window (17) which are the same, the lower end of the upper separation tank (16) is connected with the right end of a first backflow pipeline (28), the left end of the first backflow pipeline (28) is connected with the tank wall of the distillation tank (4), the left part of the first backflow pipeline (28) is provided with a first backflow valve (34), the middle part of the first backflow pipeline (28) is connected with the upper end of a through-flow pipeline (30), the lower end of the through-flow pipeline (30) is connected with a water recovery device (19) arranged on the bottom plate (1), the middle part of the through-flow pipeline (30) is provided with a stop valve (35), the lower end of the lower separation tank (16) is connected with the right end of a second backflow pipeline (29), the left end of the second backflow pipeline (29) is connected with the lower part of the through-flow pipeline (30), and the middle part of the second backflow pipeline (29) is provided with a second, the upper end of below knockout drum (16) links to each other with reposition of redundant personnel pipeline (32) right-hand member, the left end of reposition of redundant personnel pipeline (32) links to each other with the right part of first backflow pipeline (28), reposition of redundant personnel pipeline (32) middle part is equipped with shunt valve (37).
2. The shaddock ped essential oil extraction device as claimed in claim 1, characterized in that the right end of the first return line (28), the right end of the second return line (29) are connected with the delivery pipe (27) of the upper knockout drum (16) and the lower knockout drum (16) respectively, the upper and lower ends of the first separation line (31) are connected with the lower end of the separation pipe (25) of the upper knockout drum (16) and the upper end of the main inlet pipe (15) of the lower knockout drum (16) respectively, the joint of the first separation line (31) and the main inlet pipe (15) is provided with a blending joint and connected, the right end of the diversion line (32) is connected with the upper end of the secondary inlet pipe (24) of the lower knockout drum (16), the upper end of the second separation line (33) is connected with the lower end of the separation pipe (25) of the lower knockout drum (16), the first return line (28), The diameter of the through-flow duct (30) corresponds to the duct diameter of the outlet duct (27), and the diameter of the first separation duct (31) and the diameter of the second separation duct (33) correspond to the diameter of the separation duct (25).
3. The shaddock ped essential oil extraction device as recited in claim 2, wherein the lower part of the main introduction pipe (15) is extended into the separation tank (16) and the length of the extended part is one half of the height of the separation tank (16), and the upper part of the separation pipe (25) is extended into the separation tank (16) and the length of the extended part is three quarters of the height of the separation tank (16).
4. The shaddock ped essential oil extraction device as recited in claim 1, wherein the connection of the through-flow conduit (30) and the first return conduit (28) is disposed to the left of the connection of the diversion conduit (32) and the first return conduit (28).
5. The shaddock ped essential oil extraction device as claimed in claim 2, wherein two observation windows (17) are respectively arranged on the tank wall at the one fourth and three quarters of the height of the separation tank (16), the upper part of the delivery pipe (27) does not extend into the separation tank (16), and the pipeline diameter sizes of the main inlet pipe (15), the delivery pipe (27), the separation pipe (25) and the secondary inlet pipe (24) are sequentially reduced.
6. The shaddock ped essential oil extraction device as claimed in claim 1, wherein the heater (3) is a hemispherical internal hollow structure, the inner diameter of the heater (3) is equal to the outer diameter of the distillation tank (4), and a heat conduction frame (38) is welded on the lower surface wall inside the distillation tank (4).
7. The shaddock ped essential oil extraction device as claimed in claim 1, wherein a flow guide rod (20) is fixedly connected inside the condenser pipe (13) through a thin rod, both ends of the flow guide rod (20) are semicircular, the flow guide rod (20) and the condenser pipe (13) are parallel to each other, and the flow guide rod (20) is located on a central line inside the condenser pipe (13).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011375093.8A CN112481038A (en) | 2020-11-30 | 2020-11-30 | Shaddock ped essential oil extraction element |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011375093.8A CN112481038A (en) | 2020-11-30 | 2020-11-30 | Shaddock ped essential oil extraction element |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN112481038A true CN112481038A (en) | 2021-03-12 |
Family
ID=74937473
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202011375093.8A Pending CN112481038A (en) | 2020-11-30 | 2020-11-30 | Shaddock ped essential oil extraction element |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN112481038A (en) |
Citations (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR815102A (en) * | 1935-12-23 | 1937-07-06 | Colgate Palmolive Peet Co | Method and apparatus for the distillation of glycerin |
| CN205850272U (en) * | 2016-08-02 | 2017-01-04 | 江西国化实业有限公司 | A kind of high efficiente callback solvent distillation device |
| CN107325889A (en) * | 2017-09-04 | 2017-11-07 | 梁溪区昊星工业设计工作室 | A kind of industrial production raw material extraction element |
| CN207545858U (en) * | 2017-11-29 | 2018-06-29 | 江西新生命制药有限公司 | A kind of Chinese medicine distills device for refining |
| CN207545861U (en) * | 2017-11-27 | 2018-06-29 | 太极集团重庆中药二厂有限公司 | A kind of Chinese medicine Distallation systm |
| CN207685227U (en) * | 2017-11-13 | 2018-08-03 | 南京汉尔斯生物科技有限公司 | A kind of extraction element of rose aromatic oil |
| CN108998244A (en) * | 2018-08-08 | 2018-12-14 | 甘肃瑰隆生物科技有限公司 | Rose ethereal oil extraction element |
| CN208414360U (en) * | 2018-05-15 | 2019-01-22 | 重庆市洲仨科技发展有限公司 | A kind of essential oil extraction device |
| CN209989346U (en) * | 2019-04-23 | 2020-01-24 | 贵州晨阳机械科技有限公司 | Essential oil distillation extraction recovery system |
| CN210580823U (en) * | 2019-08-19 | 2020-05-22 | 贵州荔波亿隆之家农业科技有限公司 | Enzyme killing device |
| CN210620743U (en) * | 2019-08-28 | 2020-05-26 | 宁夏嘉禾花语生态农业有限公司 | Scented tea distillation extraction equipment |
| CN211179667U (en) * | 2019-10-14 | 2020-08-04 | 南召县岭南艾叶制品有限公司 | Purity detection device for wormwood essential oil extraction |
-
2020
- 2020-11-30 CN CN202011375093.8A patent/CN112481038A/en active Pending
Patent Citations (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR815102A (en) * | 1935-12-23 | 1937-07-06 | Colgate Palmolive Peet Co | Method and apparatus for the distillation of glycerin |
| CN205850272U (en) * | 2016-08-02 | 2017-01-04 | 江西国化实业有限公司 | A kind of high efficiente callback solvent distillation device |
| CN107325889A (en) * | 2017-09-04 | 2017-11-07 | 梁溪区昊星工业设计工作室 | A kind of industrial production raw material extraction element |
| CN207685227U (en) * | 2017-11-13 | 2018-08-03 | 南京汉尔斯生物科技有限公司 | A kind of extraction element of rose aromatic oil |
| CN207545861U (en) * | 2017-11-27 | 2018-06-29 | 太极集团重庆中药二厂有限公司 | A kind of Chinese medicine Distallation systm |
| CN207545858U (en) * | 2017-11-29 | 2018-06-29 | 江西新生命制药有限公司 | A kind of Chinese medicine distills device for refining |
| CN208414360U (en) * | 2018-05-15 | 2019-01-22 | 重庆市洲仨科技发展有限公司 | A kind of essential oil extraction device |
| CN108998244A (en) * | 2018-08-08 | 2018-12-14 | 甘肃瑰隆生物科技有限公司 | Rose ethereal oil extraction element |
| CN209989346U (en) * | 2019-04-23 | 2020-01-24 | 贵州晨阳机械科技有限公司 | Essential oil distillation extraction recovery system |
| CN210580823U (en) * | 2019-08-19 | 2020-05-22 | 贵州荔波亿隆之家农业科技有限公司 | Enzyme killing device |
| CN210620743U (en) * | 2019-08-28 | 2020-05-26 | 宁夏嘉禾花语生态农业有限公司 | Scented tea distillation extraction equipment |
| CN211179667U (en) * | 2019-10-14 | 2020-08-04 | 南召县岭南艾叶制品有限公司 | Purity detection device for wormwood essential oil extraction |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102311705B (en) | Method for producing rosin | |
| CN102952629B (en) | Technological method for extracting natural cinnamon oil | |
| CN1679730A (en) | Material of Chinese medicine extracting process and apparatus thereof | |
| CN206252860U (en) | A kind of constant single effect evaporator of secondary steam flow rate | |
| CN208911492U (en) | A kind of kettle material purification system again | |
| CN112481038A (en) | Shaddock ped essential oil extraction element | |
| CN208136162U (en) | A kind of integration crude oil production processing unit | |
| CN209989346U (en) | Essential oil distillation extraction recovery system | |
| CN1114458C (en) | Crude oil atmospheric vacuum distillation method with deep stripping process | |
| CN207384892U (en) | Extraction and separation device and system thereof | |
| CN114317112B (en) | Deacidification device for refining and processing edible vegetable oil and use method thereof | |
| CN105237358B (en) | Natural borneol extraction system and method capable of increasing yield | |
| CN209144109U (en) | A kind of essential oil extract knockout drum | |
| CN205701819U (en) | Kitchen garbage grease pretreatment unit | |
| CN208678442U (en) | A kind of oily water separating equipment of san-mou oil | |
| CN109395428A (en) | Extraction and separation device and system and extraction and separation method thereof | |
| CN209669157U (en) | A kind of high acid value lipin deacidifying deodorization device | |
| CN206008077U (en) | The distillating still of feeding can be facilitated | |
| CN206269112U (en) | A kind of energy-conservation regular unloading container | |
| CN202161822U (en) | Rosin refining kettle | |
| CN214360814U (en) | Oil-water separator for kitchen waste | |
| CN200946143Y (en) | Gas-electric dual-using aromatic oil distiller | |
| RU224950U1 (en) | Evaporation device | |
| CN219507694U (en) | Tritium sample distillation filter equipment | |
| KR101538960B1 (en) | Method and apparatus for seperating oil and water from waste oil of duck as raw material |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20210312 |
|
| RJ01 | Rejection of invention patent application after publication |