CN206008077U - The distillating still of feeding can be facilitated - Google Patents

The distillating still of feeding can be facilitated Download PDF

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Publication number
CN206008077U
CN206008077U CN201620967659.9U CN201620967659U CN206008077U CN 206008077 U CN206008077 U CN 206008077U CN 201620967659 U CN201620967659 U CN 201620967659U CN 206008077 U CN206008077 U CN 206008077U
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CN
China
Prior art keywords
distillating still
valve
air inlet
tube
probe tube
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201620967659.9U
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Chinese (zh)
Inventor
佟云
王玉国
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Yancheng City East Chemical Co Ltd
Original Assignee
Yancheng City East Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Yancheng City East Chemical Co Ltd filed Critical Yancheng City East Chemical Co Ltd
Priority to CN201620967659.9U priority Critical patent/CN206008077U/en
Application granted granted Critical
Publication of CN206008077U publication Critical patent/CN206008077U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

The utility model discloses a kind of distillating still, including distillating still body, charging aperture is set at the top of distillating still body, feed pipe is set at charging aperture, its bottom arranges discharge gate, discharge gate connects drainage conduit, air inlet is also set up in distillating still bottom, and described air inlet connection conveys the air inlet pipe of vapor, the discharge for making feedstock vapor escape is additionally provided with distillating still body top, also include probe tube, caliber of the caliber of probe tube described in the probe tube less than drainage conduit;One end of probe tube is arranged on transverse tube, and the other end is upwardly extended, and is arranged elbow in its end, is arranged the first valve and the second valve in drainage conduit.This utility model compared with prior art, which increases caliber less probe tube and chemical industry bed material is sampled, and the flow of chemical industry bed material is significantly controlled, and chemical industry bed material is released automatically, and without the need for manually take, security performance has ensured.

Description

The distillating still of feeding can be facilitated
Technical field
This utility model is related to a kind of chemical production equipment, specifically, is a kind of distillating still.
Background technology
Distillating still be in Chemical Manufacture commonly use reaction utensil, its chemical industry bed material in kettle is carried out using water vapour plus Heat, and then the steam of industrial chemicals is produced, industrial chemicals steam is input into material collection device by discharge.Distilling Need to be monitored the progress that distills in real time in journey, i.e., the chemical industry bed material in regularly needing to distillating still is sampled, tradition Distillating still sample when need open bottom discharge gate, to discharge chemicals bed material carry out concentration analysis, so as to obtain The progress of distillation.In general, all than larger, can cause during sampling substantial amounts of to ensure the speed of discharge, drainage conduit caliber Bed material is released, and the waste for causing resource of certainty, the method for only controlling its flow manually by slight Open valve are entered Row sampling, and control that its subjectivity is larger manually, flow can not be controlled very precisely.And distillation work must be stopped by sampling work Can carry out after only, what which was invisible extends the time of work, and in still-process can produce substantial amounts of heat, if cooling is not filled Divide and be then easy to be burned in sampling process.Huge hidden danger is caused to the personal safety of operator.
Content of the invention
The purpose of this utility model is to provide a kind of wasting of resources few, safe distillating still.
This utility model is realized using following technological means:One kind can facilitate feeding distillating still, including distillating still sheet Body, arranges charging aperture at the top of distillating still body, arranges feed pipe at charging aperture, and its bottom arranges discharge gate, and discharge gate connects Run in expects pipe, drainage conduit is divided into straight tube and transverse tube, and transverse tube is connected with each other with one end of straight tube, the other end connection of transverse tube is filtered Groove, also sets up air inlet in distillating still bottom, and described air inlet connection conveys the air inlet pipe of vapor, on distillating still body top End is additionally provided with the discharge for making feedstock vapor escape, and also includes probe tube, and described in the probe tube, the caliber of probe tube is less than The caliber of drainage conduit;
Described probe tube is L-type pipe, and the horizontal ends of L-type pipe are connected on the straight tube of drainage conduit.The end of vertical end sets Put elbow, the second valve be arranged on transverse tube near with the position of straight tube junction on;
Air intake branch is also set up in air inlet pipe, and one end of described air intake branch connects air inlet pipe, and the other end stretches into steaming The top of kettle body is evaporated, the 3rd valve is set on air intake branch, in the air inlet pipe of air intake branch Yu air inlet pipe junction bottom The 4th valve of upper setting.
Also include that heat reclaim unit, described heat reclaim unit include condenser and escape pipe, one end of condenser Connection discharge, the other end connect one end of escape pipe, and the other end connection material collection device of escape pipe is set on discharge Put the 5th valve.
Control device, the remotely controlled case control of control device are set on described valve.
This utility model compared with prior art, which increases caliber less probe tube and chemical industry bed material is taken Sample, the flow of chemical industry bed material are significantly controlled, and chemical industry bed material is released automatically, without the need for manually taking, safety Can ensure, this utility model also sets up heat reclaim unit and carries out the recovery of heat to industrial chemicals steam, which achieves The circulation of the energy, so that avoid the waste of the energy.
Description of the drawings
Fig. 1 is this utility model structural representation.
Wherein 1- distillating stills body, 2- drainage conduits, the first valves of 3-, 4- probe tubes, 5- air inlet pipe, 6- air intake branches, 7- 3rd valve, the 4th valves of 8-, 9- discharges, 10- condensers, 11- escape pipes, the 5th valves of 12-, the second valves of 13-.
Specific embodiment
This utility model is described in further detail with reference to Figure of description:
This utility model relate to a kind of distillating still, and which includes a distillating still body 1, at the top of distillating still body 1 And bottom, charging aperture and discharge gate is respectively provided with, feed pipe is set at charging aperture, drainage conduit 2 is set at discharge gate, steamed The bottom for evaporating kettle also sets up air inlet, and air inlet connection conveys the air inlet pipe 5 of vapor, and top also sets up collection QI KOU, in gas collection Discharge 9 is set on mouth, and chemical industry bed material is put in distillating still body by charging aperture, then passes through 5 inside input water of air inlet pipe Steam is distilled to which, is distilled the industrial chemicals steam for obtaining and is transferred out by discharge 9, distills remaining material residue Outside distillating still body is discharged by drainage conduit 2, complete distillation action is completed once.
In this utility model, described distillating still also includes that a probe tube 4, probe tube 4 are set to L-type, and described takes Sample pipe 4 is arranged on vertical tube, and the horizontal ends of probe tube are connected with vertical tube, arranges elbow, the elbow in the end of its vertical end Direction facing away from distillating still body, and can arbitrarily adjust in the range of 180 °.In this utility model, described probe tube 4 Caliber of the caliber less than transverse tube, specifically, between 3-5cm, in its unit interval, flow is constant, i.e., for the caliber of probe tube 4 Just every time Open valve when open that size is different, which still can guarantee that the maximum of flows per unit time, make the user will not be by Scald.
In this utility model, valve is set in described drainage conduit, specifically, valve arranges 2, is divided into the first valve Door 3 and the second valve 13, the first valve 3 are arranged on vertical tube, and the second valve 13 is arranged on transverse tube, specifically, described Second valve 13 is arranged on transverse tube near the adjacent one end with vertical tube junction, its object is to timely block in transverse tube and flows Bed material, make which rapidly enter in probe tube 4.
Drainage conduit 2 is arranged on the downside of vertical tube, also can be in same level with transverse tube, if being in same level, Then the junction of transverse tube and vertical tube arranges threeway, arranges a connecting tube in the junction of threeway and probe tube, and the two of connecting tube Port footpath is adapted with threeway and probe tube respectively
This utility model also includes that an air intake branch 6, one end of air intake branch 6 are arranged in air inlet pipe 5, and the other end is stretched Enter in distillating still body 1, specifically, air intake branch 6 stretches into the top of distillating still body 1, the 3rd is arranged on air intake branch 6 Valve 7, arranges the 4th valve 8 in air inlet pipe, and specifically, the 4th valve 8 is arranged on the bottom of air inlet pipe 5, more specific next Say, be arranged on the bottom of air intake branch 6 and 5 junction of air inlet pipe.
This utility model also includes that a heat reclaim unit, the heat reclaim unit are arranged on discharge 9, and which wraps A condenser 10 and an escape pipe 11 is included, one end of condenser 10 is arranged on the end of discharge 9, and the other end connects outlet One end of pipe 11, arranges water inlet and outlet on condenser, and water inlet is connected a water circulating pump, recirculated water with outlet Pump connect a hot-water cylinder, by condenser in water constantly circulate, by flow into condenser in industrial chemicals steam carry out cold But, stored in cooling water input hot-water cylinder, then heated water is sent into and produces vapor, realize energy The recycling of amount, arranges the 5th valve 12 on discharge 9 in this utility model.
Condenser described in the utility model also directly can be socketed on discharge 9, in condenser arrange spiral element Road is used for conveying condensed water.The caliber of described serpentine pipe equal with the caliber of discharge 9 or be slightly larger than its caliber, such one Come, the heat of chemical industry feedstock vapor just can be fully absorbed in discharge 9, more save energy.
In order to ensure the safety of operator, which can arrange control device at valve, be carried out using control chamber long-range Control, specifically, exactly assigns instruction by control chamber, makes opening and closing and the opening angle of control device operation valve, so as to Order operation is safer, also more accurate.
Describe in detail below by a specific example:
During distillation process is carried out, the first valve closing, the second valve are also switched off, and the 3rd valve opens conveying water Steam, the 4th valve closing, the 5th valve open release chemical raw material vapour, once need to sample, then by the 3rd valve closing, 4th valve is opened, the 5th valve is also switched off, while opening the 4th valve carries out vapor output from upper end, open the first valve Door, due to vapor, constantly conveying causes pressure increase in kettle, and under pressure, chemical industry bed material is extruded from probe tube, real Now sample;After sampling is finished, the first valve and the 4th valve is closed, open the 3rd valve and proceed to give birth to the 5th valve Produce.When distillation completes discharging, by the 3rd valve and the 5th valve closing, opening the first valve and the second valve carries out discharging, Due to probe tube different from drainage conduit caliber, and in kettle pressure also less, therefore bed material will not be spilt from probe tube.

Claims (3)

1. a kind of distillating still for facilitating feeding, including distillating still body, arranges charging aperture, charging at the top of distillating still body Mouthful place arranges feed pipe, and its bottom arranges discharge gate, and discharge gate connects drainage conduit, and drainage conduit is divided into straight tube and transverse tube, transverse tube and One end of straight tube is connected with each other, the other end connection filter tank of transverse tube, also sets up air inlet, described air inlet in distillating still bottom The air inlet pipe of mouth connection conveying vapor, is additionally provided with the discharge for making feedstock vapor escape on distillating still body top, and which is special Levy and be:Also include probe tube, caliber of the caliber of probe tube described in the probe tube less than drainage conduit;
Described probe tube is L-type pipe, and the horizontal ends of L-type pipe are connected on the straight tube of drainage conduit, and the end of vertical end arranges curved Head, the second valve be arranged on transverse tube near with the position of straight tube junction on;
Air intake branch is also set up in air inlet pipe, and one end of described air intake branch connects air inlet pipe, and the other end stretches into distillating still The top of body, on air intake branch arranges the 3rd valve, sets in the air inlet pipe of air intake branch with air inlet pipe junction bottom Put the 4th valve.
2. distillating still according to claim 1, it is characterised in that:Also include heat reclaim unit, described heat recovery Device includes that condenser and escape pipe, one end connection discharge of condenser, the other end connect one end of escape pipe, escape pipe The other end connects material collection device, arranges the 5th valve on discharge.
3. distillating still according to claim 1, it is characterised in that:Control device, control device are set on described valve Remotely controlled case control.
CN201620967659.9U 2016-08-26 2016-08-26 The distillating still of feeding can be facilitated Expired - Fee Related CN206008077U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201620967659.9U CN206008077U (en) 2016-08-26 2016-08-26 The distillating still of feeding can be facilitated

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201620967659.9U CN206008077U (en) 2016-08-26 2016-08-26 The distillating still of feeding can be facilitated

Publications (1)

Publication Number Publication Date
CN206008077U true CN206008077U (en) 2017-03-15

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201620967659.9U Expired - Fee Related CN206008077U (en) 2016-08-26 2016-08-26 The distillating still of feeding can be facilitated

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Country Link
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109621474A (en) * 2018-12-27 2019-04-16 昆山城东化工有限公司 A kind of multistage cooling recovery system for organic solvent of automatic control

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109621474A (en) * 2018-12-27 2019-04-16 昆山城东化工有限公司 A kind of multistage cooling recovery system for organic solvent of automatic control

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Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20170315

Termination date: 20180826

CF01 Termination of patent right due to non-payment of annual fee