CN206127245U - Distillation edulcoration device of raw oil - Google Patents

Distillation edulcoration device of raw oil Download PDF

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Publication number
CN206127245U
CN206127245U CN201621041909.2U CN201621041909U CN206127245U CN 206127245 U CN206127245 U CN 206127245U CN 201621041909 U CN201621041909 U CN 201621041909U CN 206127245 U CN206127245 U CN 206127245U
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CN
China
Prior art keywords
distillating still
raw oil
distillation
condenser
kettle
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Expired - Fee Related
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CN201621041909.2U
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Chinese (zh)
Inventor
钟志富
王国良
谭时成
高顺华
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Cofco Dexin Health Industry Co Ltd
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Cofco Dexin Health Industry Co Ltd
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Priority to CN201621041909.2U priority Critical patent/CN206127245U/en
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Publication of CN206127245U publication Critical patent/CN206127245U/en
Expired - Fee Related legal-status Critical Current
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Abstract

The utility model provides a distillation edulcoration device of raw oil, include stills, condenser, fractionation cauldron and heat up in a steamer the cauldron again, be equipped with heating coil between stills outer wall and the inner wall bottom reaching, stills has the condenser through the pipe connection, the other end of condenser passes through backflow pipeline and condensation flue is connected with stills's top and cooler respectively, the condenser has the cooler through the pipe connection, the cooler lower extreme links to each other with the top of distillating fractionally the cauldron, it jar links to each other with heating up in a steamer cauldron, essential oil collection tank again and catchment respectively to distillate fractionally the cauldron, the upper end that the steam outlet that heats up in a steamer the cauldron again passes through pipeline and cooler links to each other. This edulcoration device utilizes during the vacuum pump inhales the cauldron to raw oil, and heating distillation under the negative pressure detaches the thing that mixes in the oil, raises the efficiency, reduces the cost, improves product quality.

Description

A kind of distillation knot screen of raw oil
Technical field
This utility model belongs to plant ingredient extracting equipment technical field, and in particular to a kind of distillation remove impurity dress of raw oil Put.
Background technology
Plant material oil is the compound being bound up by unsaturated fatty acid and glycerol, is distributed widely in nature, It is such as Oleum Arachidis hypogaeae semen, Oleum Glycines, oleum lini, Oleum Ricini, rapeseed oil etc. with rich grease-contained plant kernel as raw material, Jing cleaning remove impurity, After the pretreatment such as shelling, broken, softening, strip plate, extruding puffing, then acquisition is extracted slightly using mechanical expression or solvent extraction method Oil.The main component of plant material oil is the ester that straight chain higher fatty acids and glycerol are generated, mainly contain Vitamin E, K, calcium, The mineral such as ferrum, phosphorus, potassium.Typically can all contain mechanical admixture in natural plant raw material oil(Mud, sand, rust etc.)Material, and There are a variety of chemical compositions, general Filterses utilization rate is low, loss is big, and high cost, can't meet the quality requirement.
Existing distilling apparatus can utilize the mode of vacuum distillation, in plant material oil suction distillating still, open vacuum Pump, is, in negative pressure state, to reduce the boiling point of raw oil, open heating system and heated, steam raw oil inside distillating still Send out, liquefied by chiller, then the moisture in raw oil, impurity and vegetable oil are separated by fractionating device, produce Efficiency high, good impurity removing effect.
It is " CN205258422U " in Chinese utility model patent application publication number, Shen Qing Publication day is May 25 in 2016 Day, it is entitled《A kind of rose ethereal oil distillation extraction device》File in, disclose a kind of rose ethereal oil distillation extraction device, Kettle is evaporated including distillating still, drainer, gs-oil separator and again, the distillating still includes kettle and kettle cover, the bottom of the kettle It is hemispherical and steam pipe coil is distributed with the bottom of kettle, one end of oil gas conduit, the oil are connected with the kettle cover The other end connection drainer of airway, is provided with serpentine pipe in the drainer, one end connection oil gas of the serpentine pipe is led Pipe, the other end of the serpentine pipe connect the top of gs-oil separator, and the bottom of the drainer is provided with cold water inlet, cold It is provided with cold water outlet at the top of solidifying tank, a upper lateral part of the gs-oil separator, another side lower part and bottom are provided with three Root delivery line and it is connected to Flos Rosae Rugosae quintessence oil collecting tank, rose flower water collecting tank and evaporates kettle again.The technical scheme is used for Flos Rosae Rugosae The distillation extraction of flower essential oil, the gs-oil separator respectively with Flos Rosae Rugosae quintessence oil collecting tank, rose flower water collecting tank and evaporate kettle phase again Even, can realize carrying out the water layer after oil-water separation again multiple steaming, but the condensed fluid that quintessence oil is distilled out is easy to emulsifying occur Phenomenon, oil-water separation are difficult, for oil-water separation, generally condensed fluid need to be stood 2 ~ 3 days or the water layer after oil-water separation Multiple steaming is carried out again, as the temperature-sensitive sexual element of some of heating extraction for a long time, quintessence oil can be decomposed, the quality of quintessence oil is produced Harmful effect, and as You Heshui is immiscible, steam pipe coil is provided with autoclave body bottom only and is likely to make raw oil be heated Uneven, local temperature is too high, causes raw oil bumping, easily produces security incident.
Utility model content
The technical problems to be solved in the utility model overcomes existing defect, there is provided a kind of distillation remove impurity dress of raw oil Put, by arrange stirring motor and between distillating still outer wall and inwall and its bottom arrange heating duct, ensure raw oil On the premise of being heated evenly, from different directions raw oil is heated, and can be with by the setting of condenser pump and condenser Cooling treatment rapidly and efficiently is realized, while accelerating evaporation rate and cooldown rate, it is ensured that the extraction quality of raw oil and extraction Speed, can be with the problem in effectively solving background technology.
In order to solve above-mentioned technical problem, this utility model provides following technical scheme:
A kind of distillation knot screen of raw oil, including distillating still, condenser and fractional distillation kettle, the distillating still outer wall and interior Between wall and distillating still bottom is provided with heating coil, and the distillating still is connected with condenser by pipeline, the distillating still with it is cold Condenser pump is installed on the pipeline between condenser, the other end of the condenser pass through reflux line and condensation pipe respectively with steaming Top and the cooler connection of kettle are evaporated, the cooler lower end is connected with the top of fractional distillation kettle, a side lower part of the fractional distillation kettle, Another upper lateral part and bottom be respectively provided with three conduits respectively with evaporate kettle, oil storage tank and water tank again and be connected, the steaming for evaporating kettle again Vapor outlet is connected with the upper end of cooler by pipeline, and the reflux pipe is provided with U-tube, and being provided with below the U-tube can Depending on safety flack, the safety flack bottom is provided with drainage conduit.
Further, stirring motor is installed at the top of the distillating still, the stirring motor is connected with downwards shaft, institute State shaft to be placed in inside distillating still, the shaft lower end is provided with heat block.
Further, the distillating still outer wall is fixed with a vacuum pump, and the vacuum pump is by connecting tube and distillating still Portion is connected.
Further, the distillating still outer wall is provided with external jacket, and the distillating still inwall is provided with temperature sensor.
Further, the distillating still bottom offers, the charging aperture On be connected with charging lid.
Further, pressure gauge, temperature indicator and liquidometer are provided with the top of the distillating still.
Further, the cooling water that the cooler is used is frozen water, and the temperature range of the frozen water is 0 ~ 4 DEG C.
Further, the fractional distillation kettle and evaporate again and on kettle, be respectively provided with mirror mouth.
Further, the raw oil is plant material oil.
Compared with prior art, the beneficial effects of the utility model are:The setting of stirring motor can be sufficiently stirred for material, Heater can be heated to raw oil from different directions, intuitively reflect steaming by temperature indicator, piezometer, liquidometer Temperature inside kettle, pressure and amount of liquid are evaporated, operator can handle it in time, condenser pump makes steaming with the setting of condenser Vapour rate of cooling is fast, and frozen water is passed through in cooler makes condensed fluid reduce emulsifying as far as possible, and oil-water separation is fast, and loss of oil volume is few, yield It is high.In distillation cooling procedure, if after cooling water is leaked into reflux line or condensation pipe accidentally, flowing through in cooling water U-shaped Guan Shi is into safety flack in communication, different from raw oil proportion according to water, it can be determined that to go out in condensed raw oil Water is entered, the raw oil of water mixing is released from the drainage conduit of safety flack bottom immediately, it is to avoid cooling water enters distillating still in a large number Cause production accident.Its simple structure, easy to use, safe, simple to operate, low cost, heating and cooling effectiveness height, stirring fill Point, temperature can be surveyed.
Description of the drawings
In order to be illustrated more clearly that this utility model embodiment or technical scheme of the prior art, below will be to embodiment Or accompanying drawing to be used is briefly described needed for description of the prior art, it should be apparent that, drawings in the following description are only It is some embodiments of the present utility model, for those of ordinary skill in the art, in the premise for not paying creative work Under, can be with according to these other accompanying drawings of accompanying drawings acquisition.
Structural representations of the Fig. 1 for this utility model embodiment.
Reference in above-mentioned accompanying drawing is as follows:1 is distillating still, and 2 is condenser pump, and 3 is condenser, and 4 is cooler, and 5 are Fractional distillation kettle, 6 to evaporate kettle again, and 7 is oil storage tank, and 8 is water tank, and 9 is condensation pipe, and 10 is reflux line, and 11 is U-tube, and 12 are Safety flack, 13 is stirring motor, and 14 is heating coil, and 15 is vacuum pump, and 16 is external jacket, and 17 is residual cake valve, and 18 is charging aperture, 19 is pressure gauge, and 20 is temperature indicator, and 21 is liquidometer, and 22 is mirror mouth, and 23 is drainage conduit.
Specific embodiment
Below in conjunction with the accompanying drawing in this utility model, the technical scheme in this utility model is carried out clearly and completely Description, it is clear that the described only a part of embodiment of this utility model, rather than the embodiment of whole.Based on this practicality Embodiment in new, it is every other that those of ordinary skill in the art are obtained on the premise of creative work is not made Embodiment, belongs to the scope of this utility model protection.
As shown in figure 1, a kind of distillation knot screen of raw oil, including distillating still 1, condenser 3 and fractional distillation kettle 5, it is described Between 1 outer wall of distillating still and inwall and 1 bottom of distillating still is provided with heating coil 14, and the distillating still 1 is connected with cold by pipeline Condenser 3, is provided with condenser pump 2 on the pipeline between the distillating still 1 and condenser 3, the other end of the condenser 1 passes through back Flow tube road 10 and condensation pipe 9 are connected with the top of distillating still 1 and cooler 4 respectively, 4 lower end of the cooler and fractional distillation kettle 5 Top be connected, a side lower part of the fractional distillation kettle 5, another upper lateral part and bottom be respectively provided with three conduits respectively with evaporate again kettle 6, Oil storage tank 7 is connected with water tank 8, and the steam (vapor) outlet for evaporating kettle 6 again is connected with the upper end of cooler 4 by pipeline, described time Flow tube road 10 is provided with U-tube 11, and visible safety bottle 12 is provided with below the U-tube 11, and 12 bottom of the safety flack is provided with row Expects pipe 23;Stirring motor 13 is installed at the top of the distillating still 1, the stirring motor 13 connects downwards a shaft, described to stir Mix axle to be placed in inside distillating still 1, shaft lower end is provided with heat block;1 outer wall of the distillating still is fixed with a vacuum pump 15, institute State vacuum pump 15 to be connected with inside distillating still 1 by connecting tube;1 outer wall of the distillating still is provided with external jacket 16, the steaming Evaporate 1 inwall of kettle and be provided with temperature sensor;1 bottom of the distillating still offers and charging is offered on residual cake valve 17, and distillating still 1 Mouth 18, is connected with charging lid on the charging aperture 18;Pressure gauge 19, temperature indicator 20 are provided with the top of the distillating still With liquidometer 21;The cooling water that the cooler 3 is used is frozen water, and the temperature range of the frozen water is 0 ~ 4 DEG C;The fractional distillation kettle 5 and evaporate again and on kettle 6, be respectively provided with mirror mouth 22;The raw oil is plant material oil.
When the device is used, charging aperture is first turned on, opens vacuum pump, raw oil is added toward in kettle, charging aperture is closed, The heating duct of between unlatching outer wall and inwall and its bottom, while starting stirring motor, heats to raw oil, forms temperature Spend the oil mixing with water gas for 95-100 DEG C;During oil gas sequentially enters condenser and cooler by pipeline, condenser pump is opened, to oil Gas carries out forced condensation, and then condensed fluid carries out ice-water bath in entering back into cooler, makes condensed fluid reduce emulsifying, distillate as far as possible Fractional distillation kettle is entered back into, the raw oil isolated enters oil storage tank by conduit, the moisture isolated enters water tank by conduit, Now operator can pass through fractional distillation kettle and evaporate the mirror mouth observation raw material oil separating situation of kettle again, it is impossible to be kept completely separate Oil water mixture is entered by pipeline and evaporates kettle again and reenter cooler after distilling again, is again introduced into point after condensation process Evaporate kettle to be separated, the involatile constituent and impurity in raw oil is discharged from the slag-drip opening of distillating still bottom.Operator can To adjust temperature inside distillating still, pressure and amount of liquid in time by temperature indicator, piezometer, liquidometer.It is cold distilling But during, if after cooling water is leaked into reflux line or condensation pipe accidentally, when cooling water flows through U-tube, enter with Connection safety flack, it is different from raw oil proportion according to water, it can be determined that to go out in condensed raw oil and enter water, stand The raw oil of water mixing is released from the drainage conduit of safety flack bottom, it is to avoid cooling water enters distillating still in a large number and causes to produce thing Therefore.
It follows that the utility model has the advantage of:The setting of stirring motor can be sufficiently stirred for material, heater From different directions raw oil can be heated, intuitively be reflected inside distillating still by temperature indicator, piezometer, liquidometer Temperature, pressure and amount of liquid, operator can handle it in time, and condenser pump makes steam cool down speed with the setting of condenser Degree is fast, and frozen water is passed through in cooler makes condensed fluid reduce emulsifying as far as possible, and oil-water separation is fast, and loss of oil volume is few, high income.In distillation In cooling procedure, if after cooling water is leaked into reflux line or condensation pipe accidentally, when cooling water flows through U-tube, entering Safety flack in communication, it is different from raw oil proportion according to water, it can be determined that to go out in condensed raw oil and enter water, The raw oil of water mixing is released from the drainage conduit of safety flack bottom immediately, it is to avoid cooling water enters distillating still in a large number and causes to produce thing Therefore.Its simple structure, easy to use, safe, simple to operate, low cost, heating and cooling effectiveness height, stirring are abundant, and temperature can Survey.
Above content is with reference to specific preferred implementation further detailed description of the utility model, it is impossible to Identification is of the present utility model to be embodied as being confined to these explanations.For the ordinary skill of this utility model art For personnel, without departing from the concept of the premise utility, some simple deduction or replace can also be made, should be all regarded To belong to protection domain of the present utility model.

Claims (9)

1. a kind of distillation knot screen of raw oil, including distillating still, condenser and fractional distillation kettle, it is characterised in that:The distillation Between kettle outer wall and inwall and distillating still bottom is provided with heating coil, and the distillating still is connected with condenser by pipeline, described Condenser pump is installed on the pipeline between distillating still and condenser, the other end of the condenser passes through reflux line and condensing tube Road is connected with the top of distillating still and cooler respectively, and the cooler lower end is connected with the top of fractional distillation kettle, the fractional distillation kettle A side lower part, another upper lateral part and bottom be respectively provided with three conduits respectively with evaporate kettle, oil storage tank and water tank again and be connected, it is described The steam (vapor) outlet for evaporating kettle again is connected with the upper end of cooler by pipeline, and the reflux pipe is provided with U-tube, the U-tube Lower section is provided with visible safety bottle, and the safety flack bottom is provided with drainage conduit.
2. the distillation knot screen of a kind of raw oil according to claim 1, it is characterised in that pacify at the top of the distillating still Equipped with stirring motor, the stirring motor is connected with downwards shaft, and the shaft is placed in inside distillating still, the shaft Lower end is provided with heat block.
3. the distillation knot screen of a kind of raw oil according to claim 1, it is characterised in that the distillating still outer wall is solid Surely there is a vacuum pump, the vacuum pump is connected with inside distillating still by connecting tube.
4. the distillation knot screen of a kind of raw oil according to claim 1, it is characterised in that the distillating still outer wall sets External jacket is equipped with, the distillating still inwall is provided with temperature sensor.
5. the distillation knot screen of a kind of raw oil according to claim 1, it is characterised in that open the distillating still bottom It is provided with residual cake valve, and distillating still and offers charging aperture, on the charging aperture, is connected with charging lid.
6. the distillation knot screen of a kind of raw oil according to claim 1, it is characterised in that set at the top of the distillating still There are pressure gauge, temperature indicator and liquidometer.
7. the distillation knot screen of a kind of raw oil according to claim 1, it is characterised in that what the cooler was used Cooling water is frozen water, and the temperature range of the frozen water is 0 ~ 4 DEG C.
8. the distillation knot screen of a kind of raw oil according to claim 1, it is characterised in that the fractional distillation kettle and evaporate again Mirror mouth is respectively provided with kettle.
9. the distillation knot screen of a kind of raw oil according to claim 1, it is characterised in that the raw oil is plant Raw oil.
CN201621041909.2U 2016-09-07 2016-09-07 Distillation edulcoration device of raw oil Expired - Fee Related CN206127245U (en)

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CN201621041909.2U CN206127245U (en) 2016-09-07 2016-09-07 Distillation edulcoration device of raw oil

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Application Number Priority Date Filing Date Title
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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107525356A (en) * 2017-08-11 2017-12-29 中南林业科技大学 The steam drying of camphorwood vaporization water and essential oil and waste-heat recovery device and application method
CN108102786A (en) * 2018-01-10 2018-06-01 刘芬 A kind of essential oil method of purification and equipment
CN108404450A (en) * 2018-05-18 2018-08-17 河南莱帕克化工设备制造有限公司 Universal natural product extraction integrated production line
CN110760331A (en) * 2018-07-25 2020-02-07 中国石油天然气股份有限公司 Petroleum Distillation Plant

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107525356A (en) * 2017-08-11 2017-12-29 中南林业科技大学 The steam drying of camphorwood vaporization water and essential oil and waste-heat recovery device and application method
CN108102786A (en) * 2018-01-10 2018-06-01 刘芬 A kind of essential oil method of purification and equipment
CN108404450A (en) * 2018-05-18 2018-08-17 河南莱帕克化工设备制造有限公司 Universal natural product extraction integrated production line
CN108404450B (en) * 2018-05-18 2023-06-20 河南莱帕克化工设备制造有限公司 General type natural product draws comprehensive production line
CN110760331A (en) * 2018-07-25 2020-02-07 中国石油天然气股份有限公司 Petroleum Distillation Plant
CN110760331B (en) * 2018-07-25 2024-07-30 中国石油天然气股份有限公司 Petroleum distillation device

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20170426

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