CN102952644B - Device for extracting natural cinnamon oil - Google Patents
Device for extracting natural cinnamon oil Download PDFInfo
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- CN102952644B CN102952644B CN201210519008.XA CN201210519008A CN102952644B CN 102952644 B CN102952644 B CN 102952644B CN 201210519008 A CN201210519008 A CN 201210519008A CN 102952644 B CN102952644 B CN 102952644B
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- 239000010630 cinnamon oil Substances 0.000 title abstract 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 52
- 238000004821 distillation Methods 0.000 claims abstract description 17
- 238000004519 manufacturing process Methods 0.000 claims abstract description 12
- 235000019198 oils Nutrition 0.000 claims description 43
- 235000013372 meat Nutrition 0.000 claims description 14
- 230000015572 biosynthetic process Effects 0.000 claims description 8
- 238000009826 distribution Methods 0.000 claims description 8
- 238000000605 extraction Methods 0.000 claims description 8
- 235000019476 oil-water mixture Nutrition 0.000 claims description 8
- 230000008676 import Effects 0.000 claims description 7
- 239000010865 sewage Substances 0.000 claims description 7
- 238000001556 precipitation Methods 0.000 claims description 6
- 239000007788 liquid Substances 0.000 claims description 5
- 239000012530 fluid Substances 0.000 claims description 4
- 238000007789 sealing Methods 0.000 claims description 3
- 239000000126 substance Substances 0.000 abstract description 2
- 239000003921 oil Substances 0.000 description 65
- 238000002156 mixing Methods 0.000 description 13
- 241000522254 Cassia Species 0.000 description 11
- 239000000203 mixture Substances 0.000 description 8
- 238000009833 condensation Methods 0.000 description 7
- 230000005494 condensation Effects 0.000 description 7
- 238000000034 method Methods 0.000 description 6
- 238000004062 sedimentation Methods 0.000 description 4
- 239000002826 coolant Substances 0.000 description 3
- 238000010586 diagram Methods 0.000 description 3
- 238000001704 evaporation Methods 0.000 description 3
- 239000000284 extract Substances 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- 239000010620 bay oil Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 238000007667 floating Methods 0.000 description 2
- 238000001256 steam distillation Methods 0.000 description 2
- 241000723346 Cinnamomum camphora Species 0.000 description 1
- 235000019082 Osmanthus Nutrition 0.000 description 1
- 241000333181 Osmanthus Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 230000002026 carminative effect Effects 0.000 description 1
- 235000019504 cigarettes Nutrition 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 244000045947 parasite Species 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 238000010025 steaming Methods 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
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- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The invention discloses a device for extracting natural cinnamon oil, which relates to the technical field of manufacturing a forest chemical device. The device comprises a condenser, multiple distillation kettles and multiple oil-water separators, wherein the multiple distillation kettles are mutually connected, a re-distillation kettle is connected between the distillation kettles and the condenser, and a water pump is connected between the multiple oil-water separators and the re-distillation kettle. According to the device disclosed by the invention, the problems of low output rate and high production cost during the extracting of the cinnamon oil can be solved.
Description
Technical field
The present invention relates to forest chemical equipment manufacturing technology field, especially a kind of equipment that extracts natural meat oil of bay for the branch from xylocinnamomum and leaf.
Background technology
Chinese cassia tree is Lauraceae camphor tree aiphyllium, has another name called beautiful osmanthus.Mainly be distributed at home the damp-heat areas such as Guangxi, Guangdong, Fujian, Taiwan, Yunnan.From the branch of xylocinnamomum, leaf, all can extract perfume oil, i.e. natural meat oil of bay.Natural meat oil of bay has higher pharmaceutical use, is good carminative and stomachic.In addition, it also has the effect of expelling parasite, mildew-resistant and sterilization, is widely used in food, beverage, cigarette, medicine and other fields.
The extracting method of natural meat oil of bay is a lot, but the method for generally using is steam distillation.The equipment of common extraction by steam distillation natural meat oil of bay mainly contains three parts: 1, still kettle, 2, condenser, 3, water-and-oil separator; The flow process of extracting natural meat oil of bay is: Chinese cassia tree branch, basyleaves are put into still kettle, add again certain water, under normal pressure, be heated to boiling, water vapor steams rear formation containing the steam of oil of bay by the Oleum Cinnamomi in Chinese cassia tree branch, basyleaves in still, contains the steam of oil of bay through condenser condenses, and gained phlegma enters water-and-oil separator layering, oil reservoir is oil of bay product, in water layer, still contain a small amount of oil of bay, be milky white shape, return in still kettle; The extraction that adopts these equipment to carry out natural meat oil of bay exists oil of bay oil yield low, the problem that production cost is high.
Summary of the invention
The problem to be solved in the present invention is to provide a kind of natural meat oil of bay extraction equipment, and it is low that it can solve natural meat oil of bay extraction Oleum Cinnamomi oil yield, the problem that production cost is high.
In order to address the above problem, the technical solution used in the present invention is: this natural meat oil of bay extraction equipment includes condenser, a plurality of interconnective still kettles and water-and-oil separator; Between described still kettle and described condenser, be connected with multiple still kettle; Between described a plurality of water-and-oil separator and described multiple still kettle, be connected with water pump;
Described multiple still kettle, comprise the multiple distillation kettle that is provided with liquid outlet and fluid inlet, the described kettle inside of distilling is again provided with vapor distribution device, described vapor distribution device surrounds annular by pipe, in annular, there is cross pipes, and all pipes interconnect, and have at least one to stretch out the external pipe formation of described multiple still kettle, on the described pipe of described vapor distribution device, be distributed with a plurality of production wells; The described kettle top of distilling is again provided with tensimeter; The described autoclave body bottom that distills is again provided with sewage draining exit, in the pipeline being communicated with described sewage draining exit, is provided with wash water valve;
Described condenser, include tank body and be located at steam inlet, condensate outlet, water-in and the water outlet on described tank body, described tank inner chamber is equipped with You Liangkuaiyou center to the vortex steam flow passage of the side plate of inner rotary expansion and the upper port of these two blocks of side plates of sealing and lower port formation; The import of described vortex steam flow passage is communicated with the described steam inlet that is located at tank body upper end, and the outlet of described vortex steam flow passage is communicated with the condensate outlet being located on described tank wall; The bottom of described tank body is provided with and fills valvular drain outlet;
Described water-and-oil separator, comprise that the tank body that is provided with oil-water mixture import, oil export and water out is provided with dividing plate at described tank inner chamber, the bottom of described dividing plate becomes certain inclination angle and is fixed on the sidewall of described tank body with the bottom of described tank body, described dividing plate is separated into precipitation chamber and profit chamber two chambers by described tank inner chamber, described precipitation chamber and profit chamber, by the cross current being installed on described dividing plate, are provided with oil export in bottom, described profit chamber.
Owing to having adopted technique scheme, the present invention compared with prior art has following beneficial effect:
1, because the mixture of Oleum Cinnamomi and water passes through natural sedimentation at water-and-oil separator, oil of bay sedimentation, waterborne floating, but oil of bay is thoroughly not separated with water, also contains certain oil of bay in the water on upper strata.The mixture of the oil of bay on water-and-oil separator upper strata and water is drawn into multiple still kettle, utilizes from still pot mixing steam out and make its heating, the oil of bay in the mixture of the oil of bay on water-and-oil separator upper strata and water is evaporated again; And the multiple oil of bay of still kettle and the mixture of water be after multiple steaming, then the still pot that is extracted into an operation is reused as bottom pot water, therefore adopts multiple still kettle, and oil of bay oil yield can improve 10%, and the while also reduces production costs.
2, the present invention is owing to having used slab type spiral water-cooled tube in condenser tank body, the area that the Chinese cassia tree profit mixing steam that makes to draw through still kettle evaporation contacts with water-cooled tube in condenser tank body has increased, the corresponding time stopping in condenser tank body has also increased, thereby improved the condensation efficiency of condenser, also reduced production cost simultaneously.
3, the present invention is owing to having increased dividing plate and cross water pipe in water-and-oil separator tank body, the stroke of oil-water mixture in water-and-oil separator increased, the time of corresponding oil-water mixture in water-and-oil separator has also increased, thereby the efficiency of oily water separation is improved, thereby can reduce the quantity of using water-and-oil separator, originally at least need 15 water-and-oil separators, showed 7 to 10 of a need just enough, when raising the efficiency, reduced cost.
Accompanying drawing explanation
Fig. 1 is structural representation of the present invention.
Fig. 2 is that in the present invention, the master of condenser looks schematic diagram.
Fig. 3 is A-A sectional view in Fig. 2.
Fig. 4 is that in the present invention, the master of water-and-oil separator looks schematic diagram
Fig. 5 is B-B sectional view in Fig. 4.
Fig. 6 is that the master of multiple still kettle in the present invention looks schematic diagram
Fig. 7 is C-C sectional view in Fig. 6.
Embodiment
Below in conjunction with accompanying drawing example, structure of the present invention is described in further detail:
The natural meat oil of bay extraction equipment of Fig. 1, includes two by the interconnective still kettle 1 of pipe, and one of them still kettle 1 is connected with the steam-pipe of boiler 6; Condenser 2 and 8 are with the interconnective water-and-oil separator 3 of pipe; By pipe and two still kettles, 1 one of them multiple still kettle 4 being connected; Between multiple still kettle 4 and condenser 2, with pipe, be connected; Between 8 water-and-oil separators 3 and multiple still kettle 4, be connected with water pump 5.
Shown in Fig. 2 and Fig. 3 is the condenser 2 in the present invention, include tank body 2-1 and be located at steam inlet 2-1-1, condensate outlet 2-1-2, water-in 2-2-1 and the water outlet 2-2-2 on tank body 2-1, tank body 2-1 inner chamber is equipped with You Liangkuaiyou center to the vortex steam flow passage 2-2 of the side plate of inner rotary expansion and the upper port of these two blocks of side plates of sealing and lower port formation; The import of vortex steam flow passage 2-2 is communicated with the steam inlet 2-1-1 that is located at tank body 2-1 upper end, and the outlet of vortex steam flow passage 2-2 is communicated with the condensate outlet 2-1-2 being located on tank body 2-1 sidewall; The bottom of tank body 2-1 is provided with the drain outlet 2-1-3 that valve 2-3 is housed; The profile cross section of vortex steam flow passage 2-2 is that length is 1 meter, and wide is the rectangle of 0.02 meter; The upper head plate of vortex steam flow passage 2-2 and tank body 2-1 and bottom plate are separated into the inner chamber of tank body 2-1 eddy airstream passage and the vortex water flow passage 2-2-3 being parallel to each other, water-in 2-2-1 is located at the bottom of tank body 2-1 sidewall, and water outlet 2-2-2 is located on the upper head plate of tank body 2-1.
In extracting the production process of Oleum Cinnamomi, the Chinese cassia tree profit mixing steam drawing through multiple still kettle 4 evaporations, steam inlet 2-1-1 through tank body 2-1 enters in the vortex steam flow passage 2-2 in tank body 2-1, carry out heat exchange and obtain condensation with the water coolant of the vortex water flow passage 2-2-3 of tank body 2-1 inner chamber, the oil-water mixture that condensation obtains enters water-and-oil separator from condensate outlet 2-1-2 output; The water coolant of tank body 2-1 inner chamber is to pass into from being located at the water-in 2-2-1 of tank body 2-1 lower sidewall, through vortex water flow passage 2-2-3, the Chinese cassia tree profit mixing steam in tank body 2-1 inner chamber and vortex steam flow passage 2-2 carries out after heat exchange water coolant, from the water outlet 2-2-2 being located at the upper head plate of tank body 2-1, flow out, constantly circulation, makes Chinese cassia tree profit mixing steam obtain sufficient condensation;
Condenser used after for some time, and the valve 2-3 in sewage draining exit 2-1-3 is opened, and will in tank body 2-1, discharge by residue outside tank body 2-1; Vortex steam flow passage 2-2 is set, has increased the heat exchange contact area of Chinese cassia tree profit mixing steam and water of condensation, improved condensation effect and reduced production cost.
Shown in Fig. 4 and Fig. 5 is water-and-oil separator 3 in the present invention, the tank body 3-1 of water-and-oil separator 3 is provided with oil-water mixture import 3-1-1, water out 3-1-2, oil export 3-1-3 and oil export 3-1-4, at tank body 3-1 inner chamber, be installed by welding with dividing plate 3-3, the bottom of dividing plate 3-3 becomes the inclination angle of one 20 degree and is welded on tank body 3-1 sidewall with the bottom of tank body 3-1, dividing plate 3-3 is separated into precipitation chamber 3-4 and two chambers of profit chamber 3-5 by tank body 3-1 inner chamber, described precipitation chamber 3-4 and profit chamber 3-5 are communicated with by water pipe 3-2, water pipe 3-2 is also firmly welded on dividing plate 3-3 through dividing plate 3-3.
Owing to having increased dividing plate 3-3 and water pipe 3-2, oil-water mixture is entered tank body 3-1 from oil-water mixture import 3-1-1, separated in two chambers in tank body 3-1, stroke in tank body 3-1 has increased, corresponding profit also increased in the time of tank body 3-1, thereby the efficiency of oily water separation has been improved, can effectively reduce the quantity of using water-and-oil separator 3, prior art at least needs 15 water-and-oil separators, the present invention only need 8 just enough, when raising the efficiency, reduced cost.
Shown in Fig. 6 and Fig. 7 is multiple still kettle 4 in the present invention, include multiple distillation kettle 4-1, distill again kettle 4-1 and be provided with liquid outlet 4-1-1 and fluid inlet 4-1-3, distill again kettle 4-1 bottom and be provided with vapor distribution device 4-2, vapor distribution device 4-2 surrounds annular by 8 pipes, two tubes crisscross in annular, and all pipes interconnect formation, above pipe, offer a plurality of production wells, these pipes have one to stretch out outside multiple distillation kettle 4-1.Distill again kettle 4-1 top tensimeter 4-4 is installed; Distill again kettle 4-1 bottom and be provided with sewage draining exit 4-1-2, in the pipeline being communicated with sewage draining exit 4-1-2, be provided with wash water valve 4-3.
The mixture of Oleum Cinnamomi and water is water-and-oil separator 3 process natural sedimentations, oil of bay sedimentation, waterborne floating; But oil of bay is thoroughly not separated with water, in the water on upper strata, also contain oil of bay, the mixture of the oil of bay on water-and-oil separator 3 upper stratas and water is input in multiple distillation kettle 4-1 from fluid inlet 4-1-3, the mixing steam distilling from still kettle 1 enters in multiple distillation kettle 4-1 from delivery of steam gas-distributing pipe road 4-2, hole from delivery of steam gas-distributing pipe 4-2 steam out, mixture to oil of bay and water heats, and in the process of multiple distillation, by tensimeter 4-4 monitoring, distills again the pressure in kettle 4-1; The mixture of oil of bay and water, after evaporating again, is evaporated the oil of bay including to enter condenser 2 through liquid outlet 4-1-1, and remaining water is discharged and distilled again outside kettle 4-1 via wash water valve 4-3.
Natural meat oil of bay extracts: by Chinese cassia tree branch, basyleaves are put into respectively two still kettles 1, then the water vapor in boiler 6 is sprayed into the bottom of first still kettle 1 by steam-pipe, water vapor is by Chinese cassia tree branch in still, Oleum Cinnamomi in basyleaves steams rear formation mixing steam, mixing steam is through the bottom of second still kettle 1 of the top of first still kettle 1 input, Chinese cassia tree branch in second still kettle 1, Oleum Cinnamomi in basyleaves is also evaporated together, mixing steam is made the thermal source of distillation mixing steam through the multiple still kettle 4 of the top of second still kettle 1 input, multiple still kettle 4 tops mixing steam is out through condenser 2 condensations, after cooling, enter water-and-oil separator 3 and carry out oily water separation, after steam supply number minute, the multiple still kettle 4 of mixing steam input of separating in water-and-oil separator 3 is carried out to multiple distillation, after distillation, residual waste liquid in multiple still kettle 4 is transported to first still kettle 1, in upper once distillation once discharge afterwards of multiple distillation again while carrying out.
Claims (1)
1. a natural meat oil of bay extraction equipment, includes condenser (2), and a plurality of interconnective still kettles (1) and water-and-oil separator (3), is characterized in that: between described still kettle (1) and described condenser (2), be connected with multiple still kettle (4); Between described a plurality of water-and-oil separator (3) and described multiple still kettle (4), be connected with water pump (5);
Described multiple still kettle (4), comprise the multiple distillation kettle (4-1) that is provided with liquid outlet (4-1-1) and fluid inlet (4-1-3), described kettle (4-1) inside of distilling is again provided with vapor distribution device (4-2), described vapor distribution device (4-2) surrounds annular by pipe, in annular, there is cross pipes, and all pipes interconnect, and have at least one to stretch out the described outer pipe formation of kettle (4-1) of distilling again, on the described pipe of described vapor distribution device (4-2), be distributed with a plurality of production wells;
Described kettle (4-1) top of distilling is again provided with tensimeter (4-4); Described kettle (4-1) bottom of distilling is again provided with sewage draining exit (4-1-2), in the pipeline being communicated with described sewage draining exit (4-1-2), is provided with wash water valve (4-3);
Described condenser (2), include tank body (2-1) and be located at steam inlet (2-1-1), condensate outlet (2-1-2), water-in (2-2-1) and the water outlet (2-2-2) on described tank body (2-1), described tank body (2-1) inner chamber is equipped with You Liangkuaiyou center to the vortex steam flow passage (2-2) of the side plate of inner rotary expansion and the upper port of these two blocks of side plates of sealing and lower port formation; The import of described vortex steam flow passage (2-2) is communicated with the described steam inlet (2-1-1) that is located at tank body (2-1) upper end, and the outlet of described vortex steam flow passage (2-2) is communicated with the condensate outlet (2-1-2) being located on described tank body (2-1) sidewall; The bottom of described tank body (2-1) is provided with the drain outlet (2-1-3) that valve (2-3) is housed;
Described water-and-oil separator (3), comprise and be provided with oil-water mixture import (3-1-1), the tank body (3-1) of oil export (3-1-4) and water out (3-1-2), at described tank body (3-1) inner chamber, dividing plate (3-3) is installed, the bottom of described dividing plate (3-3) becomes certain inclination angle and is fixed on the sidewall of described tank body (3-1) with the bottom of described tank body (3-1), described dividing plate (3-3) is separated into precipitation chamber (3-4) and profit chamber (3-5) two chambers by described tank body (3-1) inner chamber, described precipitation chamber (3-4) and profit chamber (3-5) are communicated with by the water pipe (3-2) being installed on described dividing plate (3-3), in bottom, described profit chamber, be provided with oil export (3-1-3).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210519008.XA CN102952644B (en) | 2012-12-06 | 2012-12-06 | Device for extracting natural cinnamon oil |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210519008.XA CN102952644B (en) | 2012-12-06 | 2012-12-06 | Device for extracting natural cinnamon oil |
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| Publication Number | Publication Date |
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| CN102952644A CN102952644A (en) | 2013-03-06 |
| CN102952644B true CN102952644B (en) | 2014-04-23 |
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| CN201210519008.XA Active CN102952644B (en) | 2012-12-06 | 2012-12-06 | Device for extracting natural cinnamon oil |
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| CN207324119U (en) * | 2017-08-01 | 2018-05-08 | 张永森 | A kind of Distallation systm |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN87215211U (en) * | 1987-12-23 | 1988-08-31 | 湖南省津市市香料厂 | Equipment for refining fragrant oil |
| CN1133737C (en) * | 2001-09-18 | 2004-01-07 | 沈雪荣 | Cassia oil extracting process from cassia twig and leaf |
| CN2721190Y (en) * | 2003-07-02 | 2005-08-31 | 冯锦堃 | Oil and water separator |
| CN1528871A (en) * | 2003-09-26 | 2004-09-15 | 沈雪荣 | Improved method for extracting cinnamon barkoil from cinnamon branck and leaf |
| CN1232622C (en) * | 2004-03-31 | 2005-12-21 | 邱云彪 | Technique for extracting rhodamine oil |
| CN201940071U (en) * | 2011-03-03 | 2011-08-24 | 河北奥星集团药业有限公司 | Separation and collection device for traditional Chinese medicinevolatile oil |
| CN202030729U (en) * | 2011-04-28 | 2011-11-09 | 成都永泰制药化工机械厂 | Plant distillation separating device |
| CN202968523U (en) * | 2012-12-06 | 2013-06-05 | 广西京桂香料有限公司 | Natural cinnamon oil extraction equipment |
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Application publication date: 20130306 Assignee: Guangxi Tengxian Fuhua Chemical Co.,Ltd. Assignor: Guangxi Jingguo Perfume Co.,Ltd. Contract record no.: X2024980000323 Denomination of invention: Natural cinnamon oil extraction equipment Granted publication date: 20140423 License type: Common License Record date: 20240108 |