CN101721338B - Cosmetic containing Rosa setate X R. rugosa water - Google Patents

Abstract

The invention relates to a cosmetic containing Rosa setate X R. rugosa water, which is characterized by comprising the following components in percentage by weight: 11-16 percent of Rosa setate X R. rugosa water, 0.1 percent of polyamino propyl guar, 0.5-1.0 percent of beta-cyclodextrin, 5-8 percent of glycerol, 3-5 percent of alcohol and the balance of deionized water. Meanwhile, the invention also discloses a preparation method of the cosmetic. By adopting the Rosa setate X R. rugosa water which has stable performance and is abundant in various compounds of aldehyde, acid, phenol, terpene and carbonyl as the additive of the cosmetic, the cosmetic has the obvious effect in aspects of nutritionally moisturizing human skin, promoting skin metabolism, softening the skin, inhibiting pigmentation and resisting aging.

Description

A kind of cosmetics that contain Rose grievances water

Technical field

The present invention relates to a kind of cosmetics, relate in particular to a kind of cosmetics that contain Rose grievances water.

Background technology

Market research shows, consumer begins favor and buys organic cosmetics at present, and some consumers are because skin self than factors such as sensitivities, is tending towards natural, organic, safety to the demand of cosmetics; And medium injure conducting vigorous propaganda of skin to synthesis of chemicals, and demand and the market sale share of further impelling natural organic to make up article progressively increase.

Make up in the article raw materials for production at numerous natural organics, Flos Rosae Rugosae receives much concern.Flos Rosae Rugosae is the perennial evergreen or the fallen leaves property shrub of Rosaceae Rosa, and the general designation Rose in the west is Chinese then different lifting manipulation and differentiations such as Flos Rosae Rugosae, Flos Rosae Multiflorae, Mo Hong and Chinese rose are arranged.Flos Rosae Rugosae sweet in the mouth, little hardship, warm in nature; The function that liver-smoothing, qi-regulating, regulating menstruation by adjusting the flow of blood are arranged; Can be used for treating stomachache due to hyperactive liver-QI attacking the stomach, lack of appetite vomiting and nausea, menoxenia, fall and pounce on the pain of injury, its root has the effect with blood, regulating menstruation, leukorrhagia stopping, cures mainly menoxenia, leukorrhagia, traumatic injury, rheumatic arthralgia.In recent years; Both at home and abroad the Flos Rosae Rugosae effective ingredient is studied; Find to contain multiple nutritional components such as polyphenol, flavone, 18 seed amino acids (comprising 8 seed amino acids that human body is necessary) and vitamin C in the Flos Rosae Rugosae, pharmacological research shows the effect that it has stronger antioxidation, removes free radical simultaneously.

It is the cosmetics of raw material production with the Bulgarian Rose that many moneys are arranged in the market, but the Rose grievances few people shows any interest of one of main rose variety of conduct China plantation.Rose grievances (Rosa stertata * Rosa rugosa Yuet Ku) is the Hybrid of Chinese Flos Rosae Rugosae and cognate Flos Rosae Multiflorae, and the cultivation history in more than 200 year is arranged, and mainly cultivates in the Yongdeng County, Gansu the misery area because of it and gains the name.Annual late May blooms, and about about 25 days of florescence was the representative of Luzhou-flavor Flos Rosae Rugosae.Though both at home and abroad Rose grievances is possessed some special knowledge in recent years, the degree of depth is not enough, and also unmanned at present the concern with the Rose grievances is the cosmetics research and development of raw material.

Summary of the invention

Technical problem to be solved by this invention provides the cosmetics that contain Rose grievances water of a kind of Pear Power, crease-resistant, delaying decrepitude of skin and moisture-keeping efficacy.

Another technical problem to be solved by this invention provides a kind of method for preparing that contains the cosmetics of Rose grievances water.

For addressing the above problem; A kind of cosmetics that contain Rose grievances water of the present invention; It is characterized in that: these cosmetics comprise the Rose grievances water that accounts for gross weight 11～16%, 0.1% gather aminopropyl acid guanidine, 0.5～1.0% beta-schardinger dextrin-, 5～8% glycerin and 3～5% ethanol, its surplus is a deionized water.

Said Rose grievances water is meant the deionized water that adds saliferous 20% behind the roguing of cup-shaped Rose grievances flower, the calyx of deflorating by 1: 4 feed liquid quality-volume ratio, the product that contains the Flos Rosae Rugosae quintessence oil water soluble ingredient that after distillation, separation, obtains.

A kind ofly prepare the aforesaid method that contains the cosmetics of Rose grievances water, it may further comprise the steps:

(1) by each raw material of proportioning weighing;

(2) beta-schardinger dextrin-is put into deionized water, the heating for dissolving postcooling obtains lysate to room temperature;

(3) in lysate, add other raw material respectively, stir;

(4) add natural Rose grievances pigment toning to solution and be blush, obtain mixture;

(5) filtering mixt can be produced through ageing 1～February.

The present invention compared with prior art has the following advantages:

1, the present invention is the transparent uniform liquid of pale red, and is free from foreign meter, detects the requirement (referring to table 1) that meets health, sense organ and physical and chemical index by QB/T 2660-2004 " astringent ".

Table 1: each item index testing result of the present invention

2, because the present invention has adopted stable performance; Be rich in the additive (referring to table 2, table 3) of the Rose grievances water of multiple aldehydes, acids, phenols, terpenes and carbonyl complex as cosmetics, thus the present invention to the nourishing and moisturizing of human skin, promote skin metabolism, softening skin, inhibition pigmentation and defying age aspect to have remarkable result.

Table 2: Rose grievances water physical and chemical index testing result

The index project	Testing result
		Outward appearance	Colourless transparent liquid
Abnormal smells from the patient	Typical case's Rose grievances fragrance of a flower
		PH value	5.8
Proportion	0.998
		Index of refraction	1.341
Hydrargyrum	Do not have
		Arsenic	Do not have
Plumbous	Do not have

Table 3: Rose grievances aqueous vapor analysis of hplc result

Retention time (branch)	Molecular formula	The chemical compound title	Relative peak area (%)
				5.13	CH 3ON	Nitric acid methane	0.16
5.32	C 2H 6O	Ethanol	1.32
				5.46	C 2H 6S	Dimethyl sulfide	0.22
5.66	C 3H 6O	Methoxy-ethylene	0.07
				7.25	C 4H 8O 2	Ethyl acetate	0.61
7.54	C 4H 8O	2-butanone	1.1
				10.41	C 5H 10O	2 pentanone	0.05
10.63	C 5H 10O	Propione	0.23
				12.83	C 6H 12O	2-methyl-propione	0.02
14.96	C 5H 12O	The 1-amylalcohol	0.12
				15.47	C 6H 12O	Methyl-n-butyl ketone	0.01
17.60	C 8H 10	Diphenylphosphino ethane	0.01
				18.07	C 8H 10	1,4-xylene	0.02
19.99	C 8H 10	O-Dimethylbenzene	0.02
				20.97	C 6H 12O	Blatter alcohol	0.3
21.32	C 6H 14O	Hexanol	1.21
				21.95	C 7H 14O	Methyl amyl ketone	1.3
22.67	C 7H 16O	The 2-enanthol	1.02
				23.10	C 7H 12O	5-alkene-2-heptanone	0.03
23.44	C 10H 18O	2-vinyl-2,6,6-trimethyl tetrahydrochysene-2H-pyrans	0.17
				23.70	C 12H 20O 2	Linalyl acetate	0.01
24.51	C 10H 16	Myrcene	1.24
				25.69	C 10H 16	α-phellandrene	0.02
26.08	C 10H 14	2,6-dimethyl-1,3,5,7-octatetraene	0.01
				26.28	C 10H 18	2,6-dimethyl-1,6-octadiene	0.13
26.46	C 8H 16O	6-methyl-2-heptanone	0.14
				26.69	C 10H 16	1-methyl-4-(1-Methylethyl)-1, the 3-hexadiene	0.06
27.37	C 10H 16	Limonene	0.43
				27.70	C 14H 26O 2	Acetic acid-(Z)-9-laurylene ester	0.11
27.96	C 10H 16	(E)-3,7-dimethyl-1,3, the 6-sarohornene-	0.33
				28.45	C 7H 16O	Enanthol	0.79
29.03	C 10H 18O	Eucalyptole	0.35
				29.22	C 8H 14O	6-methyl-methyl heptenone	1.28
29.72	C 8H 16O	6-methyl-5-heptene-2-alcohol	0.39
				30.53	C 10H 18O 2	2-methyl-2-Hexyl 2-propenoate	0.02
32.51	C 8H 18O	2-Ethylhexyl Alcohol	0.06
				32.76	C 10H 16O	3,6-dihydro-4-methyl-2-(2-methyl isophthalic acid-acrylic)-2H-pyrans	1.28
33.03	C 10H 20O	Citronellol 1	0.07
				33.36	C 8H 14O	Cyclooctanone	0.1
34.00	C 10H 18O	2-methyl-5-(1-methyl ethylene) Hexalin	0.2
				34.53	C 6H 10	The 3-methyl isophthalic acid, the 4-pentadiene	0.34
34.65	C 10H 18O 2	Suitable-α, α-5-trimethyl-5-vinyl tetrahydrofuran-2-methanol	0.52
				35.70	C 10H 18O	Rose oxide	2.71
36.06	C 10H 18O 2	Instead-and α, α-5-trimethyl-5-vinyl tetrahydro-2-furancarbinol	0.21
				36.65	C 9H 18O	Methyl n-heptyl ketone	0.2
36.88	C 10H 18O	Suitable-rose oxide	0.53
				37.34	C 10H 18O	Linalool	29.79
37.75	C 11H 2O	2-isobutyl group-norbornane	0.02
				38.23	C 7H 8O	Benzylalcohol	3.11
39.77	C 10H 18O	Myrcenol	0.01
				40.33	C 6H 12O	2-ethyl butyraldehyde	0.01
40.64	C 8H 12O	(E)-and 6-methyl-3,5-diene-2-heptanone	0.08
				40.99	C 10H 18O	Isopulegol	0.18
41.10	C 10H 18O	Citronellal	0.04
				41.29	C 10H 16O	10-Pinen-3-ol	0.06
42.79	C 10H 18O	Terpenol	0.14
				44.23	C 10H 18O	2,6,6-3-methyl cyclohexanol-2-alkene-1-methanol	0.24
44.43	C 19H 40O	Nonadecanol	0.16
				45.01	C 10H 18O	α, α-4-trimethyl-3-cyclohexene-1-methanol	7.1
45.74	C 8H 8O 3	Wintergreen oil	0.1
				46.02	C 10H 16O	Carveol	0.13
46.36	C 10H 16	Red camphor oil	0.15
				46.53	C 10H 16O	6,6-dimethyl bicyclo-[3.1.1] hept-2-ene"-2-methanol	0.3
48.37	C 10H 18O	Nerol	0.63
				48.49	C 10H 18O	An unusually sweet smell leaf grass alcohol	0.26
48.83	C 10H 18O	Myrtanol	0.94
				49.15	C 10H 16O	4-(1-methyl ethylene)-1-cyclohexene-1-methanol	0.01
49.91	C 11H 18O 2	3,7-dimethyl-1,6-octadiene-3-alcohol formic acid esters	20.25
				50.04	C 10H 16O	Geranial	0.12
50.38	C 10H 14O	3-methyl-6-(1-methyl ethylidene)-2-cyclohexene-1-ketone	0.34
				50.70	C 15H 24	Beta-elemene	0.05
50.95	C 12H 26O	The 2-lauryl alcohol	0.63
				51.21	C 14H 30	The tetradecane	0.23
51.40	C 10H 16O	Neral	0.01
				52.04	C 9H 12O 2	The propylene glycol phenylate	1.27
52.36	C 9H 12O 2	3-phenoxy group-1-propanol	0.27
				52.83	C 10H 12O 3	Isopropyl salicylate	0.3
53.30	C 12H 22O 2	Fragrant fragrant and mellow acetas	1.24
				53.75	C 6H 12O	Instead-the 3-hexenol	0.04
54.28	C 12H 20O 2	The orange blossom acetas	0.1
				55.56	C 12H 20O 2	Geranyl acetate	0.24
57.17	C 9H 10O 2	4-vinyl-2-methoxyl group-phenol	0.07
				57.35	C 15H 24	β-farnesene	0.03
57.56	C 15H 32	Pentadecane	0.31
				57.75	C 12H 24	The 5-laurylene	0.06
58.06	C 11H 22O	The hendecanal	0.03
				58.48	C 13H 18O	Damascone	0.19
58.80	C 10H 12O 2	Eugenol	4.01
				59.56	C 6H 6O 3	5-hydroxymethyl furtural	0.06
59.87	C 11H 14O 2	Eugenol methyl ether	7.16
				60.87	C 15H 24	(E, E)-3,7,11-trimethyl-1,3,6,10-dodecane tetraene	0.09
61.35	C 14H 30	2-methyl-tridecane	0.01
				62.55	C 12H 26O	Lauryl alcohol	0.04
65.58	C 10H 12O 2	Isoeugenol	0.16
				66.47	C 11H 14O 2	The isoeugenol methyl ether	0.28

3, the present invention and the common commercially available cosmetics that do not contain Rose grievances water are compared experiment, the result shows that the present invention has tangible skin care effect.

Select 50 routine experimenters; Smear all to be massaged into fully after the present invention, the right hand back of the body smear the commercially available prod at its left hand back of the body and absorb, every day 1 time is after 30 days; Observe that experimenter's left hand butt skin is obviously lubricious than right hand butt skin, exquisiteness and the colour of skin be comparatively pale, elasticity obviously increases.

4, raw material of the present invention is easy to get, and technology is simple, is easy to suitability for industrialized production.

The specific embodiment

Reagent: gathering aminopropyl acid guanidine is U.S.'s Qi Chemical Manufacture difficult to understand; Beta-schardinger dextrin-is that the happy and auspicious Fine Chemical Co., Ltd in Wuhan produces; Glycerin is that Tianjin chemical reagent factory produces; Ethanol is that Tianjin chemical reagent factory produces.Mentioned reagent is cosmetics-stage.

1 one kinds of cosmetics that contain Rose grievances water of embodiment, contain 11% Rose grievances water, 0.1% gather aminopropyl acid guanidine, 0.5% beta-schardinger dextrin-, 5% glycerin, 3% ethanol, 80.4% deionized water.

Wherein: Rose grievances water is meant putting into distillator behind the roguing of cup-shaped Rose grievances flower, the calyx of deflorating; Add the deionized water of saliferous 20% by 1: 4 feed liquid quality-volume ratio, with flow per hour be distillating liquid 8% speed distillation 3 hours distillate; After the oil water separator that adopts Gansu Agriculture University, to produce distillate carries out oil-water separation, can obtain containing the product of Flos Rosae Rugosae quintessence oil water soluble ingredient.

Before distillation, also can use the ultrasonic cell disruption instrument assisted extraction to handle the back redistillation.

A kind of preparation contains the method for the cosmetics of Rose grievances water, and it may further comprise the steps:

(1) by each raw material of proportioning weighing;

(2) deionized water is poured in the 1000ml container, then beta-schardinger dextrin-is put into deionized water, heating in water bath in the HS6-A electric-heated thermostatic water bath that 40～60 ℃ of Huangshi medical apparatus and instruments factories produce,, dissolve postcooling fully to room temperature, obtain lysate;

(3) in lysate, add other raw material respectively, the speed with 3000 rev/mins in the accurate motor stirrer of the JJ-1 that produces in Hua Cheng Katyuan experimental apparatus factory stirs 15min, makes it even;

(4) add natural Rose grievances pigment toning to solution and be blush, obtain mixture;

(5) use the buchner funnel filtering mixt, filtrating is poured in the standard mouth conical flask cover vacuum stopper, ageing can be produced for 1～February under the room temperature.

2 one kinds of cosmetics that contain Rose grievances water of embodiment, contain 14.3% Rose grievances water, 0.1% gather aminopropyl acid guanidine, 1.0% beta-schardinger dextrin-, 7% glycerin, 3% ethanol, 74.6% deionized water.

Other is with embodiment 1.

3 one kinds of cosmetics that contain Rose grievances water of embodiment, contain 13% Rose grievances water, 0.1% gather aminopropyl acid guanidine, 0.8% beta-schardinger dextrin-, 6% glycerin, 4% ethanol, 76.1% deionized water.

Other is with embodiment 1.

4 one kinds of cosmetics that contain Rose grievances water of embodiment, contain 16% Rose grievances water, 0.1% gather aminopropyl acid guanidine, 1.0% beta-schardinger dextrin-, 8% glycerin, 5% ethanol, 69.9% deionized water.

Other is with embodiment 1.

Claims (2)

1. cosmetics that contain Rose grievances water; It is characterized in that: these cosmetics comprise the Rose grievances water that accounts for gross weight 11～16%, 0.1% gather aminopropyl acid guanidine, 0.5～1.0% beta-schardinger dextrin-, 5～8% glycerin and 3～5% ethanol, its surplus is a deionized water; Rose grievances water is meant putting into distillator behind the roguing of cup-shaped Rose grievances flower, the calyx of deflorating, and adds the deionized water of saliferous 20% by 1: 4 feed liquid quality-volume ratio, with flow per hour be distillating liquid 8% speed distillation 3 hours distillate; After the oil water separator that adopts Gansu Agriculture University, to produce distillate carries out oil-water separation, can obtain containing the product of Flos Rosae Rugosae quintessence oil water soluble ingredient.

2. one kind prepares the method that contains the cosmetics of Rose grievances water as claimed in claim 1, and it may further comprise the steps:

(1) by each raw material of proportioning weighing;

(2) beta-schardinger dextrin-is put into deionized water, the heating for dissolving postcooling obtains lysate to room temperature;

(3) in lysate, add other raw material respectively, stir;

(4) add natural Rose grievances pigment toning to solution and be blush, obtain mixture;

(5) filtering mixt can be produced through ageing 1～February.