CN101721338B - Cosmetic containing Rosa setate X R. rugosa water - Google Patents

Cosmetic containing Rosa setate X R. rugosa water Download PDF

Info

Publication number
CN101721338B
CN101721338B CN2009101176128A CN200910117612A CN101721338B CN 101721338 B CN101721338 B CN 101721338B CN 2009101176128 A CN2009101176128 A CN 2009101176128A CN 200910117612 A CN200910117612 A CN 200910117612A CN 101721338 B CN101721338 B CN 101721338B
Authority
CN
China
Prior art keywords
water
rose grievances
cosmetics
rose
grievances
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN2009101176128A
Other languages
Chinese (zh)
Other versions
CN101721338A (en
Inventor
蒋玉梅
李霁昕
毕阳
齐志国
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Gansu Agricultural University
Original Assignee
Gansu Agricultural University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Gansu Agricultural University filed Critical Gansu Agricultural University
Priority to CN2009101176128A priority Critical patent/CN101721338B/en
Publication of CN101721338A publication Critical patent/CN101721338A/en
Application granted granted Critical
Publication of CN101721338B publication Critical patent/CN101721338B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Cosmetics (AREA)

Abstract

The invention relates to a cosmetic containing Rosa setate X R. rugosa water, which is characterized by comprising the following components in percentage by weight: 11-16 percent of Rosa setate X R. rugosa water, 0.1 percent of polyamino propyl guar, 0.5-1.0 percent of beta-cyclodextrin, 5-8 percent of glycerol, 3-5 percent of alcohol and the balance of deionized water. Meanwhile, the invention also discloses a preparation method of the cosmetic. By adopting the Rosa setate X R. rugosa water which has stable performance and is abundant in various compounds of aldehyde, acid, phenol, terpene and carbonyl as the additive of the cosmetic, the cosmetic has the obvious effect in aspects of nutritionally moisturizing human skin, promoting skin metabolism, softening the skin, inhibiting pigmentation and resisting aging.

Description

A kind of cosmetics that contain Rose grievances water
Technical field
The present invention relates to a kind of cosmetics, relate in particular to a kind of cosmetics that contain Rose grievances water.
Background technology
Market research shows, consumer begins favor and buys organic cosmetics at present, and some consumers are because skin self than factors such as sensitivities, is tending towards natural, organic, safety to the demand of cosmetics; And medium injure conducting vigorous propaganda of skin to synthesis of chemicals, and demand and the market sale share of further impelling natural organic to make up article progressively increase.
Make up in the article raw materials for production at numerous natural organics, Flos Rosae Rugosae receives much concern.Flos Rosae Rugosae is the perennial evergreen or the fallen leaves property shrub of Rosaceae Rosa, and the general designation Rose in the west is Chinese then different lifting manipulation and differentiations such as Flos Rosae Rugosae, Flos Rosae Multiflorae, Mo Hong and Chinese rose are arranged.Flos Rosae Rugosae sweet in the mouth, little hardship, warm in nature; The function that liver-smoothing, qi-regulating, regulating menstruation by adjusting the flow of blood are arranged; Can be used for treating stomachache due to hyperactive liver-QI attacking the stomach, lack of appetite vomiting and nausea, menoxenia, fall and pounce on the pain of injury, its root has the effect with blood, regulating menstruation, leukorrhagia stopping, cures mainly menoxenia, leukorrhagia, traumatic injury, rheumatic arthralgia.In recent years; Both at home and abroad the Flos Rosae Rugosae effective ingredient is studied; Find to contain multiple nutritional components such as polyphenol, flavone, 18 seed amino acids (comprising 8 seed amino acids that human body is necessary) and vitamin C in the Flos Rosae Rugosae, pharmacological research shows the effect that it has stronger antioxidation, removes free radical simultaneously.
It is the cosmetics of raw material production with the Bulgarian Rose that many moneys are arranged in the market, but the Rose grievances few people shows any interest of one of main rose variety of conduct China plantation.Rose grievances (Rosa stertata * Rosa rugosa Yuet Ku) is the Hybrid of Chinese Flos Rosae Rugosae and cognate Flos Rosae Multiflorae, and the cultivation history in more than 200 year is arranged, and mainly cultivates in the Yongdeng County, Gansu the misery area because of it and gains the name.Annual late May blooms, and about about 25 days of florescence was the representative of Luzhou-flavor Flos Rosae Rugosae.Though both at home and abroad Rose grievances is possessed some special knowledge in recent years, the degree of depth is not enough, and also unmanned at present the concern with the Rose grievances is the cosmetics research and development of raw material.
Summary of the invention
Technical problem to be solved by this invention provides the cosmetics that contain Rose grievances water of a kind of Pear Power, crease-resistant, delaying decrepitude of skin and moisture-keeping efficacy.
Another technical problem to be solved by this invention provides a kind of method for preparing that contains the cosmetics of Rose grievances water.
For addressing the above problem; A kind of cosmetics that contain Rose grievances water of the present invention; It is characterized in that: these cosmetics comprise the Rose grievances water that accounts for gross weight 11~16%, 0.1% gather aminopropyl acid guanidine, 0.5~1.0% beta-schardinger dextrin-, 5~8% glycerin and 3~5% ethanol, its surplus is a deionized water.
Said Rose grievances water is meant the deionized water that adds saliferous 20% behind the roguing of cup-shaped Rose grievances flower, the calyx of deflorating by 1: 4 feed liquid quality-volume ratio, the product that contains the Flos Rosae Rugosae quintessence oil water soluble ingredient that after distillation, separation, obtains.
A kind ofly prepare the aforesaid method that contains the cosmetics of Rose grievances water, it may further comprise the steps:
(1) by each raw material of proportioning weighing;
(2) beta-schardinger dextrin-is put into deionized water, the heating for dissolving postcooling obtains lysate to room temperature;
(3) in lysate, add other raw material respectively, stir;
(4) add natural Rose grievances pigment toning to solution and be blush, obtain mixture;
(5) filtering mixt can be produced through ageing 1~February.
The present invention compared with prior art has the following advantages:
1, the present invention is the transparent uniform liquid of pale red, and is free from foreign meter, detects the requirement (referring to table 1) that meets health, sense organ and physical and chemical index by QB/T 2660-2004 " astringent ".
Table 1: each item index testing result of the present invention
Figure G2009101176128D00021
Figure G2009101176128D00031
2, because the present invention has adopted stable performance; Be rich in the additive (referring to table 2, table 3) of the Rose grievances water of multiple aldehydes, acids, phenols, terpenes and carbonyl complex as cosmetics, thus the present invention to the nourishing and moisturizing of human skin, promote skin metabolism, softening skin, inhibition pigmentation and defying age aspect to have remarkable result.
Table 2: Rose grievances water physical and chemical index testing result
The index project Testing result
Outward appearance Colourless transparent liquid
Abnormal smells from the patient Typical case's Rose grievances fragrance of a flower
PH value 5.8
Proportion 0.998
Index of refraction 1.341
Hydrargyrum Do not have
Arsenic Do not have
Plumbous Do not have
Table 3: Rose grievances aqueous vapor analysis of hplc result
Retention time (branch) Molecular formula The chemical compound title Relative peak area (%)
5.13 CH 3ON Nitric acid methane 0.16
5.32 C 2H 6O Ethanol 1.32
5.46 C 2H 6S Dimethyl sulfide 0.22
5.66 C 3H 6O Methoxy-ethylene 0.07
7.25 C 4H 8O 2 Ethyl acetate 0.61
7.54 C 4H 8O 2-butanone 1.1
10.41 C 5H 10O 2 pentanone 0.05
10.63 C 5H 10O Propione 0.23
12.83 C 6H 12O 2-methyl-propione 0.02
14.96 C 5H 12O The 1-amylalcohol 0.12
15.47 C 6H 12O Methyl-n-butyl ketone 0.01
17.60 C 8H 10 Diphenylphosphino ethane 0.01
18.07 C 8H 10 1,4-xylene 0.02
19.99 C 8H 10 O-Dimethylbenzene 0.02
20.97 C 6H 12O Blatter alcohol 0.3
21.32 C 6H 14O Hexanol 1.21
21.95 C 7H 14O Methyl amyl ketone 1.3
22.67 C 7H 16O The 2-enanthol 1.02
23.10 C 7H 12O 5-alkene-2-heptanone 0.03
23.44 C 10H 18O 2-vinyl-2,6,6-trimethyl tetrahydrochysene-2H-pyrans 0.17
23.70 C 12H 20O 2 Linalyl acetate 0.01
24.51 C 10H 16 Myrcene 1.24
25.69 C 10H 16 α-phellandrene 0.02
26.08 C 10H 14 2,6-dimethyl-1,3,5,7-octatetraene 0.01
26.28 C 10H 18 2,6-dimethyl-1,6-octadiene 0.13
26.46 C 8H 16O 6-methyl-2-heptanone 0.14
26.69 C 10H 16 1-methyl-4-(1-Methylethyl)-1, the 3-hexadiene 0.06
27.37 C 10H 16 Limonene 0.43
27.70 C 14H 26O 2 Acetic acid-(Z)-9-laurylene ester 0.11
27.96 C 10H 16 (E)-3,7-dimethyl-1,3, the 6-sarohornene- 0.33
28.45 C 7H 16O Enanthol 0.79
29.03 C 10H 18O Eucalyptole 0.35
29.22 C 8H 14O 6-methyl-methyl heptenone 1.28
29.72 C 8H 16O 6-methyl-5-heptene-2-alcohol 0.39
30.53 C 10H 18O 2 2-methyl-2-Hexyl 2-propenoate 0.02
32.51 C 8H 18O 2-Ethylhexyl Alcohol 0.06
32.76 C 10H 16O 3,6-dihydro-4-methyl-2-(2-methyl isophthalic acid-acrylic)-2H-pyrans 1.28
33.03 C 10H 20O Citronellol 1 0.07
33.36 C 8H 14O Cyclooctanone 0.1
34.00 C 10H 18O 2-methyl-5-(1-methyl ethylene) Hexalin 0.2
34.53 C 6H 10 The 3-methyl isophthalic acid, the 4-pentadiene 0.34
34.65 C 10H 18O 2 Suitable-α, α-5-trimethyl-5-vinyl tetrahydrofuran-2-methanol 0.52
35.70 C 10H 18O Rose oxide 2.71
36.06 C 10H 18O 2 Instead-and α, α-5-trimethyl-5-vinyl tetrahydro-2-furancarbinol 0.21
36.65 C 9H 18O Methyl n-heptyl ketone 0.2
36.88 C 10H 18O Suitable-rose oxide 0.53
37.34 C 10H 18O Linalool 29.79
37.75 C 11H 2O 2-isobutyl group-norbornane 0.02
38.23 C 7H 8O Benzylalcohol 3.11
39.77 C 10H 18O Myrcenol 0.01
40.33 C 6H 12O 2-ethyl butyraldehyde 0.01
40.64 C 8H 12O (E)-and 6-methyl-3,5-diene-2-heptanone 0.08
40.99 C 10H 18O Isopulegol 0.18
41.10 C 10H 18O Citronellal 0.04
41.29 C 10H 16O 10-Pinen-3-ol 0.06
42.79 C 10H 18O Terpenol 0.14
44.23 C 10H 18O 2,6,6-3-methyl cyclohexanol-2-alkene-1-methanol 0.24
44.43 C 19H 40O Nonadecanol 0.16
45.01 C 10H 18O α, α-4-trimethyl-3-cyclohexene-1-methanol 7.1
45.74 C 8H 8O 3 Wintergreen oil 0.1
46.02 C 10H 16O Carveol 0.13
46.36 C 10H 16 Red camphor oil 0.15
46.53 C 10H 16O 6,6-dimethyl bicyclo-[3.1.1] hept-2-ene"-2-methanol 0.3
48.37 C 10H 18O Nerol 0.63
48.49 C 10H 18O An unusually sweet smell leaf grass alcohol 0.26
48.83 C 10H 18O Myrtanol 0.94
49.15 C 10H 16O 4-(1-methyl ethylene)-1-cyclohexene-1-methanol 0.01
49.91 C 11H 18O 2 3,7-dimethyl-1,6-octadiene-3-alcohol formic acid esters 20.25
50.04 C 10H 16O Geranial 0.12
50.38 C 10H 14O 3-methyl-6-(1-methyl ethylidene)-2-cyclohexene-1-ketone 0.34
50.70 C 15H 24 Beta-elemene 0.05
50.95 C 12H 26O The 2-lauryl alcohol 0.63
51.21 C 14H 30 The tetradecane 0.23
51.40 C 10H 16O Neral 0.01
52.04 C 9H 12O 2 The propylene glycol phenylate 1.27
52.36 C 9H 12O 2 3-phenoxy group-1-propanol 0.27
52.83 C 10H 12O 3 Isopropyl salicylate 0.3
53.30 C 12H 22O 2 Fragrant fragrant and mellow acetas 1.24
53.75 C 6H 12O Instead-the 3-hexenol 0.04
54.28 C 12H 20O 2 The orange blossom acetas 0.1
55.56 C 12H 20O 2 Geranyl acetate 0.24
57.17 C 9H 10O 2 4-vinyl-2-methoxyl group-phenol 0.07
57.35 C 15H 24 β-farnesene 0.03
57.56 C 15H 32 Pentadecane 0.31
57.75 C 12H 24 The 5-laurylene 0.06
58.06 C 11H 22O The hendecanal 0.03
58.48 C 13H 18O Damascone 0.19
58.80 C 10H 12O 2 Eugenol 4.01
59.56 C 6H 6O 3 5-hydroxymethyl furtural 0.06
59.87 C 11H 14O 2 Eugenol methyl ether 7.16
60.87 C 15H 24 (E, E)-3,7,11-trimethyl-1,3,6,10-dodecane tetraene 0.09
61.35 C 14H 30 2-methyl-tridecane 0.01
62.55 C 12H 26O Lauryl alcohol 0.04
65.58 C 10H 12O 2 Isoeugenol 0.16
66.47 C 11H 14O 2 The isoeugenol methyl ether 0.28
3, the present invention and the common commercially available cosmetics that do not contain Rose grievances water are compared experiment, the result shows that the present invention has tangible skin care effect.
Select 50 routine experimenters; Smear all to be massaged into fully after the present invention, the right hand back of the body smear the commercially available prod at its left hand back of the body and absorb, every day 1 time is after 30 days; Observe that experimenter's left hand butt skin is obviously lubricious than right hand butt skin, exquisiteness and the colour of skin be comparatively pale, elasticity obviously increases.
4, raw material of the present invention is easy to get, and technology is simple, is easy to suitability for industrialized production.
The specific embodiment
Reagent: gathering aminopropyl acid guanidine is U.S.'s Qi Chemical Manufacture difficult to understand; Beta-schardinger dextrin-is that the happy and auspicious Fine Chemical Co., Ltd in Wuhan produces; Glycerin is that Tianjin chemical reagent factory produces; Ethanol is that Tianjin chemical reagent factory produces.Mentioned reagent is cosmetics-stage.
1 one kinds of cosmetics that contain Rose grievances water of embodiment, contain 11% Rose grievances water, 0.1% gather aminopropyl acid guanidine, 0.5% beta-schardinger dextrin-, 5% glycerin, 3% ethanol, 80.4% deionized water.
Wherein: Rose grievances water is meant putting into distillator behind the roguing of cup-shaped Rose grievances flower, the calyx of deflorating; Add the deionized water of saliferous 20% by 1: 4 feed liquid quality-volume ratio, with flow per hour be distillating liquid 8% speed distillation 3 hours distillate; After the oil water separator that adopts Gansu Agriculture University, to produce distillate carries out oil-water separation, can obtain containing the product of Flos Rosae Rugosae quintessence oil water soluble ingredient.
Before distillation, also can use the ultrasonic cell disruption instrument assisted extraction to handle the back redistillation.
A kind of preparation contains the method for the cosmetics of Rose grievances water, and it may further comprise the steps:
(1) by each raw material of proportioning weighing;
(2) deionized water is poured in the 1000ml container, then beta-schardinger dextrin-is put into deionized water, heating in water bath in the HS6-A electric-heated thermostatic water bath that 40~60 ℃ of Huangshi medical apparatus and instruments factories produce,, dissolve postcooling fully to room temperature, obtain lysate;
(3) in lysate, add other raw material respectively, the speed with 3000 rev/mins in the accurate motor stirrer of the JJ-1 that produces in Hua Cheng Katyuan experimental apparatus factory stirs 15min, makes it even;
(4) add natural Rose grievances pigment toning to solution and be blush, obtain mixture;
(5) use the buchner funnel filtering mixt, filtrating is poured in the standard mouth conical flask cover vacuum stopper, ageing can be produced for 1~February under the room temperature.
2 one kinds of cosmetics that contain Rose grievances water of embodiment, contain 14.3% Rose grievances water, 0.1% gather aminopropyl acid guanidine, 1.0% beta-schardinger dextrin-, 7% glycerin, 3% ethanol, 74.6% deionized water.
Other is with embodiment 1.
3 one kinds of cosmetics that contain Rose grievances water of embodiment, contain 13% Rose grievances water, 0.1% gather aminopropyl acid guanidine, 0.8% beta-schardinger dextrin-, 6% glycerin, 4% ethanol, 76.1% deionized water.
Other is with embodiment 1.
4 one kinds of cosmetics that contain Rose grievances water of embodiment, contain 16% Rose grievances water, 0.1% gather aminopropyl acid guanidine, 1.0% beta-schardinger dextrin-, 8% glycerin, 5% ethanol, 69.9% deionized water.
Other is with embodiment 1.

Claims (2)

1. cosmetics that contain Rose grievances water; It is characterized in that: these cosmetics comprise the Rose grievances water that accounts for gross weight 11~16%, 0.1% gather aminopropyl acid guanidine, 0.5~1.0% beta-schardinger dextrin-, 5~8% glycerin and 3~5% ethanol, its surplus is a deionized water; Rose grievances water is meant putting into distillator behind the roguing of cup-shaped Rose grievances flower, the calyx of deflorating, and adds the deionized water of saliferous 20% by 1: 4 feed liquid quality-volume ratio, with flow per hour be distillating liquid 8% speed distillation 3 hours distillate; After the oil water separator that adopts Gansu Agriculture University, to produce distillate carries out oil-water separation, can obtain containing the product of Flos Rosae Rugosae quintessence oil water soluble ingredient.
2. one kind prepares the method that contains the cosmetics of Rose grievances water as claimed in claim 1, and it may further comprise the steps:
(1) by each raw material of proportioning weighing;
(2) beta-schardinger dextrin-is put into deionized water, the heating for dissolving postcooling obtains lysate to room temperature;
(3) in lysate, add other raw material respectively, stir;
(4) add natural Rose grievances pigment toning to solution and be blush, obtain mixture;
(5) filtering mixt can be produced through ageing 1~February.
CN2009101176128A 2009-11-20 2009-11-20 Cosmetic containing Rosa setate X R. rugosa water Expired - Fee Related CN101721338B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2009101176128A CN101721338B (en) 2009-11-20 2009-11-20 Cosmetic containing Rosa setate X R. rugosa water

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2009101176128A CN101721338B (en) 2009-11-20 2009-11-20 Cosmetic containing Rosa setate X R. rugosa water

Publications (2)

Publication Number Publication Date
CN101721338A CN101721338A (en) 2010-06-09
CN101721338B true CN101721338B (en) 2012-08-22

Family

ID=42443297

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2009101176128A Expired - Fee Related CN101721338B (en) 2009-11-20 2009-11-20 Cosmetic containing Rosa setate X R. rugosa water

Country Status (1)

Country Link
CN (1) CN101721338B (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106798694A (en) * 2017-02-17 2017-06-06 中国科学院近代物理研究所 A kind of preparation method of bitter water rose toner
CN114983899A (en) * 2022-07-05 2022-09-02 陇南市祥宇油橄榄开发有限责任公司 Plant type scrub cream and preparation method thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1563311A (en) * 2004-03-31 2005-01-12 邱云彪 Technique for extracting rhodamine oil
CN101402900A (en) * 2008-11-16 2009-04-08 兰州大学 Method for extracting rhodamine toner oil and line products from brackish water rose

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1563311A (en) * 2004-03-31 2005-01-12 邱云彪 Technique for extracting rhodamine oil
CN101402900A (en) * 2008-11-16 2009-04-08 兰州大学 Method for extracting rhodamine toner oil and line products from brackish water rose

Also Published As

Publication number Publication date
CN101721338A (en) 2010-06-09

Similar Documents

Publication Publication Date Title
KR100910747B1 (en) Herb medicine mixture extracts having antifungal, antiacne, skin calming, moisturizing and sebum controlling activities
Santos et al. Chemical composition, antioxidant activity and thermal analysis of oil extracted from favela (Cnidoscolus quercifolius) seeds
CN101721338B (en) Cosmetic containing Rosa setate X R. rugosa water
KR101326556B1 (en) Cosmetic composition for ultraviolet-proof containing the extract of sanguisorba officinalis and v. linariaefolia
CN103113991A (en) Preparation method of ginger flower peakodor
Adeyemo et al. Antioxidant activity, total phenolic contents and functional group identification of leaf extracts among lemongrass (Cymbopogon citratus) accessions
KR101009904B1 (en) Antinflammatory composition comprising natural plant extract
CN104982553A (en) Health-maintenance margarine
KR101126984B1 (en) Cosmetic composition comprising extract of taxodium distichum and viburnum sargentii for sterile for whitening and antioxdiant
CN101721339B (en) Cosmetic containing Rosa setate X R. rugosa wax
Eze-Steven et al. Evaluation of antioxidant potential of Monodora myristica (African Nutmeg)
Abera Extraction and physicochemical analysis of essential oils in lemongrass leaves grown in Arbaminch, Ethiopia
CN101721337B (en) Cosmetic containing Rosa setate X R. rugosa extract
JP2022167197A (en) Hyaluronic Acid Production Promoter, Epidermal Hyaluronic Acid Production Promoter, and Dermal Hyaluronic Acid Production Promoter
JP5896618B2 (en) Melanin production inhibitor
Chiru Phytochemical study of Centaurea cyanus L
JP5820220B2 (en) Dispersion method of nymphaeols
Nwanisobi et al. FATTY ACID COMPOSITION OF FICUS SUR SEED OIL (moraceae) OBTAINED IN ENUGU STATE, NIGERIA.
Abd Rashid et al. Evaluation of Butterfly Pea Flowers for Antioxidant Activity and its Potential as Antioxidant Soap
Gonçalves et al. Beneficial properties of olive tree leaves concerning personal care ingredients: Herbal tincture.
CN113116786B (en) Anti-aging moisturizing cosmetic prepared from August melon and efficacy evaluation method thereof
Ghortale et al. Design And Evaluation of Lemongrass Lotion for Skin Nourishment
Singh et al. Evaluation of Guava (Psidium Guajava L.) Leaves of Various Varieties For Preparing Leaf Tea
KR20050117975A (en) Natural antioxidant composition with an extract of chinese parasol tree and manufacturing method thereof
TW201008505A (en) Bioactive peanut sprout powders bearing lifespan extension and anti-oxidative activities, its preparation, composition and products containing the active compounds

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20120822

Termination date: 20161120