CN1059929A - Method with preparing edible perfume with wild star-anise - Google Patents
Method with preparing edible perfume with wild star-anise Download PDFInfo
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- CN1059929A CN1059929A CN 90107883 CN90107883A CN1059929A CN 1059929 A CN1059929 A CN 1059929A CN 90107883 CN90107883 CN 90107883 CN 90107883 A CN90107883 A CN 90107883A CN 1059929 A CN1059929 A CN 1059929A
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Abstract
With the method for preparing edible perfume with wild star-anise, relate to and extract the method that vegetables oil is made spices, it is the method for a kind of novel flavouring agent of development of raw materials that purpose is to provide with wild anise.Method of the present invention is after earlier the anistree mature fruit in open country being pulverized, by distilling with vapor distillation or direct heating.To distillate part then carries out oily water separation and obtains the product essential oil.The essential oil of producing with this law has peat-reek, can be used as novel fragrance, and edible safety, nontoxic helps improving flavour of food products, enriches people's life.
Description
The present invention relates to crude vegetal, specifically, relate to the method for anistree plant extract spices from the open country.
Wild anistree (Illicium Simonsii Maxim) is a kind of Winteraceae Illicium on plant classification, mainly is distributed in the northwestward, Guizhou Province.Be commonly called as the mountain anise in the growth area, be evergreen shrubs, high 1-3 rice, complete stool has fragrance, and its fruit, leaf all contain volatile plant oil.Food Sanitation Inst., Guizhou once used gas chromatography-mass spectrum-robot calculator coupling technique (GC-MS-DS) to analyze wild anise tree volatile oil, detected 47 kinds of compositions in the oil, wherein based on monoterpenes compound limonene and myrcene, accounted for 73.4% and 9.9% respectively; This institute has carried out the toxic research of wild anise, studies on acute toxicity and mutagenesis test, teratogenesis test again simultaneously, also the edible intake of place of production crowd is investigated, conclusive evidence is wild anistree nontoxic to human body in a certain amount of scope, can be used as flavouring agent.In the area that wild anistree growth distribution is arranged, the masses normal directly with it, halogen food or mix red chilly powder and dip in material salts down.Yet owing to wild anise is very similar to leaf, the fruit of deleterious lanceolata fennel (being commonly called as " thick grass "), unfamiliar people is difficult to identification, and a lot of areas people, animal all once took place eat poisoning even dead accident by mistake.Up to now, be that the method that raw material is made flavouring agent is not seen in report as yet with wild anise, also never sold wild anistree converted products on the market.
Provide a kind of is the method for a kind of novel flavouring agent of development of raw materials with wild anise to being of ending of the present invention, both can avoid people to poison because of eating by mistake, can transport this flavouring agent to various places easily again, enriches people's life.
For achieving the above object, the method that the present invention takes is earlier mellow fruit to be distilled after pre-treatment is pulverized, and will distillate component then and carry out oily water separation and obtain the product essential oil.
Still-process can adopt the distillation of vapor distillation or direct heating, and must be to raw materials pretreatment before the distillation: soon raw material pulverizes, and the meal of gained is soaked in water.
When using vapor distillation, be 4.0 * 10 with pressure
4Handkerchief-9.0 * 10
4The steam of handkerchief feeds and soaks 2-4 hour material time, system's distillation under normal pressure or decompression.During underpressure distillation, control vacuum tightness is 2.67 * 10
4In the handkerchief.Distillate part and secondary and steam bubble by flowing into water-and-oil separator behind the condensing tube condensation, till essential oil no longer distillates.Because underpressure distillation essential oil yield is lower, so adopt air distillation usually.
When distilling with direct heating, earlier the material that soaks is moved in the steam bottle, directly with low-temperature prewarming to boiling, controlled temperature is 98 ℃ then, and distillation is 3-4 hour under normal pressure, distillates part and steam and passes through condensing tube condensation, flow into the water-and-oil separator of below, till essential oil distillates fully.
Profit miscellany layering in water-and-oil separator that distillation obtains, available top and bottom process is separated, and also available suction pipe is stored in brown ampoule or the bottle carefully from upper strata sucking-off essential oil, is sealed in then under the low temperature to place, and often places 4 ℃ environment.
The essential oil of producing with this law is colourless or faint yellow, runny liquid, and peat-reek is arranged, and can be used as a kind of novel fragrance, and edible safety is nontoxic, helps improving flavour of food products; Also can be used as the production makeup, enrich people's life.
Following embodiment can further specify the present invention:
Embodiment 1: wild Fructus Anisi Stellati dried fruit is ground into meal in baking under 60 ℃ the low temperature after 2-3 hour.In the matrass, water in advance is soaked and was made it whole infiltrations in 3 hours at the bottom of the title 100 gram meal immigration gardens.Sample after the immersion is inserted steam bottle, and to boiling, controlled temperature is protected the skill slight boiling condition for 98 ℃ again with low-temperature heat, and the fraction that steams cools off with cold water by prolong, in the water-and-oil separator that phlegma is connect below flowing into.Direct heating 2 hours 30 minutes is till distillating fully to the essential oil distillate.Distillate is layering in water-and-oil separator, with syringe or suction pipe essential oil is moved in the ampoule carefully to seal, and is stored in the water tank under 4 ℃, makes essential oil 0.938 gram altogether.
Embodiment 2: The pretreatment is with embodiment 1.Sample after the immersion is inserted steam bottle, inserts a steam duct and directly feed steam in sample, sample is heated to boils and keeps slight boiling condition, distillates component and cools off with cold water by prolong, in the water-and-oil separator that phlegma is connect below flowing into.Fed steam 3 hours, till no longer distillating to distillate.Phlegma suction pipe sucking-off seals in the immigration ampoule, places down in 4 ℃, obtains essential oil 0.7 gram.
Embodiment 3: The pretreatment is with embodiment 1.Sample after the immersion is inserted steam bottle, inserts a steam duct in sample, steam is fed in the sample to boiling, and keep slight boiling condition, and vapor pressure is 4.736 * 10
4Handkerchief (gauge pressure).The steam bottle below connects a prolong, connects an airtight distillate receiving flask again.Total system sealing back is connected with a vacuum pump.Controlled temperature is 80 ℃ during distillation, and under reduced pressure (vacuum tightness is 2.6 * 10 in control
4Handkerchief) distillation is 2 hours 30 minutes, then with the essential oil sucking-off in the distillate, preserves with method with embodiment 1, obtains essential oil 0.9 gram.
Claims (7)
1, with the wild anistree method of extracting flavouring agent, it is characterized in that earlier mellow fruit being distilled after pre-treatment, it distillates component and carries out oily water separation and obtain essential oil.
2, in accordance with the method for claim 1, it is characterized in that the fruit pre-treatment as raw material is that its meal that pulverizes the back gained was soaked in water 3 hours, make it to soak into.
3, in accordance with the method for claim 1, it is characterized in that still-process can adopt vapor distillation or direct heating distillation, vapor distillation can carry out under normal pressure or under the decompression again.
4, in accordance with the method for claim 3, vapor pressure is 4.0 * 10 when it is characterized in that adopting vapor distillation
4Handkerchief-9.0 * 10
4Handkerchief, distillation time are 2-4 hour.
5, in accordance with the method for claim 4, when it is characterized in that adopting the vapor distillation under the decompression, vacuum degree control is 2.67 * 10
4In the handkerchief.
6, in accordance with the method for claim 3, it is characterized in that adopting direct heating when distillation, raw material be directly with low-temperature heat to boiling, controlled temperature is 98 ℃, distillation is 3-4 hour under normal pressure.
7, in accordance with the method for claim 1, it is characterized in that the component that distillates that obtains by distillation is an oil-water mixture, utilize water-and-oil separator to make it layering, can directly separate or with the suction pipe essential oil on sucking-off upper strata carefully.After should sealing, stores at low temperatures essential oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 90107883 CN1059929A (en) | 1990-09-18 | 1990-09-18 | Method with preparing edible perfume with wild star-anise |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 90107883 CN1059929A (en) | 1990-09-18 | 1990-09-18 | Method with preparing edible perfume with wild star-anise |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1059929A true CN1059929A (en) | 1992-04-01 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 90107883 Pending CN1059929A (en) | 1990-09-18 | 1990-09-18 | Method with preparing edible perfume with wild star-anise |
Country Status (1)
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| CN (1) | CN1059929A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1086948C (en) * | 1998-01-24 | 2002-07-03 | 曾福成 | Process for preparing medicine for treating burn |
| CN106422407A (en) * | 2016-11-15 | 2017-02-22 | 重庆市梁平张鸭子食品有限公司 | Method for purifying and extracting spices |
-
1990
- 1990-09-18 CN CN 90107883 patent/CN1059929A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1086948C (en) * | 1998-01-24 | 2002-07-03 | 曾福成 | Process for preparing medicine for treating burn |
| CN106422407A (en) * | 2016-11-15 | 2017-02-22 | 重庆市梁平张鸭子食品有限公司 | Method for purifying and extracting spices |
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| PB01 | Publication | ||
| C03 | Withdrawal of patent application (patent law 1993) | ||
| WD01 | Invention patent application deemed withdrawn after publication |