CN106381227A - Extraction method of Fructus Momordicae sweet component, and application of Fructus Momordicae sweet component in tobacco product - Google Patents
Extraction method of Fructus Momordicae sweet component, and application of Fructus Momordicae sweet component in tobacco product Download PDFInfo
- Publication number
- CN106381227A CN106381227A CN201610801728.3A CN201610801728A CN106381227A CN 106381227 A CN106381227 A CN 106381227A CN 201610801728 A CN201610801728 A CN 201610801728A CN 106381227 A CN106381227 A CN 106381227A
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- China
- Prior art keywords
- fructus momordicae
- momordicae sweet
- methanol
- extracting method
- sweet component
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Confectionery (AREA)
Abstract
The invention relates to an extraction method of a Fructus Momordicae sweet component. The extraction method comprises the following steps: crushing dried Fructus Momordicae, and sieving the crushed dried Fructus Momordicae; adding the crushed dried Fructus Momordicae to a solvent, and carrying out ultrasonic extraction under an ultrasonic power of 300-500 W for 20-100 min, wherein the solvent is 100 DEG C boiling water, 70 DEG C hot water, methanol, anhydrous ethanol or 75% ethanol, and a material-to-liquid ratio of 1:15 to 1:35 g/mL; carrying out centrifuge and impurity removal treatment; and concentrating the obtained component, and carrying out vacuum drying to obtain the Fructus Momordicae sweet component product. The invention also provides an application of the Fructus Momordicae sweet component product in a tobacco product. The Fructus Momordicae sweet component product is added to the tobacco product, and the Fructus Momordicae sweet component product and a tobacco base undergo a complex chemical reaction, so the smoke fragrance and the mouthfeel are enriched, and acidic components are generated to neutralize alkaline components in the smoke in order to realize smooth smoke and irritation reduction.
Description
Technical field
The invention belongs to field of biology, it is related to a kind of Fructus Momordicae, specifically the carrying of a kind of Fructus Momordicae sweet ingredient
Take method and the application in tobacco product.
Background technology
The Fructus Momordicae source place of production is China, and advantageous natural resourcess make China's Fructus Momordicae and Fructus Momordicae sweet ingredient in state
Come out top on market in border.Fructus Momordicae belongs to the distinctive health-related medical material of China, and Momordica-Glycosides are wherein main sweet taste one-tenth
Point, but it is not belonging to glucide, and therefore it is the ideal type sweeting agent of the patients such as obesity, hyperlipidemia, hyperglycemia, its tool
Have aromatic odour, low in calories, sugariness is high, heat stability is good, good water solubility the features such as.Additionally, it is not susceptible to go mouldy, belong to non-
Fermentation class material, be commonly used for beverage, medicine, in food production.
Cigarette smoke is a kind of extremely complex mixture, is by result of combustion of tobacco, cracking and steaming during cigarette smoking
Evaporate and produce.Smoking is always one of much-talked-about topic of concern with health problem, and tobacco industry does one's utmost to reduce flue gas at present
Coal-tar middle oil content, so can lead to the weakening of the loss of fragrance and mouthfeel in flue gas.
Content of the invention
For technical problem of the prior art, the invention provides a kind of extracting method of Fructus Momordicae sweet ingredient and
Application in tobacco product, the described extracting method of this Fructus Momordicae sweet ingredient and the application in tobacco product will solve
The content reducing tar in Nicotiana tabacum L. of the prior art can lead to the technical problem of the loss of fragrance and mouthfeel weakening in flue gas.
The invention provides a kind of extracting method of Fructus Momordicae sweet ingredient, comprise the steps：
1) first arhat dried fruitss are carried out pulverizing, sieve；
2) the arhat dried fruitss after pulverizing are added in solvent and carry out ultrasonic extraction, described solvent be 100 DEG C boiling water, 70 DEG C
Hot water, methanol, dehydrated alcohol or ethanol that mass percent concentration is 75%；Solid-liquid ratio：1:15 g/mL-1:35 g/
mL；Ultrasonic power：300W-500W；Extraction time：20 min-100min；
3) then carry out centrifugation and remove impurity process；
4) finally concentrated, vacuum drying, obtained Fructus Momordicae sweet taste component product.
Further, described solvent is 100 DEG C of boiling water, 70 DEG C of hot water, methanol, dehydrated alcohol or quality hundred
The ethanol that specific concentration is 75%, ultrasonic power is divided to be 500W；Solid-liquid ratio is 1:20 g/mL；Extraction time is 40 min.
Further, described solvent is methanol；Ultrasonic power is 300 W-500W；Solid-liquid ratio is 1:20 g/mL；Leaching
The time that carries is 40 min.
Further, described solvent is methanol；Ultrasonic power is 500W；Solid-liquid ratio is 1:15-1:35 g/mL；Leaching
The time that carries is 40 min.
Further, described solvent is methanol；Ultrasonic power is 500W；Solid-liquid ratio is 1:25 g/mL；Extraction time
For 20-100 min.
Present invention also offers the Fructus Momordicae sweet taste component product of above-mentioned method preparation.
Present invention also offers application in tobacco product for the Fructus Momordicae sweet taste component product that obtains of said method.
Further, described tobacco product is Medicated cigarette, cigar, tobacco shred or redried leaf tobacco.
The present invention with Fructus Momordicae as raw material, extract to the sweet ingredient in Fructus Momordicae by the method using ultrasonic wave added,
The Fructus Momordicae sweet ingredient that the present invention is obtained is dissolved in dehydrated alcohol, is placed in larynx spray bottle, and Fructus Momordicae sweet taste is become
Divide in uniformly sprinkling and tobacco shred, dry moisture, make cigarette, finally carry out sensory evaluating smoking's identification.
Described sensory evaluating smoking's authentication method is the sense organ reviewer composition evaluation group of more than 20 length of smoking 2-3,
Using secretly commenting method, according to makings fragrant and sweet in Medicated cigarette, sweet taste amount, the thoroughly property sent out, miscellaneous QI, sweet concentration, strength, fine and smooth degree, one-tenth
Group's property, zest, dry sensation, residual and Hui Tian carry out tasting marking.
Accurately and reliably, and extraction ratio is higher, has use value for cigarette Fructus Momordicae sweet taste component extracting method of the present invention.To carry
The Fructus Momordicae sweet ingredient taking is applied to tobacco product, and it occurs complex chemical reaction, abundant cigarette when burning and sucking with Nicotiana tabacum L. substrate
Gas fragrance and mouthfeel, can generate acid ingredient simultaneously, can neutralize flue gas neutral and alkali composition, play submissive flue gas, reduce stimulation
Effect.
The present invention compares with prior art, and its technological progress is significant.The Fructus Momordicae sweet ingredient of the present invention can change
The mouthfeel of kind Nicotiana tabacum L., makes one to feel to be in a cheerful frame of mind, and the height of its content in Nicotiana tabacum L. largely affects cigarette quality.
Specific embodiment
Below by specific embodiment, the present invention is expanded on further, but is not intended to limit the present invention.
Embodiment 1
A kind of ultrasonically auxiliary extracting method of Fructus Momordicae sweet ingredient and the application in tobacco product, ultrasonically auxiliary extracting method
For：
Solvent：100 DEG C of boiling water, 70 DEG C of hot water, methanol, dehydrated alcohol, 75% ethanol；
Ultrasonic power： 500W；
Throw material liquid ratio： 1:20 g/mL；
Extraction time： 40 min
A kind of above-mentioned ultrasonically auxiliary extracting method of Fructus Momordicae sweet ingredient and the application in tobacco product, its ultrasonic wave added
Extracting method is：
First arhat dried fruitss are carried out pulverizing, look over so as to check（80 mesh）；
Then carry out ultrasonic assistant extraction；
Then carry out centrifugation and remove impurity etc. to process；
Finally concentrated, vacuum drying, obtained Fructus Momordicae sweet taste component product.
The method of above-mentioned gained, the extraction ratio of Fructus Momordicae sweet ingredient is 53.3-66.19%
Embodiment 2
A kind of ultrasonically auxiliary extracting method of Fructus Momordicae sweet ingredient and the application in tobacco product, ultrasonically auxiliary extracting method
For：
Solvent：Methanol；
Ultrasonic power：300 W-500W；
Throw material liquid ratio： 1:20 g/mL；
Extraction time： 40 min
A kind of above-mentioned ultrasonically auxiliary extracting method of Fructus Momordicae sweet ingredient and the application in tobacco product, its ultrasonic wave added
Extracting method is：
First arhat dried fruitss are carried out pulverizing, look over so as to check（80 mesh）；
Then carry out ultrasonic assistant extraction；
Then carry out centrifugation and remove impurity etc. to process；
Finally concentrated, vacuum drying, obtained Fructus Momordicae sweet taste component product.
The method of above-mentioned gained, the extraction ratio of Fructus Momordicae sweet ingredient is 58.14-76.44%.
Embodiment 3
A kind of ultrasonically auxiliary extracting method of Fructus Momordicae sweet ingredient and the application in tobacco product, ultrasonically auxiliary extracting method
For：
Solvent：Methanol；
Ultrasonic power： 500W ；
Throw material liquid ratio： 1:15-1:35 g/mL；
Extraction time： 40 min
A kind of above-mentioned ultrasonically auxiliary extracting method of Fructus Momordicae sweet ingredient and the application in tobacco product, its ultrasonic wave added
Extracting method is：
First arhat dried fruitss are carried out pulverizing, look over so as to check（80 mesh）；
Then carry out ultrasonic assistant extraction；
Then carry out centrifugation and remove impurity etc. to process；
Finally concentrated, vacuum drying, obtained Fructus Momordicae sweet taste component product.
The method of above-mentioned gained, the extraction ratio of Fructus Momordicae sweet ingredient is 58.7-74.11%.
Embodiment 4
A kind of ultrasonically auxiliary extracting method of Fructus Momordicae sweet ingredient and the application in tobacco product, ultrasonically auxiliary extracting method
For：
Solvent：Methanol；
Ultrasonic power： 500W ；
Throw material liquid ratio： 1:25 g/mL；
Extraction time： 20-100 min
A kind of above-mentioned ultrasonically auxiliary extracting method of Fructus Momordicae sweet ingredient and the application in tobacco product, its ultrasonic wave added
Extracting method is：
First arhat dried fruitss are carried out pulverizing, look over so as to check（80 mesh）；
Then carry out ultrasonic assistant extraction；
Then carry out centrifugation and remove impurity etc. to process；
Finally concentrated, vacuum drying, obtained Fructus Momordicae sweet taste component product.
The method of above-mentioned gained, the extraction ratio of Fructus Momordicae sweet ingredient is 57.48-71.23%.
Embodiment 5
The Fructus Momordicae sweet ingredient that the present invention obtains is dissolved in dehydrated alcohol, and the flushing liquor being configured to 0.5%-2% is placed in larynx
In spray bottle, Fructus Momordicae sweet ingredient is uniformly sprayed in tobacco shred, dries moisture, make cigarette, finally carry out sensory evaluating smoking
Identification.
Described sensory evaluating smoking's authentication method is the sense organ reviewer composition evaluation group of more than 20 length of smoking 2-3,
Using secretly commenting method, according to makings fragrant and sweet in Medicated cigarette, sweet taste amount, the thoroughly property sent out, miscellaneous QI, sweet concentration, strength, fine and smooth degree, one-tenth
Group's property, zest, dry sensation, residual and Hui Tian carry out tasting marking.
Sensory evaluating smoking's result shows, add Fructus Momordicae sweet ingredient Medicated cigarette with without Medicated cigarette compared with, sweet taste amount, honey
Sweet concentration, fine and smooth degree, strength and dry sensation are more strong, and the concentration with Fructus Momordicae sweet ingredient increases, and returns sweet effect more
Substantially, fragrant and sweet makings becomes big, and fine and smooth degree increases, but dry sensation is more strong, miscellaneous QI DeGrain, and conglobation property also becomes
Change less it was demonstrated that preferable quality-improving effect is had by the Fructus Momordicae sweet ingredient of ultrasound assisted extraction to the quality of Medicated cigarette.
The above is only the basic explanation under present inventive concept, and according to technical scheme made any etc.
Effect conversion, all should belong to protection scope of the present invention.
Claims (8)
1. a kind of extracting method of Fructus Momordicae sweet ingredient is it is characterised in that comprise the steps：
1）First arhat dried fruitss are carried out pulverizing, sieve；
2）Arhat dried fruitss after pulverizing are added in solvent and carry out ultrasonic extraction, described solvent be 100 DEG C boiling water, 70 DEG C
Hot water, methanol, dehydrated alcohol or ethanol that mass percent concentration is 75%；Solid-liquid ratio is 1:15 g/mL-1:35 g/
mL；Ultrasonic power is 300W-500W；Extraction time is 20 min-100min；
3）Then carry out centrifugation and remove impurity is processed；
4）Finally concentrated, vacuum drying, obtained Fructus Momordicae sweet taste component product.
2. a kind of Fructus Momordicae sweet ingredient according to claim 1 extracting method it is characterised in that：
Described solvent is 100 DEG C of boiling water, 70 DEG C of hot water, methanol, dehydrated alcohol or mass percent concentration is 75%
Ethanol, ultrasonic power be 500W；Solid-liquid ratio is 1:20 g/mL；Extraction time is 40 min.
3. a kind of Fructus Momordicae sweet ingredient according to claim 1 extracting method it is characterised in that：
Described solvent is methanol；Ultrasonic power is 300 W-500W；Solid-liquid ratio is 1:20 g/mL；Extraction time is 40
min.
4. a kind of Fructus Momordicae sweet ingredient according to claim 1 extracting method it is characterised in that：
Described solvent is methanol；Ultrasonic power is 500W；Solid-liquid ratio is 1:15-1:35 g/mL；Extraction time is 40 min.
5. a kind of Fructus Momordicae sweet ingredient according to claim 1 extracting method it is characterised in that：
Described solvent is methanol；Ultrasonic power is 500W；Solid-liquid ratio is 1:25 g/mL；Extraction time is 20-100 min.
6. the Fructus Momordicae sweet taste component product that in claim 1-5 prepared by arbitrary described method.
7. application in tobacco product for the Fructus Momordicae sweet taste component product obtained by claim 6.
8. the application according to claim 7 it is characterised in that：Described tobacco product be Medicated cigarette, cigar, tobacco shred or
Redried leaf tobacco.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610801728.3A CN106381227A (en) | 2016-09-05 | 2016-09-05 | Extraction method of Fructus Momordicae sweet component, and application of Fructus Momordicae sweet component in tobacco product |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610801728.3A CN106381227A (en) | 2016-09-05 | 2016-09-05 | Extraction method of Fructus Momordicae sweet component, and application of Fructus Momordicae sweet component in tobacco product |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106381227A true CN106381227A (en) | 2017-02-08 |
Family
ID=57939607
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610801728.3A Pending CN106381227A (en) | 2016-09-05 | 2016-09-05 | Extraction method of Fructus Momordicae sweet component, and application of Fructus Momordicae sweet component in tobacco product |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109090702A (en) * | 2018-06-29 | 2018-12-28 | 郑州轻工业学院 | The preparation method and applications of Luo Han Guo Paste In Foods maillard reaction product |
| CN112545049A (en) * | 2020-12-25 | 2021-03-26 | 河南中烟工业有限责任公司 | Cigar tobacco processing method |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1683387A (en) * | 2005-03-16 | 2005-10-19 | 桂林莱茵生物科技股份有限公司 | Method for extracting momordica glycoside from momordica grosvenori |
| CN101138435A (en) * | 2007-09-30 | 2008-03-12 | 广西中烟工业公司 | Additive agent for natural polypropylene filter tip cigarette and method of producing the same |
| CN101444333A (en) * | 2008-11-28 | 2009-06-03 | 华芳烟用香料有限公司 | Method of preparing Grosvenor momordica extract and application thereof |
| CN104762132A (en) * | 2015-03-05 | 2015-07-08 | 云南中烟工业有限责任公司 | Preparation method and application of Siraitia grosvenorii extract |
-
2016
- 2016-09-05 CN CN201610801728.3A patent/CN106381227A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1683387A (en) * | 2005-03-16 | 2005-10-19 | 桂林莱茵生物科技股份有限公司 | Method for extracting momordica glycoside from momordica grosvenori |
| CN101138435A (en) * | 2007-09-30 | 2008-03-12 | 广西中烟工业公司 | Additive agent for natural polypropylene filter tip cigarette and method of producing the same |
| CN101444333A (en) * | 2008-11-28 | 2009-06-03 | 华芳烟用香料有限公司 | Method of preparing Grosvenor momordica extract and application thereof |
| CN104762132A (en) * | 2015-03-05 | 2015-07-08 | 云南中烟工业有限责任公司 | Preparation method and application of Siraitia grosvenorii extract |
Non-Patent Citations (3)
| Title |
|---|
| 曾晓鹰 等: "《卷烟调香体系构建 以云烟品牌为例》", 28 February 2013, 西南交通大学出版社 * |
| 李倩: "高纯罗汉果苷V的提取纯化技术研究", 《中国优秀硕士学位论文全文数据库 农业科技辑》 * |
| 杨祖金 等: "超声波法强化提取罗汉果皂苷的工艺研究", 《中药材》 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109090702A (en) * | 2018-06-29 | 2018-12-28 | 郑州轻工业学院 | The preparation method and applications of Luo Han Guo Paste In Foods maillard reaction product |
| CN109090702B (en) * | 2018-06-29 | 2021-08-24 | 郑州轻工业学院 | Preparation method and application of Maillard reaction product of fructus momordicae extract |
| CN112545049A (en) * | 2020-12-25 | 2021-03-26 | 河南中烟工业有限责任公司 | Cigar tobacco processing method |
| CN112545049B (en) * | 2020-12-25 | 2022-07-26 | 河南中烟工业有限责任公司 | Cigar tobacco processing method |
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Application publication date: 20170208 |