CN106376700A - 一种贻贝玉竹复合压片糖果的制备方法 - Google Patents
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Abstract
本发明涉及一种利用贻贝和玉竹提取物加工制备一种复合压片糖果。具体制备方法为：将鲜活贻贝去除壳后，洗净后沸水热烫，加水绞碎后加入复合蛋白酶酶解，灭酶离心后取酶解上清液，冷冻干燥，得到贻贝蛋白酶解粉。玉竹以浸润后加入水打浆，加入纤维素酶进行酶解，酶解后煮沸提取，得到提取液，过滤，减压浓缩后，冷冻干燥，粉碎，得到玉竹提取物。将贻贝蛋白酶解粉、玉竹提取物、糖醇分别粉碎过筛，然后将预混合的物料置入搅拌机中，加入适量的水进行混合。将片剂放在紫外灯下照射分钟后包装，即为成品。该工艺的主要特点是促进现有的海参养殖资源高值化利用，并且满足市场需求，其操作简单，技术含量高，产品具有极高的经济价值。
Description
技术领域
本发明涉及一种海产品的综合利用，主要是一种利用贻贝和玉竹提取物加工制备一种复合压片糖果。
背景技术
贻贝(Mytilus edulis)，俗称“海红”、“淡菜”，是一种高蛋白、低脂肪、富含多种营养成分且分布范围较广的常见海产品。我国贻贝的产量居于世界首位，且90％的贻贝产品用于鲜品出口，目前由于贻贝的加工技术比较落后，导致其加工利用率低下，产品附加值低，其蛋白资源浪费严重。药理学研究显示贻贝具有补肝肾，益精血，消瘿瘤。治虚劳羸瘦，眩晕，盗汗，阳痿，腰痛，吐血，崩漏，带下，瘿瘤，疝瘕。随着人们生活水平的提高和生活质量的改善，对于贻贝的需求也日趋旺盛。
玉竹，学名:Polygonatum odoratum(Mill.)Druce，为百合科多年生草本植物。根茎横走，肉质黄白色，密生多数须根。叶面绿色，下面灰色。花腋生，通常1～3朵簇生。原产中国西南地区，但野生分布很广。耐寒，亦耐阴，喜潮湿环境，适宜生长于含腐殖质丰富的疏松土壤。《本草经集注》云"茎干强直，似竹箭杆，有节"，故有玉竹之名。植物的根茎可供药用，中药名亦为玉竹，秋季采挖，洗净，晒至柔软后，反复揉搓，晾晒至无硬心，晒干，或蒸透后，揉至半透明，晒干，切厚片或段用。玉竹提取类黄酮物质与桑叶提取物脱氧野尻霉素结合形成一种新物质--洗胰清糖素(cics)，具有降血糖、血脂、血压等作用。
压片糖果又称粉糖或片糖，也常被称作汽水糖，这种糖果以风味多样，便于携带受到广大消费者的喜欢。随着生活质量的不断提高，大众对饮食健康的关注度不断提升，对压片糖果的要求也向着功能化的方向发展。本发明以贻贝和玉竹为主要原料，分别制备提取物后，配以辅料，开发具有功能性的压片糖果产品，对于促进贻贝和玉竹产品精深加工，提高压片糖果类产品附加值，丰富市场上休闲食品种类具有重要意义。
发明内容
本发明解决其技术问题所采用的技术方案是：一种是将鲜活贻贝去除壳后，洗净后沸水热烫，加水绞碎后加入复合蛋白酶酶解，灭酶离心后取酶解上清液，浓缩后，以分子量5000Da为截留值进行超滤，冷冻干燥，得到贻贝蛋白酶解粉。
玉竹放入水中浸润1-3个小时后，切断，加入水打浆，加入纤维素酶进行酶解，酶解后煮沸提取1-3h，得到提取液，过滤，减压浓缩后，冷冻干燥，粉碎，得到玉竹提取物。
将贻贝蛋白酶解粉、玉竹提取物、糖醇分别粉碎过80-100目筛，然后将预混合的物料置入搅拌机中，加入适量的水进行混合。将总混的物料倒入压片机的料斗中，在室温、相对湿度小于40％的环境中进行压片成型。将片剂放在紫外灯下照射30-60分钟后包装，即为成品。
上述用于酶解的复合蛋白酶添加量与贻贝的质量比0.45-0.9％，酶解温度为50-70℃，酶解时间为2.5-4h。
上述用于酶解玉竹的纤维素酶用量与玉竹的质量比为1.5-3％，酶解温度为55-75℃，酶解时间为1-3h。
上述用于压片的糖醇为为木糖醇、山梨糖醇、麦芽糖醇的一种或者多种。
上述用于压片的原料的重量配比：贻贝蛋白酶解粉9-20份、玉竹提取物20-40份、糖醇50-70份、硬脂酸镁1-3份。
上述用于混料加入水的量为所述预混合的物料总重量的1-3％。
本发明的优势是：本发明是将贻贝利用复合蛋白酶进行酶解，将蛋白质酶解称为小分子的肽类或游离氨基酸，促进营养物质的吸收与利用，并且改善贻贝的风味；将贻贝酶解液离心后将可溶性蛋白质与游离性氨基酸等活性物质分离，并且利用冷冻干燥技术固体化。另外针对玉竹纤维素含量较高，硬度大，不易加工的特点，采用纤维素酶进行破壁处理，以提高玉竹活性物质的提取效率。将贻贝酶解粉、玉竹提取物粉和糖醇粉粹过筛可以提高片剂的均匀性；将糖醇应用于压片糖果中，不仅能够保持压片糖果的风味，还适用于多种人群服用；加入适量的水分对压片糖果的片剂成型起着重要的作用；将片剂放在紫外灯下照射30-60分钟后包装可以提高成品的保质期。该工艺的主要特点是促进现有的贻贝养殖资源高值化利用，拉伸贻贝产业链发展，延长贻贝加工产业链，促进贻贝产业良性发展，并且满足市场需求，其操作简单，技术含量高，产品具有极高的经济价值。
具体实施方式
下面结合实施例结本发明做进一步说明。
实施例1
一种利用贻贝和玉竹提取物粉加工复合压片糖果的工艺方法工艺方法，其具体步骤如下：
(1)将鲜活贻贝去除内脏后清洗干净，利用沸水热烫10min，捞出后加入3倍的水打浆，将贻贝绞碎。
(2)在磨碎的贻贝浆中加入复合蛋白酶酶解，复合蛋白酶添加量，与贻贝的质量比0.45％，酶解温度为50℃，酶解时间2.5h。
(3)将酶解液离心，取上清液备用，离心条件为5000r/min，时间为15min。
(4)酶解上清液减压浓缩后，以分子量5000Da为截留值进行超滤分离，将所得滤过液收集，减压浓缩。
(5)将(4)所得浓缩液，冷冻干燥(真空度为30Pa，24h)，干燥完成后粉碎过80目筛后备用。
(6)取玉竹饮片放入水中浸润1-3个小时后，切断，加入5倍量水打浆处理，添加纤维素酶1.5％(以玉竹质量计)，55℃搅拌酶解1h，加热提取1.5h，过滤，提取液减压浓缩后，冷冻干燥，粉碎得到玉竹提取物。
(7)将玉竹提取物粉、山梨糖醇及贻贝酶解物粉碎过80目筛后备用。
(8)然后将预混合的物料置入搅拌机中，加入适量的水进行混合。将总混的物料倒入压片机的料斗中，在室温、相对湿度小于40％的环境中进行压片成型。上述原料的重量配比：20份、玉竹提取物27份、山梨糖醇50份、硬脂酸镁3份。用于混料加入水的量为所述预混合的物料总重量的3％。
(9)将片剂放在紫外灯下照射30min后包装，即为成品。
实施例2
一种利用贻贝和玉竹提取物粉加工复合压片糖果的工艺方法工艺方法，其具体步骤如下：
(1)将鲜活贻贝去除内脏后清洗干净，利用100摄氏度沸水热烫15min，捞出后加入2倍的水打浆，将贻贝绞碎。
(2)在磨碎的贻贝浆中加入复合蛋白酶酶解，复合蛋白酶添加量，与贻贝的质量比0.9％，酶解温度为70℃，酶解时间4h。
(3)将酶解液离心，取上清液备用，离心条件为6000r/min，时间为15min。
(4)酶解上清液减压浓缩后，以分子量5000Da为截留值进行超滤分离，将所得滤过液收集，减压浓缩。
(5)将(4)所得浓缩液，冷冻干燥(真空度为30Pa，20h)，干燥完成后粉碎过100目筛后备用。
(6)取玉竹放入水中浸润1-3个小时后，切断，加入10倍量水打浆处理，添加纤维素酶3％(以玉竹质量计)，75℃搅拌酶解1h，加热提取1.5h，过滤，提取液减压浓缩后，冷冻干燥，粉碎得到玉竹提取物。
(7)将玉竹提取物粉、木糖醇及贻贝酶解物粉碎过80目筛后备用。
(8)然后将预混合的物料置入搅拌机中，加入适量的水进行混合。将总混的物料倒入压片机的料斗中，在室温、相对湿度小于40％的环境中进行压片成型。上述原料的重量配比：20份、玉竹提取物27份、木糖醇50份、硬脂酸镁3份。用于混料加入水的量为所述预混合的物料总重量的3％。
(9)将片剂放在紫外灯下照射30min后包装，即为成品。
Claims (6)
1.一种贻贝玉竹复合压片糖果的制备方法，其特征在于：
具体制备方法为：
(1)将鲜活贻贝去除壳后，洗净后100℃沸水热烫5-15min，加入1-5倍重量的水绞碎后加入复合蛋白酶酶解，灭酶离心后取酶解上清液，减压浓缩后至固形物含量为20-40wt％，以分子量5000Da为截留值进行超滤，冷冻干燥，得到贻贝蛋白酶解粉,备用；
(2)玉竹放入水中浸润1-3个小时后，切断至0.5cm-2cm的段状，加入5-10倍重量的水打浆，加入纤维素酶进行酶解，酶解后煮沸提取1-3h，得到提取液，过滤，减压浓缩至固形物含量为40-60wt％后，冷冻干燥，粉碎后过80-100目筛，得到玉竹提取物，备用；
(3)将贻贝蛋白酶解粉、玉竹提取物、糖醇粉碎过80-100目筛，然后将上述混合过筛得到的物料置入搅拌机中，加入预混合的物料总重量的1-3％的水进行混合；
(4)将与水混合得到的总物料倒入压片机的料斗中，在室温、相对湿度小于40％的环境中进行压片成片剂，即为成品。
2.根据权利要求1所述的贻贝玉竹复合压片糖果的制备方法，其特征在于：
将片剂放在紫外灯下照射30-60分钟后包装即可。
3.根据权利要求1所述的贻贝玉竹复合压片糖果的制备方法，其特征在于：
步骤(1)用于酶解的复合蛋白酶添加量与贻贝的质量比0.45-0.9％，酶解温度为50-70℃，酶解时间为2.5-4h。
4.根据权利要求1所述的贻贝玉竹复合压片糖果的制备方法，其特征在于：
步骤(2)用于酶解玉竹的纤维素酶用量与玉竹的质量比为1.5-3％，酶解温度为55-75℃，酶解时间为1-3h。
5.根据权利要求1所述的贻贝玉竹复合压片糖果的制备方法，其特征在于：
步骤(3)的糖醇为木糖醇、山梨糖醇、麦芽糖醇的一种或者多种。
6.根据权利要求1所述的贻贝玉竹复合压片糖果的制备方法，其特征在于：
步骤(3)中原料的重量配比：贻贝蛋白酶解粉9-20份、玉竹提取物20-40份、糖醇50-70份、硬脂酸镁1-3份。
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| CN110679709A (zh) * | 2019-09-26 | 2020-01-14 | 浙江海洋大学 | 一种贻贝压片糖果的制备方法及贻贝压片糖果 |
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| CN110679709A (zh) * | 2019-09-26 | 2020-01-14 | 浙江海洋大学 | 一种贻贝压片糖果的制备方法及贻贝压片糖果 |
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