CN106344478A - Preparation method of dendrobium officinale extractive used for cosmetics - Google Patents
Preparation method of dendrobium officinale extractive used for cosmetics Download PDFInfo
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- CN106344478A CN106344478A CN201610991154.0A CN201610991154A CN106344478A CN 106344478 A CN106344478 A CN 106344478A CN 201610991154 A CN201610991154 A CN 201610991154A CN 106344478 A CN106344478 A CN 106344478A
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- herba dendrobii
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
Abstract
The invention relates to a preparation method of dendrobium officinale extractive used for cosmetics. According to the invention, the preparation method comprises the following steps: washing and smashing 60-70 parts by weight of dendrobium officinale, dispersing in water and mixing; adding 1.0-1.2 parts by weight of cellulase to a dendrobium officinale suspension liquid, agitating, and reacting for 2-5h; adding 0.7-1.0 part by weight of hemicellulase, agitating, and reacting for 2-3h; adding 0.6-1.2 parts by weight of pectinase, agitating, and reacting for 1-2h; readjusting temperature and adjusting pH value to 4-6, adding 0.6-1.2 parts by weight of mannase, then agitating, and sufficiently reacting for 2-3h; adding 1.0-1.5 parts by weight of neutral protease, agitating, sufficiently reacting, then filtering, and removing residue; and concentrating to 120-150 parts by weight to obtain the dendrobium officinale extractive. The preparation method is mild in process conditions, high in extraction rate, and wide in material source, the extractive is non-toxic and harmless to people, is good in moisturizing effect, and has wide development prospect.
Description
Technical field
The invention belongs to washing product field is and in particular to a kind of preparation side of Herba Dendrobii extract used for cosmetic
Method.
Background technology
Herba Dendrobii, perennial orchid family herbaceous plant, by kind preciousness degree be divided into Herba Dendrobii, Dendrobium nobile, dendrobium loddigesii Rolfe,
HERBA DENDROBII, Herba Dendrobii oculati etc. more than 70 are planted, and wherein Herba Dendrobii is come out top.Herba Dendrobii (dendrobium officinale
Kimura et migo) it is Chinese Second Class Key Protected Plant, there is extraordinary health preserving and medical value.In the health preserving that China is long
In culture, Herba Dendrobii, because of its outstanding effect, becomes the health preserving superfine product that ancient Chinese medicine doctor and the nobility praise highly.
Herba Dendrobii chemical composition is various, mainly has alkaloid, polysaccharide, aminoacid, luxuriant and rich with fragrance class compound etc., these materials hold
Easily destroyed, how to make full use of its effective ingredient it is ensured that Herba Dendrobii use during functional component be retained as need
A difficult problem to be captured.
Content of the invention
It is an object of the invention to provide a kind of Herba Dendrobii extract used for cosmetic, this extract can ensure in skin Herba Dendrobii
The reservation of functional component during use.
In order to reach above-mentioned technical purpose it is characterised in that:
(1) 60～75 weight portion Herba Dendrobii cleaned, pulverize, be dispersed in water, stirring is sufficiently mixed；
(2) add 1.0～1.2 part by weight of cellulose enzymes under the conditions of 40～55 DEG C in Herba Dendrobii suspension, stir, fully
Reaction 2～5h；
(3) add 0.7～1.0 weight portion hemicellulase, stirring, fully react 2～3h；
(4) add 0.6～1.2 weight portion pectase, stirring, fully react 1～2h；
(5) from new adjustment temperature to 40～50 DEG C, adjust ph to 4～6, stir after adding 0.6～1.2 weight portion mannase
Mix, fully react 2～3h；
(6) add 1.0～1.5 weight portion neutral protease stirrings, 1～3h after reaction fully, filter, remove filtering residue；
(7) concentrate the filtrate to 120～150 weight portions, obtain final product Herba Dendrobii extract.
Described Herba Dendrobii is dispersed in water, Herba Dendrobii: the weight part ratio of water is 1:5～15.
The extract of the present invention is nontoxic to people, to environment non-secondary pollution, raw material sources are extensively it is easy to processing, warp
Ji is practical, being a kind of Green Product, thus reaching the purpose of environmental protection, having vast potential for future development.
The present invention prepares Herba Dendrobii extract, and process conditions are gentle, and extraction ratio is high, not only facilitates holding active ingredient
Original property, and reducing energy consumption, low for equipment requirements, with low cost, be conducive to industrialized production.
The thing of the present invention is added to cream, in washing product, have that moistening effect is good, can desalinate microgroove, persistently protect
Wet, the effects such as repair impaired skin quality, also there is the no any zest of safety simultaneously.
Specific embodiment
The present invention will be further described with reference to embodiments.
Embodiment 1
(1) 65g Herba Dendrobii cleaned, pulverize, be scattered in 650g water, stirring is sufficiently mixed；
(2) add 1.1g cellulase, stirring in Herba Dendrobii suspension under the conditions of 45 DEG C, fully react 2.5h；
(3) add 0.8g hemicellulase, stirring, fully react 2.5h；
(4) add 0.8g pectase, stirring, fully react 1.5h；
(5) reduce temperature to 45 DEG C, adjust ph to 5, stir after adding 0.8g mannase, fully react 2.5h；
(6) add the stirring of 1.2g neutral protease, 2h after reaction fully in suspension, filter, remove filtering residue；
(7) concentrate the filtrate to 130g, obtain final product Herba Dendrobii extract.
Embodiment 2
(1) 65g Herba Dendrobii cleaned, pulverize, be scattered in 650g water, so that stirring is sufficiently mixed；
(2) add 1.1g cellulase, stirring in Herba Dendrobii suspension under the conditions of 45 DEG C, fully react 2.5h；
(3) add 0.75g hemicellulase, stirring, fully react 2.5h；
(4) add 0.75g pectase, stirring, fully react 1.5h；
(5) reduce temperature to 45 DEG C, adjust ph to 4.5, stir after adding 1g mannase, fully react 2.5h；
(6) add the stirring of 1.2g neutral protease, 2h after reaction fully in suspension, filter, remove filtering residue；
(7) concentrate the filtrate to 130g, obtain final product Herba Dendrobii extract.
Embodiment 3
(1) 60g Herba Dendrobii cleaned, pulverize, be scattered in 600g water, stirring is sufficiently mixed；
(2) add 1.15g cellulase, stirring in Herba Dendrobii suspension under the conditions of 45 DEG C, fully react 2.5h；
(3) add 0.8g hemicellulase, stirring, fully react 2.25h；
(4) add 0.8g pectase, stirring, fully react 1.25h；
(5) reduce temperature to 45 DEG C, adjust ph to 5, stir after adding 0.75g mannase, fully react 2.5h；
(6) add the stirring of 1.2g neutral protease, 2h after reaction fully in suspension, filter, remove filtering residue；
(7) concentrate the filtrate to 130g, obtain final product Herba Dendrobii extract.
Embodiment 4
(1) 70g Herba Dendrobii cleaned, pulverize, be scattered in 700g water, stirring is sufficiently mixed；
(2) add 1.1g cellulase, stirring in Herba Dendrobii suspension under the conditions of 50 DEG C, fully react 3h；
(3) add 1g hemicellulase, stirring, fully react 2.5h；
(4) add 0.75g pectase, stirring, fully react 1.5h；
(5) reduce temperature to 45 DEG C, adjust ph to 5.5, stir after adding 0.8g mannase, fully react 2.5h；
(6) add the stirring of 1.2g neutral protease, 2h after reaction fully in suspension, filter, remove filtering residue；
(7) concentrate the filtrate to 140g, obtain final product Herba Dendrobii extract.
Embodiment 5
(1) 70g Herba Dendrobii cleaned, pulverize, be scattered in 700g water, stirring is sufficiently mixed；
(2) add 1.05g cellulase, stirring in Herba Dendrobii suspension under the conditions of 50 DEG C, fully react 2.25h；
(3) add 0.8g hemicellulase, stirring, fully react 2.5h；
(4) add 0.8g pectase, stirring, fully react 1.5h；
(5) reduce temperature to 45 DEG C, adjust ph to 5, stir after adding 1g mannase, fully react 2.5h；
(6) add the stirring of 1.25g neutral protease, 2.5h after reaction fully in suspension, filter, remove filtering residue；
(7) concentrate the filtrate to 140g, obtain final product Herba Dendrobii extract.
Embodiment 6
(1) 60g Herba Dendrobii cleaned, pulverize, be scattered in 600g water, stirring is sufficiently mixed；
(2) add 1.05g cellulase, stirring in Herba Dendrobii suspension under the conditions of 50 DEG C, fully react 2.5h；
(3) add 0.75g hemicellulase, stirring, fully react 2.5h；
(4) add 0.75g pectase, stirring, fully react 1.5h；
(5) reduce temperature to 50 DEG C, adjust ph to 5.5, stir after adding 1g mannase, fully react 2.5h；
(6) add the stirring of 1.25g neutral protease, 2.25h after reaction fully in suspension, filter, remove filtering residue；
(7) concentrate the filtrate to 140g, obtain final product Herba Dendrobii extract.
Embodiment 7
(1) 75g Herba Dendrobii cleaned, pulverize, be scattered in 750g water, stirring is sufficiently mixed；
(2) add 1.1g cellulase, stirring in Herba Dendrobii suspension under the conditions of 45 DEG C, fully react 2.5h；
(3) add 0.75g hemicellulase, stirring, fully react 2.5h；
(4) add 1g pectase, stirring, fully react 1.5h；
(5) reduce temperature to 45 DEG C, adjust ph to 5, stir after adding 1g mannase, fully react 2.5h；
(6) add the stirring of 1.3g neutral protease, 2h after reaction fully in suspension, filter, remove filtering residue；
(7) concentrate the filtrate to 145g, obtain final product Herba Dendrobii extract.
Embodiment 8
(1) 72.5g Herba Dendrobii cleaned, pulverize, be scattered in 725g water, stirring is sufficiently mixed；
(2) add 1.1g cellulase, stirring in Herba Dendrobii suspension under the conditions of 50 DEG C, fully react 2h；
(3) add 0.8g hemicellulase, stirring, fully react 2.5h；
(4) add 1g pectase, stirring, fully react 1.5h；
(5) reduce temperature to 45 DEG C, adjust ph to 5, stir after adding 1g mannase, fully react 2.5h；
(6) add the stirring of 1.3g neutral protease, 2h after reaction fully in suspension, filter, remove filtering residue；
(7) concentrate the filtrate to 145g, obtain final product Herba Dendrobii extract.
The foregoing is only embodiments of the invention, not thereby limit the protection domain of the patent application of the present invention, all
It is the equivalent structure or equivalent flow conversion made using present specification, or it is related to be directly or indirectly used in other
Technical field, all include in the same manner in the protection domain of the patent application of the present invention.
Claims (2)
1. a kind of preparation method of Herba Dendrobii extract used for cosmetic it is characterised in that:
(1) 60～75 weight portion Herba Dendrobii cleaned, pulverize, be dispersed in water, stirring is sufficiently mixed；
(2) add 1.0～1.2 part by weight of cellulose enzymes under the conditions of 40～55 DEG C in Herba Dendrobii suspension, stir, fully
Reaction 2～5h；
(3) add 0.7～1.0 weight portion hemicellulase, stirring, fully react 2～3h；
(4) add 0.6～1.2 weight portion pectase, stirring, fully react 1～2h；
(5) from new adjustment temperature to 40～50 DEG C, adjust ph to 4～6, stir after adding 0.6～1.2 weight portion mannase
Mix, fully react 2～3h；
(6) add 1.0～1.5 weight portion neutral protease stirrings, 1～3h after reaction fully, filter, remove filtering residue；
(7) concentrate the filtrate to 120～150 weight portions, obtain final product Herba Dendrobii extract.
2. a kind of Herba Dendrobii extract used for cosmetic according to claim 1 is it is characterised in that described iron sheet stone
Dry measure used in former times is dispersed in water, Herba Dendrobii: the weight part ratio of water is 1:5～15.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610991154.0A CN106344478A (en) | 2016-11-11 | 2016-11-11 | Preparation method of dendrobium officinale extractive used for cosmetics |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610991154.0A CN106344478A (en) | 2016-11-11 | 2016-11-11 | Preparation method of dendrobium officinale extractive used for cosmetics |
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| CN106344478A true CN106344478A (en) | 2017-01-25 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201610991154.0A Pending CN106344478A (en) | 2016-11-11 | 2016-11-11 | Preparation method of dendrobium officinale extractive used for cosmetics |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106890128A (en) * | 2017-03-09 | 2017-06-27 | 安徽省霍山县农伯乐开发有限公司 | A kind of Huoshan rice dry measure used in former times Essence |
| CN117106832A (en) * | 2023-08-28 | 2023-11-24 | 东莞巨微新材料科技有限公司 | Dendrobium officinale polysaccharide extract with high and low molecular weight as well as preparation method and application thereof |
Citations (3)
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| CN105085695A (en) * | 2015-06-12 | 2015-11-25 | 浙江仙人草保健品有限公司 | Preparation method for dendrobium candidum extract powder |
| CN105395402A (en) * | 2015-11-28 | 2016-03-16 | 铜仁市金农绿色农业科技有限公司 | Facial cleanser and preparation method thereof |
| CN105943437A (en) * | 2016-05-31 | 2016-09-21 | 安徽皖斛堂生物科技有限公司 | Dendrobium officinale toothpaste with antisepsis and anti-inflammation effects |
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2016
- 2016-11-11 CN CN201610991154.0A patent/CN106344478A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105085695A (en) * | 2015-06-12 | 2015-11-25 | 浙江仙人草保健品有限公司 | Preparation method for dendrobium candidum extract powder |
| CN105395402A (en) * | 2015-11-28 | 2016-03-16 | 铜仁市金农绿色农业科技有限公司 | Facial cleanser and preparation method thereof |
| CN105943437A (en) * | 2016-05-31 | 2016-09-21 | 安徽皖斛堂生物科技有限公司 | Dendrobium officinale toothpaste with antisepsis and anti-inflammation effects |
Non-Patent Citations (1)
| Title |
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| 文洪宇 等: "应用于中药提取分离中的酶的综述", 《中国医药指南》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106890128A (en) * | 2017-03-09 | 2017-06-27 | 安徽省霍山县农伯乐开发有限公司 | A kind of Huoshan rice dry measure used in former times Essence |
| CN117106832A (en) * | 2023-08-28 | 2023-11-24 | 东莞巨微新材料科技有限公司 | Dendrobium officinale polysaccharide extract with high and low molecular weight as well as preparation method and application thereof |
| CN117106832B (en) * | 2023-08-28 | 2024-03-08 | 东莞巨微新材料科技有限公司 | Dendrobium officinale polysaccharide extract with high and low molecular weight as well as preparation method and application thereof |
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Application publication date: 20170125 |