CN106821864A - A kind of preparation method of the multifunction environment-protection type cream containing tea-seed oil - Google Patents
A kind of preparation method of the multifunction environment-protection type cream containing tea-seed oil Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/55—Phosphorus compounds
- A61K8/553—Phospholipids, e.g. lecithin
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
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- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/925—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of animal origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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- A61K2800/72—Hypo-allergenic
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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Abstract
The present invention relates to cosmetic field, and in particular to a kind of preparation method of the multifunction environment-protection type cream containing tea-seed oil.Ratio pours into mould banyan palpus, giant knotweed, kiss-me, soapberry, the extract solution of Saponaria officinalis and the antibacterial adhesive of tea seed cake powder, purple soil and odium stearate after heating water bath, mixing and stirring in batches by weight, it is molded with pressure pressing mold, Temperature fall solidifies, and obtains pure natural anti-inflammation laundry soap of the present invention.Simple production process of the present invention, smear after without thick and heavy greasy feeling, not only moistening effect is good, and can effectively inhibiting bacteria and diminishing inflammation it is antipruritic;Organoleptic indicator and physical and chemical index meet regulation requirement.
Description
Technical field
The present invention relates to cosmetic field, and in particular to a kind of preparation side of the multifunction environment-protection type cream containing tea-seed oil
Method.
Background technology
In recent years, with the improvement of people ' s living standards, the spending amount proportion of washing product constantly increases, and people are to flesh
The nursing of skin is increasingly paid attention to, and natural cosmetics are extremely pursued.But the environmental pollution in process of industrialization, the daily four seasons are more
The temperature change and pressure brought for, air conditioner eructation, and human normal metabolism, the reason such as skin senescence causes skin
Water loss, any season, age, skin quality are all that intensive care is carried out on the basis of skin replenishing water and preserving moisture.
Water shortage is the basic reason that the aging phenomenons such as dim, dry skin, jaundice, lax and wrinkle are produced.Conventional guarantor
Humectant has soybean lecithin, sorbierite, the propane diols can be absorbed water from environment, and sodium hyaluronate be in tissue skin corium from
The material for so existing, with surprising water absorbing capacity, powerful moisture-keeping function.Disappear with green with the improvement of people ' s living standards
Take the enhancing of consciousness, people are increasingly favored in the Chinese herbal medicine with curative effect and trophism, plant extraction liquid and natural nutrition
The compounding cream of product.Therefore containing compositions such as natural Chinese medicinal herbs, with various functions such as moisturizing, antibacterial, anti-inflammatory anti-itch, whitening
Cream is suddenly waited to develop.
The content of the invention
It is an object of the invention to provide a kind of preparation method of the multifunction environment-protection type cream containing tea-seed oil.This kind of cream
With the effect such as good moisturizing, antibacterial, anti-inflammatory, antipruritic, whitening.
1st, meter formula by weight is:
15~25 parts of tea seed extract solution;
2~7 parts of clover extract solution;
2~8 parts of kiss-me extract solution;
2~6 parts of fruit of summer cypress extract solution;
2~5 parts of snake oil;
2~5 parts of gumbo extract solution;
2~5 parts of giant knotweed extract solution;
2~5 parts of ecliptae herba extract solution;
0.1~1.0 part of sodium hyaluronate;
1~5 part of ethoxy urea;
5~12 parts of soybean lecithin;
3~8 parts of beeswax;
0.3~1.5 part of citric acid;
0.5~1 part of natural essence;
Balance of deionized water, total amount is 100 parts.
2nd, preparation process:
(1)First by ecliptae herba extract solution, sodium hyaluronate, ethoxy urea, clover extract solution, kiss-me extract solution, the fruit of summer cypress
Extract solution, gumbo extract solution are added in deionized water by weight, and being warmed up to 70~80 DEG C under magnetic agitation effect obtains water
Phase A liquid;
(2)Snake oil, beeswax, soybean lecithin, tea seed extract solution are sequentially added by reaction weight portion in another reactor, is put
It is placed in heating in 70~80 DEG C of water-baths and is completely dissolved to obtain oil phase B liquid;
(3)After water phase A liquid, oil phase B liquid material all melt, oil phase B liquid is uniformly poured into water under quick stirring action
In phase A liquid, water phase and an oil phase is reacted completely, pH value is determined after 2min, with lemon acid for adjusting pH between 6.5~7;
(4)Mixture is placed under refiner, 4min is homogenized under 1.8w/min power;
(5)It is to be cooled to 40 DEG C when, perfuming accurate adjustment is fragrant, after being cooled to room temperature, stands 3d, can tinning after stabilization.
The preparation method of wherein described tea seed extract solution is as follows:
(1)100 weight portion tea seeds are crushed to 30-50 mesh, are dispersed in water, make raw material be 1 with the weight part ratio of water:5, stir
Mix and be sufficiently mixed;
(2)0.35 part by weight of cellulose enzyme is added under the conditions of 50 DEG C in suspension, is stirred, fully react 3h;
(3)0.25 weight starch enzyme is added, is stirred, fully react 2h;
(4)0.35 weight portion protease is added, is stirred, fully react 1.5h, filtered, remove filter residue;
(5)2.5 parts by weight of sodium hydroxide, stirring reaction 2h under the conditions of 60 DEG C are added then to concentrate the filtrate to 150 parts in filtrate
Amount, obtains final product tea seed extract solution.
The preparation method of the kiss-me extract solution is as follows:
(1)100 weight portion kiss-mes are cleaned, is crushed, be scattered in 75% alcoholic solution, make raw material: the weight portion of alcoholic solution
Than being 1:10, stirring is sufficiently mixed;
(2)0.5 part by weight of cellulose enzyme is added under the conditions of 50 DEG C in kiss-me suspension, is stirred, fully react 2h;Cross
Filter, removes filter residue;
(3)Recovered alcohol, and 300 weight portions are concentrated the filtrate to, obtain final product kiss-me extract solution.
The preparation method of the giant knotweed extract solution is as follows:
(1)100 weight portion giant knotweeds are cleaned, is crushed, be dispersed in water, make raw material be 1 with the weight part ratio of water:10, stirring is filled
Divide mixing;
(2)0.75 part by weight of cellulose enzyme is added under the conditions of 50 DEG C in suspension, is stirred, fully react 1.5h;
(3)0.5 weight portion hemicellulase is added, is stirred, fully react 0.5h;
(4)0.5 weight portion protease is added to stir in suspension, 2h after reaction fully, filtering removes filter residue;
(5)450 parts are concentrated the filtrate to, giant knotweed extract solution is obtained final product.
The preparation method of the fruit of summer cypress extract solution is as follows:
(1)The 100 weight portion fruit of summer cypress are crushed to 30-50 mesh, are dispersed in water, make raw material: the mass ratio of solvent is 1:5, stir
Mix and be sufficiently mixed, 0.5h is incubated under the conditions of 70 DEG C, filter, filtrate is standby;
(2)Filter residue in step 1 is dispersed in water, makes raw material be 1 with the weight part ratio of water:5, in 50 DEG C of bars in suspension
0.3 part by weight of cellulose enzyme is added under part, is stirred, fully react 3h;
(3)0.3 weight starch enzyme is added, is stirred, fully react 2h;
(4)0.5 weight portion protease is added, is stirred, fully react 1.5h, filtered, remove filter residue;
(5)Filtrate is merged with the filtrate in step 1,300 weight portions are concentrated into, fruit of summer cypress extract solution is obtained final product.
The preparation method of the gumbo extract solution is as follows:
(1)100 weight portion gumbos are cleaned, is crushed, be scattered in 75% alcohol water blend, make raw material with alcohol water blend
Weight part ratio is 1:5, stirring is sufficiently mixed;1.5h is incubated under the conditions of 60 DEG C, is filtered, remove filter residue;
(2)Recovered alcohol, and 200 weight portions are concentrated the filtrate to, obtain final product stone gumbo extract solution.
The preparation method of ecliptae herba extract solution is as follows:
(1)100 weight portion ecliptae herbas are cleaned, is crushed, be scattered in 75% alcohol water blend, make raw material and alcohol water blend
Weight part ratio be 1:5, stirring is sufficiently mixed;2.5h is incubated under the conditions of 60 DEG C, is filtered, remove filter residue;
(2)Recovered alcohol, and 200 weight portions are concentrated the filtrate to, obtain final product ecliptae herba extract solution.
The preparation method of clover extract solution is as follows:
(1)100 weight portion clovers are cleaned, is crushed, be scattered in 75% alcohol water blend, make raw material and alcohol water blend
Weight part ratio be 1:5, stirring is sufficiently mixed;2h is incubated under the conditions of 60 DEG C, is filtered, remove filter residue;
(2)Recovered alcohol, and 200 weight portions are concentrated the filtrate to, obtain final product clover extract solution.
Advantages of the present invention is:The present invention makes full use of tea seed, clover, kiss-me, the fruit of summer cypress, gumbo, giant knotweed, drought
The moisturizings such as grease, vitamin E, saponin(e, the polysaccharide of the natural products such as Mo Lian, antibacterial, antipruritic, inflammation-diminishing function, and combine snake oil, glass
The composition science such as uric acid, soybean lecithin, beeswax is made, the effect with moisturizing whitening, bright color, stingless to skin
Swash property, and have inhibitory action to various bacteria and dermatophyte, have resist inflammation on repercussive function to scytitis.It is easy with raw material
, it is easy to operate, reaction condition is gentle, effect is obvious, the advantages of with low cost.
The organoleptic indicator of finished product of the present invention and physical and chemical index meet regulation requirement.
Specific embodiment
Below with reference to embodiment, the present invention will be further described.
Embodiment 1
(One)Formula
A kind of multifunction environment-protection type cream containing tea-seed oil is made up of following parts by weight of component:
Tea seed extract solution 170g, clover extract solution 30g, kiss-me extract solution 30g, the fruit of summer cypress extract solution 30g, snake oil 25g,
Gumbo extract solution 30g, giant knotweed extract solution 25g, ecliptae herba extract solution 25g, sodium hyaluronate 5g, ethoxy urea 20g, soybean lecithin
75g, beeswax 50g, citric acid 6g, natural essence 7.5g, balance of deionized water, total amount is 1000g.
(Two)Prepare
(1)First by ecliptae herba extract solution, sodium hyaluronate, ethoxy urea, clover extract solution, kiss-me extract solution, the fruit of summer cypress
Extract solution, gumbo extract solution are added in deionized water by weight, and 80 DEG C are warmed up under magnetic agitation effect;
(2)Snake oil, beeswax, soybean lecithin, tea seed extract solution are sequentially added by reaction weight portion in another reactor, is put
It is placed in be heated in 70 DEG C of water-baths and is completely dissolved;
(3)After water phase, oil phase substance are all melted, oil phase is uniformly poured into water phase under quick stirring action, makes water
Oily two-phase is reacted completely, and pH value is determined after 2min, with lemon acid for adjusting pH between 6.5~7;
(4)Mixture is placed under refiner, 4min is homogenized under 1.8w/min power;
(5)It is to be cooled to 40 DEG C when, perfuming accurate adjustment is fragrant, after being cooled to room temperature, stands 3d, can tinning after stabilization.
Embodiment 2
(One)Formula
A kind of multifunction environment-protection type cream containing tea-seed oil is made up of the component of following weight portion:
Tea seed extract solution:175g;Clover extract solution:35g;Kiss-me extract solution:35g;Fruit of summer cypress extract solution:35g;Snake
Oil:30g;Gumbo extract solution:35g;Giant knotweed extract solution:25g;Ecliptae herba extract solution:25g;Sodium hyaluronate:5g;Ethoxy urea:
20g;Soybean lecithin:80g;Beeswax:50g;Citric acid:5g;Natural essence:6g;Balance of deionized water, total amount is 1000g.
(Two)Prepare
(1)First by ecliptae herba extract solution, sodium hyaluronate, ethoxy urea, clover extract solution, kiss-me extract solution, the fruit of summer cypress
Extract solution, gumbo extract solution are added in deionized water by weight, and 70 DEG C are warmed up under magnetic agitation effect;
(2)Snake oil, beeswax, soybean lecithin, tea seed extract solution are sequentially added by reaction weight portion in another reactor, is put
It is placed in be heated in 80 DEG C of water-baths and is completely dissolved;
(3)After water phase, oil phase substance are all melted, oil phase is uniformly poured into water phase under quick stirring action, makes water
Oily two-phase is reacted completely, and pH value is determined after 2min, with lemon acid for adjusting pH between 6.5~7;
(4)Mixture is placed under refiner, 4min is homogenized under 1.8w/min power;
(5)It is to be cooled to 40 DEG C when, perfuming accurate adjustment is fragrant, after being cooled to room temperature, stands 3d, can tinning after stabilization.
Embodiment 3
(One)Formula
A kind of multifunction environment-protection type cream containing tea-seed oil is made up of the component of following weight portion:
Tea seed extract solution:190g;Clover extract solution:30g;Kiss-me extract solution:30g;Fruit of summer cypress extract solution:30g;Snake
Oil:30g;Gumbo extract solution:30g;Giant knotweed extract solution:30g;Ecliptae herba extract solution:25g;Sodium hyaluronate:5g;Ethoxy urea:
15g;Soybean lecithin:40g;Beeswax:40g;Citric acid:5g;Natural essence:6g;Balance of deionized water, total amount is 1000g.
(Two)Prepare
(1)First by ecliptae herba extract solution, sodium hyaluronate, ethoxy urea, clover extract solution, kiss-me extract solution, the fruit of summer cypress
Extract solution, gumbo extract solution are added in deionized water by weight, and 70 DEG C are warmed up under magnetic agitation effect;
(2)Snake oil, beeswax, soybean lecithin, tea seed extract solution are sequentially added by reaction weight portion in another reactor, is put
It is placed in be heated in 70 DEG C of water-baths and is completely dissolved;
(3)After water phase, oil phase substance are all melted, oil phase is uniformly poured into water phase under quick stirring action, makes water
Oily two-phase is reacted completely, and pH value is determined after 2min, with lemon acid for adjusting pH between 6.5~7;
(4)Mixture is placed under machine, 4min is homogenized under 1.8w/min power;
(5)It is to be cooled to 40 DEG C when, perfuming accurate adjustment is fragrant, after being cooled to room temperature, stands 3d, can tinning after stabilization.
Embodiment 4
(One)Formula
A kind of multifunction environment-protection type cream containing tea-seed oil is made up of the component of following weight portion:
Tea seed extract solution:190g;Clover extract solution:40g;Kiss-me extract solution:50g;Fruit of summer cypress extract solution:25g;Snake
Oil:30g;Gumbo extract solution:25g;Giant knotweed extract solution:25g;Ecliptae herba extract solution:25g;Sodium hyaluronate:5g;Ethoxy urea:
15g;Soybean lecithin:100g;Beeswax:40g;Citric acid:5g;Natural essence:7.5g;Balance of deionized water, total amount is
1000g。
(Two)Prepare
(1)First by ecliptae herba extract solution, sodium hyaluronate, ethoxy urea, clover extract solution, kiss-me extract solution, the fruit of summer cypress
Extract solution, gumbo extract solution are added in deionized water by weight, and 75 DEG C are warmed up under magnetic agitation effect;
(2)Snake oil, beeswax, soybean lecithin, tea seed extract solution are sequentially added by reaction weight portion in another reactor, is put
It is placed in be heated in 75 DEG C of water-baths and is completely dissolved;
(3)After water phase, oil phase substance are all melted, oil phase is uniformly poured into water phase under quick stirring action, makes water
Oily two-phase is reacted completely, and pH value is determined after 2min, with lemon acid for adjusting pH between 6.5~7;
(4)Mixture is placed under refiner, 4min is homogenized under 1.8w/min power;
(5)It is to be cooled to 40 DEG C when, perfuming accurate adjustment is fragrant, after being cooled to room temperature, stands 3d, can tinning after stabilization.
Embodiment 5
(One)Formula
A kind of multifunction environment-protection type cream containing tea-seed oil is made up of the component of following weight portion:
Tea seed extract solution:175g;Clover extract solution:50g;Kiss-me extract solution:50g;Fruit of summer cypress extract solution:50g;Snake
Oil:45g;Gumbo extract solution:25g;Giant knotweed extract solution:25g;Ecliptae herba extract solution:25g;Sodium hyaluronate:7.5g;Ethoxy urea:
15g;Soybean lecithin:75g;Beeswax:50g;Citric acid:7.5g;Natural essence:7.5g;Balance of deionized water, total amount is
1000g。
(Two)Prepare
(1)First by ecliptae herba extract solution, sodium hyaluronate, ethoxy urea, clover extract solution, kiss-me extract solution, the fruit of summer cypress
Extract solution, gumbo extract solution are added in deionized water by weight, and 80 DEG C are warmed up under magnetic agitation effect;
(2)Snake oil, beeswax, soybean lecithin, tea seed extract solution are sequentially added by reaction weight portion in another reactor, is put
It is placed in be heated in 70 DEG C of water-baths and is completely dissolved;
(3)After water phase, oil phase substance are all melted, oil phase is uniformly poured into water phase under quick stirring action, makes water
Oily two-phase is reacted completely, and pH value is determined after 2min, with lemon acid for adjusting pH between 6.5~7;
(4)Mixture is placed under refiner, 4min is homogenized under 1.8w/min power;
(5)It is to be cooled to 40 DEG C when, perfuming accurate adjustment is fragrant, after being cooled to room temperature, stands 3d, can tinning after stabilization.
Embodiment 6
(One)Formula
A kind of multifunction environment-protection type cream containing tea-seed oil is made up of the component of following weight portion:
Tea seed extract solution:225g;Clover extract solution:30g;Kiss-me extract solution:30g;Fruit of summer cypress extract solution:25g;Snake
Oil:45g;Gumbo extract solution:35g;Giant knotweed extract solution:40g;Ecliptae herba extract solution:40g;Sodium hyaluronate:8g;Ethoxy urea:
30g;Soybean lecithin:100g;Beeswax:40g;Citric acid:8g;Natural essence:8g;Balance of deionized water, total amount is
1000g。
(Two)Prepare
(1)First by ecliptae herba extract solution, sodium hyaluronate, ethoxy urea, clover extract solution, kiss-me extract solution, the fruit of summer cypress
Extract solution, gumbo extract solution are added in deionized water by weight, and 70~80 DEG C are warmed up under magnetic agitation effect;
(2)Snake oil, beeswax, soybean lecithin, tea seed extract solution are sequentially added by reaction weight portion in another reactor, is put
It is placed in be heated in 70~80 DEG C of water-baths and is completely dissolved;
(3)After water phase, oil phase substance are all melted, oil phase is uniformly poured into water phase under quick stirring action, makes water
Oily two-phase is reacted completely, and pH value is determined after 2min, with lemon acid for adjusting pH between 6.5~7;
(4)Mixture is placed under refiner, work 4min under 1.8w/min power;
(5)It is to be cooled to 40 DEG C when, perfuming accurate adjustment is fragrant, after being cooled to room temperature, stands 3d, can tinning after stabilization.
Embodiment 7
(One)Formula
A kind of multifunction environment-protection type cream containing tea-seed oil is made up of the component of following weight portion:
Tea seed extract solution:225g;Clover extract solution:50g;Kiss-me extract solution:40g;Fruit of summer cypress extract solution:30g;Snake
Oil:25g;Gumbo extract solution:25g;Giant knotweed extract solution:30g;Ecliptae herba extract solution:35g;Sodium hyaluronate:5g;Ethoxy urea:
20g;Soybean lecithin:75g;Beeswax:50g;Citric acid:5g;Natural essence:7.5g;Balance of deionized water, total amount is
1000g。
(Two)Prepare
(1)First by ecliptae herba extract solution, sodium hyaluronate, ethoxy urea, clover extract solution, kiss-me extract solution, the fruit of summer cypress
Extract solution, gumbo extract solution are added in deionized water by weight, and 80 DEG C are warmed up under magnetic agitation effect;
(2)Snake oil, beeswax, soybean lecithin, tea seed extract solution are sequentially added by reaction weight portion in another reactor, is put
It is placed in be heated in 80 DEG C of water-baths and is completely dissolved;
(3)After water phase, oil phase substance are all melted, oil phase is uniformly poured into water phase under quick stirring action, makes water
Oily two-phase is reacted completely, and pH value is determined after 2min, with lemon acid for adjusting pH between 6.5~7;
(4)Mixture is placed under refiner, 4min is homogenized under 1.8w/min power;
(5)It is to be cooled to 40 DEG C when, perfuming accurate adjustment is fragrant, after being cooled to room temperature, stands 3d, can tinning after stabilization.
Embodiments of the invention are the foregoing is only, the protection domain of patent application of the invention is not thereby limited, it is all
It is the equivalent structure or equivalent flow conversion made using present specification content, or is directly or indirectly used in other related skills
Art field, is similarly included in the protection domain of patent application of the invention.
Claims (9)
1. a kind of preparation method of the multifunction environment-protection type cream containing tea-seed oil, it is characterised in that count by weight, by with
Lower raw material is prepared from:
Tea seed extract solution:15~25 parts;
Clover extract solution:2~7 parts;
Kiss-me extract solution:2~8 parts;
Fruit of summer cypress extract solution:2~6 parts;
Snake oil:2~5 parts;
Gumbo extract solution:2~5 parts;
Giant knotweed extract solution:2~5 parts;
Ecliptae herba extract solution:2~5 parts;
Sodium hyaluronate:0.1~1.0 part;
Ethoxy urea:1~5 part;
Soybean lecithin:5~12 parts;
Beeswax:3~8 parts;
Citric acid:0.3~1.5 part;
Natural essence:0.5~1 part;
Balance of deionized water, total amount is 100 parts.
2. a kind of preparation method of multifunction environment-protection type cream containing tea-seed oil according to claim 1, its feature exists
In preparation process includes as follows:
(1)First by ecliptae herba extract solution, sodium hyaluronate, ethoxy urea, clover extract solution, kiss-me extract solution, the fruit of summer cypress
Extract solution, gumbo extract solution are added in deionized water by weight, and 70~80 DEG C are warmed up under magnetic agitation effect;
(2)Snake oil, beeswax, soybean lecithin, tea seed extract solution are sequentially added by reaction weight portion in another reactor, is put
It is placed in be heated in 70~80 DEG C of water-baths and is completely dissolved;
(3)After water phase, oil phase substance are all melted, oil phase is uniformly poured into water phase under quick stirring action, makes water
Oily two-phase is reacted completely, and pH value is determined after 2min, with lemon acid for adjusting pH between 6.5~7;
(4)Mixture is placed under refiner, work 4min under 1.8w/min power;
(5)It is to be cooled to 40 DEG C when, perfuming accurate adjustment is fragrant, after being cooled to room temperature, stands 3d, can tinning after stabilization.
3. a kind of preparation method of multifunction environment-protection type cream containing tea-seed oil according to claim 1, its feature exists
In the preparation method of the tea seed extract solution is as follows:
(1)100 parts of tea seeds are crushed to 30-50 mesh, are dispersed in water, make raw material: the mass ratio of solvent is 1:5, stirring is filled
Divide mixing;
(2)0.35 part of cellulase is added under the conditions of 50 DEG C in suspension, 3h is fully reacted in stirring;
(3)0.25 part of amylase is added, 2h is fully reacted in stirring;
(4)0.35 part of protease is added, stirring is fully reacted 1.5h, filtered, and removes filter residue;
(5)2.5 parts of NaOH, stirring reaction 2h under the conditions of 60 DEG C are added then to concentrate the filtrate to 150 deals in filtrate,
Obtain final product tea seed extract solution.
4. a kind of preparation method of multifunction environment-protection type cream containing tea-seed oil according to claim 1, its feature exists
In the preparation method of the kiss-me extract solution is as follows:
(1)100 portions of kiss-mes are cleaned, is crushed, be scattered in 75% alcoholic solution, make raw material: the mass ratio of solvent is 1:10,
Stirring is sufficiently mixed;
(2)0.5 part of cellulase is added under the conditions of 50 DEG C in kiss-me suspension, 2h is fully reacted in stirring;Filtering, removes
Remove filter residue;
(3)Recovered alcohol, and concentrate the filtrate to 300 parts, obtain final product kiss-me extract solution.
5. a kind of preparation method of multifunction environment-protection type cream containing tea-seed oil according to claim 1, its feature exists
In the preparation method of the giant knotweed extract solution is as follows:
(1)100 parts of giant knotweeds are cleaned, is crushed, be dispersed in water, make raw material: the mass ratio of solvent is 1:10, stirring is fully mixed
Close;
(2)0.75 part of cellulase is added under the conditions of 50 DEG C in suspension, 1.5h is fully reacted in stirring;
(3)0.5 portion of hemicellulase is added, 0.5h is fully reacted in stirring;
(4)0.5 part of protease stirring, 2h after reaction fully, filtering is added to remove filter residue in suspension;
(5)450 parts are concentrated the filtrate to, giant knotweed extract solution is obtained final product.
6. a kind of preparation method of multifunction environment-protection type cream containing tea-seed oil according to claim 1, its feature exists
In the preparation method of the fruit of summer cypress extract solution is as follows:
(1)100 parts of fruit of summer cypress are crushed to 30-50 mesh, are dispersed in water, make raw material: the mass ratio of solvent is 1:5, stirring is filled
Divide mixing, 0.5h is incubated under the conditions of 70 DEG C, filter, filtrate is standby;
(2)Filter residue in step 1 is dispersed in water, makes raw material: the mass ratio of solvent is 1:5, in 50 DEG C of bars in suspension
0.3 part of cellulase is added under part, 3h is fully reacted in stirring;
(3)0.3 part of amylase is added, 2h is fully reacted in stirring;
(4)0.5 part of protease is added, stirring is fully reacted 1.5h, filtered, and removes filter residue;
(5)Filtrate is merged with the filtrate in step 1,300 deals are concentrated into, fruit of summer cypress extract solution is obtained final product.
7. a kind of preparation method of multifunction environment-protection type cream containing tea-seed oil according to claim 1, its feature exists
In the preparation method of the gumbo extract solution is as follows:
(1)100 portions of gumbos are cleaned, is crushed, be scattered in 75% alcohol water blend, make raw material:The mass ratio of solvent is 1:5,
Stirring is sufficiently mixed;1.5h is incubated under the conditions of 60 DEG C, is filtered, remove filter residue;
(2)Recovered alcohol, and concentrate the filtrate to 200 parts, obtain final product stone gumbo extract solution.
8. a kind of preparation method of multifunction environment-protection type cream containing tea-seed oil according to claim 1, its feature exists
In the preparation method of the ecliptae herba extract solution is as follows:
(1)100 parts of ecliptae herbas are cleaned, is crushed, be scattered in 75% alcohol water blend, make raw material:The mass ratio of solvent is 1:
5, stirring is sufficiently mixed;2.5h is incubated under the conditions of 60 DEG C, is filtered, remove filter residue;
(2)Recovered alcohol, and concentrate the filtrate to 200 parts, obtain final product ecliptae herba extract solution.
9. a kind of preparation method of multifunction environment-protection type cream containing tea-seed oil according to claim 1, its feature exists
In the preparation method of the clover extract solution is as follows:
(1)100 portions of clovers are cleaned, is crushed, be scattered in 75% alcohol water blend, make raw material:The mass ratio of solvent is 1:
5, stirring is sufficiently mixed;2h is incubated under the conditions of 60 DEG C, is filtered, remove filter residue;
(2)Recovered alcohol, and concentrate the filtrate to 200 parts, obtain final product clover extract solution.
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CN107970157A (en) * | 2017-12-16 | 2018-05-01 | 唐雪平 | A kind of preparation method of the crease-resistant plant essence containing natural lemon acid |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN107693445A (en) * | 2017-10-18 | 2018-02-16 | 湖南大三湘油茶生态产业有限公司 | Gentle camellia oleifera fruit skin cream and preparation method thereof |
CN107970157A (en) * | 2017-12-16 | 2018-05-01 | 唐雪平 | A kind of preparation method of the crease-resistant plant essence containing natural lemon acid |
CN107970157B (en) * | 2017-12-16 | 2020-06-05 | 广州药妆日用化工有限公司 | Preparation method of anti-wrinkle plant essence containing natural citric acid |
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