CN106176316A - A kind of tea saponin shampoo - Google Patents
A kind of tea saponin shampoo Download PDFInfo
- Publication number
- CN106176316A CN106176316A CN201610741073.5A CN201610741073A CN106176316A CN 106176316 A CN106176316 A CN 106176316A CN 201610741073 A CN201610741073 A CN 201610741073A CN 106176316 A CN106176316 A CN 106176316A
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- CN
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- Prior art keywords
- tea saponin
- tea
- shampoo
- concentrated solution
- seed oil
- Prior art date
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Emergency Medicine (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of tea saponin shampoo, including tea saponin concentrated solution, tea-seed oil, glycerol, silk peptide, guar gum, Kazon, essence and deionized water, waste liquid after wherein tea saponin concentrated solution is by extracting tea seed oil by using enzymatic hydrolysis is that raw material prepares, its concentration is 50%～55%, the invention also discloses extraction and the preparation method of tea saponin shampoo of tea saponin.Natural non-stimulated, the fungistatic effect of the present invention and antidandruff efficacy are good, and gentleness does not hinder hair quality and scalp, wash and protect effective and to human body and environmentally friendly, and preparation technology is simple, and controllability is strong, and environmental protection is suitable to produce on a large scale, and application prospect is extensive.
Description
Technical field
The present invention relates to daily-use chemical industry technology, particularly relate to a kind of tea saponin shampoo.
Background technology
People's living standard improves now, and increasingly attaching importance to environmental protection and the application of natural prodcuts, the most daily washing protects use
Product.Shampoo currently as one of requisite washing product in daily is based on chemical composition mostly, rarer sky
So composition, though having stronger cleaning effect, but life-time service has certain infringement to hair quality, root of hair, scalp, is easily caused and sends out
Matter is fragile, cracking, and scalp is sensitive and the problem such as alopecia；And in production process and use waste liquid big for environment pollution, it is difficult to
Degraded, does not meets the development trend of environmental protection.Therefore people modulate to have preferably to wash in the urgent need to natural materials simultaneously and protect effect
The shampoo of fruit.
Summary of the invention
The invention provides a kind of tea saponin shampoo, which overcome the deficiency existing for the shampoo of prior art it
Place.
The technical solution adopted for the present invention to solve the technical problems is: a kind of tea saponin shampoo, this shampoo formula
For: the tea saponin concentrated solution of 15～25 weight portions, 5～15 weight portion activating agent 6501,0.5～2 weight portion tea-seed oil,
The glycerol of 5～10 weight portions, 1～4 silk peptide, 0.5～2 guar gum, 0.05～0.2 cards of weight portion of weight portion of weight portion
Pine, 0～0.2 weight portion essence and the deionized water of 50～70 weight portions；In wherein said tea saponin concentrated solution, tea saponin
Mass percent be 50%～55%；
The preparation method of this tea saponin shampoo is: first prepare tea saponin concentrated solution, under continuously stirred state, by institute
After stating tea saponin concentrated solution and the deionized water mixed dissolution of ratio, regulate pH to 5～6, add activating agent 6501, tea-seed
Oil, glycerol and silk peptide, react 0.5～2h at 45 DEG C～65 DEG C, and mixing speed is 20～40r/min, be subsequently adding guar gum,
Kazon and essence, obtain described tea saponin shampoo after dissolving and stirring.
Preferably, described tea saponin shampoo by 15%～25% tea saponin concentrated solution, 5%～15% 6501,
The guar gum of the silk peptide of the glycerol of tea-seed oil, 5%～10%, 1%～4%, 0.5%～2% of 0.5%～2%, 0.05%
～the deionized water composition of the essence of the Kazon of 0.2%, 0～0.2% and surplus.
Preferably, described tea saponin shampoo by 20% tea saponin concentrated solution, the 6501 of 10%, the tea-seed oil of 1%,
The glycerol of 7%, the silk peptide of 2%, the guar gum of 1%, the Kazon of 0.1%, 0～the essence of 0.1% and the deionized water of surplus
Composition.
Preferably, in described tea saponin concentrated solution, the mass percent of tea saponin is 53.15%.
Preferably, the preparation process of described tea saponin concentrated solution is: it is former for taking the waste liquid after extracting tea seed oil by using enzymatic hydrolysis
Material, the ethanol of raw material and 60% concentration mixes with 1:3, regulates pH to 8, acts on 1h at 70 DEG C, takes supernatant and add after being centrifuged
Chitosan solution stirring 1min, adds auxiliary agent stirring 2min, stands 6h under room temperature, take supernatant and add calcium oxide, room after being centrifuged
2.5h is stirred under temperature, centrifugal after standing overnight, with water, precipitation is moved in beaker, add ammonium hydrogen carbonate as transforming agent, stirring
Reacting 3.5h after Jun Yun at 40 DEG C, the supernatant after being centrifuged is dried and is prepared described tea saponin concentrated solution.
Preferably, described pH value is 5.5.
Preferably, described reaction temperature is 60 DEG C, and the response time is 1h.
Tea saponin is the nonionic surfactant of a kind of pure natural, not only has emulsifying, decontamination, dispersion, moistening, foaming
Etc. kinds of surface activity, and there is anti-dandruff, antipruritic function.And itself readily biodegradable does not pollutes the environment, performance
Soft, aqueous solution is subacidity.
Tea saponin has stronger inhibitory action to escherichia coli, staphylococcus aureus, bacillus subtilis, yeast,
The existing gram positive bacteria of repressed strain has again gram negative bacteria, existing coccus to have again bacillus, it is seen that tea saponin has
The bacteriostasis of spectrum.
The tea saponin shampoo of the present invention, with tea saponin and 6,501 two kinds of surfactant compounds, adds Folium Camelliae sinensis simultaneously
Seed oil, silk peptide and glycerol are as conditioner and a small amount of additive such as thickening agent, preservative, and product is natural non-stimulated, antibacterial
Effect and antidandruff efficacy are good, and gentleness does not hinder hair quality and scalp, wash protect effective and to human body and environmentally friendly.
The tea saponin of the present invention is to extract, using the waste liquid after extracting tea seed oil by using enzymatic hydrolysis, the tea saponin obtained as raw material
Concentrated solution form coordinates with other components, it is achieved that the utilization to waste liquid, and shampoo preparation technology is simple, and controllability is strong, green
Environmental protection, is suitable to produce on a large scale, and application prospect is extensive.
The present invention is described in further detail by following example；But a kind of tea saponin shampoo of the present invention is not limited to
Embodiment.
Detailed description of the invention
A kind of tea saponin shampoo, its formula includes the tea saponin concentrated solution of 15～25 weight portions, 5～15 work of weight portion
The property tea-seed oil of agent 6501,0.5～2 weight portion, 5～10 glycerol, 1～4 silk peptide, 0.5～2 weight of weight portion of weight portion
Part guar gum, 0.05～0.2 weight portion Kazon, 0～0.2 weight portion essence and the deionization of 50～70 weight portions
Water.
As one preferred embodiment, tea saponin shampoo by 15%～25% tea saponin concentrated solution, 5%～
The melon of the silk peptide of the glycerol of tea-seed oil, 5%～10%, 1%～4%, 0.5%～2% of 6501,0.5%～the 2% of 15%
The deionized water composition of that glue, 0.05%～the essence of the Kazon of 0.2%, 0～0.2% and surplus.
Further preferably, tea saponin shampoo by 20% tea saponin concentrated solution, the 6501 of 10%, the tea-seed oil of 1%,
The glycerol of 7%, the silk peptide of 2%, the guar gum of 1%, the Kazon of 0.1%, 0～the essence of 0.1% and the deionized water of surplus
Composition.
Wherein, tea saponin concentrated solution and activating agent 6501 are as surfactant, and the foam stability of tea saponin is extremely strong,
And foaming power is not affected by hardness of water change, foam performance is preferable, but foaming power is the strongest.Activating agent 6501 is soluble in water,
Having good foaming, steady bubble, infiltration decontamination, the function such as hard water resistance, both compound the shampoo obtained, comprehensive clean-up performance
Good, zest can be reduced simultaneously, improve shampoo outward appearance.
Tea-seed oil, glycerol and silk peptide are as conditioner, and little molecule silk peptide just can penetrate into keratodermatitis, play moisturizing
Effect, it is i.e. combined with skin epithelial cell through horny layer, and by cytosis absorption of nutrient ingredients, participates in and promote cell
Metabolism, makes skin gloss, moist, soft, high resilience；Glycerol has preferable moisturizing effect；Tea-seed oil has guarantor
Wet, moist, the function of hair care, can effectively prevent hairs break and alopecia.Conditioner nourishes hair while clean hair
And scalp, maintenance effect is good.
Guar gum is as thickening agent, and Kazon is as preservative, and essence improves fragrance, and three's trace adds, the hair washing obtained
Aqueous shape is stable, it is simple to preserves and uses, and fragrance is pleasant simultaneously, and experience is good.
The preparation method of tea saponin shampoo, first prepares tea saponin concentrated solution, under continuously stirred state, by described ratio
After the tea saponin concentrated solution of example and deionized water mixed dissolution, regulate pH to 5～6, add activating agent 6501, tea-seed oil, sweet
Oil and silk peptide, react 0.5～2h at 45 DEG C～65 DEG C, and mixing speed is 20～40r/min, is subsequently adding guar gum, Kazon
And essence, obtain tea saponin shampoo after dissolving and stirring.
Wherein, the preparation method of tea saponin concentrated solution, be the waste liquid after taking extracting tea seed oil by using enzymatic hydrolysis be raw material, raw material
Mix with 1:3 with the ethanol of 60% concentration, regulate pH to 8, at 70 DEG C, act on 1h, take supernatant addition chitosan after being centrifuged molten
Liquid stirring 1min, adds auxiliary agent stirring 2min, stands 6h under room temperature, take supernatant and add calcium oxide, stir under room temperature after being centrifuged
2.5h, centrifugal after standing overnight, with water, precipitation is moved in beaker, addition ammonium hydrogen carbonate as transforming agent, after stirring
Reacting 3.5h at 40 DEG C, the supernatant after being centrifuged is dried and is prepared.In tea saponin concentrated solution, the mass percent of tea saponin is 50%
～55%.
As one preferred embodiment, the preparation of tea saponin shampoo, it is under continuously stirred state, by content is
After the tea saponin concentrated solution of 53.15% and deionized water mixed dissolution, regulate pH to 5.5, add activating agent 6501, tea-seed
Oil, glycerol and silk peptide, react 1h at 60 DEG C, and mixing speed is 30r/min, is subsequently adding guar gum, Kazon and fragrant in right amount
Essence, obtains after dissolving and stirring.
The shampoo made meets GB/T 29679-2013 shampoo, hair cream state compulsion standard, and physicochemical property is shown in Table
1:
The physicochemical property of table 1 shampoo
Above-described embodiment is only used for further illustrating a kind of tea saponin shampoo of the present invention, but the invention is not limited in
Embodiment, every any simple modification, equivalent variations and modification above example made according to the technical spirit of the present invention,
Each fall within the protection domain of technical solution of the present invention.
Claims (7)
1. a tea saponin shampoo, it is characterised in that: include the tea saponin concentrated solution of 15～25 weight portions, 5～15 weight portions
The tea-seed oil of activating agent 6501,0.5～2 weight portion, 5～10 glycerol, 1～4 silk peptide, 0.5～2 of weight portion of weight portion
The guar gum of weight portion, 0.05～0.2 weight portion Kazon, 0～0.2 weight portion essence and 50～70 weight portions go from
Sub-water；In wherein said tea saponin concentrated solution, the mass percent of tea saponin is 50%～55%；
The preparation method of this tea saponin shampoo is: first prepare tea saponin concentrated solution, under continuously stirred state, by described ratio
After the tea saponin concentrated solution of example and deionized water mixed dissolution, regulate pH to 5～6, add activating agent 6501, tea-seed oil, sweet
Oil and silk peptide, react 0.5～2h at 45 DEG C～65 DEG C, and mixing speed is 20～40r/min, is subsequently adding guar gum, Kazon
And essence, obtain described tea saponin shampoo after dissolving and stirring.
Tea saponin shampoo the most according to claim 1, it is characterised in that: described tea saponin shampoo is by 15%～25%
The glycerol of the tea-seed oil of the 6501 of tea saponin concentrated solution, 5%～15%, 0.5%～2%, 5%～10%, 1%～4%
The essence of the Kazon of the guar gum of silk peptide, 0.5%～2%, 0.05%～0.2%, 0～0.2% and the deionization of surplus
Water forms.
Tea saponin shampoo the most according to claim 2, it is characterised in that: described tea saponin shampoo by 20% tea soap
Element concentrated solution, the 6501 of 10%, the tea-seed oil of 1%, the glycerol of 7%, the silk peptide of 2%, the guar gum of 1%, the card of 0.1%
The deionized water composition of pine, 0～the essence of 0.1% and surplus.
Tea saponin shampoo the most according to claim 1, it is characterised in that: in described tea saponin concentrated solution, tea saponin
Mass percent is 53.15%.
Tea saponin shampoo the most according to claim 1, it is characterised in that: the preparation process of described tea saponin concentrated solution
For: taking the waste liquid after extracting tea seed oil by using enzymatic hydrolysis is raw material, and the ethanol of raw material and 60% concentration mixes with 1:3, and regulation pH is extremely
8, at 70 DEG C, act on 1h, take supernatant after being centrifuged and add chitosan solution stirring 1min, add auxiliary agent stirring 2min, under room temperature
Stand 6h, take supernatant after being centrifuged and add calcium oxide, under room temperature, stir 2.5h, centrifugal after standing overnight, with water, precipitation is moved into
In beaker, addition ammonium hydrogen carbonate, as transforming agent, reacts 3.5h at 40 DEG C after stirring, the supernatant after being centrifuged dries system
Obtain described tea saponin concentrated solution.
Tea saponin shampoo the most according to claim 1, it is characterised in that: described pH value is 5.5.
Tea saponin shampoo the most according to claim 1, it is characterised in that: described reaction temperature is 60 DEG C, the response time
It is 1h.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610741073.5A CN106176316A (en) | 2016-08-26 | 2016-08-26 | A kind of tea saponin shampoo |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610741073.5A CN106176316A (en) | 2016-08-26 | 2016-08-26 | A kind of tea saponin shampoo |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106176316A true CN106176316A (en) | 2016-12-07 |
Family
ID=57527038
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610741073.5A Pending CN106176316A (en) | 2016-08-26 | 2016-08-26 | A kind of tea saponin shampoo |
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| Country | Link |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108904392A (en) * | 2018-09-18 | 2018-11-30 | 广西壮族自治区农业科学院农产品加工研究所 | A kind of Tea Saponin shampoo and preparation method thereof |
| CN108904370A (en) * | 2018-06-24 | 2018-11-30 | 覃海平 | A kind of shampoo and preparation method thereof that nuisanceless, moisturizing is taken care of hair |
| CN109846737A (en) * | 2019-02-27 | 2019-06-07 | 广东医科大学 | One kind is containing disposable hand cleanser of Tea Saponin and preparation method thereof |
| CN111686040A (en) * | 2019-03-11 | 2020-09-22 | 中国科学院青岛生物能源与过程研究所 | Tea saponin shampoo and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101830948A (en) * | 2010-05-11 | 2010-09-15 | 武汉工业学院 | Method for preparing tea saponin by using tea seed degreased dreg |
| CN103520036A (en) * | 2013-10-12 | 2014-01-22 | 湖南金浩茶油股份有限公司 | Hair-loss-preventing shampoo |
| CN104622738A (en) * | 2015-01-07 | 2015-05-20 | 安徽省华银茶油有限公司 | Novel high-permeability tea seed oil liquid shampoo |
-
2016
- 2016-08-26 CN CN201610741073.5A patent/CN106176316A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101830948A (en) * | 2010-05-11 | 2010-09-15 | 武汉工业学院 | Method for preparing tea saponin by using tea seed degreased dreg |
| CN103520036A (en) * | 2013-10-12 | 2014-01-22 | 湖南金浩茶油股份有限公司 | Hair-loss-preventing shampoo |
| CN104622738A (en) * | 2015-01-07 | 2015-05-20 | 安徽省华银茶油有限公司 | Novel high-permeability tea seed oil liquid shampoo |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108904370A (en) * | 2018-06-24 | 2018-11-30 | 覃海平 | A kind of shampoo and preparation method thereof that nuisanceless, moisturizing is taken care of hair |
| CN108904392A (en) * | 2018-09-18 | 2018-11-30 | 广西壮族自治区农业科学院农产品加工研究所 | A kind of Tea Saponin shampoo and preparation method thereof |
| CN109846737A (en) * | 2019-02-27 | 2019-06-07 | 广东医科大学 | One kind is containing disposable hand cleanser of Tea Saponin and preparation method thereof |
| CN111686040A (en) * | 2019-03-11 | 2020-09-22 | 中国科学院青岛生物能源与过程研究所 | Tea saponin shampoo and preparation method thereof |
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Application publication date: 20161207 |