CN106955248A - A kind of plant profit supports shampoo and its method for preparing extractive and preparation method thereof - Google Patents

A kind of plant profit supports shampoo and its method for preparing extractive and preparation method thereof Download PDF

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Publication number
CN106955248A
CN106955248A CN201710209029.4A CN201710209029A CN106955248A CN 106955248 A CN106955248 A CN 106955248A CN 201710209029 A CN201710209029 A CN 201710209029A CN 106955248 A CN106955248 A CN 106955248A
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parts
oil
extract
plant
sodium
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辛桂彬
刘志彬
李峻青
孙晓炜
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Shanghai If Biotechnology Co Ltd
Shanghai Pu Da Industry & Trade Co Ltd
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Shanghai If Biotechnology Co Ltd
Shanghai Pu Da Industry & Trade Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • A61K8/375Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • A61K8/442Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4906Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/678Tocopherol, i.e. vitamin E
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/737Galactomannans, e.g. guar; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/86Polyethers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/002Preparations for repairing the hair, e.g. hair cure
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/02Preparations for cleaning the hair

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  • Cosmetics (AREA)

Abstract

Shampoo is supported the invention discloses a kind of profit of plant in daily chemical product field, is made up of the raw material of following parts by weight:0.5 ~ 1.5 part of disodium ethylene diamine tetraacetate, 25 ~ 35 parts of laureth sodium sulfovinate, 6 ~ 10 parts of sodium cocoyl glycinate, 4 ~ 8 parts of sodium methyl cocoyl taurate, 3 ~ 5 parts of butanediol, 0.3 ~ 0.5 part of xanthans, 0.3 ~ 0.5 part of citric acid, 0.01 ~ 0.03 part of methylisothiazolinone, 25 ~ 35 parts of Cocoamidopropyl betaine, 10 0.6 ~ 1 part of polyquaternium, 0.6 ~ 1 part of guar hydroxypropyltrimonium chloride, beautiful 1 ~ 5 part of Ao Biniya palm kernel oils, 1 ~ 5 part of oil with hydrogenated soybean, 1 ~ 5 part of coconut oil, 1 ~ 5 part of linseed oil, 1 ~ 5 part of tocopherol, 4 ~ 8 parts of coconut palm oleoyl monoethanolamine, 3 ~ 5 parts of glycol distearate, 0.5 ~ 1.5 part of Phenoxyethanol, 1 ~ 5 part of fleece-flower root root extract, 1 ~ 3 part of grapefruit seed extract, 1 ~ 5 part of Semen Sesami Nigrum extract, 100 ~ 200 parts of deionized water, the present invention has preferably cleaning lubricant effect.

Description

A kind of plant profit supports shampoo and its method for preparing extractive and preparation method thereof
Technical field
The present invention relates to a kind of daily chemical product, more particularly to a kind of shampoo.
Background technology
Because the personnel's Active workings narrow space, working environment dust and greasy dirt in coal mine working are big, hair is cleaned not Thoroughly, hair follicle blocking is easily caused.And operating personnel's bathing frequency is high, mining area domestic water hardness is larger, is damaged for hair quality Wound is than more serious.
The content of the invention
Shampoo and its method for preparing extractive and preparation method thereof are supported it is an object of the invention to provide a kind of plant profit, can Deeply cleaning hair and hair follicle, efficiently wash away dust, greasy dirt, eliminate hard water influence.
The object of the present invention is achieved like this:A kind of plant profit supports shampoo, it is characterised in that by following parts by weight Raw material is constituted:0.5 ~ 1.5 part of disodium ethylene diamine tetraacetate, 25 ~ 35 parts of laureth sodium sulfovinate, sodium cocoyl glycinate 6 ~ 10 parts, 4 ~ 8 parts of sodium methyl cocoyl taurate, 3 ~ 5 parts of butanediol, 0.3 ~ 0.5 part of xanthans, 0.3 ~ 0.5 part of citric acid, first 0.01 ~ 0.03 part of base OIT, 25 ~ 35 parts of Cocoamidopropyl betaine, 0.6 ~ 1 part of Polyquaternium-10, melon glue 0.6 ~ 1 part of hydroxypropyl-trimethyl ammonium chloride, beautiful 1 ~ 5 part of Ao Biniya palm kernel oils, 1 ~ 5 part of oil with hydrogenated soybean, coconut oil 1 ~ 5 Part, 1 ~ 5 part of linseed oil, 1 ~ 5 part of tocopherol, 4 ~ 8 parts of coconut palm oleoyl monoethanolamine, 3 ~ 5 parts of glycol distearate, benzene oxygen second 0.5 ~ 1.5 part of alcohol, 1 ~ 5 part of fleece-flower root root extract, 1 ~ 3 part of grapefruit seed extract, 1 ~ 5 part of Semen Sesami Nigrum extract, deionization 100 ~ 200 parts of water.
It is used as the further restriction of the present invention, 0.7 ~ 1.3 part of disodium ethylene diamine tetraacetate, laureth sodium sulfovinate 25 ~ 30 parts, 7 ~ 9 parts of sodium cocoyl glycinate, 5 ~ 7 parts of sodium methyl cocoyl taurate, 4 parts of butanediol, 0.4 part of xanthans, lemon 0.4 part of lemon acid, 0.02 part of methylisothiazolinone, 25 ~ 30 parts of Cocoamidopropyl betaine, Polyquaternium-10 0.7 ~ 0.9 Part, 0.7 ~ 0.9 part of guar hydroxypropyltrimonium chloride, beautiful 2 ~ 4 parts of Ao Biniya palm kernel oils, 2 ~ 4 parts of oil with hydrogenated soybean, 2 ~ 4 parts of coconut oil, 2 ~ 4 parts of linseed oil, 2 ~ 4 parts of tocopherol, 5 ~ 7 parts of coconut palm oleoyl monoethanolamine, glycol distearate 4 Part, 0.5 ~ 1.0 part of Phenoxyethanol, 2 ~ 4 parts of fleece-flower root root extract, 2 parts of grapefruit seed extract, 2 ~ 4 parts of Semen Sesami Nigrum extract, 100 ~ 150 parts of deionized water.
It is used as the further restriction of the present invention, 1 part of disodium ethylene diamine tetraacetate, 28 parts of laureth sodium sulfovinate, coconut palm 8 parts of oleoyl Sodium Glycinate, 5 parts of sodium methyl cocoyl taurate, 4 parts of butanediol, 0.4 part of xanthans, 0.4 part of citric acid, first 0.02 part of base OIT, 25 parts of Cocoamidopropyl betaine, 0.8 part of Polyquaternium-10, melon glue hydroxypropyl trimethylammonium 0.8 part of ammonium chloride, beautiful 2 parts of Ao Biniya palm kernel oils, 2 parts of oil with hydrogenated soybean, 2 parts of coconut oil, 2 parts of linseed oil, fertility 2 parts of phenol, 5 parts of coconut palm oleoyl monoethanolamine, 3 parts of glycol distearate, 1 part of Phenoxyethanol, 3 parts of fleece-flower root root extract, Portugal 2 parts of grape shaddock seed extract, 3 parts of Semen Sesami Nigrum extract, 150 parts of deionized water.
A kind of plant profit supports shampoo method for preparing extractive, comprises the following steps:
1)Raw material is chosen, the fleece-flower root, grapefruit seed and Semen sesami nigrum is chosen, the going mouldy, damage by worms of plant, sick scar part is removed, and go Except the field trash in plant;
2)Surface clean, the plant by selection is respectively placed in supersonic wave cleaning machine, adds the sodium bicarbonate that concentration is 3 ~ 5% The aqueous solution, is cleaned by ultrasonic 10 ~ 20 minutes, removes plant surface dirt and residues of pesticides, then with after distilled water flushing 3 times, dries in the air It is dry stand-by;
3)Infiltration is crushed, the plant after selection cleaning is crushed, coarse crushing to granularity is less than 50mm, will be planted at normal temperatures Thing particle deionized water, the mass ratio of plant particle deionized water is 1:3, soak 10 ~ 20 minutes, shaken using cell disruptor Swing 10 ~ 20 minutes, obtain suspension;
4)Solvent extraction, heating and refluxing extraction is carried out by gained suspension with mass concentration for 60% glycerin solution, and the third three The mass ratio of alcohol solution and suspension is 2:1, temperature control is at 80 DEG C, and refluxing extraction 3 hours, extraction is cooled down after terminating and carried Thing is taken to less than 38 DEG C;
5)Fine filtering, with the filter material that filtering accuracy is 100 mesh, clear liquid is obtained through vacuum filtration, why first respectively Crow, grapefruit seed and Semen sesami nigrum.
A kind of plant profit supports shampoo preparation method, comprises the following steps:
1)Each component is weighed by formula ratio, it is standby;
2)By step 1)The deionized water that weighs, disodium ethylene diamine tetraacetate, laureth sodium sulfovinate, cocounut oil acyl glycine Sodium, sodium methyl cocoyl taurate are mixed, stirred evenly, and are warming up to vacuum after 75 ~ 90 DEG C and are pumped into main reaction pot;
3)By the butanediol weighed, xanthans, citric acid and methylisothiazolinone, with step 2)Mixed liquor 20 ~ 30 It is sufficiently stirred under rev/min 80 ~ 100 minutes;
4)To step 3)Mixed liquor in add weighed Cocoamidopropyl betaine, Polyquaternium-10, melon glue hydroxypropyl Base trimethyl ammonium chloride, beauty Ao Biniya palm kernel oils, oil with hydrogenated soybean, coconut oil, linseed oil, tocopherol, cocounut oil acyl list Monoethanolamine and glycol distearate, mixing speed are stirred 25 ~ 35 minutes at 20 ~ 30 revs/min;
5)By step 4)The mixed liquor of gained is cooled to 40 ~ 50 DEG C, add the Phenoxyethanol weighed, fleece-flower root root extract, Grapefruit seed extract and Semen Sesami Nigrum extract are sufficiently stirred for 55 ~ 65 minutes under 20 ~ 30 revs/min;
6)By step 5)The mixed liquor of gained is cooled to 38 DEG C of room temperatures, stands 60 ~ 70 minutes and can obtain product.
Compared with prior art, the beneficial effects of the present invention are the present invention has preferable lubricity, efficiently washes away powder Dirt, greasy dirt, while the present invention is preferable to calcium ions and magnesium ions elimination effect, eliminates hard water influence, nourish and submissive stiff hair, repair The fragile position easy to break of hair, protection hair quality is injury-free, hair is become more glossy and toughness, is harmful into without any Point, gentle, non-stimulated, the shop floor worker for being particularly suitable for use in coal mine working is used, and the effect that each component in the present invention is brought is such as Under:
Disodium ethylene diamine tetraacetate:It is used as complexing agent;
Laureth sodium sulfovinate:Surfactant, for the effect such as washing, emulsifying, soak, is not influenceed by the water hardness;
Sodium cocoyl glycinate:It is the main component glycine of human body skin collagen and the coco-nut oil fatty acid institute extracted in plant The amino acid surfactant of generation, belongs to neutral-alkaline, can obtain smooth and rich springy foam, use cunning It is refreshing not tight;
Sodium methyl cocoyl taurate:Formed by the aliphatic acid and the condensation of N-methyltaurine sodium of natural origin, be a kind of amino Acid type surfactant, it has good foaming effect under hard water conditions, with it is excellent go to degrease, dust and breast Change, dispersibility, low irritant, and the excitant of other surfactants can be reduced;
Butanediol:Do NMF and solvent is used, while also there is certain bacteriostasis;
Xanthans:Emulsifying agent, stabilizer in shampoo formula, thickening agent, size;
Citric acid:Citric acid belongs to one kind of tartaric acid, and main function is to speed up cutin renewal, and the receipts of pore are thin;
Methylisothiazolinone:It is efficient germicide in cosmetics;
Cocoamidopropyl betaine:It is a kind of zwitterionic surfactant, is respectively provided with acid and alkalescence condition excellent Stability, excitant is small, and soluble in water, to ph stability, foam is more, strong detergency, with excellent thickening property, softness Property, bactericidal properties, antistatic behaviour, hard water resistance property;
Polyquaternium-10:Hair skin moistening can be kept, affinity is strong, maintenance hair jag, position easy to break, forms saturating on hair Bright, continuous film, improves damaged hair;
Guar hydroxypropyltrimonium chloride:Compatibility with hair is good, can form thin film in hair and skin surface, With good protective effect, hair compliance prevents damage, with good dry and wet cardability, it is possible to decrease surfactant pair The excitant of eyes and skin;
Beautiful Ao Biniya palm kernel oils:Nonionic surface active agent, as emulsifying agent, has moist nourish to send out skin effect;
Oil with hydrogenated soybean:With fabulous emulsification and stable emulsifying performance, the protective layer formed, which can be improved, dries hair skin Moisture-retaining capacity, can also improve the healing ability of damaged skin;
Coconut oil:It can effectively penetrate into inside hair, reduce the dilation of keratin, enemy initiates to protection well to make With;
Linseed oil:Linseed oil unsaturated fatty acid content is high, has excellent affinity and penetration to hair skin, can Releive hair follicle, surfactant is fully contacted root of hair, improve clean result, contained a variety of aliphatic acid are readily absorbed by, and make head Hair keeps moistening smooth flexible;
Tocopherol:In shampoo, pigment granule when can reduce tissue aging in cell can also improve hair skin elasticity, have Anti-aging and oxidation resistant effect;
Coconut palm oleoyl monoethanolamine:Main component as detergent, wetting agent and emulsifying agent, the performance with stable foam is resistance to Performance of hard water is good;
Glycol distearate:Can be produced in shampoo obvious pearly-lustre moisten effect, and with thickening, skin care, Hair care hair care and antistatic property, it is non-stimulated to skin, to hair not damaged;
Phenoxyethanol:With antibacterial, corrosion-resistant effect;
Fleece-flower root root extract:Containing nutritional ingredients such as lecithin, with hairy root nourishing, promote the pigmentogenic work of hair black With being a kind of good hair conditioner;
Grapefruit seed extract:There are releive well hair skin and strong anti-oxidation efficacy;
Semen Sesami Nigrum extract:Hair increased gloss, improved the foster effect of profit, promote natural on-off cycles of hair growth and regrowth, also resist head Effect of bits, dry, deep layer regulation hair quality etc..
Embodiment
With reference to specific embodiment, the invention will be further described.
Embodiment 1
A kind of plant profit supports shampoo and its method for preparing extractive and preparation method thereof, and the shampoo is by following parts by weight Raw material is constituted:0.5 part of disodium ethylene diamine tetraacetate, 25 parts of laureth sodium sulfovinate, 6 parts of sodium cocoyl glycinate, methyl 4 parts of cocoyl sodium taurocholate, 3 parts of butanediol, 0.3 part of xanthans, 0.3 part of citric acid, 0.01 part of methylisothiazolinone, coconut palm 25 parts of oleamide CAB, 0.6 part of Polyquaternium-10,0.6 part of guar hydroxypropyltrimonium chloride, beautiful ratio difficult to understand 1 part of the palm kernel oil in Buddhist nun Asia, 1 part of oil with hydrogenated soybean, 1 part of coconut oil, 1 part of linseed oil, 1 part of tocopherol, coconut palm oleoyl monoethanolamine 4 Part, 3 parts of glycol distearate, 0.5 part of Phenoxyethanol, 1 part of fleece-flower root root extract, 1 part of grapefruit seed extract, black sesame 1 part of nettle extract, 100 parts of deionized water;
The method for preparing extractive comprises the following steps:
1)Raw material is chosen, the fleece-flower root, grapefruit seed and Semen sesami nigrum is chosen, the going mouldy, damage by worms of plant, sick scar part is removed, and go Except the field trash in plant;
2)Surface clean, the plant by selection is respectively placed in supersonic wave cleaning machine, adds the sodium bicarbonate that concentration is 3 ~ 5% The aqueous solution, is cleaned by ultrasonic 10 ~ 20 minutes, removes plant surface dirt and residues of pesticides, then with after distilled water flushing 3 times, dries in the air It is dry stand-by;
3)Infiltration is crushed, the plant after selection cleaning is crushed, coarse crushing to granularity is less than 50mm, will be planted at normal temperatures Thing particle deionized water, the mass ratio of plant particle deionized water is 1:3, soak 10 ~ 20 minutes, shaken using cell disruptor Swing 10 ~ 20 minutes, obtain suspension;
4)Solvent extraction, heating and refluxing extraction is carried out by gained suspension with mass concentration for 60% glycerin solution, and the third three The mass ratio of alcohol solution and suspension is 2:1, temperature control is at 80 DEG C, and refluxing extraction 3 hours, extraction is cooled down after terminating and carried Thing is taken to less than 38 DEG C;
5)Fine filtering, with the filter material that filtering accuracy is 100 mesh, clear liquid is obtained through vacuum filtration, why first respectively Crow, grapefruit seed and Semen sesami nigrum;
The shampoo preparation method comprises the following steps:
1)Each component is weighed by formula ratio, it is standby;
2)By step 1)The deionized water that weighs, disodium ethylene diamine tetraacetate, laureth sodium sulfovinate, cocounut oil acyl glycine Sodium, sodium methyl cocoyl taurate are mixed, stirred evenly, and are warming up to vacuum after 75 ~ 90 DEG C and are pumped into main reaction pot;
3)By the butanediol weighed, xanthans, citric acid and methylisothiazolinone, with step 2)Mixed liquor 20 ~ 30 It is sufficiently stirred under rev/min 80 ~ 100 minutes;
4)To step 3)Mixed liquor in add weighed Cocoamidopropyl betaine, Polyquaternium-10, melon glue hydroxypropyl Base trimethyl ammonium chloride, beauty Ao Biniya palm kernel oils, oil with hydrogenated soybean, coconut oil, linseed oil, tocopherol, cocounut oil acyl list Monoethanolamine and glycol distearate, mixing speed are stirred 25 ~ 35 minutes at 20 ~ 30 revs/min;
5)By step 4)The mixed liquor of gained is cooled to 40 ~ 50 DEG C, add the Phenoxyethanol weighed, fleece-flower root root extract, Grapefruit seed extract and Semen Sesami Nigrum extract are sufficiently stirred for 55 ~ 65 minutes under 20 ~ 30 revs/min;
6)By step 5)The mixed liquor of gained is cooled to 38 DEG C of room temperatures, stands 60 ~ 70 minutes and can obtain product.
Embodiment 2
It is distinguished as with embodiment 1:
0.7 part of disodium ethylene diamine tetraacetate, 7 parts of sodium cocoyl glycinate, 5 parts of sodium methyl cocoyl taurate, butanediol 4 Part, 0.4 part of xanthans, 0.4 part of citric acid, 0.02 part of methylisothiazolinone, 0.7 part of Polyquaternium-10, melon glue hydroxypropyl 0.7 part of base trimethyl ammonium chloride, beautiful 2 parts of Ao Biniya palm kernel oils, 2 parts of oil with hydrogenated soybean, 2 parts of coconut oil, linseed oil 2 Part, 2 parts of tocopherol, 5 parts of coconut palm oleoyl monoethanolamine, 4 parts of glycol distearate, 0.5 part of Phenoxyethanol, fleece-flower root root are extracted 2 parts of thing, 2 parts of grapefruit seed extract, 2 parts of Semen Sesami Nigrum extract.
Embodiment 3
It is distinguished as with embodiment 1:
1 part of disodium ethylene diamine tetraacetate, 28 parts of laureth sodium sulfovinate, 8 parts of sodium cocoyl glycinate, methyl cocoyl 5 parts of sodium taurocholate, 4 parts of butanediol, 0.4 part of xanthans, 0.4 part of citric acid, 0.02 part of methylisothiazolinone, polyquaternium- 10 0.8 parts, 0.8 part of guar hydroxypropyltrimonium chloride, beautiful 2 parts of Ao Biniya palm kernel oils, 2 parts of oil with hydrogenated soybean, coconut palm 2 parts of seed oil, 2 parts of linseed oil, 2 parts of tocopherol, 5 parts of coconut palm oleoyl monoethanolamine, 3 parts of glycol distearate, Phenoxyethanol 1 Part, 3 parts of fleece-flower root root extract, 2 parts of grapefruit seed extract, 3 parts of Semen Sesami Nigrum extract, 150 parts of deionized water.
Embodiment 4
It is distinguished as with embodiment 1:
1.3 parts of disodium ethylene diamine tetraacetate, 30 parts of laureth sodium sulfovinate, 9 parts of sodium cocoyl glycinate, methyl cocoyl acyl 7 parts of base sodium taurocholate, 4 parts of butanediol, 0.4 part of xanthans, 0.4 part of citric acid, 0.02 part of methylisothiazolinone, coconut oleoyl amine 30 parts of CAB, 0.9 part of Polyquaternium-10,0.9 part of guar hydroxypropyltrimonium chloride, beautiful Ao Biniya palm fibres 4 parts of benevolence oil, 4 parts of oil with hydrogenated soybean, 4 parts of coconut oil, 4 parts of linseed oil, 4 parts of tocopherol, 7 parts of coconut palm oleoyl monoethanolamine, second two 4 parts of alcohol distearate, 1.0 parts of Phenoxyethanol, 4 parts of fleece-flower root root extract, 2 parts of grapefruit seed extract, Semen sesami nigrum is extracted 4 parts of thing, 150 parts of deionized water.
Embodiment 5
It is distinguished as with embodiment 1:
1.5 parts of disodium ethylene diamine tetraacetate, 35 parts of laureth sodium sulfovinate, 10 parts of sodium cocoyl glycinate, methyl cocoyl 8 parts of acyl taurines sodium, 5 parts of butanediol, 0.5 part of xanthans, 0.5 part of citric acid, 0.03 part of methylisothiazolinone, cocounut oil acyl 35 parts of amine CAB, 1 part of Polyquaternium-10,1 part of guar hydroxypropyltrimonium chloride, beautiful Ao Biniya palm kernels 5 parts of oil, 5 parts of oil with hydrogenated soybean, 5 parts of coconut oil, 5 parts of linseed oil, 5 parts of tocopherol, 8 parts of coconut palm oleoyl monoethanolamine, ethylene glycol 5 parts of distearate, 1.5 parts of Phenoxyethanol, 5 parts of fleece-flower root root extract, 3 parts of grapefruit seed extract, Semen Sesami Nigrum extract 5 Part, 200 parts of deionized water.
Raw material in the present invention derive from purchased in market, and purchase source is as shown in table 1.
Table 1
Randomly select 100 triers of colliery scene front man, using two kinds of common shower creams of in the market with Each 10 times of the product of five embodiments of the invention, contrasts situation:Obtain data and table 2 is made.
Table 2
Note:Tester evaluates obtained assessment result.Effect:10 points best, and 0 point worst.
Assessment result shows that the present invention can bring preferably cleaning lubricant effect to colliery shop floor worker.
, being capable of profound cleaning hair follicle hair and dermatoglyph under hard water environment;Reduce many frequency bathings to hair and The damage of skin;There are plant extracts profit hair treatment and nourishes rough skin.
The invention is not limited in above-described embodiment, on the basis of technical scheme disclosed by the invention, the skill of this area Art personnel are according to disclosed technology contents, it is not necessary to which performing creative labour just can make one to some of which technical characteristic A little to replace and deform, these are replaced and deformed within the scope of the present invention.

Claims (5)

1. a kind of plant profit supports shampoo, it is characterised in that be made up of the raw material of following parts by weight:Disodium ethylene diamine tetraacetate 0.5 ~ 1.5 part, 25 ~ 35 parts of laureth sodium sulfovinate, 6 ~ 10 parts of sodium cocoyl glycinate, sodium methyl cocoyl taurate 4 ~ 8 parts, 3 ~ 5 parts of butanediol, 0.3 ~ 0.5 part of xanthans, 0.3 ~ 0.5 part of citric acid, 0.01 ~ 0.03 part of methylisothiazolinone, 25 ~ 35 parts of Cocoamidopropyl betaine, 0.6 ~ 1 part of Polyquaternium-10, guar hydroxypropyltrimonium chloride 0.6 ~ 1 Part, beautiful 1 ~ 5 part of Ao Biniya palm kernel oils, 1 ~ 5 part of oil with hydrogenated soybean, 1 ~ 5 part of coconut oil, 1 ~ 5 part of linseed oil, tocopherol 1 ~ 5 parts, 4 ~ 8 parts of coconut palm oleoyl monoethanolamine, 3 ~ 5 parts of glycol distearate, 0.5 ~ 1.5 part of Phenoxyethanol, fleece-flower root root is extracted 1 ~ 5 part of thing, 1 ~ 3 part of grapefruit seed extract, 1 ~ 5 part of Semen Sesami Nigrum extract, 100 ~ 200 parts of deionized water.
2. a kind of plant profit according to claim 1 supports shampoo, it is characterised in that and disodium ethylene diamine tetraacetate 0.7 ~ 1.3 parts, 25 ~ 30 parts of laureth sodium sulfovinate, 7 ~ 9 parts of sodium cocoyl glycinate, sodium methyl cocoyl taurate 5 ~ 7 Part, 4 parts of butanediol, 0.4 part of xanthans, 0.4 part of citric acid, 0.02 part of methylisothiazolinone, Cocoamidopropyl betaine 25 ~ 30 parts, 0.7 ~ 0.9 part of Polyquaternium-10,0.7 ~ 0.9 part of guar hydroxypropyltrimonium chloride, beautiful Ao Biniya 2 ~ 4 parts of palm kernel oil, 2 ~ 4 parts of oil with hydrogenated soybean, 2 ~ 4 parts of coconut oil, 2 ~ 4 parts of linseed oil, 2 ~ 4 parts of tocopherol, cocounut oil acyl list second 5 ~ 7 parts of hydramine, 4 parts of glycol distearate, 0.5 ~ 1.0 part of Phenoxyethanol, 2 ~ 4 parts of fleece-flower root root extract, grapefruit seed 2 parts of extract, 2 ~ 4 parts of Semen Sesami Nigrum extract, 100 ~ 150 parts of deionized water.
3. a kind of plant profit according to claim 2 supports shampoo, it is characterised in that 1 part of disodium ethylene diamine tetraacetate, 28 parts of laureth sodium sulfovinate, 8 parts of sodium cocoyl glycinate, 5 parts of sodium methyl cocoyl taurate, 4 parts of butanediol is yellow 0.4 part of virgin rubber, 0.4 part of citric acid, 0.02 part of methylisothiazolinone, 25 parts of Cocoamidopropyl betaine, Polyquaternium-10 0.8 part, 0.8 part of guar hydroxypropyltrimonium chloride, beautiful 2 parts of Ao Biniya palm kernel oils, 2 parts of oil with hydrogenated soybean, coconut 2 parts of oil, 2 parts of linseed oil, 2 parts of tocopherol, 5 parts of coconut palm oleoyl monoethanolamine, 3 parts of glycol distearate, Phenoxyethanol 1 Part, 3 parts of fleece-flower root root extract, 2 parts of grapefruit seed extract, 3 parts of Semen Sesami Nigrum extract, 150 parts of deionized water.
4. a kind of plant profit as described in claim 1-3 supports shampoo method for preparing extractive, it is characterised in that including following Step:
1)Raw material is chosen, the fleece-flower root, grapefruit seed and Semen sesami nigrum is chosen, the going mouldy, damage by worms of plant, sick scar part is removed, and go Except the field trash in plant;
2)Surface clean, the plant by selection is respectively placed in supersonic wave cleaning machine, adds the sodium bicarbonate that concentration is 3 ~ 5% The aqueous solution, is cleaned by ultrasonic 10 ~ 20 minutes, removes plant surface dirt and residues of pesticides, then with after distilled water flushing 3 times, dries in the air It is dry stand-by;
3)Infiltration is crushed, the plant after selection cleaning is crushed, coarse crushing to granularity is less than 50mm, will be planted at normal temperatures Thing particle deionized water, the mass ratio of plant particle deionized water is 1:3, soak 10 ~ 20 minutes, shaken using cell disruptor Swing 10 ~ 20 minutes, obtain suspension;
4)Solvent extraction, heating and refluxing extraction is carried out by gained suspension with mass concentration for 60% glycerin solution, and the third three The mass ratio of alcohol solution and suspension is 2:1, temperature control is at 80 DEG C, and refluxing extraction 3 hours, extraction is cooled down after terminating and carried Thing is taken to less than 38 DEG C;
5)Fine filtering, with the filter material that filtering accuracy is 100 mesh, clear liquid is obtained through vacuum filtration, why first respectively Crow, grapefruit seed and Semen sesami nigrum.
5. a kind of plant profit as described in claim 1-3 supports shampoo preparation method, it is characterised in that comprise the following steps:
1)Each component is weighed by formula ratio, it is standby;
2)By step 1)The deionized water that weighs, disodium ethylene diamine tetraacetate, laureth sodium sulfovinate, cocounut oil acyl glycine Sodium, sodium methyl cocoyl taurate are mixed, stirred evenly, and are warming up to vacuum after 75 ~ 90 DEG C and are pumped into main reaction pot;
3)By the butanediol weighed, xanthans, citric acid and methylisothiazolinone, with step 2)Mixed liquor 20 ~ 30 It is sufficiently stirred under rev/min 80 ~ 100 minutes;
4)To step 3)Mixed liquor in add weighed Cocoamidopropyl betaine, Polyquaternium-10, melon glue hydroxypropyl Base trimethyl ammonium chloride, beauty Ao Biniya palm kernel oils, oil with hydrogenated soybean, coconut oil, linseed oil, tocopherol, cocounut oil acyl list Monoethanolamine and glycol distearate, mixing speed are stirred 25 ~ 35 minutes at 20 ~ 30 revs/min;
5)By step 4)The mixed liquor of gained is cooled to 40 ~ 50 DEG C, add the Phenoxyethanol weighed, fleece-flower root root extract, Grapefruit seed extract and Semen Sesami Nigrum extract are sufficiently stirred for 55 ~ 65 minutes under 20 ~ 30 revs/min;
6)By step 5)The mixed liquor of gained is cooled to 38 DEG C of room temperatures, stands 60 ~ 70 minutes and can obtain product.
CN201710209029.4A 2017-03-31 2017-03-31 A kind of plant profit supports shampoo and its method for preparing extractive and preparation method thereof Pending CN106955248A (en)

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CN108096076A (en) * 2018-01-05 2018-06-01 湖北瑞晟生物有限责任公司 A kind of shampoo and preparation method thereof
CN108703893A (en) * 2018-06-20 2018-10-26 花安堂生物科技集团有限公司 A kind of detergent composition and its application
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CN113576947A (en) * 2020-07-21 2021-11-02 集思美创(广州)科技有限公司 Organic silicon shampoo and preparation method thereof
CN112791028A (en) * 2021-03-04 2021-05-14 澳宝化妆品(惠州)有限公司 Grapefruit extract and preparation method and application thereof
WO2023278726A1 (en) * 2021-06-30 2023-01-05 L'oreal Compositions containing direct dyes for imparting color and tone to the hair
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