CN108619027A - One kind taste of dispelling nourishes shampoo and preparation method thereof - Google Patents

Abstract

The invention discloses one kind tastes of dispelling to nourish shampoo and preparation method thereof.The shampoo of the present invention is made of following raw materials：Baical Skullcap root P.E 0.1~5%,Gotu Kola P.E 0.1~5%,Candlenut tree seed extract 0.1~5%,Semen Cuscutae extract 0.1~5%,Tea-seed oil 0.1~2.5%,Zinc ricinate 0.1~5%,Propylene glycol 0.5~5%,Cocoyl Sodium Glycinate 10~30%,Sodium methyl cocoyl taurate 10~50%,Cocoyl Sodium L-alaninate 10~30%,Octyl/Plantacare 818 0.5~5%,Cocoamidopropyl betaine 5~20%,120 methyl tristearates 0.1~5% of PEG,Glycol laurate 0.1~5%,Polyquaternium 10 0.1~1%,40 4 oleate 0.1~1.5% of sorbeth,Glycerine 0.1~15%,EDTA 2Na 0.1~0.5%,Sodium chloride 0.1~3%,Citric acid 0.01~2%,Essence 0.1~1%,Preservative 0.1~2%,Surplus is water.Product quality of the present invention is stable, pleasant aroma, can remove hair peculiar smell, and effectively inhibit dandruff production, submissive healthy hair.

Description

One kind taste of dispelling nourishes shampoo and preparation method thereof

Technical field

The present invention relates to a kind of hair-washing compositions, belong to daily cosmetics field, and in particular to one kind dispel taste wash nourishing hair Water and preparation method thereof.

Background technology

For shampoo as the product that disappears soon, developed recently is rapid, it was reported that the Chinese shampoo market sales revenue reaches within 2014 To 286.75 hundred million yuan.Shampoo remove cleaning efficacy, mainly also anti-dandruff and itching-relieving, it is submissive repair etc. additional functions.With life Horizontal raising is scalded, hair dyeing sweeps the country.Scald, contaminate it is latter to several weeks hair it is remaining scald, hair dye distribute not pleasant gas Taste.Remaining chemicals smell is pungent, easily causes runny nose or allergy.

Therefore, a shampoo for having and removing and scalding, contaminate residual agent is developed, it will have broad application prospects.

Invention content

The object of the present invention is to provide one kind dispel taste nourish shampoo, peculiar smell smell can be effectively removed, especially suitable for It scalds, smell caused by the residual chemicals after dye, reduces allergy after boiling hot, dye.

It is a further object of the present invention to provide the preparation method that a kind of above-mentioned taste of dispelling nourishes shampoo, the product qualities of preparation Stablize, pleasant aroma, hair peculiar smell can be removed, and effectively inhibits dandruff production, submissive healthy hair.

The present invention is by the following technical programs to realize above-mentioned purpose.

One kind dispel taste nourish shampoo, be made of the raw material of following weight percent meter：

Baical Skullcap root P.E 0.1~5%, Gotu Kola P.E 0.1~5%, candlenut tree seed extract 0.1~5%, Semen Cuscutae carry Take object 0.1~5%, tea-seed oil 0.1~2.5%, zinc ricinate 0.1~5%, propylene glycol 0.5~5%, the sweet ammonia of cocoyl Sour sodium 10~30%, sodium methyl cocoyl taurate 10~50%, cocoyl Sodium L-alaninate 10~30%, octyl/decyl Glucoside 0.5~5%, Cocoamidopropyl betaine 5~20%, PEG-120 methyls tristearate 0.1~5%, third It is glycol laurate 0.1~5%, Polyquaternium-10 0.1~1%, four oleate 0.1~1.5% of sorbeth -40, sweet Oil 0.1~15%, sodium chloride 0.1~3%, citric acid 0.01~2%, essence 0.1~1%, is prevented EDTA-2Na0.1~0.5% Rotten agent 0.1~2%, surplus are water.

As the preferred embodiment of the present invention, the taste of dispelling nourishes shampoo, by weight percentage, by following original Material is made：

Plant extracts 1~4%, tea-seed oil 0.8~2.0%, zinc ricinate 0.5~3.5%, propylene glycol 1~4%, Cocoyl Sodium Glycinate 10~20%, sodium methyl cocoyl taurate 15~35%, cocoyl Sodium L-alaninate 15~ 25%, octyl/Plantacare 818 1~5%, Cocoamidopropyl betaine 10~15%, three stearic acid of PEG-120 methyls Ester 0.5~1.0%, glycol laurate 1.5%, Polyquaternium-10 0.5%, four oleate 0.5 of sorbeth -40~ 1.0%, glycerine 5~10%, EDTA-2Na 0.1~0.3%, sodium chloride 0.8~2.5%, citric acid 0.3~1.8%, essence 0.25~0.5%, preservative 0.6~1.5%, surplus are water.

As the preferred embodiment of the present invention, the taste of dispelling nourishes raw material system of the shampoo by following weight percent meter At：

Plant extracts 4%, tea-seed oil 2%, zinc ricinate 1%, propylene glycol 3%, cocoyl Sodium Glycinate 10%, Sodium methyl cocoyl taurate 15%, cocoyl Sodium L-alaninate 15%, octyl/Plantacare 818 1%, cocamidopropyl propyl amide Glycine betaine 10%, PEG-120 methyls tristearate 1.5%, glycol laurate 1.5%, Polyquaternium-10 0.5%, four oleate 0.5% of sorbeth -40, glycerine 4%, EDTA-2Na 0.1%, sodium chloride 0.8%, citric acid 0.3%, essence 0.25%, preservative 0.6%, water 28.95%.

Further, the plant extracts is Baical Skullcap root P.E 0.1~5%, Gotu Kola P.E 0.1~5%, candlenut tree The combination of seed extract 0.1~5%, Semen Cuscutae extract 0.1~5% 4 kind ingredient.

Further, the preservative is the mixture of Phenoxyethanol and Sensiva SC50, Phenoxyethanol and ethyl hexyl The weight ratio of base glycerol is 9：1.

The present invention also provides a kind of preparation methods of above-mentioned taste shampoo of dispelling, and include the following steps：

1) by Baical Skullcap root P.E, Gotu Kola P.E, candlenut tree seed extract, Semen Cuscutae extract, tea-seed oil, ricinoleic acid Zinc is added in propylene glycol, stirs evenly, is prepared into taste composition of dispelling, spare；

2) enough water is added in reaction pot, opens stirring, EDTA-2Na is added to the water；

3) primary surfactant is added (includes：Cocoyl Sodium Glycinate, sodium methyl cocoyl taurate, cocounut oil acyl Base Sodium L-alaninate, octyl/Plantacare 818, Cocoamidopropyl betaine, PEG-120 methyls tristearate, the third two Alcohol laurate, four oleate of sorbeth -40, glycerine), 75 DEG C or so are heated to, stirring to dissolving；

4) system is cooled to 55~65 DEG C, water-dispersible good Polyquaternium-10 in advance is added, and stir evenly；

5) system is cooled to 35~45 DEG C, and sodium chloride, citric acid, essence are then added into system, stirs to completely molten Solution adjusts pH to 5.5~6.5；

6) the taste composition of dispelling of step 1) is added, stirs evenly, is eventually adding preservative, stir evenly.

Compared with prior art, advantage of the invention is that：

1) present invention taste shampoo taste effect of dispelling of dispelling is strong, to the smelly of sulfohydrate, mercaptan, thioether, isothiocyanic acid and ammonia etc. Taste removal rate is up to 98%, especially suitable for newly scalding the hair nursing contaminated.

2) present invention dispels taste shampoo with fungistatic effect, 30min is acted on to staphylococcus aureus, to escherichia coli 20min is acted on, 40min is acted on to Candida albicans, killing rate is up to 99.9% or more.

3) present invention dispel taste shampoo have the function of moisturizing, moisten, blacking hair and nourishing face, for taking care of hair, can anti-hairs break and Alopecia；Present invention taste shampoo of dispelling is mildly nonirritant simultaneously, is particularly suitable for having dandruff and scalp sensitive users, contributes to it slow Symptom is solved, can be applicable.

Specific implementation mode

The present invention is further described below by way of specific implementation mode, but the present invention is not limited only to following embodiment. In the scope of the present invention or present disclosure is not being departed from, in spirit and scope, to taste shampoo of the present invention of dispelling And preparation method thereof be suitably modified, replace the identical component of effect, be apparent to those skilled in the art , they are considered as being included within the scope of the present invention.

Unless stated otherwise, all percentages of the invention are all calculated with the mass percentage of composition, all proportions It is mass percent.

Following raw material components are commercial product；Following Baical Skullcap root P.E, Gotu Kola P.E, candlenut tree seed extract, Tu Silk seed extract Four Plants extract and tea-seed oil, zinc ricinate, propylene glycol constitute taste composition of dispelling；And the extract It can be extracting solution ingredient.

A kind of taste of dispelling nourishes the preparation method of shampoo, including each raw material component as shown in table 1 below：

The taste of dispelling of 1 embodiment 1-3 of table nourishes the component proportion (weight percent %) of shampoo and comparative example 1-2

Comparative example 1 is not added with plant extraction liquid compared to embodiment 1, and comparison row 2 are not added with castor oil compared to embodiment 2 Sour zinc and tea-seed oil, comparative example 3 are not added with zinc ricinate compared to embodiment 3.

Taste shampoo of dispelling in embodiment 1 is prepared according to the following steps：

1) by Baical Skullcap root P.E, Gotu Kola P.E, candlenut tree seed extract, Semen Cuscutae extract, tea-seed oil, ricinoleic acid Zinc is added in propylene glycol, stirs evenly, is prepared into taste composition of dispelling, spare；

2) enough water is added in reaction pot, opens stirring, EDTA-2Na is added to the water；

3) primary surfactant is added (includes：Cocoyl Sodium Glycinate, sodium methyl cocoyl taurate, cocounut oil acyl Base Sodium L-alaninate, octyl/Plantacare 818, Cocoamidopropyl betaine, PEG-120 methyls tristearate, the third two Alcohol laurate, four oleate of sorbeth -40, glycerine), 75 DEG C or so are heated to, stirring to dissolving；

4) system is cooled to 60 DEG C, water-dispersible good Polyquaternium-10 in advance is added, and stir evenly；

5) system is cooled to 40 DEG C, and sodium chloride, citric acid, essence are then added into system, and stirring is adjusted to being completely dissolved Save pH to 6.

6) the taste composition of dispelling of step 1) is added, stirs evenly, is eventually adding preservative, stir evenly.

Embodiment 2~3 and 1~3 preparation process of comparative example are similar to Example 1.

It is the content of effete test embodiment part below.

1, taste shampoo of dispelling dispel taste experiment

Experimental method：

10g test samples are put in salable bottle, 10mL ammonium hydroxide is added or are passed through 10mL hydrogen sulfide, is sealed, puts 10min is set, 5 microlitres of headspace sampling tests the surplus of ammonium hydroxide and hydrogen sulfide after removal with gas-chromatography, while with without taste group of dispelling The shampoo for closing object does blank control, and the removal rate to ammonium hydroxide and hydrogen sulfide of product has deducted control group removal amount.

Test result see the table below shown in 2.

2 present invention of table dispels the effect that eliminates the unusual smell (removal rate/%) of taste shampoo

Project	Embodiment 1	Embodiment 2	Embodiment 3	Comparative example 1	Comparative example 2	Comparative example 3
							Ammonium hydroxide	99%	98%	97%	90%	50%	5%
Hydrogen sulfide	98%	98%	96%	93%	70%	6%

From 2 data of table it is found that embodiment 1 is dispelled, taste shampoo is best to the removal rate of ammonium hydroxide and hydrogen sulfide, illustrates the proportioning Relatively rationally.

Comparative example 1 is not added with plant extraction liquid compared to embodiment 1, and comparison row 2 are not added with castor oil compared to embodiment 2 Sour zinc and tea-seed oil, comparative example 3 are not added with zinc ricinate compared to embodiment 3.

The taste shampoo of dispelling of comparative example 2 and comparative example 3 is very low to the removal rate of ammonium hydroxide and hydrogen sulfide, illustrates ricinoleic acid Zinc has very strong removal effect, plant extraction liquid and tea oil taste effect of dispelling to it to have synergistic work in ammonium hydroxide, hydrogen sulfide etc. With.

2, it dispels taste shampoo bacteriostatic experiment

It is the fungistatic effect (bacteriostasis rate/%) that table 3 is taste shampoo of the invention of dispelling below.

3 present invention of table dispels the fungistatic effect (bacteriostasis rate/%) of taste shampoo

Project	Embodiment 1	Embodiment 2	Embodiment 3	Comparative example 1	Comparative example 2	Comparative example 3
							Escherichia coli	99%	93%	97%	90%	50%	3%
Staphylococcus aureus	98%	98%	99%	93%	30%	6%
							Candida albicans	99%	96%	97%	90%	50%	5%
Chlosma	98%	98%	96%	93%	40%	7%

Remarks：Action time is 5min, activity 1:1.

It can be obtained by upper table 3, the good antimicrobial effect of 1~3 shampoo of the embodiment of the present invention, to escherichia coli, golden yellow Staphylococcus, Candida albicans killing rate up to 95%, reach《Resist antibacterial detergent》The requirement of bacteriostasis rate >=90% in standard, Therefore the present invention dispels taste shampoo to there is extremely strong inhibiting effect to chlosma, can be effectively anti-dandruff.Wherein embodiment 1 is antibacterial Rate highest illustrates that 1 each component of embodiment and proportioning synergistic effect are most strong.Plant extracts, comparison are free of in 1 shampoo of comparative example 2 shampoo of example only contains plant extracts, and bacteriostasis rate will be low compared to Examples 1 to 3, illustrates plant extract of the present invention For object with tea-seed oil and zinc ricinate there are very strong synergistic effect, three's compounding can play very strong bacteriostasis.

3, the taste shampoo consumer that dispels experiment on probation

Experimental method：By the taste shampoo of dispelling of Examples 1 to 3 and comparative example 1~3, recruit scalded in one week contaminated hair or Hair scalp is easy peculiar smell or has each 30 people of the volunteer of dandruff, tries out two weeks, is evaluated according to the anti-dandruff, effect that eliminates the unusual smell Marking, have positive effect makes 5 scores, and no improvement makes 1 score.

4 present invention of table dispels the use result of taste shampoo

Be free of plant extracts in 1 shampoo of comparative example it can be seen from the structure of table 4 above, moisturizing hair care and mild Property is significantly worse than Examples 1 to 3, and 2 shampoo of comparative example only contains plant extracts, and anti-dandruff and taste effect of dispelling is compared to reality That applies example 1~3 will be low, illustrates plant extracts of the present invention and tea-seed oil and zinc ricinate there are very strong synergistic effect, Three's compounding can play that very strong taste of dispelling is anti-dandruff and hair care.

The above described is only a preferred embodiment of the present invention, be not intended to limit the present invention in any form, therefore It is every without departing from technical solution of the present invention content, simply repaiied to any made by above example according to the technical essence of the invention Change, equivalent variations and modification, in the range of still falling within technical solution of the present invention.

Claims (6)

1. one kind is dispelled, taste nourishes shampoo, it is characterised in that：By percentage to the quality, including following each component

Plant extracts 0.1~5%, tea-seed oil 0.1~2.5%, zinc ricinate 0.1~5%, propylene glycol 0.5~5%, coconut palm Oleoyl Sodium Glycinate 10~30%, sodium methyl cocoyl taurate 10~50%, cocoyl Sodium L-alaninate 10~30%, Octyl/Plantacare 818 0.5~5%, Cocoamidopropyl betaine 5~20%, PEG-120 methyl tristearates 0.1~5%, propylene glycol monolaurate 0.1~5%, Polyquaternium-10 0.1~1%, four oleate of sorbeth -40 0.1~1.5%, glycerine 0.1~15%, EDTA-2Na 0.1~0.5%, sodium chloride 0.1~3%, citric acid 0.01~2%, Essence 0.1~1%, preservative 0.1~2%, surplus are water.

2. taste as described in claim 1 of dispelling nourishes shampoo, it is characterised in that：By weight percentage, by following raw material system At：

Plant extracts 1~4%, tea-seed oil 0.8~2.0%, zinc ricinate 0.5~3.5%, propylene glycol 1~4%, cocounut oil It is acylglycine sodium 10~20%, sodium methyl cocoyl taurate 15~35%, cocoyl Sodium L-alaninate 15~25%, pungent Base/Plantacare 818 1~5%, Cocoamidopropyl betaine 10~15%, PEG-120 methyls tristearate 0.5~ 1.0%, glycol laurate 1.5%, polyquaternium~10 0.5%, the oleate of sorbeth~40 4 0.5~ 1.0%, glycerine 5~10%, EDTA-2Na 0.1~0.3%, sodium chloride 0.8~2.5%, citric acid 0.3~1.8%, essence 0.25~0.5%, preservative 0.6~1.5%, surplus are water.

3. taste as claimed in claim 2 of dispelling nourishes shampoo, it is characterised in that：By weight percentage, by following raw material system At：

Plant extracts 4%, tea-seed oil 2%, zinc ricinate 1%, propylene glycol 3%, cocoyl Sodium Glycinate 10%, methyl Cocoyl sodium taurocholate 15%, cocoyl Sodium L-alaninate 15%, octyl/Plantacare 818 1%, cocamidopropyl propyl amide beet Alkali 10%, PEG-120 methyls tristearate 1.5%, glycol laurate 1.5%, Polyquaternium-10 0.5%, Four oleate 0.5% of sorbeth -40, glycerine 4%, EDTA-2Na 0.1%, sodium chloride 0.8%, citric acid 0.3%, perfume Essence 0.25%, preservative 0.6%, water 28.95%.

4. taste as claimed in claim 1 or 2 of dispelling nourishes shampoo, it is characterised in that：The plant extracts extracts for radix scutellariae Object 0.1~5%, Gotu Kola P.E 0.1~5%, candlenut tree seed extract 0.1~5%, Semen Cuscutae extract 0.1~5% 4 kind The combination of ingredient.

5. the taste of dispelling as described in any one of claim 1-4 nourishes shampoo, it is characterised in that：The preservative is benzene oxygen second The weight ratio of the mixture of alcohol and methylisothiazolinone, Phenoxyethanol and methylisothiazolinone is 9：1.

6. the taste of dispelling described in claim 5 nourishes the preparation method of shampoo, it is characterised in that：Include the following steps：

1) by Baical Skullcap root P.E, Gotu Kola P.E, candlenut tree seed extract, Semen Cuscutae extract, tea-seed oil, zinc ricinate adds Enter in propylene glycol, stir evenly, is prepared into taste composition of dispelling, it is spare；

2) enough water is added in reaction pot, opens stirring, EDTA-2Na is added to the water；

3) primary surfactant is added (includes：Cocoyl Sodium Glycinate, sodium methyl cocoyl taurate, cocoyl third Propylhomoserin sodium, octyl/Plantacare 818, Cocoamidopropyl betaine, PEG-120 methyls tristearate, the propylene glycol moon Cinnamic acid ester, four oleate of sorbeth -40, glycerine), 75 DEG C or so are heated to, stirring to dissolving；

4) system is cooled to 55~65 DEG C, water-dispersible good Polyquaternium-10 in advance is added, and stir evenly；

5) system is cooled to 35~45 DEG C, and sodium chloride, citric acid, essence are then added into system, and stirring is adjusted to being completely dissolved Save pH to 5.5~6.5；

6) the taste composition of dispelling of step 1) is added, stirs evenly, is eventually adding preservative, stir evenly.