CN108904370A - A kind of shampoo and preparation method thereof that nuisanceless, moisturizing is taken care of hair - Google Patents
A kind of shampoo and preparation method thereof that nuisanceless, moisturizing is taken care of hair Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/04—Pretreatment of vegetable raw material
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/06—Production of fats or fatty oils from raw materials by pressing
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/008—Refining fats or fatty oils by filtration, e.g. including ultra filtration, dialysis
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Abstract
The present invention relates to a kind of technical fields of shampoo, specifically disclose a kind of nuisanceless, moisturizing hair care shampoo, which is characterized in that the raw material including following parts by weight is made：1~13 part of green tea oil, 3~21 parts of tea-seed oil, 3~6 parts of Jasmine juice, 0.3~2.5 part of green-tea extract, 0.1~1 part of foaming agent.The present invention has the features such as being used for hair-washing hair-care and moisturize the skin, nuisanceless, moist environmental protection.
Description
Technical field
The present invention relates to a kind of technical fields of shampoo, and in particular to a kind of nuisanceless, moisturizing hair care shampoo and
Preparation method.
Background technique
Green tea tree is Camellia Plants, and tea tree is evergreen shrubs or dungarunga, high l~6m:Tea tree is mostly in 10~November
Generally bloom, it is the main object of people's harvesting that leaf, which is the important nutrition organs of tea tree, the leaf of tea tree can tea making, tea is the world
One of three big beverages, tea are China's famous product, are the traditional exported products in China.China is Chan Cha big country, and the whole nation has 19 according to statistics
A province produces tealeaves, possesses more than 2,500 ten thousand mu of tea place, tea seeds can be about 25 kilograms with oil-producing per acre, by the produced tea in 30% tea place
Leaf seed can use, and produces good tea seed oil per year then and can reach 18.75 ten thousand tons, for the output value up to 7,500,000,000 yuan, tea seeds resource is sufficient.
Tea seeds are not exploited for a long time, if by tea seeds become produce tea seed oil raw material, so that it may for tea grower with
Carry out additional income, the commodity that tea seeds are just increased income at tea grower are conducive to the source for stablizing enterprise's raw materials for production, promote agricultural
Industry restructuring keeps the sustainable development of Tea Production.
However for thousands of years, people concentrate on the focus of tea tree always " tealeaves " part, and for tea seeds
Development and utilization are but difficult to make substantial breakthroughs progress.Therefore, mature tea seeds are except in addition to sexual propagation tea tree, remaining
It is most of all to fall off naturally, it rots in the ground, causes the significant wastage of resource.The production technology for studying tea seed oil has extensively
Wealthy market prospects.Tea seed oil using conventional hot moulding method production easily makes natural nutrient component in tea seed oil, active matter
It is deep that tea seed oil color is made in matter and intrinsic loss of aroma.Cold pressing method produces bitter edible plant leaf seed oil, and shelling and separation of hull from kernel are tired
Difficulty, tea seeds benevolence oil content is high after shelling, and pressurization is difficult, and easily knot thorax, common oil press can not operate normally.
It is not only that tea tree is used, and tea-seed oil is equally by deep processing and utilization.Tea-seed oil also known as camellia oil, tea pear oil
（Fujian is commonly called as）, Wild camellia seed oil, camellia seed oil, tea oil seeds of trees oil.Camellia is Dabie Mountain of China, Fujian, Jiangxi, Hunan（Often
Rather）Etc. ground specialty, good camellia oil, i.e. tea-seed oil can be extracted in fruit；Tea-seed oil is a kind of important food of south China
With oily raw material, exocarp and tea-seed oil benevolence shell are generally had.Tea-seed oil is rich in oil rich in unsaturated fatty acids such as linoleic acid
The physiological activators such as tea seed polyphenol, vitamin E, nutrition and physiological function can match in excellence or beauty olive oil, be better than soybean oil, peanut
The vegetable oil such as oil, better than animal oil.In addition to using, how by the utilization of tea-seed oil bigizationner, constantly assault the main target at this stage
Direction.
Related Chinese patent literature is retrieved, is now enumerated some as follows：
1, Chinese patent<Application number>201510365660. 4<Denomination of invention>Shampoo<Abstract>The invention discloses one kind to wash
Lotion is made of the following ingredient of parts by weight：Dish washing liquid stoste 5-10, coconut oil sodium acetate 10-15, sodium laureth sulfate 5-
10, rose skims the cream off milk 1-5, essence 1-2, olive oil 2-5, wire drawing powder 0.5-2,0. 2-0.4 of Rosemary Oil.The present invention has
Effect cleaning scalp, improves scalp quality, improves antipruritic effect, keep scalp more healthy active, be widely used in various hairs
Matter.
2, Chinese patent<Application number> 201610987890.9<Denomination of invention>A kind of hand cleanser<Abstract>It is of the invention public
A kind of hand cleanser has been opened, has been made of the material of following mass fraction：6~9 parts of glycerol, 3~5 parts of ethyl alcohol, deionized water 30~40
Part, 6~8 parts of asparagus juice, 2~3 parts of laruyl alcohol olein, 3~6 parts of cocoanut fatty acid diethanolamide, 6~7 parts of citric acid,
5~6 parts of milk grass.Dirt-removing power of the present invention is good, removes contamination thoroughly, can reliably be removed to intractable grease stain, will not be to skin
Damage, and can sterilize, antibacterial and antibacterial prevents the intrusion of bacterium, fungi.
From the document retrieved we it can be appreciated that these shampoo or hand cleanser are all applied alone, lack moisturizing hair care；
Also it is applied in combination without open green tea oil and tea-seed oil；So how to overcome the deficiencies of existing technologies, preparation can have one's hair wash and wash
The shampoo of hand double-purpose, this just needs to carry out innovation improvement to the prior art.
Summary of the invention
The purpose of the present invention is overcoming defect in the prior art, and providing one kind can be used to have one's hair wash and be used for wash
Hand；It has no stimulation of the skin, it can the anti-dandruff shampoo taken care of hair with nourishing hair care, the nuisanceless of sterilizing skin moistening, moisturizing and its system
Preparation Method.
In order to realize the purpose of foregoing invention, the technical solution taken is：
A kind of nuisanceless, moisturizing hair care shampoo, the raw material including following parts by weight are made：
1~13 portion of green tea oil, 3~6 parts of Jasmine juice of 3~21 parts of tea-seed oil
0.3~2.5 part of green-tea extract, 0.1~1 part of foaming agent.
Preferably, the preparation method of the green tea oil is：
（1）The fruit of picking 3 years or more green tea trees, obtains tea seeds；
（2）By tea seeds natural drying 8~10 days, until the moisture content of tea seeds is reduced to 6~8%, and tealeaves during sunning
Seed sloughs the green shell on surface naturally, obtains the tea seeds that just shell；
（3）Mechanical dejacketing processing is carried out to first shelling tea seeds, to remove the inner casing of tea seeds, obtains tea seeds benevolence；
（4）Tea seeds benevolence is put into crusher and carries out break process, forms the particle of 8~12 mesh, obtains tea seeds benevolence particle；
（5）Tea seeds benevolence particle is squeezed in such a way that physics cold pressing is squeezed, obtains crude oil；
（6）Crude oil filtering, filter screen cleaning, the fishing continuous cycle operation of slag deslagging are collected under normal pressure；
（7）Stand crude oil, be heated to 50~60 DEG C of heat preservations, and constant temperature stands 60~72 hours, separate moisture in oil removing and
Impurity；
(8) again will clean crude oil 2~3h of low temperature dewatering under 65~70 DEG C, 800mmHg vacuum, removing water content in oil to 0.1% with
Under；
(9) water removal crude oil is stood at 5 DEG C, is passed through ozone, the wax in oil and ester matter is precipitated simultaneously in crystallization, 48~64h of growing the grain
Separation；
（10）Tea seed oil carries out diaphragm filters pressing after crystalline substance will be removed, and operating pressure 0.3Mpa goes the wax and ester matter in oil removing, obtains
Purified green-tea oil.
Preferably, the preparation method of the green-tea extract is：Dewatered fresh green tea leaf is rubbed to broken, addition green tea
The boiling of 8~10 times of weight of weight is boiled 2~3 hours, filtering, and the boiling that filter residue adds 2~3 times of weight is boiled 2~3 hours, is closed
And filtrate twice, being concentrated into the relative densities that 60 DEG C of heat are surveyed is 1.1, obtains green-tea extract.
Preferably, the preparation method of the tea-seed oil is：
The tea seed of decortication removal of impurities is placed in mixer, is heated to 40~50 DEG C and insulated and stirred 3~5 hours, in heating process
The hot water that temperature is 40~50 DEG C is sprayed into, hot water is sprayed by the amount of tea seed gross mass 1~2%, tea seed moisture content after control balance
8~10%, and the difference for the highest moisture content and minimum moisture content for controlling same batch tea seed is no more than 0.2%；Again by tea
Seed is sent into oil expression in squeezer, squeezes resulting tea seed crude oil low temperature alkali refining and takes off free fatty acid；First time ceramic super-filtering film is de-
Soap；Wash degumming；Active bamboo absorption；Level-one tea-seed oil is made in second of ceramic super-filtering film low temperature ultrafiltration impurity elimination；With 50~90
DEG C above-mentioned ceramic super-filtering film of hot water backwash；
The low temperature alkali refining takes off free fatty acid process, be by tea seed crude oil be heated to 50~60 DEG C, weight percent is added
The food grade sodium hydroxide aqueous solution that specific concentration is 1~21%, is slowly stirred about 25~30min, becomes mixing after mixing well
Oil；
The first time ceramic super-filtering film takes off soap process, is by the miscella after de- free fatty acid, it is heated rapidly to 85~
90 DEG C, into first time ceramic super-filtering film, the soap stock in miscella is filtered to isolate, becomes de- soap oil；
The washing Degumming Procedures are in the de- soap oil after first time ceramic super-filtering film takes off soap process, and addition accounts for tea
Seed crude oil total weight 8~10%, the hot water that temperature is 96~97 DEG C enter in static mixer be sufficiently mixed together, enters back into butterfly
It is washed in formula seperator, degumming, dehydration；
The active bamboo absorption, is before active bamboo to be placed in the second ceramic super-filtering film；It is imitated using the flocculation of active bamboo
Benzene contained in oil after degumming, dehydration, chlorine residual should be adsorbed with drainage effect；Reach deodorising effect；
Second of ceramic super-filtering film low temperature ultrafiltration impurity elimination, be after being deodorized oil again second enter ceramic super-filtering film,
Ultrafiltration pressure：0.2Mpa, ultrafiltrate temperature：15~27 DEG C, molecular cut off：5000~10000；With decoloration and paraffin removal, de- again
It is smelly.
Preferably, the static mixer, by the mixed cell of different size of the series installation in hollow pipe
Composition, it is that the flight group of the left and right torsion of one channel is welded that the basic structure of these mixed cells is identical, its technology
Performance：Highest degree of scatter≤5um, liquid-liquid, one solid phase unevenness coefficient S x≤4% of liquid are suitable for viscosity≤105 centipoises
Fluid.
Preferably, the foaming agent includes coconut monoethanolamide, Cocoamidopropyl betaine, 25~32% mono decaglycerin moons
Cinnamic acid ester sulfosuccinic acid monoesters disodium aqua, laurel sodium acyl taurine and the bimonthly cinnamic alcohol ester sodium of citric acid, the coconut monoethanolamide,
Cocoamidopropyl betaine, 25~32% mono decadepolyglycerol laurate sulpho mono succinates, lauroyl ox sulphur
The weight ratio of sour sodium and the bimonthly cinnamic alcohol ester sodium of citric acid is 0.8~1: 1~1.2: 0.8~1.2: 0.5~0.8: 0.8.
Preferably, the anhydrous ten polyglycereol list of the mono decadepolyglycerol laurate sulpho mono succinate system
Monoesters is made in 80~100 DEG C of 1~2h of esterification with equimolar ratio in laurate and maleic anhydride, then with sodium sulfite
With equimolar than 75~98 DEG C of 3~4h of sulfonating reaction of temperature control in an aqueous medium, it is neutralized to neutral products therefrom with sodium hydroxide, is used
Before take its 25~32% aqueous solution, addition 0.1~0.5% pharmaceutical grade decoloration special-purpose activated charcoal is mixed at least 2 in 50~60 DEG C
Filters pressing, decoloration removal of impurities after~3h.
Preferably, the preparation method of the shampoo is：
（1）The petal for winning the Jasmine after raising flowers and spitting perfume (or spice), petal is put into dryer and is dehydrated, take off to water content be 50~
60%, then petal is put into juice extractor and is squeezed the juice, it filters to get Jasmine juice；
（2）Green tea oil is mixed with tea-seed oil, is heated while stirring, is heated to 60~80 DEG C；Heat preservation is added green tea and extracts
Object stirs evenly, and obtains mixture A；
（3）Mixture A is cooled to 45~50 DEG C, foaming agent is added, stirs evenly, obtains mixture B；
（4）Mixture B temperature is down to room temperature, then is slowly added to Jasmine juice among the top surface of mixture B, stands 3~4
Hour is to get shampoo.
Compared with the prior art the present invention, has substantive distinguishing features outstanding and significant progress is：
1, the shampoo of the double-purpose of the invention that can have one's hair wash and wash one's hands；The anti-dandruff hair care of hair washing energy, and nourish scalp；It washes one's hands to sterilize and go
Dirt can effectively remove greasy dirt caused by machine oil；Moreover, the fragrance of Jasmine can be remained with；Preparation process of the invention is without dirt
Dye generates, environmentally protective；Preparation process is terse.
2, the DNA purity of green tea oil is high in the present invention, can effectively keep the pharmacological of green tea, improve the use of green tea oil
Efficiency.
3, tea-seed oil DNA purity is high in the present invention, and the larger raising oil production of energy, and tea seed is maximized
Utilization, extraction process there is no destroy tea seed characteristic, the pharmacological and nutriment of tea seed can be effectively retained, so that making
Used time, the effect of capable of maximumlly playing tea-seed oil；The present invention handles oil-tea camellia seed crude oil and uses ceramic super-filtering film twice, can
It solves the problems, such as that conventional refinery process denaturation tea seed albumen generates color reversion, effectively removes colloid, oil-soluble etc. in camellia seed oil
Impurity；And the micro-nutrient composition that can be effectively maintained in tea oil；Food grade sodium hydroxide aqueous solution is uniquely added in process,
Degumming does not use organic solvent with water as solvent, and not only production cost is low, can also overcome two brought by addition chemical agent
Secondary pollution is conducive to keep the safety in production and prevent to pollute；And after active bamboo is placed in first time ceramic super-filtering film, the second Ceramic excessive filtration
Before film, i.e., active bamboo absorption process is designed and take off soap process and second of ceramic super-filtering film low temperature in first time ceramic super-filtering film
Between ultrafiltration impurity elimination process；Not only benzene contained in oil after degumming, dehydration, chlorine residual absorption can be reached into deodorising effect；Together
When, in practice it has proved that the effect for improving mouthfeel is also acted, unexpected technical effect is produced；Tea-seed oil product yield 90%
More than, purity is up to 100%.
4, Jasmine juice is added in the present invention, improves the fragrance degree of shampoo, Jasmine fragrance can calm the nerves peaceful gas, Jasmine
Juice is added by top, and Jasmine juice can be made slowly to penetrate into from top to bottom, so that entire liquid is all adsorbed with jasmin
Gas, meanwhile, the pharmacological property and nutriment of Jasmine are also absorbed and are merged by liquid.
5, the present invention heats the mixed liquor of green tea oil and tea-seed oil when preparing shampoo, can larger raising mixing
The mobility of liquid, and rate is merged in the absorption that larger can be improved between the two, after fused, generates new pharmacological property, energy
Effectively anti-dandruff, moisturizing hair care；So that the submissive light of hair, moisturizing, reply submissive, lubrication, are full of gloss.
Specific embodiment
It is to combine the embodiment of the present invention below, invention is further described in detail：
Embodiment 1：
A kind of nuisanceless, moisturizing hair care shampoo, the raw material including following parts by weight are made：1 portion of tea-seed oil 3 of green tea oil
Part, 3 parts of Jasmine juice, 0.3 part of green-tea extract, 0.1 part of foaming agent.
Preferably, the preparation method of the green tea oil is：
（1）The fruit of picking 3 years or more green tea trees, obtains tea seeds；
（2）By tea seeds natural drying 8~10 days, until the moisture content of tea seeds is reduced to 6~8%, and tealeaves during sunning
Seed sloughs the green shell on surface naturally, obtains the tea seeds that just shell；
（3）Mechanical dejacketing processing is carried out to first shelling tea seeds, to remove the inner casing of tea seeds, obtains tea seeds benevolence；
（4）Tea seeds benevolence is put into crusher and carries out break process, forms the particle of 8~12 mesh, obtains tea seeds benevolence particle；
（5）Tea seeds benevolence particle is squeezed in such a way that physics cold pressing is squeezed, obtains crude oil；
（6）Crude oil filtering, filter screen cleaning, the fishing continuous cycle operation of slag deslagging are collected under normal pressure；
（7）Crude oil is stood, is heated to 50 DEG C of heat preservations, and constant temperature stands 60 hours, separates the moisture and impurity in oil removing；
(8) will clean crude oil 2~3h of low temperature dewatering under 65 DEG C, 800mmHg vacuum again, 0.1% or less removing water content in oil to；
(9) water removal crude oil is stood at 5 DEG C, is passed through ozone, the wax in oil and ester matter is precipitated simultaneously in crystallization, 48~64h of growing the grain
Separation；
（10）Tea seed oil carries out diaphragm filters pressing after crystalline substance will be removed, and operating pressure 0.3Mpa goes the wax and ester matter in oil removing, obtains
Purified green-tea oil.
Preferably, the preparation method of the green-tea extract is：Dewatered fresh green tea leaf is rubbed to broken, addition green tea
The boiling of 8 times of weight of weight is boiled 2~3 hours, filtering, and the boiling that filter residue adds 2 times of weight is boiled 2~3 hours, and merging is filtered twice
Liquid, being concentrated into the relative density that 60 DEG C of heat are surveyed is 1.1, obtains green-tea extract.
Preferably, the preparation method of the tea-seed oil is：
The tea seed of decortication removal of impurities is placed in mixer, 40 DEG C and insulated and stirred 3~5 hours is heated to, is sprayed into heating process
Temperature is 40 DEG C of hot water, and hot water is sprayed by the amount of tea seed gross mass 1~2%, after control balance tea seed moisture content 8%, and
The difference of the highest moisture content and minimum moisture content that control same batch tea seed is no more than 0.2%；Tea seed is sent into squeezer again
Interior oil expression squeezes resulting tea seed crude oil low temperature alkali refining and takes off free fatty acid；First time ceramic super-filtering film takes off soap；Wash degumming；
Active bamboo absorption；Level-one tea-seed oil is made in second of ceramic super-filtering film low temperature ultrafiltration impurity elimination；It is above-mentioned with 50 DEG C of hot water backwashes
Ceramic super-filtering film；
The low temperature alkali refining takes off free fatty acid process, be by tea seed crude oil be heated to 50 DEG C, it is dense that weight percent is added
The food grade sodium hydroxide aqueous solution that degree is 1%, is slowly stirred about 25min, becomes miscella after mixing well；
The first time ceramic super-filtering film takes off soap process, is that the miscella after de- free fatty acid is heated rapidly to 85 DEG C,
Into first time ceramic super-filtering film, the soap stock in miscella is filtered to isolate, becomes de- soap oil；
The washing Degumming Procedures are in the de- soap oil after first time ceramic super-filtering film takes off soap process, and addition accounts for tea
Seed crude oil total weight 8%, the hot water that temperature is 96 DEG C enter in static mixer be sufficiently mixed together, enters back into butterfly seperator
In washed, degumming, dehydration；
The active bamboo absorption, is before active bamboo to be placed in the second ceramic super-filtering film；It is imitated using the flocculation of active bamboo
Benzene contained in oil after degumming, dehydration, chlorine residual should be adsorbed with drainage effect；Reach deodorising effect；
Second of ceramic super-filtering film low temperature ultrafiltration impurity elimination, be after being deodorized oil again second enter ceramic super-filtering film,
Ultrafiltration pressure：0.2Mpa, ultrafiltrate temperature：15 DEG C, molecular cut off：5000~10000；With decoloration and paraffin removal again, deodorization.
Preferably, the static mixer, by the mixed cell of different size of the series installation in hollow pipe
Composition, it is that the flight group of the left and right torsion of one channel is welded that the basic structure of these mixed cells is identical, its technology
Performance：Highest degree of scatter≤5um, liquid-liquid, one solid phase unevenness coefficient S x≤4% of liquid are suitable for viscosity≤105 centipoises
Fluid.
Preferably, the foaming agent includes coconut monoethanolamide, Cocoamidopropyl betaine, 25~32% mono decaglycerin moons
Cinnamic acid ester sulfosuccinic acid monoesters disodium aqua, laurel sodium acyl taurine and the bimonthly cinnamic alcohol ester sodium of citric acid, the coconut monoethanolamide,
Cocoamidopropyl betaine, 25~32% mono decadepolyglycerol laurate sulpho mono succinates, lauroyl ox sulphur
The weight ratio of sour sodium and the bimonthly cinnamic alcohol ester sodium of citric acid is 0.8: 1: 0.8: 0.5: 0.8.
Preferably, the anhydrous ten polyglycereol list of the mono decadepolyglycerol laurate sulpho mono succinate system
Monoesters is made in 80 DEG C of 1~2h of esterification with equimolar ratio in laurate and maleic anhydride, then with sodium sulfite with etc.
Molar ratio 75 DEG C of 3~4h of sulfonating reaction of temperature control in an aqueous medium, are neutralized to neutral products therefrom with sodium hydroxide, with before taking it
25% aqueous solution, addition 0.1% pharmaceutical grade decoloration special-purpose activated charcoal filters pressing, decoloration removal of impurities after 50 DEG C of mixing at least 2~3h.
Preferably, the preparation method of the shampoo is：
（1）The petal for winning the Jasmine after raising flowers and spitting perfume (or spice), petal is put into dryer and is dehydrated, and taking off to water content is 50%,
Petal is put into juice extractor again and is squeezed the juice, is filtered to get Jasmine juice；
（2）Green tea oil is mixed with tea-seed oil, is heated while stirring, is heated to 60 DEG C；Green-tea extract is added in heat preservation,
It stirs evenly, obtains mixture A；
（3）Mixture A is cooled to 45 DEG C, foaming agent is added, stirs evenly, obtains mixture B；
（4）Mixture B temperature is down to room temperature, then is slowly added to Jasmine juice among the top surface of mixture B, stands 3~4
Hour is to get shampoo.
Embodiment 2：
A kind of nuisanceless, moisturizing hair care shampoo, the raw material including following parts by weight are made：7 portions of tea-seed oils 12 of green tea oil
Part, 4.5 parts of Jasmine juice, 1.4 parts of green-tea extract, 0.55 part of foaming agent.
Preferably, the preparation method of the green tea oil is：
（1）The fruit of picking 3 years or more green tea trees, obtains tea seeds；
（2）By tea seeds natural drying 8~10 days, until the moisture content of tea seeds is reduced to 7%, and tea seeds during sunning
Naturally the green shell on surface is sloughed, the tea seeds that just shell are obtained；
（3）Mechanical dejacketing processing is carried out to first shelling tea seeds, to remove the inner casing of tea seeds, obtains tea seeds benevolence；
（4）Tea seeds benevolence is put into crusher and carries out break process, forms the particle of 8~12 mesh, obtains tea seeds benevolence particle；
（5）Tea seeds benevolence particle is squeezed in such a way that physics cold pressing is squeezed, obtains crude oil；
（6）Crude oil filtering, filter screen cleaning, the fishing continuous cycle operation of slag deslagging are collected under normal pressure；
（7）Crude oil is stood, is heated to 55 DEG C of heat preservations, and constant temperature stands 66 hours, separates the moisture and impurity in oil removing；
(8) will clean crude oil 2~3h of low temperature dewatering under 68 DEG C, 800mmHg vacuum again, 0.1% or less removing water content in oil to；
(9 stand water removal crude oil at 5 DEG C, are passed through ozone, crystallization, growing the grain 56h, and the wax and ester matter being precipitated in oil simultaneously separate；
（10）Tea seed oil carries out diaphragm filters pressing after crystalline substance will be removed, and operating pressure 0.3Mpa goes the wax and ester matter in oil removing, obtains
Purified green-tea oil.
Preferably, the preparation method of the green-tea extract is：Dewatered fresh green tea leaf is rubbed to broken, addition green tea
The boiling of 9 times of weight of weight is boiled 2~3 hours, filtering, and the boiling that filter residue adds 2.5 times of weight is boiled 2~3 hours, is merged twice
Filtrate, being concentrated into the relative density that 60 DEG C of heat are surveyed is 1.1, obtains green-tea extract.
Preferably, the preparation method of the tea-seed oil is：
The tea seed of decortication removal of impurities is placed in mixer, 45 DEG C and insulated and stirred 3~5 hours is heated to, is sprayed into heating process
Temperature is 45 DEG C of hot water, and hot water is sprayed by the amount of tea seed gross mass 1~2%, after control balance tea seed moisture content 8~
10%, and the difference for the highest moisture content and minimum moisture content for controlling same batch tea seed is no more than 0.2%；Tea seed is sent into again
Oil expression in squeezer squeezes resulting tea seed crude oil low temperature alkali refining and takes off free fatty acid；First time ceramic super-filtering film takes off soap；Washing
Degumming；Active bamboo absorption；Level-one tea-seed oil is made in second of ceramic super-filtering film low temperature ultrafiltration impurity elimination；With in 70 DEG C of hot water backwashes
The ceramic super-filtering film stated；
The low temperature alkali refining takes off free fatty acid process, be by tea seed crude oil be heated to 55 DEG C, it is dense that weight percent is added
The food grade sodium hydroxide aqueous solution that degree is 11%, is slowly stirred about 28min, becomes miscella after mixing well；
The first time ceramic super-filtering film takes off soap process, is that the miscella after de- free fatty acid is heated rapidly to 88 DEG C,
Into first time ceramic super-filtering film, the soap stock in miscella is filtered to isolate, becomes de- soap oil；
The washing Degumming Procedures are in the de- soap oil after first time ceramic super-filtering film takes off soap process, and addition accounts for tea
Seed crude oil total weight 9%, the hot water that temperature is 97 DEG C enter in static mixer be sufficiently mixed together, enters back into butterfly seperator
In washed, degumming, dehydration；
The active bamboo absorption, is before active bamboo to be placed in the second ceramic super-filtering film；It is imitated using the flocculation of active bamboo
Benzene contained in oil after degumming, dehydration, chlorine residual should be adsorbed with drainage effect；Reach deodorising effect；
Second of ceramic super-filtering film low temperature ultrafiltration impurity elimination, be after being deodorized oil again second enter ceramic super-filtering film,
Ultrafiltration pressure：0.2Mpa, ultrafiltrate temperature：21 DEG C, molecular cut off：5000~10000；With decoloration and paraffin removal again, deodorization.
Preferably, the static mixer, by the mixed cell of different size of the series installation in hollow pipe
Composition, it is that the flight group of the left and right torsion of one channel is welded that the basic structure of these mixed cells is identical, its technology
Performance：Highest degree of scatter≤5um, liquid-liquid, one solid phase unevenness coefficient S x≤4% of liquid are suitable for viscosity≤105 centipoises
Fluid.
Preferably, the foaming agent includes coconut monoethanolamide, Cocoamidopropyl betaine, 25~32% mono decaglycerin moons
Cinnamic acid ester sulfosuccinic acid monoesters disodium aqua, laurel sodium acyl taurine and the bimonthly cinnamic alcohol ester sodium of citric acid, the coconut monoethanolamide,
Cocoamidopropyl betaine, 25~32% mono decadepolyglycerol laurate sulpho mono succinates, lauroyl ox sulphur
The weight ratio of sour sodium and the bimonthly cinnamic alcohol ester sodium of citric acid is 0.9: 1.1: 1: 0.7: 0.8.
Preferably, the anhydrous ten polyglycereol list of the mono decadepolyglycerol laurate sulpho mono succinate system
Monoesters is made in 90 DEG C of 1~2h of esterification with equimolar ratio in laurate and maleic anhydride, then with sodium sulfite with etc.
Molar ratio 87 DEG C of 3~4h of sulfonating reaction of temperature control in an aqueous medium, are neutralized to neutral products therefrom with sodium hydroxide, with before taking it
30% aqueous solution, addition 0.3% pharmaceutical grade decoloration special-purpose activated charcoal filters pressing, decoloration removal of impurities after 55 DEG C of mixing at least 2~3h.
Preferably, the preparation method of the shampoo is：
（1）The petal for winning the Jasmine after raising flowers and spitting perfume (or spice), petal is put into dryer and is dehydrated, and taking off to water content is 55%,
Petal is put into juice extractor again and is squeezed the juice, is filtered to get Jasmine juice；
（2）Green tea oil is mixed with tea-seed oil, is heated while stirring, is heated to 70 DEG C；Green-tea extract is added in heat preservation,
It stirs evenly, obtains mixture A；
（3）Mixture A is cooled to 48 DEG C, foaming agent is added, stirs evenly, obtains mixture B；
（4）Mixture B temperature is down to room temperature, then is slowly added to Jasmine juice among the top surface of mixture B, stands 3~4
Hour is to get shampoo.
Embodiment 3：
A kind of nuisanceless, moisturizing hair care shampoo, the raw material including following parts by weight are made：13 portions of tea-seed oils of green tea oil
21 parts, 6 parts of Jasmine juice, 2.5 parts of green-tea extract, 1 part of foaming agent.
Preferably, the preparation method of the green tea oil is：
（1）The fruit of picking 3 years or more green tea trees, obtains tea seeds；
（2）By tea seeds natural drying 8~10 days, until the moisture content of tea seeds is reduced to 6~8%, and tealeaves during sunning
Seed sloughs the green shell on surface naturally, obtains the tea seeds that just shell；
（3）Mechanical dejacketing processing is carried out to first shelling tea seeds, to remove the inner casing of tea seeds, obtains tea seeds benevolence；
（4）Tea seeds benevolence is put into crusher and carries out break process, forms the particle of 8~12 mesh, obtains tea seeds benevolence particle；
（5）Tea seeds benevolence particle is squeezed in such a way that physics cold pressing is squeezed, obtains crude oil；
（6）Crude oil filtering, filter screen cleaning, the fishing continuous cycle operation of slag deslagging are collected under normal pressure；
（7）Crude oil is stood, is heated to 60 DEG C of heat preservations, and constant temperature stands 72 hours, separates the moisture and impurity in oil removing；
(8) will clean crude oil 2~3h of low temperature dewatering under 70 DEG C, 800mmHg vacuum again, 0.1% or less removing water content in oil to；
(9) water removal crude oil is stood at 5 DEG C, is passed through ozone, the wax in oil and ester matter is precipitated simultaneously in crystallization, 48~64h of growing the grain
Separation；
（10）Tea seed oil carries out diaphragm filters pressing after crystalline substance will be removed, and operating pressure 0.3Mpa goes the wax and ester matter in oil removing, obtains
Purified green-tea oil.
Preferably, the preparation method of the green-tea extract is：Dewatered fresh green tea leaf is rubbed to broken, addition green tea
The boiling of 10 times of weight of weight is boiled 2~3 hours, filtering, and the boiling that filter residue adds 3 times of weight is boiled 2~3 hours, is merged twice
Filtrate, being concentrated into the relative density that 60 DEG C of heat are surveyed is 1.1, obtains green-tea extract.
Preferably, the preparation method of the tea-seed oil is：
The tea seed of decortication removal of impurities is placed in mixer, 50 DEG C and insulated and stirred 3~5 hours is heated to, is sprayed into heating process
The hot water that temperature is 50 DEG C, hot water are sprayed by the amount of tea seed gross mass 2%, and tea seed moisture content is 10% after control balance, and controls
The difference of the highest moisture content and minimum moisture content of making same batch tea seed is no more than 0.2%；Tea seed is sent into squeezer again
Oil expression squeezes resulting tea seed crude oil low temperature alkali refining and takes off free fatty acid；First time ceramic super-filtering film takes off soap；Wash degumming；It is living
Property bamboo Charcoal Adsorption；Level-one tea-seed oil is made in second of ceramic super-filtering film low temperature ultrafiltration impurity elimination；With the above-mentioned pottery of 90 DEG C of hot water backwashes
Porcelain ultrafiltration membrane；
The low temperature alkali refining takes off free fatty acid process, be by tea seed crude oil be heated to 60 DEG C, it is dense that weight percent is added
The food grade sodium hydroxide aqueous solution that degree is 21%, is slowly stirred about 30min, becomes miscella after mixing well；
The first time ceramic super-filtering film takes off soap process, is that the miscella after de- free fatty acid is heated rapidly to 90 DEG C,
Into first time ceramic super-filtering film, the soap stock in miscella is filtered to isolate, becomes de- soap oil；
The washing Degumming Procedures are in the de- soap oil after first time ceramic super-filtering film takes off soap process, and addition accounts for tea
Seed crude oil total weight 10%, the hot water that temperature is 97 DEG C enter in static mixer be sufficiently mixed together, enter back into butterfly separation
It is washed in machine, degumming, dehydration；
The active bamboo absorption, is before active bamboo to be placed in the second ceramic super-filtering film；It is imitated using the flocculation of active bamboo
Benzene contained in oil after degumming, dehydration, chlorine residual should be adsorbed with drainage effect；Reach deodorising effect；
Second of ceramic super-filtering film low temperature ultrafiltration impurity elimination, be after being deodorized oil again second enter ceramic super-filtering film,
Ultrafiltration pressure：0.2Mpa, ultrafiltrate temperature：27 DEG C, molecular cut off：5000~10000；With decoloration and paraffin removal again, deodorization.
Preferably, the static mixer, by the mixed cell of different size of the series installation in hollow pipe
Composition, it is that the flight group of the left and right torsion of one channel is welded that the basic structure of these mixed cells is identical, its technology
Performance：Highest degree of scatter≤5um, liquid-liquid, one solid phase unevenness coefficient S x≤4% of liquid are suitable for viscosity≤105 centipoises
Fluid.
Preferably, the foaming agent includes coconut monoethanolamide, Cocoamidopropyl betaine, 25~32% mono decaglycerin moons
Cinnamic acid ester sulfosuccinic acid monoesters disodium aqua, laurel sodium acyl taurine and the bimonthly cinnamic alcohol ester sodium of citric acid, the coconut monoethanolamide,
Cocoamidopropyl betaine, 25~32% mono decadepolyglycerol laurate sulpho mono succinates, lauroyl ox sulphur
The weight ratio of sour sodium and the bimonthly cinnamic alcohol ester sodium of citric acid is 1: 1.2: 1.2: 0.8: 0.8.
Preferably, the anhydrous ten polyglycereol list of the mono decadepolyglycerol laurate sulpho mono succinate system
Monoesters is made in 100 DEG C of 1~2h of esterification with equimolar ratio in laurate and maleic anhydride, then with sodium sulfite with etc.
Molar ratio 98 DEG C of 3~4h of sulfonating reaction of temperature control in an aqueous medium, are neutralized to neutral products therefrom with sodium hydroxide, with before taking it
32% aqueous solution, addition 00.5% pharmaceutical grade decoloration special-purpose activated charcoal filters pressing, decoloration after 60 DEG C of mixing at least 2~3h remove
It is miscellaneous.
Preferably, the preparation method of the shampoo is：
（1）The petal for winning the Jasmine after raising flowers and spitting perfume (or spice), petal is put into dryer and is dehydrated, and taking off to water content is 60%,
Petal is put into juice extractor again and is squeezed the juice, is filtered to get Jasmine juice；
（2）Green tea oil is mixed with tea-seed oil, is heated while stirring, is heated to 80 DEG C；Green-tea extract is added in heat preservation,
It stirs evenly, obtains mixture A；
（3）Mixture A is cooled to 50 DEG C, foaming agent is added, stirs evenly, obtains mixture B；
（4）Mixture B temperature is down to room temperature, then is slowly added to Jasmine juice among the top surface of mixture B, stands 3~4
Hour is to get shampoo.
Clinical test
Deep XX, male, 28 years old, hair was withered, whether dandruff mostly itches with scalp；The shampoo for using brand in more instead, does not have
Obtain corresponding curative effect；After being introduced, using shampoo of the invention；It has one's hair wash after a week, dandruff significantly reduces, head
The number itched significantly reduces, and hair is also relatively submissive beautiful；After continuing one week of hair washing, dandruff is eliminated, and hair is soft
Frontlighting is bright, and scalp, which also occasionally has, itches, and is further continued for using a week, the submissive light of hair, without sense of itching, whole body has scalp
Light Jasmine faint scent.
Sieve XX, male, 32 years old, auto repair person, daily both hands greasy dirt, hair was stained with oil, and whole body stinky oil uses washing in the market
Clean seminal plasma is washed, and still has residual greasy dirt, shampoo and shower cream in the market can not thoroughly clean with oily taste；By people
It introduces and uses shampoo of the invention, can easily wash away greasy dirt on hand, and do not remain, completely have with light jasmin
Gas；Hair washing can quickly remove the greasy dirt on hair, the submissive light of hair.
Claims (7)
1. a kind of nuisanceless, moisturizing hair care shampoo, which is characterized in that the raw material including following parts by weight is made：
1~13 portion of green tea oil, 3~6 parts of Jasmine juice of 3~21 parts of tea-seed oil
0.3~2.5 part of green-tea extract, 0.1~1 part of foaming agent.
2. nuisanceless, moisturizing hair care shampoo according to claim 1, which is characterized in that the preparation of the green tea oil
Method is：
（1）The fruit of picking 3 years or more green tea trees, obtains tea seeds；
（2）By tea seeds natural drying 8~10 days, until the moisture content of tea seeds is reduced to 6~8%, and tealeaves during sunning
Seed sloughs the green shell on surface naturally, obtains the tea seeds that just shell；
（3）Mechanical dejacketing processing is carried out to first shelling tea seeds, to remove the inner casing of tea seeds, obtains tea seeds benevolence；
（4）Tea seeds benevolence is put into crusher and carries out break process, forms the particle of 8~12 mesh, obtains tea seeds benevolence particle；
（5）Tea seeds benevolence particle is squeezed in such a way that physics cold pressing is squeezed, obtains crude oil；
（6）Crude oil filtering, filter screen cleaning, the fishing continuous cycle operation of slag deslagging are collected under normal pressure；
（7）Stand crude oil, be heated to 50~60 DEG C of heat preservations, and constant temperature stands 60~72 hours, separate moisture in oil removing and
Impurity；
(8) again will clean crude oil 2~3h of low temperature dewatering under 65~70 DEG C, 800mmHg vacuum, removing water content in oil to 0.1% with
Under；
（9）Water removal crude oil is stood at 5 DEG C, is passed through ozone, the wax in oil and ester matter is precipitated simultaneously in crystallization, 48~64h of growing the grain
Separation；
（10）Tea seed oil carries out diaphragm filters pressing after crystalline substance will be removed, and operating pressure 0.3Mpa goes the wax and ester matter in oil removing, obtains
Purified green-tea oil.
3. nuisanceless, moisturizing hair care shampoo according to claim 1, which is characterized in that the green-tea extract
Preparation method is：Dewatered fresh green tea leaf is rubbed broken, the boiling boiling that 8~10 times of weight of green tea weight are added is 2~3 small
When, filtering, the boiling that filter residue adds 2~3 times of weight is boiled 2~3 hours, and filtrate twice is merged, and is concentrated into the phase that 60 DEG C of heat are surveyed
It is 1.1 to density, obtains green-tea extract.
4. nuisanceless, moisturizing hair care shampoo according to claim 1, which is characterized in that the preparation of the tea-seed oil
Method is：
The tea seed of decortication removal of impurities is placed in mixer, is heated to 40~50 DEG C and insulated and stirred 3~5 hours, in heating process
The hot water that temperature is 40~50 DEG C is sprayed into, hot water is sprayed by the amount of tea seed gross mass 1~2%, tea seed moisture content after control balance
8~10%, and the difference for the highest moisture content and minimum moisture content for controlling same batch tea seed is no more than 0.2%；Again by tea
Seed is sent into oil expression in squeezer, squeezes resulting tea seed crude oil low temperature alkali refining and takes off free fatty acid；First time ceramic super-filtering film is de-
Soap；Wash degumming；Active bamboo absorption；Level-one tea-seed oil is made in second of ceramic super-filtering film low temperature ultrafiltration impurity elimination；With 50~90
DEG C above-mentioned ceramic super-filtering film of hot water backwash；
The low temperature alkali refining takes off free fatty acid process, be by tea seed crude oil be heated to 50~60 DEG C, weight percent is added
The food grade sodium hydroxide aqueous solution that specific concentration is 1~21%, is slowly stirred about 25~30min, becomes mixing after mixing well
Oil；
The first time ceramic super-filtering film takes off soap process, is by the miscella after de- free fatty acid, it is heated rapidly to 85~
90 DEG C, into first time ceramic super-filtering film, the soap stock in miscella is filtered to isolate, becomes de- soap oil；
The washing Degumming Procedures are in the de- soap oil after first time ceramic super-filtering film takes off soap process, and addition accounts for tea
Seed crude oil total weight 8~10%, the hot water that temperature is 96~97 DEG C enter in static mixer be sufficiently mixed together, enters back into butterfly
It is washed in formula seperator, degumming, dehydration；
The active bamboo absorption, is before active bamboo to be placed in the second ceramic super-filtering film；It is imitated using the flocculation of active bamboo
Benzene contained in oil after degumming, dehydration, chlorine residual should be adsorbed with drainage effect；Reach deodorising effect；
Second of ceramic super-filtering film low temperature ultrafiltration impurity elimination, be after being deodorized oil again second enter ceramic super-filtering film,
Ultrafiltration pressure：0.2Mpa, ultrafiltrate temperature：15~27 DEG C, molecular cut off：5000~10000；With decoloration and paraffin removal, de- again
It is smelly.
5. nuisanceless, moisturizing hair care shampoo according to claim 1, which is characterized in that the foaming agent includes coconut palm
Sub- amide, Cocoamidopropyl betaine, 25~32% mono decadepolyglycerol laurate sulpho mono succinates, the moon
Osmanthus sodium acyl taurine and the bimonthly cinnamic alcohol ester sodium of citric acid, the coconut monoethanolamide, Cocoamidopropyl betaine, 25~32% single ten
The weight of polyglyceryl laurate sulfosuccinic acid monoesters disodium aqua, laurel sodium acyl taurine and the bimonthly cinnamic alcohol ester sodium of citric acid
Than being 0.8~1: 1~1.2: 0.8~1.2: 0.5~0.8: 0.8.
6. nuisanceless, moisturizing hair care shampoo according to claim 5, it is characterised in that：The mono decaglycerin
The anhydrous ten polyglycereol monolaurate of laurate sulfosuccinic acid monoesters disodium aqua system and maleic anhydride are with equimolar
Than monoesters is made in 80~100 DEG C of 1~2h of esterification, then with sodium sulfite with equimolar than temperature control 75~98 in an aqueous medium
DEG C 3~4h of sulfonating reaction, is neutralized to neutral products therefrom with sodium hydroxide, with before taking its 25~32% aqueous solution, addition 0.1~
0.5% pharmaceutical grade decoloration special-purpose activated charcoal filters pressing, decoloration removal of impurities after 50~60 DEG C of mixing at least 2~3h.
7. nuisanceless, moisturizing hair care shampoo according to claim 5, it is characterised in that：The preparation of the shampoo
Method is：
The petal for winning the Jasmine after raising flowers and spitting perfume (or spice), petal is put into dryer and is dehydrated, take off to water content be 50~
60%, then petal is put into juice extractor and is squeezed the juice, it filters to get Jasmine juice；
Green tea oil is mixed with tea-seed oil, is heated while stirring, is heated to 60~80 DEG C；Green-tea extract is added in heat preservation,
It stirs evenly, obtains mixture A；
Mixture A is cooled to 45~50 DEG C, foaming agent is added, stirs evenly, obtains mixture B；
Mixture B temperature is down to room temperature, then is slowly added to Jasmine juice among the top surface of mixture B, is stood 3~4 small
When to get shampoo.
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Application publication date: 20181130 |