CN108888551A - A kind of cleaning solution and preparation method thereof of moisturizing sterilizing - Google Patents
A kind of cleaning solution and preparation method thereof of moisturizing sterilizing Download PDFInfo
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- CN108888551A CN108888551A CN201810656496.6A CN201810656496A CN108888551A CN 108888551 A CN108888551 A CN 108888551A CN 201810656496 A CN201810656496 A CN 201810656496A CN 108888551 A CN108888551 A CN 108888551A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/06—Production of fats or fatty oils from raw materials by pressing
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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Abstract
The present invention relates to a kind of technical fields of cleaning solution, specifically disclose a kind of cleaning solution of moisturizing sterilizing, which is characterized in that the raw material including following parts by weight is made：It washes one's hands 1~13 part of berry extract, 3~21 parts of tea-seed oil, 3~6 parts of jasmine flower extract, 0.3~2.5 part of houttuynia extract, 0.1~1 part of foaming agent.The present invention, which has, to be moisturized the skin, sterilization, the features such as dirt-removing power is strong.
Description
Technical field
The present invention relates to a kind of technical fields of cleaning solution, and in particular to a kind of cleaning solution of moisturizing sterilizing and its preparation side
Method.
Background technique
Tea-seed oil also known as camellia oil, tea pear oil（Fujian is commonly called as）, Wild camellia seed oil, camellia seed oil, tea oil seeds of trees oil.Camellia
It is Dabie Mountain of China, Fujian, Jiangxi, Hunan（Changning）Etc. ground specialty, good camellia oil, i.e. tea seed can be extracted in fruit
Oil；Tea-seed oil is a kind of important edible oil raw material of south China, generally has exocarp and tea-seed oil benevolence shell.Tea-seed oil is rich in
The unsaturated fatty acids such as linoleic acid, and rich in the physiological activators such as tea seed polyphenol, vitamin E, nutrition and physiology function
The olive oil that can match in excellence or beauty is imitated, better than vegetable oil, better than animal oil such as soybean oil, peanut oil.In addition to using, how by tea-seed oil
The utilization of bigizationner is the direction constantly assaulted the main target at this stage.
For example, being applied to washing；For people in life and work, both hands inevitably contact greasy dirt or dirty thing,
This had both caused both hands to be stained, and contained bacterium in these dirty pools, bacterium may result in the generation of disease.Currently, hand cleanser is made
Received by commonly using articles for washing a kind of day by more and more consumers, and comes into huge numbers of families；But it is in the prior art
Hand cleanser dirt-removing power is not strong, sterilization is not strong, moreover, most of raw material components are chemical finished product, this can be to the skin of people
Stimulation and injury.Due to the extensive use of disinfection hand cleanser, people also have higher requirement to disinfection hand cleanser, and should hope for success this
It reduces, and requires bactericidal effect excellent, therefore, a kind of new technical solution of urgent need solves above-mentioned technical problem.
Related Chinese patent literature is retrieved, is now enumerated some as follows：
1, Chinese patent<Application number> 201410735077.3<Denomination of invention>Hand cleanser<Abstract>The present invention relates to hand cleanser,
It is made of according to the following number of weight ratio following components：Stearic acid：5-10, glycol stearate：1-8, wire drawing powder：1-2, rose
Rare colored extracting solution：10-20, camphor tree leaf extract：10-20, tea oil：4-8, surplus are deionized water.The present invention not only has
Rose Essentielle also has the function of refreshing restoring consciouness.
2, Chinese patent<Application number> 201610987890.9<Denomination of invention>A kind of hand cleanser<Abstract>It is of the invention public
A kind of hand cleanser has been opened, has been made of the material of following mass fraction：6~9 parts of glycerol, 3~5 parts of ethyl alcohol, deionized water 30~40
Part, 6~8 parts of asparagus juice, 2~3 parts of laruyl alcohol olein, 3~6 parts of cocoanut fatty acid diethanolamide, 6~7 parts of citric acid,
5~6 parts of milk grass.Dirt-removing power of the present invention is good, removes contamination thoroughly, can reliably be removed to intractable grease stain, will not be to skin
Damage, and can sterilize, antibacterial and antibacterial prevents the intrusion of bacterium, fungi.
3, Chinese patent<Application number> 201711234631.X<Denomination of invention>A kind of disinfection hand cleanser<Abstract>This hair
Bright to disclose a kind of disinfection hand cleanser, the disinfection hand cleanser is according to mass fraction by being formed with raw material：Surfactant 5~10
Part；3~7 parts of essence；10~20 parts of thickener；30~50 parts of deionized water；10--15 parts of cortex moutan extract；Detergent alkylate
4~9 parts of sodium sulfonate；7~11 parts of polyethylene glycol glycerol rouge；8~13 parts of stearine；1~4 part of malic acid；Maleic acid 1--
3 parts；1~6 part of glutamic acid；1~4 part of citric acid.The hand cleanser dirt-removing power is strong, and bactericidal effect is good, to skin fanout free region.
From the document retrieved we it can be appreciated that these hand cleanser raw material components be chemical agent, some meetings are to skin
Skin causes to stimulate, and lacks moisturizing；So how to overcome the deficiencies of existing technologies, the cleaning solution of safety and environmental protection is prepared, this
It just needs to carry out innovation improvement to the prior art.
Summary of the invention
The purpose of the present invention is overcoming defect in the prior art, and providing one kind can sterilize and moisturizing；To skin
Have no stimulation, can the effective moisturizing sterilizing of decontamination cleaning solution and preparation method thereof.
In order to realize the purpose of foregoing invention, the technical solution taken is：
A kind of cleaning solution of moisturizing sterilizing, the raw material including following parts by weight are made：
It washes one's hands 1~13 portion of berry extract, 3~6 parts of jasmine flower extract of 3~21 parts of tea-seed oil
0.3~2.5 part of houttuynia extract, 0.1~1 part of foaming agent.
Preferably, the preparation method of the berry extract of washing one's hands is：The preparation method of the berry extract of washing one's hands is：It will wash
Net dewatered fresh fruit of washing one's hands rub broken, the boiling boiling of addition 8~10 times of weight of fruit of washing one's hands weight 2~3 hours, filtering, filter residue
The boiling for adding 2~3 times of weight is boiled 2~3 hours, and filtrate twice is merged, and being concentrated into the relative density that 60 DEG C of heat are surveyed is 1.1,
Obtain berry extract of washing one's hands.
Preferably, the preparation method of the houttuynia extract is：Dewatered fresh cordate houttuynia is rubbed to broken, addition fish raw meat
The boiling of 8~10 times of weight of careless weight is boiled 2~3 hours, filtering, and the boiling that filter residue adds 2~3 times of weight is boiled 2~3 hours,
Merge filtrate twice, being concentrated into the relative density that 60 DEG C of heat are surveyed is 1.1, obtains houttuynia extract.
Preferably, the preparation method of the jasmine flower extract is：The petal of new fresh jasmine after raising flowers is rubbed it is broken,
The boiling that 8~10 times of weight of Jasmine petal weight are added is boiled 2~3 hours, and filtering, filter residue adds the boiling of 2~3 times of weight
Boiling 2~3 hours merges filtrate twice, and being concentrated into the relative density that 60 DEG C of heat are surveyed is 1.1, obtains jasmine flower extract.
Preferably, the preparation method of the tea-seed oil is：
The tea seed of decortication removal of impurities is placed in mixer, is heated to 40~50 DEG C and insulated and stirred 3~5 hours, in heating process
The hot water that temperature is 40~50 DEG C is sprayed into, hot water is sprayed by the amount of tea seed gross mass 1~2%, tea seed moisture content after control balance
8~10%, and the difference for the highest moisture content and minimum moisture content for controlling same batch tea seed is no more than 0.2%；Again by tea
Seed is sent into oil expression in squeezer, squeezes resulting tea seed crude oil low temperature alkali refining and takes off free fatty acid；First time ceramic super-filtering film is de-
Soap；Wash degumming；Active bamboo absorption；Level-one tea-seed oil is made in second of ceramic super-filtering film low temperature ultrafiltration impurity elimination；With 50~90
DEG C above-mentioned ceramic super-filtering film of hot water backwash；
The low temperature alkali refining takes off free fatty acid process, be by tea seed crude oil be heated to 50~60 DEG C, weight percent is added
The food grade sodium hydroxide aqueous solution that specific concentration is 1~21%, is slowly stirred about 25~30min, becomes mixing after mixing well
Oil；
The first time ceramic super-filtering film takes off soap process, is by the miscella after de- free fatty acid, it is heated rapidly to 85~
90 DEG C, into first time ceramic super-filtering film, the soap stock in miscella is filtered to isolate, becomes de- soap oil；
The washing Degumming Procedures are in the de- soap oil after first time ceramic super-filtering film takes off soap process, and addition accounts for tea
Seed crude oil total weight 8~10%, the hot water that temperature is 96~97 DEG C enter in static mixer be sufficiently mixed together, enters back into butterfly
It is washed in formula seperator, degumming, dehydration；
The active bamboo absorption, is before active bamboo to be placed in the second ceramic super-filtering film；It is imitated using the flocculation of active bamboo
Benzene contained in oil after degumming, dehydration, chlorine residual should be adsorbed with drainage effect；Reach deodorising effect；
Second of ceramic super-filtering film low temperature ultrafiltration impurity elimination, be after being deodorized oil again second enter ceramic super-filtering film,
Ultrafiltration pressure：0.2Mpa, ultrafiltrate temperature：15~27 DEG C, molecular cut off：5000~10000；With decoloration and paraffin removal, de- again
It is smelly.
Preferably, the static mixer, by the mixed cell of different size of the series installation in hollow pipe
Composition, it is that the flight group of the left and right torsion of one channel is welded that the basic structure of these mixed cells is identical, its technology
Performance：Highest degree of scatter≤5um, liquid-liquid, one solid phase unevenness coefficient S x≤4% of liquid are suitable for viscosity≤105 centipoises
Fluid.
Preferably, the foaming agent includes coconut monoethanolamide, Cocoamidopropyl betaine, 25~32% mono decaglycerin moons
Cinnamic acid ester sulfosuccinic acid monoesters disodium aqua, laurel sodium acyl taurine and the bimonthly cinnamic alcohol ester sodium of citric acid, the coconut monoethanolamide,
Cocoamidopropyl betaine, 25~32% mono decadepolyglycerol laurate sulpho mono succinates, lauroyl ox sulphur
The weight ratio of sour sodium and the bimonthly cinnamic alcohol ester sodium of citric acid is 0.8~1: 1~1.2: 0.8~1.2: 0.5~0.8: 0.8.
Preferably, the anhydrous ten polyglycereol list of the mono decadepolyglycerol laurate sulpho mono succinate system
Monoesters is made in 80~100 DEG C of 1~2h of esterification with equimolar ratio in laurate and maleic anhydride, then with sodium sulfite
With equimolar than 75~98 DEG C of 3~4h of sulfonating reaction of temperature control in an aqueous medium, it is neutralized to neutral products therefrom with sodium hydroxide, is used
Before take its 25~32% aqueous solution, addition 0.1~0.5% pharmaceutical grade decoloration special-purpose activated charcoal is mixed at least 2 in 50~60 DEG C
Filters pressing, decoloration removal of impurities after~3h.
Preferably, the preparation method of the cleaning solution is：To wash one's hands berry extract, jasmine flower extract, cordate houttuynia extraction
Object is mixed with tea-seed oil, is heated while stirring, and is heated to 60~80 DEG C, keeps the temperature 20~30min；It is cooled to 45~50 again
DEG C, foaming agent is added, stirs evenly, keeps the temperature 20~30min, cools the temperature to room temperature again, bottles, examines qualification to get washing
Wash liquid.
Compared with the prior art the present invention, has substantive distinguishing features outstanding and significant progress is：
1, the present invention can effectively decontamination sterilizing cleaning solution, greasy dirt caused by machine oil can be effectively removed, do not stimulate skin, can be moistened
Skin；Moreover, the fragrance of Jasmine can be remained with；Generation that preparation process of the invention is pollution-free, it is environmentally protective；Preparation process letter
Practice.
2, wash one's hands in the present invention berry extract DNA purity it is high, can effectively keep the pharmacological of green tea, improve fruit of washing one's hands
The service efficiency of extract.
3, tea-seed oil DNA purity is high in the present invention, and the larger raising oil production of energy, and tea seed is maximized
Utilization, extraction process there is no destroy tea seed characteristic, the pharmacological and nutriment of tea seed can be effectively retained, so that making
Used time, the effect of capable of maximumlly playing tea-seed oil；The present invention handles oil-tea camellia seed crude oil and uses ceramic super-filtering film twice, can
It solves the problems, such as that conventional refinery process denaturation tea seed albumen generates color reversion, effectively removes colloid, oil-soluble etc. in camellia seed oil
Impurity；And the micro-nutrient composition that can be effectively maintained in tea oil；Food grade sodium hydroxide aqueous solution is uniquely added in process,
Degumming does not use organic solvent with water as solvent, and not only production cost is low, can also overcome two brought by addition chemical agent
Secondary pollution is conducive to keep the safety in production and prevent to pollute；And after active bamboo is placed in first time ceramic super-filtering film, the second Ceramic excessive filtration
Before film, i.e., active bamboo absorption process is designed and take off soap process and second of ceramic super-filtering film low temperature in first time ceramic super-filtering film
Between ultrafiltration impurity elimination process；Not only benzene contained in oil after degumming, dehydration, chlorine residual absorption can be reached into deodorising effect；Together
When, in practice it has proved that the effect for improving mouthfeel is also acted, unexpected technical effect is produced；Tea-seed oil product yield 90%
More than, purity is up to 100%.
4, jasmine flower extract is added in the present invention, improves the fragrance degree of cleaning solution, Jasmine fragrance can calm the nerves peaceful gas, jasmine
Jasmine flower extract can with other raw material effective integrations, so that entire liquid is all adsorbed with Jasmine fragrance, meanwhile, the medicine of Jasmine
Reason characteristic and nutriment are also absorbed and are merged by liquid.
5, will wash one's hands when preparing cleaning solution berry extract, houttuynia extract, jasmine flower extract and tea seed of the invention
The mixed liquor of oil is heated, the larger mobility for improving mixed liquor of energy, and can the absorption fusion of larger raising between the two
Rate after fused, generates new pharmacological property, can effectively anti-dandruff, moisturizing hair care；So that the submissive light of hair, moisturizing,
Reply submissive, lubrication, full of gloss.
Specific embodiment
It is to combine the embodiment of the present invention below, invention is further described in detail：
Embodiment 1：
A kind of cleaning solution of moisturizing sterilizing, the raw material including following parts by weight are made：Wash one's hands 1 portion of berry extract, 3 parts of tea-seed oil,
3 parts of jasmine flower extract, 0.3 part of houttuynia extract, 0.1 part of foaming agent.
Preferably, the preparation method of the berry extract of washing one's hands is：The preparation method of the berry extract of washing one's hands is：It will wash
Only dewatered fresh fruit of washing one's hands are rubbed broken, and the boiling that 8 times of weight of fruit of washing one's hands weight are added is boiled 2~3 hours, and filtering, filter residue adds again
The boiling for entering 2 times of weight is boiled 2~3 hours, and filtrate twice is merged, and being concentrated into the relative density that 60 DEG C of heat are surveyed is 1.1, is washed one's hands
Berry extract.
Preferably, the preparation method of the houttuynia extract is：Dewatered fresh cordate houttuynia is rubbed to broken, addition fish raw meat
The boiling of 8 times of weight of careless weight is boiled 2~3 hours, filtering, and the boiling that filter residue adds 2 times of weight is boiled 2~3 hours, is merged twice
Filtrate, being concentrated into the relative density that 60 DEG C of heat are surveyed is 1.1, obtains houttuynia extract.
Preferably, the preparation method of the jasmine flower extract is：The petal of new fresh jasmine after raising flowers is rubbed it is broken,
The boiling that 8 times of weight of Jasmine petal weight are added is boiled 2~3 hours, filtering, and filter residue adds the boiling boiling 2~3 of 2 times of weight
Hour, merge filtrate twice, being concentrated into the relative density that 60 DEG C of heat are surveyed is 1.1, obtains jasmine flower extract.
Preferably, the preparation method of the tea-seed oil is：
The tea seed of decortication removal of impurities is placed in mixer, 40 DEG C and insulated and stirred 3~5 hours is heated to, is sprayed into heating process
Temperature is 40 DEG C of hot water, and hot water is sprayed by the amount of tea seed gross mass 1~2%, after control balance tea seed moisture content 8%, and
The difference of the highest moisture content and minimum moisture content that control same batch tea seed is no more than 0.2%；Tea seed is sent into squeezer again
Interior oil expression squeezes resulting tea seed crude oil low temperature alkali refining and takes off free fatty acid；First time ceramic super-filtering film takes off soap；Wash degumming；
Active bamboo absorption；Level-one tea-seed oil is made in second of ceramic super-filtering film low temperature ultrafiltration impurity elimination；It is above-mentioned with 50 DEG C of hot water backwashes
Ceramic super-filtering film；
The low temperature alkali refining takes off free fatty acid process, be by tea seed crude oil be heated to 50 DEG C, it is dense that weight percent is added
The food grade sodium hydroxide aqueous solution that degree is 1%, is slowly stirred about 25min, becomes miscella after mixing well；
The first time ceramic super-filtering film takes off soap process, is that the miscella after de- free fatty acid is heated rapidly to 85 DEG C,
Into first time ceramic super-filtering film, the soap stock in miscella is filtered to isolate, becomes de- soap oil；
The washing Degumming Procedures are in the de- soap oil after first time ceramic super-filtering film takes off soap process, and addition accounts for tea
Seed crude oil total weight 8%, the hot water that temperature is 96 DEG C enter in static mixer be sufficiently mixed together, enters back into butterfly seperator
In washed, degumming, dehydration；
The active bamboo absorption, is before active bamboo to be placed in the second ceramic super-filtering film；It is imitated using the flocculation of active bamboo
Benzene contained in oil after degumming, dehydration, chlorine residual should be adsorbed with drainage effect；Reach deodorising effect；
Second of ceramic super-filtering film low temperature ultrafiltration impurity elimination, be after being deodorized oil again second enter ceramic super-filtering film,
Ultrafiltration pressure：0.2Mpa, ultrafiltrate temperature：15 DEG C, molecular cut off：5000~10000；With decoloration and paraffin removal again, deodorization.
Preferably, the static mixer, by the mixed cell of different size of the series installation in hollow pipe
Composition, it is that the flight group of the left and right torsion of one channel is welded that the basic structure of these mixed cells is identical, its technology
Performance：Highest degree of scatter≤5um, liquid-liquid, one solid phase unevenness coefficient S x≤4% of liquid are suitable for viscosity≤105 centipoises
Fluid.
Preferably, the foaming agent includes coconut monoethanolamide, Cocoamidopropyl betaine, 25~32% mono decaglycerin moons
Cinnamic acid ester sulfosuccinic acid monoesters disodium aqua, laurel sodium acyl taurine and the bimonthly cinnamic alcohol ester sodium of citric acid, the coconut monoethanolamide,
Cocoamidopropyl betaine, 25~32% mono decadepolyglycerol laurate sulpho mono succinates, lauroyl ox sulphur
The weight ratio of sour sodium and the bimonthly cinnamic alcohol ester sodium of citric acid is 0.8: 1: 0.8: 0.5: 0.8.
Preferably, the anhydrous ten polyglycereol list of the mono decadepolyglycerol laurate sulpho mono succinate system
Monoesters is made in 80 DEG C of 1~2h of esterification with equimolar ratio in laurate and maleic anhydride, then with sodium sulfite with etc.
Molar ratio 75 DEG C of 3~4h of sulfonating reaction of temperature control in an aqueous medium, are neutralized to neutral products therefrom with sodium hydroxide, with before taking it
25% aqueous solution, addition 0.1% pharmaceutical grade decoloration special-purpose activated charcoal filters pressing, decoloration removal of impurities after 50 DEG C of mixing at least 2~3h.
Preferably, the preparation method of the cleaning solution is：To wash one's hands berry extract, jasmine flower extract, cordate houttuynia extraction
Object is mixed with tea-seed oil, is heated while stirring, and is heated to 60 DEG C, keeps the temperature 20min；It is cooled to 45 DEG C again, foaming agent is added,
It stirs evenly, keeps the temperature 20min, cool the temperature to room temperature again, bottle, examine qualification to get cleaning solution.
Embodiment 2：
A kind of cleaning solution of moisturizing sterilizing, the raw material including following parts by weight are made：It washes one's hands 7 portions of tea-seed oils 12 of berry extract
Part, 4.5 parts of jasmine flower extract, 1.4 parts of houttuynia extract, 0.55 part of foaming agent.
Preferably, the preparation method of the berry extract of washing one's hands is：The preparation method of the berry extract of washing one's hands is：It will wash
Only dewatered fresh fruit of washing one's hands are rubbed broken, and the boiling that 9 times of weight of fruit of washing one's hands weight are added is boiled 2~3 hours, and filtering, filter residue adds again
The boiling for entering 2.5 times of weight is boiled 2~3 hours, and filtrate twice is merged, and being concentrated into the relative density that 60 DEG C of heat are surveyed is 1.1, is washed
Hand berry extract.
Preferably, the preparation method of the jasmine flower extract is：The petal of new fresh jasmine after raising flowers is rubbed it is broken,
Be added 9 times of weight of Jasmine petal weight boiling boil 2~3 hours, filtering, filter residue add 2.5 times of weight boiling boiling 2~
3 hours, merge filtrate twice, being concentrated into the relative density that 60 DEG C of heat are surveyed is 1.1, obtains jasmine flower extract.
Preferably, the preparation method of the houttuynia extract is：Dewatered fresh cordate houttuynia is rubbed to broken, addition fish raw meat
The boiling of 9 times of weight of careless weight is boiled 2~3 hours, filtering, and the boiling that filter residue adds 2.5 times of weight is boiled 2~3 hours, merges two
Secondary filtrate, being concentrated into the relative density that 60 DEG C of heat are surveyed is 1.1, obtains houttuynia extract.
Preferably, the preparation method of the tea-seed oil is：
The tea seed of decortication removal of impurities is placed in mixer, 45 DEG C and insulated and stirred 3~5 hours is heated to, is sprayed into heating process
Temperature is 45 DEG C of hot water, and hot water is sprayed by the amount of tea seed gross mass 1~2%, after control balance tea seed moisture content 8~
10%, and the difference for the highest moisture content and minimum moisture content for controlling same batch tea seed is no more than 0.2%；Tea seed is sent into again
Oil expression in squeezer squeezes resulting tea seed crude oil low temperature alkali refining and takes off free fatty acid；First time ceramic super-filtering film takes off soap；Washing
Degumming；Active bamboo absorption；Level-one tea-seed oil is made in second of ceramic super-filtering film low temperature ultrafiltration impurity elimination；With in 70 DEG C of hot water backwashes
The ceramic super-filtering film stated；
The low temperature alkali refining takes off free fatty acid process, be by tea seed crude oil be heated to 55 DEG C, it is dense that weight percent is added
The food grade sodium hydroxide aqueous solution that degree is 11%, is slowly stirred about 28min, becomes miscella after mixing well；
The first time ceramic super-filtering film takes off soap process, is that the miscella after de- free fatty acid is heated rapidly to 88 DEG C,
Into first time ceramic super-filtering film, the soap stock in miscella is filtered to isolate, becomes de- soap oil；
The washing Degumming Procedures are in the de- soap oil after first time ceramic super-filtering film takes off soap process, and addition accounts for tea
Seed crude oil total weight 9%, the hot water that temperature is 97 DEG C enter in static mixer be sufficiently mixed together, enters back into butterfly seperator
In washed, degumming, dehydration；
The active bamboo absorption, is before active bamboo to be placed in the second ceramic super-filtering film；It is imitated using the flocculation of active bamboo
Benzene contained in oil after degumming, dehydration, chlorine residual should be adsorbed with drainage effect；Reach deodorising effect；
Second of ceramic super-filtering film low temperature ultrafiltration impurity elimination, be after being deodorized oil again second enter ceramic super-filtering film,
Ultrafiltration pressure：0.2Mpa, ultrafiltrate temperature：21 DEG C, molecular cut off：5000~10000；With decoloration and paraffin removal again, deodorization.
Preferably, the static mixer, by the mixed cell of different size of the series installation in hollow pipe
Composition, it is that the flight group of the left and right torsion of one channel is welded that the basic structure of these mixed cells is identical, its technology
Performance：Highest degree of scatter≤5um, liquid-liquid, one solid phase unevenness coefficient S x≤4% of liquid are suitable for viscosity≤105 centipoises
Fluid.
Preferably, the foaming agent includes coconut monoethanolamide, Cocoamidopropyl betaine, 25~32% mono decaglycerin moons
Cinnamic acid ester sulfosuccinic acid monoesters disodium aqua, laurel sodium acyl taurine and the bimonthly cinnamic alcohol ester sodium of citric acid, the coconut monoethanolamide,
Cocoamidopropyl betaine, 25~32% mono decadepolyglycerol laurate sulpho mono succinates, lauroyl ox sulphur
The weight ratio of sour sodium and the bimonthly cinnamic alcohol ester sodium of citric acid is 0.9: 1.1: 1: 0.7: 0.8.
Preferably, the anhydrous ten polyglycereol list of the mono decadepolyglycerol laurate sulpho mono succinate system
Monoesters is made in 90 DEG C of 1~2h of esterification with equimolar ratio in laurate and maleic anhydride, then with sodium sulfite with etc.
Molar ratio 87 DEG C of 3~4h of sulfonating reaction of temperature control in an aqueous medium, are neutralized to neutral products therefrom with sodium hydroxide, with before taking it
30% aqueous solution, addition 0.3% pharmaceutical grade decoloration special-purpose activated charcoal filters pressing, decoloration removal of impurities after 55 DEG C of mixing at least 2~3h.
Preferably, the preparation method of the cleaning solution is：To wash one's hands berry extract, jasmine flower extract, cordate houttuynia extraction
Object is mixed with tea-seed oil, is heated while stirring, and is heated to 70 DEG C, keeps the temperature 25min；It is cooled to 48 DEG C again, foaming agent is added,
It stirs evenly, keeps the temperature 25min, cool the temperature to room temperature again, bottle, examine qualification to get cleaning solution.
Embodiment 3：
A kind of cleaning solution of moisturizing sterilizing, the raw material including following parts by weight are made：It washes one's hands 13 portions of tea-seed oils 21 of berry extract
Part, 6 parts of jasmine flower extract, 2.5 parts of houttuynia extract, 1 part of foaming agent.
Preferably, the preparation method of the berry extract of washing one's hands is：The preparation method of the berry extract of washing one's hands is：It will wash
Only dewatered fresh fruit of washing one's hands are rubbed broken, and the boiling that 10 times of weight of fruit of washing one's hands weight are added is boiled 2~3 hours, and filtering, filter residue adds again
The boiling for entering 3 times of weight is boiled 2~3 hours, and filtrate twice is merged, and being concentrated into the relative density that 60 DEG C of heat are surveyed is 1.1, is washed one's hands
Berry extract.
Preferably, the preparation method of the houttuynia extract is：Dewatered fresh cordate houttuynia is rubbed to broken, addition fish raw meat
The boiling of 10 times of weight of careless weight is boiled 2~3 hours, filtering, and the boiling that filter residue adds 3 times of weight is boiled 2~3 hours, merges two
Secondary filtrate, being concentrated into the relative density that 60 DEG C of heat are surveyed is 1.1, obtains houttuynia extract.
Preferably, the preparation method of the jasmine flower extract is：The petal of new fresh jasmine after raising flowers is rubbed it is broken,
The boiling that 10 times of weight of Jasmine petal weight are added is boiled 2~3 hours, filtering, and filter residue adds the boiling boiling 2~3 of 3 times of weight
Hour, merge filtrate twice, being concentrated into the relative density that 60 DEG C of heat are surveyed is 1.1, obtains jasmine flower extract.
Preferably, the preparation method of the tea-seed oil is：
The tea seed of decortication removal of impurities is placed in mixer, 50 DEG C and insulated and stirred 3~5 hours is heated to, is sprayed into heating process
The hot water that temperature is 50 DEG C, hot water are sprayed by the amount of tea seed gross mass 2%, and tea seed moisture content is 10% after control balance, and controls
The difference of the highest moisture content and minimum moisture content of making same batch tea seed is no more than 0.2%；Tea seed is sent into squeezer again
Oil expression squeezes resulting tea seed crude oil low temperature alkali refining and takes off free fatty acid；First time ceramic super-filtering film takes off soap；Wash degumming；It is living
Property bamboo Charcoal Adsorption；Level-one tea-seed oil is made in second of ceramic super-filtering film low temperature ultrafiltration impurity elimination；With the above-mentioned pottery of 90 DEG C of hot water backwashes
Porcelain ultrafiltration membrane；
The low temperature alkali refining takes off free fatty acid process, be by tea seed crude oil be heated to 60 DEG C, it is dense that weight percent is added
The food grade sodium hydroxide aqueous solution that degree is 21%, is slowly stirred about 30min, becomes miscella after mixing well；
The first time ceramic super-filtering film takes off soap process, is that the miscella after de- free fatty acid is heated rapidly to 90 DEG C,
Into first time ceramic super-filtering film, the soap stock in miscella is filtered to isolate, becomes de- soap oil；
The washing Degumming Procedures are in the de- soap oil after first time ceramic super-filtering film takes off soap process, and addition accounts for tea
Seed crude oil total weight 10%, the hot water that temperature is 97 DEG C enter in static mixer be sufficiently mixed together, enter back into butterfly separation
It is washed in machine, degumming, dehydration；
The active bamboo absorption, is before active bamboo to be placed in the second ceramic super-filtering film；It is imitated using the flocculation of active bamboo
Benzene contained in oil after degumming, dehydration, chlorine residual should be adsorbed with drainage effect；Reach deodorising effect；
Second of ceramic super-filtering film low temperature ultrafiltration impurity elimination, be after being deodorized oil again second enter ceramic super-filtering film,
Ultrafiltration pressure：0.2Mpa, ultrafiltrate temperature：27 DEG C, molecular cut off：5000~10000；With decoloration and paraffin removal again, deodorization.
Preferably, the static mixer, by the mixed cell of different size of the series installation in hollow pipe
Composition, it is that the flight group of the left and right torsion of one channel is welded that the basic structure of these mixed cells is identical, its technology
Performance：Highest degree of scatter≤5um, liquid-liquid, one solid phase unevenness coefficient S x≤4% of liquid are suitable for viscosity≤105 centipoises
Fluid.
Preferably, the foaming agent includes coconut monoethanolamide, Cocoamidopropyl betaine, 25~32% mono decaglycerin moons
Cinnamic acid ester sulfosuccinic acid monoesters disodium aqua, laurel sodium acyl taurine and the bimonthly cinnamic alcohol ester sodium of citric acid, the coconut monoethanolamide,
Cocoamidopropyl betaine, 25~32% mono decadepolyglycerol laurate sulpho mono succinates, lauroyl ox sulphur
The weight ratio of sour sodium and the bimonthly cinnamic alcohol ester sodium of citric acid is 1: 1.2: 1.2: 0.8: 0.8.
Preferably, the anhydrous ten polyglycereol list of the mono decadepolyglycerol laurate sulpho mono succinate system
Monoesters is made in 100 DEG C of 1~2h of esterification with equimolar ratio in laurate and maleic anhydride, then with sodium sulfite with etc.
Molar ratio 98 DEG C of 3~4h of sulfonating reaction of temperature control in an aqueous medium, are neutralized to neutral products therefrom with sodium hydroxide, with before taking it
32% aqueous solution, addition 00.5% pharmaceutical grade decoloration special-purpose activated charcoal filters pressing, decoloration after 60 DEG C of mixing at least 2~3h remove
It is miscellaneous.
Preferably, the preparation method of the cleaning solution is：To wash one's hands berry extract, jasmine flower extract, cordate houttuynia extraction
Object is mixed with tea-seed oil, is heated while stirring, and is heated to 80 DEG C, keeps the temperature 30min；It is cooled to 50 DEG C again, foaming agent is added,
It stirs evenly, keeps the temperature 30min, cool the temperature to room temperature again, bottle, examine qualification to get cleaning solution.
Clinical test
Old XX, male, 30 years old, repairing motorcycle person, daily both hands were all the greasy dirts of full hand, using dish washing liquid on the market and could not
It thoroughly removes, also remains oily taste, because must not thoroughly remove for a long time, some greasy dirts invade skin；It is of the invention after being introduced
Cleaning solution, the same day use, and can once remove the greasy dirt on the same day；After continuing to use a week, at original greasy dirt for invading skin,
It is obviously thin out very much, after continuing to use 4 days, does not scrutinize and all do not see there is greasy dirt at the greasy dirt of intrusion skin, continue to use 2
After it, thoroughly both hands are cleaned up, and the originally skin cracks that have on hand and coarse, is thoroughly repaired, skin smooth.
Clock XX, male, 32 years old, auto repair person, daily both hands greasy dirt was cleaned using dish washing liquid in the market, still there is residual
Greasy dirt, dish washing liquid in the market simultaneously could not be cleaned up thoroughly；Cleaning solution of the invention is used after being introduced, can easily be washed away
Greasy dirt on hand, and do not remain, completely have with light Jasmine fragrance.
Lee XX, female, 48 years old, housewife, residual greasy dirt in the ceramic tile gap in kitchen, color was pitch-black, why how to clean
Removing all lose it is effective, after being introduced use cleaning solution of the invention, as soon as using a week, can be pitch-black by these
Greasy dirt thoroughly washes, and exposes the original appearance of ceramic tile.
Yellow XX, female, 40 years old, cleaner often contacted with rubbish, more arduous, after both hands cleaning, still, or residual
Light peculiar smell uses cleaning solution of the invention after being introduced, and using a week, skin is ruddy, and hand has lingering fragrance.
Claims (8)
1. a kind of cleaning solution of moisturizing sterilizing, which is characterized in that the raw material including following parts by weight is made：
It washes one's hands 1~13 portion of berry extract, 3~6 parts of jasmine flower extract of 3~21 parts of tea-seed oil
0.3~2.5 part of houttuynia extract, 0.1~1 part of foaming agent.
2. the cleaning solution of moisturizing sterilizing according to claim 1, which is characterized in that the preparation side of the berry extract of washing one's hands
Method is：The preparation method of the berry extract of washing one's hands is：Dewatered fresh fruit of washing one's hands will be cleaned and rub broken, addition fruit of washing one's hands weight
The boiling of 8~10 times of weight is boiled 2~3 hours, filtering, and the boiling that filter residue adds 2~3 times of weight is boiled 2~3 hours, merges two
Secondary filtrate, being concentrated into the relative density that 60 DEG C of heat are surveyed is 1.1, obtains berry extract of washing one's hands.
3. the cleaning solution of moisturizing sterilizing according to claim 1, which is characterized in that the preparation side of the houttuynia extract
Method is：Dewatered fresh cordate houttuynia is rubbed it is broken, be added 8~10 times of weight of cordate houttuynia weight boiling boil 2~3 hours, filtering,
The boiling that filter residue adds 2~3 times of weight is boiled 2~3 hours, and filtrate twice is merged, and is concentrated into the relative density that 60 DEG C of heat are surveyed and is
1.1, obtain houttuynia extract.
4. the cleaning solution of moisturizing sterilizing according to claim 1, which is characterized in that the preparation side of the jasmine flower extract
Method is：The petal of new fresh jasmine after raising flowers and spitting perfume (or spice) is rubbed to broken, the boiling of addition 8~10 times of weight of Jasmine petal weight
Boiling 2~3 hours, filtering, the boiling that filter residue adds 2~3 times of weight boil 2~3 hours, merge filtrate twice, be concentrated into 60 DEG C
The relative density that heat is surveyed is 1.1, obtains jasmine flower extract.
5. the cleaning solution of moisturizing according to claim 1 sterilizing, which is characterized in that the preparation method of the tea-seed oil is：
The tea seed of decortication removal of impurities is placed in mixer, is heated to 40~50 DEG C and insulated and stirred 3~5 hours, in heating process
The hot water that temperature is 40~50 DEG C is sprayed into, hot water is sprayed by the amount of tea seed gross mass 1~2%, tea seed moisture content after control balance
8~10%, and the difference for the highest moisture content and minimum moisture content for controlling same batch tea seed is no more than 0.2%；Again by tea
Seed is sent into oil expression in squeezer, squeezes resulting tea seed crude oil low temperature alkali refining and takes off free fatty acid；First time ceramic super-filtering film is de-
Soap；Wash degumming；Active bamboo absorption；Level-one tea-seed oil is made in second of ceramic super-filtering film low temperature ultrafiltration impurity elimination；With 50~90
DEG C above-mentioned ceramic super-filtering film of hot water backwash；
The low temperature alkali refining takes off free fatty acid process, be by tea seed crude oil be heated to 50~60 DEG C, weight percent is added
The sodium hydrate aqueous solution that specific concentration is 5~10%, is slowly stirred about 25~30min, becomes miscella after mixing well；
The first time ceramic super-filtering film takes off soap process, is by the miscella after de- free fatty acid, it is heated rapidly to 85~
90 DEG C, into first time ceramic super-filtering film, the soap stock in miscella is filtered to isolate, becomes de- soap oil；
The washing Degumming Procedures are in the de- soap oil after first time ceramic super-filtering film takes off soap process, and addition accounts for tea
Seed crude oil total weight 8~10%, the hot water that temperature is 96~97 DEG C enter in static mixer be sufficiently mixed together, enters back into butterfly
It is washed in formula seperator, degumming, dehydration；
The active bamboo absorption, is before active bamboo to be placed in the second ceramic super-filtering film；It is imitated using the flocculation of active bamboo
Benzene contained in oil after degumming, dehydration, chlorine residual should be adsorbed with drainage effect；Reach deodorising effect；
Second of ceramic super-filtering film low temperature ultrafiltration impurity elimination, be after being deodorized oil again second enter ceramic super-filtering film,
Ultrafiltration pressure：0.2Mpa, ultrafiltrate temperature：15~27 DEG C, molecular cut off：5000~10000；With decoloration and paraffin removal, de- again
It is smelly.
6. the cleaning solution of moisturizing according to claim 1 sterilizing, which is characterized in that the foaming agent include coconut monoethanolamide,
Cocoamidopropyl betaine, 25~32% mono decadepolyglycerol laurate sulpho mono succinates, lauroyl ox sulphur
Sour sodium and the bimonthly cinnamic alcohol ester sodium of citric acid, the coconut monoethanolamide, Cocoamidopropyl betaine, 25~32% mono decaglycerin moons
The weight ratio of cinnamic acid ester sulfosuccinic acid monoesters disodium aqua, laurel sodium acyl taurine and the bimonthly cinnamic alcohol ester sodium of citric acid is 0.8
~1: 1~1.2: 0.8~1.2: 0.5~0.8: 0.8.
7. the cleaning solution of moisturizing sterilizing according to claim 6, it is characterised in that：The mono decaglycerin laurate
The anhydrous ten polyglycereol monolaurate of sulfosuccinic acid monoesters disodium aqua system and maleic anhydride with equimolar ratio 80~
Monoesters is made in 100 DEG C of 1~2h of esterification, then more anti-than 75~98 DEG C of sulfonation of temperature control in an aqueous medium with equimolar with sodium sulfite
3~4h is answered, is neutralized to neutral products therefrom with sodium hydroxide, with its 25~32% aqueous solution is before taken, addition 0.1~0.5% is medicinal
Grade decoloration special-purpose activated charcoal filters pressing, decoloration removal of impurities after 50~60 DEG C of mixing at least 2~3h.
8. the cleaning solution of moisturizing sterilizing according to claim 1, it is characterised in that：The preparation method of the cleaning solution is：
To wash one's hands berry extract, jasmine flower extract, houttuynia extract is mixed with tea-seed oil, is heated, is heated to while stirring
60~80 DEG C, keep the temperature 20~30min；It is cooled to 45~50 DEG C again, foaming agent is added, stirs evenly, keeps the temperature 20~30min, then
Secondary to cool the temperature to room temperature, bottling examines qualification to get cleaning solution.
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Cited By (1)
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