CN105997740A - Skin-cleaning composition with natural plant extract formula - Google Patents

Skin-cleaning composition with natural plant extract formula Download PDF

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Publication number
CN105997740A
CN105997740A CN201610552446.4A CN201610552446A CN105997740A CN 105997740 A CN105997740 A CN 105997740A CN 201610552446 A CN201610552446 A CN 201610552446A CN 105997740 A CN105997740 A CN 105997740A
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China
Prior art keywords
extract
skin cleansing
cleansing compositions
ethyl acetate
fructus
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Pending
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CN201610552446.4A
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Chinese (zh)
Inventor
谌良福
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Guangzhou Three Biological Technology Co Ltd
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Guangzhou Three Biological Technology Co Ltd
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Priority to CN201610552446.4A priority Critical patent/CN105997740A/en
Publication of CN105997740A publication Critical patent/CN105997740A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/35Caprifoliaceae (Honeysuckle family)
    • A61K36/355Lonicera (honeysuckle)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/48Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
    • A61K36/483Gleditsia (locust)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/77Sapindaceae (Soapberry family), e.g. lychee or soapberry
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/82Theaceae (Tea family), e.g. camellia
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005Antimicrobial preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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  • Health & Medical Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Epidemiology (AREA)
  • Microbiology (AREA)
  • Biotechnology (AREA)
  • Chemical & Material Sciences (AREA)
  • Mycology (AREA)
  • Engineering & Computer Science (AREA)
  • Botany (AREA)
  • Alternative & Traditional Medicine (AREA)
  • Medicinal Chemistry (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Medical Informatics (AREA)
  • Dermatology (AREA)
  • Birds (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Cosmetics (AREA)
  • Detergent Compositions (AREA)

Abstract

The invention provides a skin-cleaning composition with a natural plant extract formula. The skin-cleaning composition with the natural plant extract formula comprises the following components in percent by mass: 0-15% of saponin extract, 70-85% of sapindus extract, 1-10% of green tea extract, 1-10% of honeysuckle extract and 0-4% of camellia oil. The skin-cleaning composition with the natural plant extract formula, provided by the invention, has a good cleaning effect and high bacteriostatic and bactericidal performances.

Description

A kind of skin cleansing compositions of natural plant extract formula
Technical field
The present invention relates to the skin cleansing compositions of a kind of natural plant extract formula.
Background technology
The major function of bath gel is cleaning whole skin, and gives fragrance.Although bath gel is referred to as shower gel abroad, The most not gel but flowable thick liquid.In China, bath only has fancy soap single variety with product the most always. The nineties in last century, bath gel comes into vogue, and quickly increases.Within 2002, national bath gel sales volume is more than 2,000,000,000 yuan, year Rate of increase is more than 30%.
The cleaning products such as bath gel the most on the market are all widely used the synthetic surfactant main merit as cleaning decontamination Can composition, the most representative is AES (laureth sulfuric acid), K12A (lauryl sulfate ester ammonium salt), CAB (lauroylamidopropyl betaine) etc..These surfactants are all synthesized by industrial chemicals after chemical reaction, and And the chemical reaction experienced generally requires high temperature, strong acid, strong alkali environment, therefore inevitably result from various by-product, As dioxanes, dioxanes etc. can be produced when producing AES.These by-products are irritant to skin, eye and respiratory system, and Liver, kidney and nervous system may be caused damage, death may be caused during acute poisoning, be classified as carcinogen by the U.S..
Existing cleaning products, such as bath gel etc., is divided three classes mostly: 1, purification work synthesis material forms;2, pure Chemical industry synthesis material and Activities of Some Plants extract form;3, plant extract and preservative form.Wherein, the most mostly Plant extract in number cleaning products is typically all slightly to carry and directly obtains, could be as adding after needing to add preservative Thing adds in formula for a product.And mostly the plant extract in cleaning products is because only through slightly carrying, wherein containing many It is prone to corrupt material, such as vegetable protein etc., therefore to the stability of product considers, it is necessary to be added thereto to chemical preservation Agent, and chemical preservative exceed a certain amount of after, life-time service, can damage to human body.
Summary of the invention
For making up some shortcomings present in prior art, it is an object of the invention to provide a kind of natural plant extract formula Skin cleansing compositions, has good cleaning effect and bacteriostasis and sterilization performance.
The present invention is for reaching its purpose, and the technical scheme of employing is as follows:
The skin cleansing compositions of a kind of natural plant extract formula, including each component of following mass percent: Fructus Gleditsia extracts Thing 0~15%, soapberry extract 70~85%, green tea extract 1~10%, Flos Lonicerae extract 1~10%, Camellia oil 0~4%.
Preferably, the mass percent of described Fructus Gleditsiae Abnormalis extract is 5~15%, and the mass percent of described Camellia oil is 0.5~4%. Use this preferred version, can be in the case of the most additionally adding any chemical preservative, it is thus achieved that stability good skin clean group Compound, safe and healthy, pollution-free.
Preferably, the preparation of described Fructus Gleditsiae Abnormalis extract, soapberry extract or Flos Lonicerae extract comprises the steps: soap Angle, Fructus Sapindi Mukouossi or Flos Lonicerae water heating extraction, filters to obtain extracting solution, extracting solution is carried out concentrating under reduced pressure and (is preferably concentrated into heat Surveying density is 1.1~1.5g/ml), in concentrated solution, add ethanol and make final concentration of 50~80% (volume) of ethanol, fully stirring Stand 12-24H after even, take supernatant, reclaim the ethanol in supernatant and supernatant concentrating under reduced pressure (is preferably concentrated into heat and surveys close Degree is 1.1~1.5g/ml, and heat surveys surveyed density value after density refers to concentrating under reduced pressure).
It is further preferred that described heating extraction is to extract twice at 80~100 DEG C, each extraction time is 0.5~2H, water Consumption is 8~12 times of Fructus Gleditsia, Fructus Sapindi Mukouossi or quality of Flos Lonicerae.
Preferably, the preparation of described green tea extract comprises the steps: to use water heating extraction, filters to obtain extracting solution, extracts Liquid is 1.05~1.07g/ml through membrance concentration to density, extracts concentrated solution by ethyl acetate, reclaims ethyl acetate in extract And concentrating under reduced pressure (being preferably concentrated into heat and surveying density is 1.1~1.5g/ml, and heat surveys surveyed density value after density refers to concentrating under reduced pressure).
Preferably, in described recovery extract, ethyl acetate is that to be recycled to the volume of ethyl acetate in extract be that ethyl acetate is total Volume 12~18% time, to reclaiming the water dissolution adding 0.5~1.5 times amount in the extract after ethyl acetate, then carry out described Concentrating under reduced pressure.
It is further preferred that described heating extraction is extracted twice at 75~85 DEG C, extract 15~45min every time, extract every time 15~45min, the consumption of water is 8~12 times of green tea quality;During extraction, the volume ratio of ethyl acetate and concentrated solution is 0.5~2:1.
Preferably, described Camellia oil is that Semen Camelliae is prepared by squeezing.
Use the extract that preferred method for preparing extractive prepares and the Camellia oil using squeezing to prepare, they combine shape The skin cleansing compositions become, it is not necessary to add other chemical preservative, still can have good stability and antibacterial, sterilization Performance, and, safety the most healthy to human body, environmentally safe;The most also there is extraordinary cleaning effect.
Described skin cleansing compositions is bath gel or face cleaning product.
The technical scheme that the present invention provides has the advantages that
1, the skin cleansing compositions of the present invention obtained by the matched combined of each component has cleaning, antibacterial, bactericidal property Good feature.
2, preferred version is used, can be in the case of the most additionally adding any chemical preservative, it is thus achieved that the good skin of stability Cleasing compositions, safe and healthy, pollution-free.
3, the skin cleansing compositions of the present invention, it is not necessary to add essence and just give out distinctive fragrance, and ingenious group of each component Close the composition product pH value formed between 5~6, it is not necessary to regulate its pH value by acid-base modifier, on the one hand avoid The interpolation of extra industrial chemicals, on the other hand the most cost-effective and production process.
4, Fructus Gleditsiae Abnormalis extract, soapberry extract, green tea extract, Flos Lonicerae extract and mountain in the optimization formula of the present invention These several natural constituents of Oleum Camelliae are mutually combined collocation, can play moisturizing, antibacterial, sterilize, the effect such as cleaning, and to eczema Also certain remissive treatment effect is had with skin pruritus etc..Can be in the case of the most additionally adding any chemical preservative, it is thus achieved that steady Qualitative good skin cleansing compositions, safe and healthy, pollution-free, the most also there is cleaning, antibacterial, bactericidal property good Feature.
Detailed description of the invention
Below in conjunction with specific embodiment, technical scheme is described further:
Embodiment 1
A kind of bath gel, its constituent is each component of following mass percent: Fructus Gleditsiae Abnormalis extract 10%, soapberry extract 78%, green tea extract 5%, Flos Lonicerae extract 5%, Camellia oil 2%.
Fructus Gleditsiae Abnormalis extract therein is prepared in accordance with the following steps: by Fructus Gleditsia with the water of 10 times amount 100 DEG C of heating extraction twice, and Once extracting 1.5H, second time extracts 1H;After extraction, filter to obtain extracting solution, extracting solution is concentrated into heat at 85 DEG C and surveys density For 1.2g/ml (density recorded the most while hot after i.e. concentrating);In concentrated solution, add ethanol and make final concentration of the 70% of ethanol (volume), stirs evenly standing 24H, takes supernatant, reclaims the ethanol in supernatant and supernatant concentration to heat is surveyed density is 1.2g/ml (density recorded the most while hot after i.e. concentrating).
Soapberry extract therein is prepared in accordance with the following steps: by Fructus Sapindi Mukouossi with the water of 10 times amount in 100 DEG C of heating extraction twice, Extracting 1.5H for the first time, second time extracts 1H;After extraction, filter to obtain extracting solution, extracting solution is evaporated to heat in 85 DEG C Survey density is 1.2g/ml (density recorded the most while hot after i.e. concentrating), adds ethanol and make the final concentration of ethanol in concentrated solution It is 60% (volume), stirs evenly standing 24H, take supernatant, reclaim the ethanol in supernatant and by supernatant concentrating under reduced pressure, immediately Measuring density while hot, the heat survey density recording concentrated solution is 1.2g/ml (density recorded the most while hot after i.e. concentrating).
Green tea extract therein is prepared in accordance with the following steps: is heated to 80 DEG C with the water of 10 times amount and extracts twice, extracts every time 30min, filters to obtain extracting solution, and extracting solution is 1.05~1.07g/ml through membrance concentration to density, carries out concentrated solution by ethyl acetate Extraction, adds a times amount when reclaiming in extract ethyl acetate to its surplus about 15% (i.e. the 15% of ethyl orthoacetate cumulative volume) Water water turn molten after in 80 DEG C be evaporated to heat survey density be 1.2g/ml.
Flos Lonicerae extract therein is prepared in accordance with the following steps: with the water of 10 times amount, Flos Lonicerae is heated to 100 DEG C and extracts twice, Extracting 1.5H for the first time, second time extracts 1H;After extraction, filter to obtain extracting solution, extracting solution is evaporated to heat at 85 DEG C Survey density is 1.2g/ml (density recorded the most while hot after i.e. concentrating), adds ethanol and make the final concentration of ethanol in concentrated solution It is 50% (volume), stirs evenly standing 24H, take supernatant, reclaim the ethanol in supernatant and supernatant is evaporated to heat survey Density is 1.2g/ml (density recorded the most while hot after i.e. concentrating).
Camellia oil therein is that Semen Camelliae obtains through squeezing.
Embodiment 2
A kind of bath gel, its constituent is each component of following mass percent: Fructus Gleditsiae Abnormalis extract 5%, soapberry extract 85%, green tea extract 2%, Flos Lonicerae extract 4%, Camellia oil 4%.
Preparation and the embodiment 1 of each component are essentially identical, repeat no more.
Embodiment 3
A kind of bath gel, its constituent is each component of following mass percent: Fructus Gleditsiae Abnormalis extract 15%, soapberry extract 80%, green tea extract 2%, Flos Lonicerae extract 2%, Camellia oil 1%.
Preparation and the embodiment 1 of each component are essentially identical, repeat no more.
Product checking is with on probation
To the product of embodiment 1~3 after the airtight placement of normal temperature condition 30 days, outward appearance, color be unchanged, without layering, abnormal smells from the patient without Abnormal etc..
Product to embodiment 1~3,40 DEG C, carry out constant temperature culture 72H, 168H under the conditions of relative humidity 75%, survey respectively Fixed total plate count therein, result shows: total plate count N < 100CFU, illustrates that product stability is well difficult to corruption.Following table 1,2 show embodiment 1 product specifically detect numerical value, the Product checking numerical value of real number example 2~3 is similar with embodiment 1, no Repeat again.
The table 1 antibacterial circle diameter (unit: MM) to several bacterial strains
Bacterial strain Antibacterial circle diameter Sensitivity
Staphylococcus aureus 16.3 Gao Min
Escherichia coli 20.1 Gao Min
Gram negative bacteria 18.2 Gao Min
Candida albicans 17.4 Gao Min
Mycete 18.6 Gao Min
Note: D≤10.5MM is less sensitive;14.5MM >=D > 10.5MM is medium sensitivity;20MM≥D>14.5MM For extremely sensitive;D > 20MM is extremely sensitive.
The table 2 minimum bactericidal concentration (unit: G/ML) to several bacterial strains
Table 1, the data of table 2 show functional to the bacteriostasis and sterilization of above-mentioned several bacterium of this formula.
Embodiment 1~3 carries out detection on probation, and each product is tried out 1 month through 50 people, and feedback on probation all represents that product uses nothing Zest, cleaning effect is good.
The above, be only presently preferred embodiments of the present invention, and the present invention not does any pro forma restriction, thus all not Depart from technical solution of the present invention content, according to the present invention technical spirit to any simple modification made for any of the above embodiments, etc. With change and modification, all still fall within the range of technical solution of the present invention.

Claims (10)

1. the skin cleansing compositions of a natural plant extract formula, it is characterised in that include each of following mass percent Component: Fructus Gleditsiae Abnormalis extract 0~15%, soapberry extract 70~85%, green tea extract 1~10%, Flos Lonicerae extract 1~10%, Camellia oil 0~4%.
Skin cleansing compositions the most according to claim 1, it is characterised in that the mass percent of described Fructus Gleditsiae Abnormalis extract Being 5~15%, the mass percent of described Camellia oil is 0.5~4%.
Skin cleansing compositions the most according to claim 1, it is characterised in that described Fructus Gleditsiae Abnormalis extract, Fructus Sapindi Mukouossi extract The preparation of thing or Flos Lonicerae extract comprises the steps:, by Fructus Gleditsia, Fructus Sapindi Mukouossi or Flos Lonicerae water heating extraction, to filter to carry Take liquid, extracting solution carried out concentrating under reduced pressure, in concentrated solution, add ethanol and make final concentration of 50~80% (volume) of ethanol, Stand 12-24H after fully stirring evenly, take supernatant, reclaim the ethanol in supernatant and supernatant is carried out concentrating under reduced pressure.
Skin cleansing compositions the most according to claim 3, it is characterised in that described heating extraction is at 80~100 DEG C Extracting twice, each extraction time is 0.5~2h, and the consumption of water is 8~12 times of Fructus Gleditsia, Fructus Sapindi Mukouossi or quality of Flos Lonicerae.
Skin cleansing compositions the most according to claim 1, it is characterised in that the preparation of described green tea extract include as Lower step: use water heating extraction, filters to obtain extracting solution, and extracting solution is 1.05~1.07g/ml through membrance concentration to density, uses acetic acid second Concentrated solution is extracted by ester, reclaims ethyl acetate, then concentrating under reduced pressure in extract.
Skin cleansing compositions the most according to claim 5, it is characterised in that in described recovery extract, ethyl acetate is Be recycled to that the volume of ethyl acetate in extract is ethyl acetate cumulative volume 12~18% time, the extract after reclaiming ethyl acetate The water dissolution of middle addition 0.5~1.5 times amount, then carries out described concentrating under reduced pressure.
Skin cleansing compositions the most according to claim 5, it is characterised in that described heating extraction is for carry at 75~85 DEG C Taking twice, extract 15~45min every time, the consumption of water is 8~12 times of green tea quality;Ethyl acetate and concentrated solution during extraction Volume ratio is 0.5~2:1.
8. according to the skin cleansing compositions described in any one of claim 3 or 5, it is characterised in that described concentrating under reduced pressure is dense Being reduced to heat and surveying density is 1.1~1.5g/ml.
Skin cleansing compositions the most according to claim 1 and 2, it is characterised in that described Camellia oil is that Semen Camelliae passes through Squeezing prepares.
Skin cleansing compositions the most according to claim 1, it is characterised in that described skin cleansing compositions is for taking a shower Dew or face cleaning product.
CN201610552446.4A 2016-07-12 2016-07-12 Skin-cleaning composition with natural plant extract formula Pending CN105997740A (en)

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107669574A (en) * 2017-09-22 2018-02-09 广西巧恩茶业有限公司 A kind of Jasmine Cleansing Foam
CN108888551A (en) * 2018-06-24 2018-11-27 覃海平 A kind of cleaning solution and preparation method thereof of moisturizing sterilizing
CN109512742A (en) * 2018-12-26 2019-03-26 株洲千金药业股份有限公司 A kind of man's essential oil shower condensation and preparation method thereof
CN112915053A (en) * 2021-02-04 2021-06-08 贵州省中国科学院天然产物化学重点实验室(贵州医科大学天然产物化学重点实验室) Plant bacteriostatic hand sanitizer and preparation method thereof
WO2021163736A1 (en) * 2020-02-10 2021-08-19 HANG, Nguyen Tuy Probiotic-containing natural composition for cleaning the body, which is capable of deodorizing, decomposing organic matters adhered to the body and the body cleaning products made from this composition
CN115252505A (en) * 2022-09-09 2022-11-01 中华全国供销合作总社南京野生植物综合利用研究所 Compound plant composition with cleaning effect and preparation method and application thereof

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107669574A (en) * 2017-09-22 2018-02-09 广西巧恩茶业有限公司 A kind of Jasmine Cleansing Foam
CN108888551A (en) * 2018-06-24 2018-11-27 覃海平 A kind of cleaning solution and preparation method thereof of moisturizing sterilizing
CN109512742A (en) * 2018-12-26 2019-03-26 株洲千金药业股份有限公司 A kind of man's essential oil shower condensation and preparation method thereof
WO2021163736A1 (en) * 2020-02-10 2021-08-19 HANG, Nguyen Tuy Probiotic-containing natural composition for cleaning the body, which is capable of deodorizing, decomposing organic matters adhered to the body and the body cleaning products made from this composition
CN112915053A (en) * 2021-02-04 2021-06-08 贵州省中国科学院天然产物化学重点实验室(贵州医科大学天然产物化学重点实验室) Plant bacteriostatic hand sanitizer and preparation method thereof
CN115252505A (en) * 2022-09-09 2022-11-01 中华全国供销合作总社南京野生植物综合利用研究所 Compound plant composition with cleaning effect and preparation method and application thereof

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Application publication date: 20161012