CN101229111A - Method of producing attapulgite herbaceous toothpaste - Google Patents

Abstract

The invention discloses a method for manufacturing a concavo convex bar herbage toothpaste the main points of the technical scheme of which is essentially characterized in that the method for manufacturing the concavo convex bar herbage toothpaste relates to ingredient mixing, low speed stirring, crushing and beating, grinding, high speed stirring, vacuum deaerating and canning to be a finished product of the concavo convex bar herbage toothpaste. The concavo convex bar herbage toothpaste comprises paste-shaped concavo convex bar clay, fresh herba cephalanoploris, fresh purslane, fresh aloe, fresh mint, fresh Cogongrass rhizome, fresh Lophatherum gracile, fresh lotus leaf, fresh liquorice, of sodium dodecyl sulfate, potassium sorbate, borneol and deionized water. The concavo convex bar herbage toothpaste has the advantages of clean paste body, suppleness and smoothness, high foaming capacity, being cool and daintily, good stability; the paste body can not flow out of a tube opening and can not separate water, has a normal fragrance and color, and a glass has no nicks. The concavo convex bar herbage toothpaste can directly absorb and remove various peculiar odors in a mouth and effectively remove tooth dirty and prevent a gum from blooding. The invention is suitable for manufacturing the concavo convex bar herbage toothpaste, the traditional Chinese medicine toothpaste and other medicine toothpaste.

Description

The production method of attapulgite herbaceous toothpaste

Technical field:

The present invention relates to toothpaste, be specifically related to a kind of production method of attapulgite herbaceous toothpaste.

Background technology:

Herbal stem, branch are soft, and plant is less, is generally annual, biennial or perennial plant, most herbaceous plant have be food be again the effect of medicine.

Herbaceous plant adding ingredient in the toothpaste relates to processes such as herbaceous plant collection, processing, effective ingredient refinement, and it has determined directly whether the elite composition that adds in the toothpaste can play a role.

The raw material that is adopted in the herbaceous plant toothpaste is the herbaceous plant finished product after drying mostly, also there is the infusion method of employing to extract its soak or its concentrated solution, still contain a large amount of effective ingredient in the garbage after herbaceous plant is soaked, cause bigger economic loss.

The abrasivus that herbaceous plant toothpaste is commonly used has calcium carbonate, calcium phosphate dibasic dihydrate, no hydration calcium hydrogen phosphate, calcium pyrophosphate, anhydride silica, aluminium hydroxide etc., because the hardness of these abrasivuss is higher relatively, granule is coarse, there is not stickiness, absorption property is poor, and life-time service easily causes wearing and tearing to the enamel of dental surface.

Summary of the invention:

The objective of the invention is to overcome weak point in the prior art, a kind of production method that contains the attapulgite herbaceous toothpaste of herbaceous plant stem and leaf is provided.

The production method of attapulgite herbaceous toothpaste is batching, stirring at low speed, pulverizing making beating, grinding, high-speed stirred, vacuum outgas, cannedly is the finished product of attapulgite herbaceous toothpaste.

Attapulgite herbaceous toothpaste is made up of lip lipstick attapulgite clay, bright Herba Cirsii, fresh Herba Portulacae, bright Aloe, bright Herba Menthae, fresh Rhizoma Imperatae, bright Herba Lophatheri, new lotus leaf, bright Radix Glycyrrhizae, sodium lauryl sulphate, potassium sorbate, Borneolum Syntheticum and deionized water.

Attapulgite clay is a kind of nanometer porous fibrous silicate clay mineral of Shuifu County's magnesium that contains, and when attapulgite content 〉=80% in the attapulgite clay was above, its specific surface area was bigger, can reach 500m ²More than/the g, most cation, hydrone and a certain size organic molecule all can directly be adsorbed in the duct, and its water absorption can reach more than 150%.

Use attapulgite ore pul making production technology, the screening of mineral such as the hydromica in the attapulgite clay, quartz, opal and carbonate is got rid of, obtain a kind of lip lipstick attapulgite clay, have the characteristics of ultrafine dust, friction little, the no sand feeling of hardness and soft fine and smooth free from extraneous odour.

Lip lipstick attapulgite clay is through powerful stirring at a high speed, become the special good natural gelinite of a kind of thixotropy and gumminess, viscosity is up to more than the 10000mPas, absorption property and performance of keeping humidity have all obtained further raising, attapulgite clay after the high-speed stirred, total characteristic with abrasivus, adhesive and wetting agent, use lip lipstick attapulgite clay to produce toothpaste and do not need to add in addition abrasivus, adhesive and wetting agent, not only can improve the quality of toothpaste, can also reduce production costs greatly.

Herba Cirsii is a perennial herb, has cooling blood for hemostasis, and the function of removing blood stasis to reduce swelling is removed impurity after tapping, and it is standby to clean chopping.

Herba Portulacae is annual meat herbaceous plant, has effects such as convergence detumescence, detoxifcation dysentery relieving, antiinflammatory hemostasis, removes impurity after tapping, and it is standby to clean chopping.

Aloe is a kind of perennial evergreen fleshiness herbaceous plant, has to regulate body immunity, anti-inflammation and sterilization, analgesia, anticorrosion, repair tissue damage and promote the restorative effect of wound healing, removes impurity after tapping, and it is standby to clean chopping.

Herba Menthae is a herbaceos perennial, and the effect of wind-dispelling heat-dissipating, appetizing is arranged, and bright stem and leaf contains protein, multivitamin, Oleum menthae and trace element, removes impurity after tapping, and it is standby to clean chopping.

Rhizoma Imperatae is a grass family herbaceos perennial Herba Imperatae rhizome, has cooling blood for hemostasis, clearing away heat-damp and promoting diuresis, and the effect of promoting the production of body fluid to quench thirst is removed impurity after excavating, and it is standby to clean chopping.

Herba Lophatheri is the stem and leaf of grass Herba Lophatheri, has clearing heat and relieving fidgetness, the diuretic function; Be used for calentura excessive thirst, hot urination pouring pain, aphtha of the mouth and tongue, remove impurity after tapping, it is standby to clean chopping.

Folium Nelumbinis is the blade of aquatic herbaceous plant lotus for many years, has effects such as clearing away summer-heat and eliminating dampness, yang invigorating are dispersed, hemostasis by removing blood stasis, removes impurity after tapping, and it is standby to clean chopping.

Radix Glycyrrhizae is the pulse family herbaceos perennial, has eliminating fire and detoxication, coordinating the actions of various ingredients in a prescription, eliminates the phlegm, effects such as pain relieving and spasmolytic, removes impurity after tapping, and it is standby to clean chopping.

Sodium lauryl sulphate belongs to anion surfactant, and is soluble in water, and compatibility is good again with anion, nonionic, has good emulsifying, foaming, infiltration, decontamination and dispersive property, and foaming power is strong.

Potassium sorbate is mould fungus inhibition effectively, the activity of yeast and aerobic bacteria, can also prevent harmful microbe growth and breedings such as bacillus botulinus, staphylococcus, Salmonella, it is stronger than bactericidal action that it restrains the effect of growing, thereby reach the holding time that prolongs toothpaste effectively, and the local flavor of maintenance toothpaste, its antiseptic effect is 5-10 a times of like product sodium benzoate.

Borneolum Syntheticum has antiinflammatory, antibiotic, pain relieving and antisepsis.

The present invention is achieved by following technical proposals:

The production method of attapulgite herbaceous toothpaste, it is characterized in that, 1. after carrying out the stirring at low speed mix homogeneously in the batching adding blender with attapulgite herbaceous toothpaste, pulverizing making beating in the input pulverizing beater is the mixture of attapulgite herbaceous toothpaste, the speed controlling of blender is at 500～800 rev/mins, the stirring at low speed time was controlled at 5～15 minutes, and the speed controlling of pulverizing beater is at 2500～3000 rev/mins; The purpose of stirring at low speed is that various batchings are stirred, and helps pulverizing the operate as normal of beater; 2. the mixture that 1. step is obtained is imported to grind in the multi-functional colloid mill and is pasty mixture, and fineness of the particles is less than 0.025 millimeter, and the speed controlling of multi-functional colloid mill is at 2900 rev/mins; Multi-functional colloid grinding tool has functions such as the pulverizing of wet processed fluid ultra micron, grinding, emulsifying, dispersion, homogenizing, stirring, mixing, can replace and be better than stone grinder, sand mill, ball mill, dispersing emulsification machine, shearing disperse pump, work efficiencies such as homogeneous emulsifying machine, three-roller, tissue mashing machine; 3. the pasty mixture after the grinding that 2. step is obtained carries out powerful stirring of high speed and is the paste semi-finished product in the input ultrahigh speed blender, and the speed controlling of ultrahigh speed blender is at 4000～11000 rev/mins, and the high-speed stirred time was controlled at 5～30 minutes; The ultrahigh speed blender has unique blade design and stepless speed-regulating device, can select optimal speed according to manufacturing technique requirent, and after the pasty mixture after the grinding stirred through ultrahigh speed, viscosity was up to more than the 10000mPas; 4. the paste semi-finished product that 3. step obtained carry out vacuum degassing process to be handled, and canned is the finished product of attapulgite herbaceous toothpaste.

The batching of described attapulgite herbaceous toothpaste is made up of following component: lip lipstick attapulgite clay 30～55%, bright Herba Cirsii 1～5%, fresh Herba Portulacae 1～5%, bright Aloe 1～5%, bright Herba Menthae 1～5%, fresh Rhizoma Imperatae 1～5%, bright Herba Lophatheri 1～5%, new lotus leaf 1～5%, bright Radix Glycyrrhizae 1～5%, sodium lauryl sulphate 0.2～2.5%, potassium sorbate 0.06～0.5%, Borneolum Syntheticum 0.05～0.5% and deionized water 5～45% by weight percentage.

The production technology of described lip lipstick attapulgite clay: will stir in the attapulgite ore deposit input blender, after extruder is squeezed into lamellar, import once more in the blender and stir, natural drying after extruder is squeezed into lamellar, air dried attapulgite ore deposit is transported in the feed reservoir soaks, dash with air pump and to turn over, post precipitation is emitted immersion water, the sieve decontamination in the input semi-finished product pond, is soaked again, dash with air pump and to turn over, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, is lip lipstick attapulgite clay.

This production technology is to adopt " the attapulgite ore pul making production technology " in application on January 6th, 2004 by the inventor, and the Chinese patent Granted publication number is: CN1287965C, Granted publication day: on December 6th, 2006.

Described lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 25～40%, water 60～75%.

Attapulgite herbaceous toothpaste uses lip lipstick attapulgite clay to be primary raw material, does not need to add in addition abrasivus, adhesive and wetting agent, not only can improve the quality of toothpaste, can also reduce production costs greatly.

Attapulgite herbaceous toothpaste uses fresh herbaceous plant stem and leaf, not only can make full use of herbal effective ingredient, reduce pollution in the dry in the sun process, go mouldy and production cost, and kept herbal Plant fiber, can increase the denseness of lotion of toothpaste, help increasing the friction of toothpaste, improve the friction effect and the stability of toothpaste.

The cleaning of attapulgite herbaceous toothpaste mastic, soft fine and smooth, strong, refrigerant tasty and refreshing, the good stability of foaming power; Mastic does not overflow the mouth of pipe, does not separate water outlet, and the fragrance color and luster is normal, the slide no marking.

Tooth dirt and prevention gingival hemorrhage are distinguished the flavor of, effectively removed to the multiple foreign odor that attapulgite herbaceous toothpaste can directly adsorb and remove in the oral cavity.

The present invention is applicable to and produces attapulgite herbaceous toothpaste, Chinese herbal toothpaste and other medicines toothpaste.

The specific embodiment:

The invention will be further described below in conjunction with embodiment:

The production method of attapulgite herbaceous toothpaste, it is characterized in that, 1. after carrying out the stirring at low speed mix homogeneously in the batching adding blender with attapulgite herbaceous toothpaste, pulverizing making beating in the input pulverizing beater is the mixture of attapulgite herbaceous toothpaste, the speed controlling of blender is at 600 rev/mins, the stirring at low speed time was controlled at 8 minutes, and the speed controlling of pulverizing beater is at 2800 rev/mins; 2. the mixture that 1. step is obtained is imported to grind in the multi-functional colloid mill and is pasty mixture, and fineness of the particles is less than 0.015 millimeter, and the speed controlling of multi-functional colloid mill is at 2900 rev/mins; 3. the pasty mixture after the grinding that 2. step is obtained carries out powerful stirring of high speed and is the paste semi-finished product in the input ultrahigh speed blender, and the speed controlling of ultrahigh speed blender is at 8000 rev/mins, and the high-speed stirred time was controlled at 25 minutes; 4. the paste semi-finished product that 3. step obtained carry out vacuum degassing process to be handled, and canned is the finished product of attapulgite herbaceous toothpaste.

The batching of described attapulgite herbaceous toothpaste is made up of following component: lip lipstick attapulgite clay 40.0%, bright Herba Cirsii 4.0%, fresh Herba Portulacae 4.0%, bright Aloe 3.0%, bright Herba Menthae 2.0%, fresh Rhizoma Imperatae 2.0%, bright Herba Lophatheri 2.0%, new lotus leaf 1.8%, bright Radix Glycyrrhizae 1.5%, sodium lauryl sulphate 1.5%, potassium sorbate 0.15%, Borneolum Syntheticum 0.05% and deionized water 38.0% by weight percentage.

Described lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 30%, water 70%.

Main physical and chemical index testing result

Project		Index	Testing result
				Physical and chemical index	Denseness, mm	9～33	26
Squeeze cream pressure, kPa≤	40	32
			Foam volume, mm 〉=		60	74
pH	5.0～10.0	8.3
			Stability		Mastic does not overflow the mouth of pipe, does not separate water outlet, and the fragrance color and luster is normal	Mastic does not overflow the mouth of pipe, does not separate water outlet, and the fragrance color and luster is normal
Cross grit	The slide no marking	The slide no marking

Claims (1)

1. the production method of an attapulgite herbaceous toothpaste, it is characterized in that, 1. after carrying out the stirring at low speed mix homogeneously in the batching adding blender with attapulgite herbaceous toothpaste, pulverizing making beating in the input pulverizing beater is the mixture of attapulgite herbaceous toothpaste, the speed controlling of blender is at 500～800 rev/mins, the stirring at low speed time was controlled at 5～15 minutes, and the speed controlling of pulverizing beater is at 2500～3000 rev/mins; 2. the mixture that 1. step is obtained is imported to grind in the multi-functional colloid mill and is pasty mixture, and fineness of the particles is less than 0.025 millimeter, and the speed controlling of multi-functional colloid mill is at 2900 rev/mins; 3. the pasty mixture after the grinding that 2. step is obtained carries out powerful stirring of high speed and is the paste semi-finished product in the input ultrahigh speed blender, and the speed controlling of ultrahigh speed blender is at 4000～11000 rev/mins, and the high-speed stirred time was controlled at 5～30 minutes; 4. the paste semi-finished product that 3. step obtained carry out vacuum degassing process to be handled, and canned is the finished product of attapulgite herbaceous toothpaste;

The batching of described attapulgite herbaceous toothpaste is made up of following component: lip lipstick attapulgite clay 30～55%, bright Herba Cirsii 1～5%, fresh Herba Portulacae 1～5%, bright Aloe 1～5%, bright Herba Menthae 1～5%, fresh Rhizoma Imperatae 1～5%, bright Herba Lophatheri 1～5%, new lotus leaf 1～5%, bright Radix Glycyrrhizae 1～5%, sodium lauryl sulphate 0.2～2.5%, potassium sorbate 0.06～0.5%, Borneolum Syntheticum 0.05～0.5% and deionized water 5～45% by weight percentage;

The production technology of described lip lipstick attapulgite clay: will stir in the attapulgite ore deposit input blender, after extruder is squeezed into lamellar, import once more in the blender and stir, natural drying after extruder is squeezed into lamellar, air dried attapulgite ore deposit is transported in the feed reservoir soaks, dash with air pump and to turn over, post precipitation is emitted immersion water, the sieve decontamination in the input semi-finished product pond, is soaked again, dash with air pump and to turn over, post precipitation is emitted immersion water, and the slurry transportation of post precipitation is arrived in the finished product pond, is lip lipstick attapulgite clay;

Described lip lipstick attapulgite clay is made up of following component by weight percentage: attapulgite clay 25～40%, water 60～75%.