CN103565654A - Montmorillonite facial cleanser - Google Patents
Montmorillonite facial cleanser Download PDFInfo
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- CN103565654A CN103565654A CN201310481264.9A CN201310481264A CN103565654A CN 103565654 A CN103565654 A CN 103565654A CN 201310481264 A CN201310481264 A CN 201310481264A CN 103565654 A CN103565654 A CN 103565654A
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- montmorillonitum
- microemulsion
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- cleansing milk
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Abstract
The invention belongs to the field of cosmetics and provides a montmorillonite facial cleanser containing montmorillonite microemulsion and one or more of a skin care agent, a humectant, a surfactant and an emulsifying agent, wherein all the components are respectively in the following percentage by mass: 0-5% of the skin care agent, 2-10% of the humectant, 0-5% of the surfactant, 0-20% of the emulsifying agent and the balance of the montmorillonite microemulsion. The facial cleanser provided by the invention is prepared by sufficiently utilizing mineral resources, so that the raw material cost is low; other auxiliary materials are reasonably allocated according to the characteristic that montmorillonite has negative charges, so that dirt can be thoroughly removed, and meanwhile, the delicate skin on the face is protected.
Description
Technical field
The invention belongs to cosmetic field, be specifically related to a kind of cosmetics containing mineral constituent.
Background technology
Cleansing milk is the essential product of daily clean, cleansing milk can cleaning skin dirt, supplement the required nutrient of skin simultaneously, but existing cleansing milk is mainly that the surfactant compound that function ratio is more single forms on the market at present, uses in a large number surfactant, easily causes the undue defat of epiderm skin, thereby make skin drier, more serious meeting causes the irreversibility infringement to skin, and function singleness, cannot meet the demand of user to the multiple efficacies such as maintenance of skin.
Montmorillonitum is the layer mineral consisting of the superfine hydrous alumino silicates of granule, is important clay mineral, and self is with the characteristic of negative charge, molecular formula (Al, Mg)
2[Si
4o
10] (OH)
2nH
2o, belongs to monoclinic moisture layer structure silicate mineral.Centre is alumina octahedral, the clay mineral of the three-layer tablet shape structure forming for silicon-oxy tetrahedron up and down, and at crystal structure interlayer, moisture and some exchange cations, have higher ion exchange capacity, have higher imbibition ability.In low bubble decontamination, there is again good skin protection and bacteriostasis.The antibacterial of comparing chemical classes, Montmorillonitum has natural bacteriostatic, the feature of performance gentleness.
Montmorillonitum after dehydration can also be reuptaked hydrone or other polar molecules.After absorbing moisture, their can also expand and surpass several times of original volume, the absorption affinity that tool is very strong and cation exchange property.This characteristic, as suitably used, can make the articles for washing of better effects if.
Summary of the invention
The weak point existing for this area, the object of the invention is to propose a kind of Montmorillonitum cleansing milk.
Another object of the present invention is to propose a kind of method of preparing Montmorillonitum cleansing milk.
The technical scheme that realizes above-mentioned purpose of the present invention is:
A cleansing milk, contains one or more in Montmorillonitum microemulsion and skin protectant, wetting agent, surfactant, emulsifying agent, and the mass percent of each component is:
Surplus is Montmorillonitum microemulsion.
Preferably, the mass percent of each component is:
Surplus is Montmorillonitum microemulsion.
Wherein, described Montmorillonitum microemulsion is that Montmorillonitum ore deposit soil adds 15-25(quality) soak after times water, screening, through ultramicronising, process the emulsion obtaining.
Wherein, described Montmorillonitum microemulsion is to soak, sieve after Montmorillonitum ore deposit soil adds 15-25 times of water, then at normal temperatures, in Montmorillonitum emulsion, add 0-2.0% sodium agent solution and concentrated sulphuric acid to regulate pH=5.5-7.5, in dispersion machine, stir after 3h, ultramicronising is processed 10-30min, then grinds 2-10min and make.
Wherein, described skin protectant is lanoline and derivant thereof, squalane, cocoa butter, one or more in Oleum Hippophae.
Wherein, described wetting agent is one or more in glycerol, propylene glycol, triethanolamine, sorbitol and derivant thereof, hyaluronic acid, ceramide, Polyethylene Glycol;
Described surfactant is one or more in MES (MES), cocoyl sodium isethionate (SCI), alkyl polyglucoside/alkyl polyglycoside (APG), cocamido propyl betaine (CAB), dodecylbenzene sodium sulfonate (LAS), aliphatic alcohol polyethenoxy sodium sulfate (AES), fatty alcohol-polyoxyethylene ether (AE), cocos nucifera oil acyl diethanolamine (6501,6502).
Wherein, described emulsifying agent is one or more the mixture of stearic acid, Tween-20, Tween-80, Span-20, Span-80.
The preparation method of Montmorillonitum cleansing milk of the present invention, is characterized in that, comprises step:
1) natural minerals is purified
First Montmorillonitum ore deposit soil is stirred with 15-25 times of pure water, soak 40-60 hour, vibrosieve, processes through slagging-off after screening more while stirring, makes Montmorillonitum emulsion;
2) preparation of Montmorillonitum microemulsion
Under room temperature, in Montmorillonitum emulsion, add 0-2.0% sodium agent solution (sodium agent accounts for complete soln 0-2wt%) and concentrated sulphuric acid to regulate pH=5.5-7.5, stir after 3h in dispersion machine, ultramicronising is processed 10-30min, grind again 2-10min, make Montmorillonitum microemulsion;
3) by component, get after skin protectant, wetting agent, surfactant, emulsifying agent and Montmorillonitum microemulsion mixing and stirring standing.
Wherein, described sodium agent is one or more in sodium carbonate, sodium bicarbonate, tetrasodium pyrophosphate; Sodium agent addition is 0.5～1.5%.
Wherein, in described step 1), use 200 mesh sieves to sieve.
Beneficial effect of the present invention is:
The cleansing milk that the present invention proposes makes full use of mineral resources, and cost of material is cheap; By the electronegative characteristic of Montmorillonitum self, other adjuvants of reasonable disposition, can thoroughly protect the tender and lovely skin of face in decontamination.
The specific embodiment
Following examples further illustrate content of the present invention, but should not be construed as limitation of the present invention.Without departing from the spirit and substance of the case in the present invention, the modification that the inventive method, step or condition are done or replacement, all belong to scope of the present invention.
If do not specialize, the conventional means that in embodiment, technological means used is well known to those skilled in the art.
Embodiment 1
1, Montmorillonitum microemulsion
1) natural minerals is purified
First Montmorillonitum ore deposit soil is stirred fully and soaked 50 hours with purifying waste water of 20 times of quality, after it fully expands, make while stirring solution sieve through 200 order vibrosieves, thereby isolate large granular impurity ore deposit soil, the Montmorillonitum emulsion after filtration is again through further slagging-off processing.
2) preparation of Montmorillonitum microemulsion
Under room temperature, add 0.8% sodium agent solution and a small amount of concentrated sulphuric acid to regulate pH=6.5 in Montmorillonitum emulsion, wherein sodium agent is sodium carbonate, in dispersion machine, stir after 3h, in ultrasonic disperser, ultramicronising is processed 20min, then grinds 5min by colloid mill, makes Montmorillonitum microemulsion.
2, Montmorillonitum cleansing milk
According to following each component and proportioning, prepare Montmorillonitum cleansing milk of the present invention:
Lanoline 4%, triethanolamine 2%, glycerol 5%, surfactant 0.1%, stearic acid 5%, Montmorillonitum microemulsion surplus.Standing after mixing and stirring.
Testing requirement according to cleansing milk industry standard (QB/T1645-2004) and cosmetics health standard (2007 editions), detects according to a conventional method, weighs and pack.
Embodiment 2
The preparation of Montmorillonitum microemulsion and Montmorillonitum cleansing milk is as embodiment 1.
According to following each component and proportioning, prepare Montmorillonitum cleansing milk of the present invention:
Lanoline 1%, triethanolamine 1%, glycerol 4%, surfactant 3%, stearic acid 15%, Montmorillonitum microemulsion surplus.
Embodiment 3
The preparation of Montmorillonitum microemulsion and Montmorillonitum cleansing milk is as embodiment 1.
According to following each component and proportioning, prepare Montmorillonitum cleansing milk of the present invention:
Lanoline 0.1%, glycerol 10%, surfactant 5%, stearic acid 20%, Montmorillonitum microemulsion surplus.
Experimental example 1 conventional physico-chemical properties detects
The conventional physico-chemical properties testing result of the product that above-described embodiment 1-3 is obtained, in Table 1.
Table 1 cleansing milk conventional physico-chemical properties testing result
| Project | Embodiment 1 | Embodiment 2 | Embodiment 3 |
| Total number of bacteria CFU/g | ＜500 | ＜500 | ＜500 |
| Noxious substance is limited the quantity of, plumbous mg/kg | 5 | 5 | 5 |
| Noxious substance is limited the quantity of, hydrargyrum mg/kg | 0.3 | 0.3 | 0.3 |
| Noxious substance is limited the quantity of, arsenic mg/kg | Do not detect | Do not detect | Do not detect |
| Heat-resisting (40 ℃ 24 hours) | Without separated | 40 ℃ of 24 hours nothings are separated | 40 ℃ of 24 hours nothings are separated |
| pH | 6.5 | 6.5 | 6.5 |
The above is only the preferred embodiment of the present invention; it should be pointed out that for those skilled in the art, do not departing under the prerequisite of the technology of the present invention principle; can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (10)
1. a Montmorillonitum cleansing milk, is characterized in that, contains one or more in Montmorillonitum microemulsion and skin protectant, wetting agent, surfactant, emulsifying agent, and the mass percent of each component is:
Surplus is Montmorillonitum microemulsion.
2. Montmorillonitum cleansing milk according to claim 1, is characterized in that, the mass percent of each component is:
Surplus is Montmorillonitum microemulsion.
3. Montmorillonitum cleansing milk according to claim 1 and 2, is characterized in that, described Montmorillonitum microemulsion is to soak, sieve after Montmorillonitum ore deposit soil adds 15-25 times of water, processes the emulsion obtaining through ultramicronising.
4. Montmorillonitum cleansing milk according to claim 3, it is characterized in that, described Montmorillonitum microemulsion is to soak, sieve after Montmorillonitum ore deposit soil adds 15-25 times of water, then at normal temperatures, in Montmorillonitum emulsion, add 0-2.0% sodium agent solution and concentrated sulphuric acid to regulate pH=5.5-7.5, in dispersion machine, stir after 3h, ultramicronising is processed 10-30min, then grinds 2-10min and make.
5. Montmorillonitum cleansing milk according to claim 1 and 2, is characterized in that, described skin protectant is lanoline and derivant thereof, squalane, cocoa butter, one or more in Oleum Hippophae.
6. Montmorillonitum cleansing milk according to claim 1 and 2, is characterized in that, described wetting agent is one or more in glycerol, propylene glycol, triethanolamine, sorbitol and derivant thereof, hyaluronic acid, ceramide, Polyethylene Glycol;
Described surfactant is one or more in MES, cocoyl sodium isethionate, alkyl polyglucoside, cocamido propyl betaine, dodecylbenzene sodium sulfonate, aliphatic alcohol polyethenoxy sodium sulfate, fatty alcohol-polyoxyethylene ether, cocos nucifera oil acyl diethanolamine.
7. Montmorillonitum cleansing milk according to claim 1 and 2, is characterized in that, described emulsifying agent is one or more the mixture of stearic acid, Tween-20, Tween-80, Span-20, Span-80.
8. the preparation method of the arbitrary described Montmorillonitum cleansing milk of claim 1-7, is characterized in that, comprises step:
1) natural minerals is purified
First Montmorillonitum ore deposit soil is stirred with 15-25 times of pure water, soak 40-60 hour, vibrosieve, processes through slagging-off after screening more while stirring, makes Montmorillonitum emulsion;
2) preparation of Montmorillonitum microemulsion
Under room temperature, add 0-2.0% sodium agent solution and concentrated sulphuric acid to regulate pH=5.5-7.5 in Montmorillonitum emulsion, stir after 3h in dispersion machine, ultramicronising is processed 10-30min, then grinds 2-10min, makes Montmorillonitum microemulsion;
3) by component, get after skin protectant, wetting agent, surfactant, emulsifying agent and Montmorillonitum microemulsion mixing and stirring standing.
9. preparation method according to claim 8, is characterized in that, described sodium agent is one or more in sodium carbonate, sodium bicarbonate, tetrasodium pyrophosphate; Sodium agent addition is 5-12%.
10. preparation method according to claim 8 or claim 9, is characterized in that, in described step 1), uses 200 mesh sieves to sieve.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310481264.9A CN103565654B (en) | 2013-10-15 | 2013-10-15 | A kind of montmorillonite facial cleanser |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310481264.9A CN103565654B (en) | 2013-10-15 | 2013-10-15 | A kind of montmorillonite facial cleanser |
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| CN103565654A true CN103565654A (en) | 2014-02-12 |
| CN103565654B CN103565654B (en) | 2015-09-16 |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104027252A (en) * | 2014-06-25 | 2014-09-10 | 无锡市崇安区科技创业服务中心 | Nano bentonite antibacterial cleaning milk and preparation method thereof |
| CN106265107A (en) * | 2016-10-25 | 2017-01-04 | 于鑫 | A kind of clean skin product and preparation method thereof |
| WO2018040415A1 (en) * | 2016-08-27 | 2018-03-08 | 朱耀灯 | Deep replenishing and moisturizing face cleanser |
| CN109771309A (en) * | 2019-03-20 | 2019-05-21 | 北京周整无为健康管理有限责任公司 | A kind of facial cleanser and application thereof based on labradorite |
| CN110897938A (en) * | 2019-12-23 | 2020-03-24 | 广州倍健医疗用品有限公司 | Quick-foaming antibacterial anti-wrinkle cleansing foam and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1326728A (en) * | 2000-06-01 | 2001-12-19 | 翟永功 | Use of montmorillonite as cosmetic ingredient |
| CN103126934A (en) * | 2013-03-12 | 2013-06-05 | 昆山威胜干燥剂研发中心有限公司 | Seabuckthorn montmorillonite liquid soap and preparation method thereof |
-
2013
- 2013-10-15 CN CN201310481264.9A patent/CN103565654B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1326728A (en) * | 2000-06-01 | 2001-12-19 | 翟永功 | Use of montmorillonite as cosmetic ingredient |
| CN103126934A (en) * | 2013-03-12 | 2013-06-05 | 昆山威胜干燥剂研发中心有限公司 | Seabuckthorn montmorillonite liquid soap and preparation method thereof |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104027252A (en) * | 2014-06-25 | 2014-09-10 | 无锡市崇安区科技创业服务中心 | Nano bentonite antibacterial cleaning milk and preparation method thereof |
| CN104027252B (en) * | 2014-06-25 | 2016-08-24 | 无锡市崇安区科技创业服务中心 | A kind of nanometer bentonite bactericidal facial milk cleanser and preparation method thereof |
| WO2018040415A1 (en) * | 2016-08-27 | 2018-03-08 | 朱耀灯 | Deep replenishing and moisturizing face cleanser |
| CN106265107A (en) * | 2016-10-25 | 2017-01-04 | 于鑫 | A kind of clean skin product and preparation method thereof |
| CN109771309A (en) * | 2019-03-20 | 2019-05-21 | 北京周整无为健康管理有限责任公司 | A kind of facial cleanser and application thereof based on labradorite |
| CN110897938A (en) * | 2019-12-23 | 2020-03-24 | 广州倍健医疗用品有限公司 | Quick-foaming antibacterial anti-wrinkle cleansing foam and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN103565654B (en) | 2015-09-16 |
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