CN109771309A - A kind of facial cleanser and application thereof based on labradorite - Google Patents
A kind of facial cleanser and application thereof based on labradorite Download PDFInfo
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- CN109771309A CN109771309A CN201910214166.6A CN201910214166A CN109771309A CN 109771309 A CN109771309 A CN 109771309A CN 201910214166 A CN201910214166 A CN 201910214166A CN 109771309 A CN109771309 A CN 109771309A
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- labradorite
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- 229910052659 labradorite Inorganic materials 0.000 title claims abstract description 187
- 239000011018 labradorite Substances 0.000 title claims abstract description 187
- 230000001815 facial effect Effects 0.000 title claims abstract description 141
- 239000000843 powder Substances 0.000 claims abstract description 155
- 239000004575 stone Substances 0.000 claims abstract description 48
- 239000011159 matrix material Substances 0.000 claims abstract description 38
- 239000000203 mixture Substances 0.000 claims abstract description 21
- 239000011148 porous material Substances 0.000 claims abstract description 9
- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 claims description 68
- 239000000284 extract Substances 0.000 claims description 59
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 45
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 41
- 238000003756 stirring Methods 0.000 claims description 40
- 239000003755 preservative agent Substances 0.000 claims description 38
- 230000002335 preservative effect Effects 0.000 claims description 38
- 239000002253 acid Substances 0.000 claims description 36
- 239000000686 essence Substances 0.000 claims description 36
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- 229910021641 deionized water Inorganic materials 0.000 claims description 35
- 125000005908 glyceryl ester group Chemical group 0.000 claims description 35
- BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 claims description 35
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims description 35
- 229920001223 polyethylene glycol Polymers 0.000 claims description 35
- 239000004166 Lanolin Substances 0.000 claims description 34
- OBETXYAYXDNJHR-UHFFFAOYSA-N alpha-ethylcaproic acid Natural products CCCCC(CC)C(O)=O OBETXYAYXDNJHR-UHFFFAOYSA-N 0.000 claims description 34
- 229940039717 lanolin Drugs 0.000 claims description 34
- 235000019388 lanolin Nutrition 0.000 claims description 34
- 229940119170 jojoba wax Drugs 0.000 claims description 33
- 229920000915 polyvinyl chloride Polymers 0.000 claims description 31
- 238000002360 preparation method Methods 0.000 claims description 28
- 238000009835 boiling Methods 0.000 claims description 25
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 21
- 239000003963 antioxidant agent Substances 0.000 claims description 21
- 230000003078 antioxidant effect Effects 0.000 claims description 21
- 235000013339 cereals Nutrition 0.000 claims description 21
- 235000013312 flour Nutrition 0.000 claims description 21
- 229960003511 macrogol Drugs 0.000 claims description 21
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 claims description 19
- 229920000053 polysorbate 80 Polymers 0.000 claims description 19
- 239000002245 particle Substances 0.000 claims description 15
- 238000000034 method Methods 0.000 claims description 12
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- 230000000694 effects Effects 0.000 claims description 8
- 238000009826 distribution Methods 0.000 claims description 7
- 238000006243 chemical reaction Methods 0.000 claims description 6
- 239000004519 grease Substances 0.000 claims description 4
- 239000002537 cosmetic Substances 0.000 claims description 2
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims description 2
- 229920002554 vinyl polymer Polymers 0.000 claims description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 1
- 241001494479 Pecora Species 0.000 claims 1
- 230000021736 acetylation Effects 0.000 claims 1
- 238000006640 acetylation reaction Methods 0.000 claims 1
- 239000002304 perfume Substances 0.000 claims 1
- 235000013599 spices Nutrition 0.000 claims 1
- 230000003255 anti-acne Effects 0.000 abstract description 4
- 230000001151 other effect Effects 0.000 abstract description 3
- 230000002087 whitening effect Effects 0.000 abstract description 3
- 210000002374 sebum Anatomy 0.000 abstract description 2
- 239000003795 chemical substances by application Substances 0.000 description 18
- 229920000136 polysorbate Polymers 0.000 description 16
- 229940057847 polyethylene glycol 600 Drugs 0.000 description 14
- 239000008267 milk Substances 0.000 description 9
- 210000004080 milk Anatomy 0.000 description 9
- 235000013336 milk Nutrition 0.000 description 9
- BJRNKVDFDLYUGJ-RMPHRYRLSA-N hydroquinone O-beta-D-glucopyranoside Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1OC1=CC=C(O)C=C1 BJRNKVDFDLYUGJ-RMPHRYRLSA-N 0.000 description 8
- 238000004140 cleaning Methods 0.000 description 5
- 239000011347 resin Substances 0.000 description 5
- 229920005989 resin Polymers 0.000 description 5
- 241000758789 Juglans Species 0.000 description 4
- 235000009496 Juglans regia Nutrition 0.000 description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 4
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 4
- 229960000271 arbutin Drugs 0.000 description 4
- BJRNKVDFDLYUGJ-UHFFFAOYSA-N p-hydroxyphenyl beta-D-alloside Natural products OC1C(O)C(O)C(CO)OC1OC1=CC=C(O)C=C1 BJRNKVDFDLYUGJ-UHFFFAOYSA-N 0.000 description 4
- 235000020234 walnut Nutrition 0.000 description 4
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- 238000003475 lamination Methods 0.000 description 3
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- 244000144725 Amygdalus communis Species 0.000 description 1
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- 241000790917 Dioxys <bee> Species 0.000 description 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
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- GVJHHUAWPYXKBD-UHFFFAOYSA-N d-alpha-tocopherol Natural products OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 1
- 238000005238 degreasing Methods 0.000 description 1
- 238000002845 discoloration Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- BEJNERDRQOWKJM-UHFFFAOYSA-N kojic acid Chemical compound OCC1=CC(=O)C(O)=CO1 BEJNERDRQOWKJM-UHFFFAOYSA-N 0.000 description 1
- 229960004705 kojic acid Drugs 0.000 description 1
- WZNJWVWKTVETCG-UHFFFAOYSA-N kojic acid Natural products OC(=O)C(N)CN1C=CC(=O)C(O)=C1 WZNJWVWKTVETCG-UHFFFAOYSA-N 0.000 description 1
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- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 description 1
Abstract
The present invention provides a kind of facial cleanser and application thereof based on labradorite.The facial cleanser based on labradorite includes the facial cleanser matrix and elongate stone powder that mass ratio is 95-116:2-10, and the elongation stone powder is prepared by labradorite, and the average grain diameter for elongating stone powder is 75 μm -200 μm；Facial cleanser provided by the invention based on labradorite can remove sebum superfluous in skin pore, keep pore unobstructed, high to the cleannes of skin, and oil stain removing rate is up to 74% or more, can also play whitening or anti-acne and other effects after adding other compositions.
Description
Technical field
The invention belongs to cosmetic field, in particular to a kind of facial cleanser and application thereof based on labradorite.
Background technique
Facial cleanser is a kind of senior face washing agent, can be used in cleaning facial dirt, makeup removing, usually by oil phase thing, aqueous-phase material,
The product that the ingredients such as surfactant, moisturizer, nutritional agents are prepared can be divided into plain edition, frosted type and auxiliary effect type,
Wherein, frosted type facial cleanser is the particle that some smiles are added in facial cleanser, passes through the friction of the pre- skin surface of these particles
Effect, can make facial cleanser more effectively remove the spongiocyte of skin dirt and skin surface aging, existing frosted type
Facial cleanser usually plays frosted effect by the way that apricot shell powder, walnut shell powder, titanium dioxide powder and Cab-O-sil etc. are added in facial cleanser
Fruit, but the effect for removing grease is general, is badly in need of a kind of facial cleanser that degreasing effect is good now.
Summary of the invention
In order to solve the above technical problems, the present invention provides a kind of facial cleanser and application thereof based on labradorite, the base
Grease superfluous in skin pore can be removed in the facial cleanser of labradorite, keeps pore unobstructed, it is high to the cleannes of skin.
Specific technical solution of the present invention is as follows:
The present invention provides a kind of facial cleansers based on labradorite, and being somebody's turn to do the facial cleanser based on labradorite includes that mass ratio is
The facial cleanser matrix and elongation stone powder of 95-116:2-10, elongates stone powder and is prepared by labradorite, elongate the flat of stone powder
Equal partial size is 75 μm -200 μm.
Wherein, facial cleanser matrix includes the auxiliary material for preparing facial cleanser and/or the ingredient with whitening, anti-acne and other effects, beauty
Bai Chengfen includes but is not limited to arbutin, kojic acid and its derivative, and anti-acne ingredient includes but is not limited to red paeonia extract, cortex moutan
Extract and Herba Equiseti Hiemalis extract；Facial cleanser provided by the invention based on labradorite can remove skin superfluous in skin pore
Rouge keeps pore unobstructed, high to the cleannes of skin, and oil stain removing rate is up to 74% or more, can also play after adding other compositions
Whitening or anti-acne and other effects.
Further, labradorite powder includes that raw mountain flour, labradorite extract powder and the labradorite of elongating includes one of powder
Or it is a variety of, the raw mountain flour that elongates is directly to grind labradorite to be made, and the raw average grain diameter for elongating mountain flour is 80 μm, and labradorite extracts
Powder is will to grind to be made after labradorite boiling, and the average grain diameter of labradorite extract powder is 75 μm, and it is with poly- second that labradorite, which includes powder,
Labradorite extract powder is included and is made by olefine resin, and the average particle size distribution that labradorite includes powder is 120 μm, 150 μm and 200 μm each
Account for 1/3.
Further, labradorite extract powder preparation method the following steps are included:
(1) pre-process: taking average diameter is the labradorite pearl of 10cm-20cm, is cleaned；
(2) boiling: it will be placed in reaction kettle and mix by pretreated labradorite pearl, and add boiling to boil, wherein labradorite
Pearl and water volume ratio are 1:5-1:7, and adjustment pressure is 200KPa-300KPa, primary every 10min-20min stirring, are stirred every time
20min-40min, mixing speed 200prm-400prm are mixed, altogether boiling 4h-6h, be down to room temperature, take out labradorite pearl, crushed
It is 75 μm to get labradorite extract powder to average grain diameter.
Further, labradorite inclusion powder preparation method the following steps are included:
A. it takes polyvinyl resin to be placed in extruder, is heated to 220 DEG C -230 DEG C, keep the temperature 20-30min, melting is made
The polyvinyl resin of state；
B. labradorite extract powder is added in extruder again, the mass ratio of labradorite extract powder and polyvinyl resin is 1:1-
1:2 stirs 30min-40min under conditions of temperature is 220 DEG C -230 DEG C, mixing speed is 250prm-300prm, is made poly-
Vinyl mixture；
C. polyvinyl resin mixture made from step B is squeezed out diameter in the ratio of 1:1:1 is respectively 120 μm, 150 μm
It is rodlike with 200 μm, it is cut to length after being water-cooled it is 120 μm, 150 μm and 200 μm and includes powder to get labradorite.
It is respectively 120 μm, 150 μm and 200 μm that polyvinyl resin mixture is squeezed out diameter in the ratio of 1:1:1 by step C
Rodlike can pass through 3 extruders and squeeze out
Preferably, facial cleanser matrix include octanoic acid/Kui acid glyceryl ester, hexadecanol, acetylated lanolin, white oil, flash
Bar oil, polyethylene glycol (400) stearate, Tween 80, Macrogol 600, preservative, antioxidant, essence, deionized water, it is pungent
Acid/Kui acid glyceryl ester, hexadecanol, acetylated lanolin, white oil, jojoba oil, polyethylene glycol (400) stearate, tween
80, Macrogol 600, preservative, antioxidant, essence, deionized water quality ratio are 2-4:1-3:2-4:58-62:2-4:3-5:
3-5:4-6:0.05-0.15:0.05-0.15:0.9-1.7:19-21。
Further, elongation stone powder, which is made a living, elongates mountain flour.
Further, it is that the raw of 3:1 elongates mountain flour and labradorite extract powder that labradorite powder, which includes mass ratio,.
Further, elongating stone powder is that labradorite includes powder.
Further, facial cleanser preparation method the following steps are included:
S1: the hexadecanol of definite quality ratio, Tween 80, octanoic acid/Kui acid glyceryl ester are heated to 70 DEG C, in 200prm-
5min-10min is stirred under conditions of 300prm, and the first mixed liquor is made；
S2: the glycerol of definite quality ratio is heated to 60 DEG C, jojoba oil is added, under conditions of 500prm-600prm
15min-20min is stirred, the second mixed liquor is made；
S3: by the acetylated lanolin of definite quality ratio, polyethylene glycol (400) stearate, deionized water, polyethylene glycol
600 are heated to 70 DEG C, stir 6min-8min under conditions of 200prm-300prm, and third mixed liquor is made；
S4: the first mixed liquor, the second mixed liquor are added in third mixed liquor, stirred evenly, is cooled to 38 DEG C -40
DEG C, elongation stone powder, essence, preservative and the antioxidant of definite quality ratio is added, is sufficiently mixed uniformly to get facial cleanser.
Based on better the effect of playing labradorite in facial cleanser, the grain for elongating stone powder can be adjusted according to the actual situation
Diameter, in inventive concept of the invention.
Facial cleanser provided by the invention based on labradorite can remove sebum superfluous in skin pore, keep pore logical
Freely, high to the cleannes of skin, 74% or more is up to the oil stain removing rate of skin of face.
Specific embodiment
Embodiment 1
A kind of facial cleanser based on labradorite is present embodiments provided, being somebody's turn to do the facial cleanser based on labradorite includes that mass ratio is
95g facial cleanser matrix and 10g elongate stone powder, elongate stone powder and are prepared by labradorite, elongate the average grain diameter of stone powder
It is 80 μm；
Elongation stone powder, which is made a living, elongates mountain flour, and it is that labradorite is directly milled to made from 80 μm which, which elongates mountain flour,；
Facial cleanser matrix includes 2g octanoic acid/Kui acid glyceryl ester, 1g hexadecanol, 2g acetylated lanolin, 58g white oil, 2g
Jojoba oil, 3g polyethylene glycol (400) stearate, 3g Tween 80,4g Macrogol 600,0.05g preservative, 0.05g antioxygen
Agent, 0.9g essence, 19g deionized water；
Preservative in all embodiments of the invention is all made of preservative DL607, and antioxidant is all made of tocopherol, and essence is equal
Using lemon extract, a kind of above only performance of the invention, can also using other kinds of preservative, antioxidant and
Essence is not specifically limited herein.
Embodiment 2
A kind of facial cleanser based on labradorite is present embodiments provided, being somebody's turn to do the facial cleanser based on labradorite includes that 116g washes one's face
Milk matrix and 4g elongate stone powder, elongate stone powder and are prepared by labradorite；
Labradorite powder includes that mass ratio is the raw elongation mountain flour of 3g and 1g labradorite extract powder, and the raw mountain flour that elongates is will to elongate
Stone, which is directly ground, to be made, and the raw average grain diameter for elongating mountain flour is 80 μm, and labradorite extract powder is that system will be ground after labradorite boiling
, the average grain diameter of labradorite extract powder is 75 μm；
Facial cleanser matrix includes 4g octanoic acid/Kui acid glyceryl ester, 3g hexadecanol, 4g acetylated lanolin, 62g white oil, 4g
Jojoba oil, 5g polyethylene glycol (400) stearate, 5g Tween 80,6g Macrogol 600,0.15g preservative, 0.15g antioxygen
Agent, 1.7g essence, 21g deionized water.
Embodiment 3
A kind of facial cleanser based on labradorite is present embodiments provided, being somebody's turn to do the facial cleanser based on labradorite includes that mass ratio is
100g facial cleanser matrix and 3g elongate stone powder, elongate stone powder and are prepared by labradorite；
Elongating stone powder is that labradorite includes powder, and it is to be included labradorite extract powder with polyvinyl resin that labradorite, which includes powder,
It is made, the average particle size distribution that labradorite includes powder is 120 μm, 150 μm and 200 μm each 1g；
Facial cleanser matrix include 3g octanoic acid/Kui acid glyceryl ester, 2g hexadecanol, 2g acetylated lanolin, 58g white oil, 3 suddenly
Bar oil, 4g polyethylene glycol (400) stearate, 4g Tween 80,4g Macrogol 600,0.05g preservative, 0.05g antioxygen suddenly
Agent, 0.9g essence, 19g deionized water.
Embodiment 4
A kind of facial cleanser based on labradorite is present embodiments provided, being somebody's turn to do the facial cleanser based on labradorite includes that 116g washes one's face
Milk matrix and 4g elongate stone powder, elongate stone powder and are prepared by labradorite；
Labradorite powder includes that mass ratio is the raw elongation mountain flour of 3g and 1g labradorite extract powder, and the raw mountain flour that elongates is will to elongate
Stone, which is directly ground, to be made, and the raw average grain diameter for elongating mountain flour is 80 μm, and labradorite extract powder is that system will be ground after labradorite boiling
, the average grain diameter of labradorite extract powder is 75 μm；
Facial cleanser matrix includes 4g octanoic acid/Kui acid glyceryl ester, 3g hexadecanol, 4g acetylated lanolin, 62g white oil, 4g
Jojoba oil, 5g polyethylene glycol (400) stearate, 5g Tween 80,6g Macrogol 600,0.15g preservative, 0.15g antioxygen
Agent, 1.7g essence, 21g deionized water；
Wherein, labradorite extract powder preparation method the following steps are included:
(1) pre-process: taking average diameter is the labradorite pearl of 10cm, is cleaned；
(2) boiling: it will be placed in reaction kettle and mix by pretreated labradorite pearl, and add boiling to boil, wherein labradorite
Pearl and water volume ratio are 1:5, and adjustment pressure is 200KPa, primary every 10min stirring, stir 20min every time, mixing speed is
200prm, boiling 4h, is down to room temperature altogether, takes out labradorite pearl, and being crushed to average grain diameter is 75 μm to get labradorite extract powder；
Wherein, facial cleanser preparation method the following steps are included:
S1: the hexadecanol of definite quality ratio, Tween 80, octanoic acid/Kui acid glyceryl ester are heated to 70 DEG C, 200prm's
Under the conditions of stir 5min, be made the first mixed liquor；
S2: the glycerol of definite quality ratio is heated to 60 DEG C, jojoba oil is added, is stirred under conditions of 500prm
The second mixed liquor is made in 15min；
S3: by the acetylated lanolin of definite quality ratio, polyethylene glycol (400) stearate, deionized water, polyethylene glycol
600 are heated to 70 DEG C, stir 6min under conditions of 200prm, and third mixed liquor is made；
S4: the first mixed liquor, the second mixed liquor being added in third mixed liquor, stirred evenly, and are cooled to 38 DEG C, are added
Elongation stone powder, essence, preservative and the antioxidant of definite quality ratio, are sufficiently mixed uniformly to get facial cleanser.
Embodiment 5
A kind of facial cleanser based on labradorite is present embodiments provided, being somebody's turn to do the facial cleanser based on labradorite includes that 116g washes one's face
Milk matrix and 4g elongate stone powder, elongate stone powder and are prepared by labradorite；
Labradorite powder includes that mass ratio is the raw elongation mountain flour of 3g and 1g labradorite extract powder, and the raw mountain flour that elongates is will to elongate
Stone, which is directly ground, to be made, and the raw average grain diameter for elongating mountain flour is 80 μm, and labradorite extract powder is that system will be ground after labradorite boiling
, the average grain diameter of labradorite extract powder is 75 μm；
Facial cleanser matrix includes 4g octanoic acid/Kui acid glyceryl ester, 3g hexadecanol, 4g acetylated lanolin, 62g white oil, 4g
Jojoba oil, 5g polyethylene glycol (400) stearate, 5g Tween 80,6g Macrogol 600,0.15g preservative, 0.15g antioxygen
Agent, 1.7g essence, 21g deionized water；
Wherein, labradorite extract powder preparation method the following steps are included:
(1) pre-process: taking average diameter is the labradorite pearl of 15cm, is cleaned；
(2) boiling: it will be placed in reaction kettle and mix by pretreated labradorite pearl, and add boiling to boil, wherein labradorite
Pearl and water volume ratio are 1:6, and adjustment pressure is 250KPa, primary every 15min stirring, stir 30min every time, mixing speed is
300prm, boiling 5h, is down to room temperature altogether, takes out labradorite pearl, and being crushed to average grain diameter is 75 μm to get labradorite extract powder；
Wherein, facial cleanser preparation method the following steps are included:
S1: the hexadecanol of definite quality ratio, Tween 80, octanoic acid/Kui acid glyceryl ester are heated to 70 DEG C, 250prm's
Under the conditions of stir 8min, be made the first mixed liquor；
S2: the glycerol of definite quality ratio is heated to 60 DEG C, jojoba oil is added, is stirred under conditions of 550prm
The second mixed liquor is made in 18min；
S3: by the acetylated lanolin of definite quality ratio, polyethylene glycol (400) stearate, deionized water, polyethylene glycol
600 are heated to 70 DEG C, stir 7min under conditions of 250prm, and third mixed liquor is made；
S4: the first mixed liquor, the second mixed liquor being added in third mixed liquor, stirred evenly, and are cooled to 39 DEG C, are added
Elongation stone powder, essence, preservative and the antioxidant of definite quality ratio, are sufficiently mixed uniformly to get facial cleanser.
Embodiment 6
A kind of facial cleanser based on labradorite is present embodiments provided, being somebody's turn to do the facial cleanser based on labradorite includes that 100g washes one's face
Milk matrix and 3g elongate stone powder, elongate stone powder and are prepared by labradorite；
Elongating stone powder is that labradorite includes powder, and it is to be included labradorite extract powder with polyvinyl resin that labradorite, which includes powder,
It is made, the average particle size distribution that labradorite includes powder is 120 μm, 150 μm and 200 μm each 1g；
Facial cleanser matrix includes 3g octanoic acid/Kui acid glyceryl ester, 2g hexadecanol, 2g acetylated lanolin, 58g white oil, 3g
Jojoba oil, 4g polyethylene glycol (400) stearate, 4g Tween 80,4g Macrogol 600,0.05g preservative, 0.05g antioxygen
Agent, 0.9g essence, 19g deionized water；
Wherein, labradorite inclusion powder preparation method the following steps are included:
A. it takes polyvinyl resin to be placed in extruder, is heated to 230 DEG C, keep the temperature 30min, the poly- second of molten condition is made
Olefine resin；
B. labradorite extract powder is added in extruder again, the mass ratio of labradorite extract powder and polyvinyl resin is 1:2,
40min is stirred under conditions of temperature is 230 DEG C, mixing speed is 300prm, polyvinyl resin mixture is made；
C. polyvinyl resin mixture made from step B is squeezed out diameter in the ratio of 1:1:1 is respectively 120 μm, 150 μm
It is rodlike with 200 μm, it is cut to length after being water-cooled it is 120 μm, 150 μm and 200 μm and includes powder to get labradorite；
Wherein, facial cleanser preparation method the following steps are included:
S1: the hexadecanol of definite quality ratio, Tween 80, octanoic acid/Kui acid glyceryl ester are heated to 70 DEG C, 300prm's
Under the conditions of stir 10min, be made the first mixed liquor；
S2: the glycerol of definite quality ratio is heated to 60 DEG C, jojoba oil is added, is stirred under conditions of 600prm
The second mixed liquor is made in 20min；
S3: by the acetylated lanolin of definite quality ratio, polyethylene glycol (400) stearate, deionized water, polyethylene glycol
600 are heated to 70 DEG C, stir 8min under conditions of 300prm, and third mixed liquor is made；
S4: the first mixed liquor, the second mixed liquor being added in third mixed liquor, stirred evenly, and are cooled to 40 DEG C, are added
Elongation stone powder, essence, preservative and the antioxidant of definite quality ratio, are sufficiently mixed uniformly to get facial cleanser.
Embodiment 7
A kind of facial cleanser based on labradorite is present embodiments provided, being somebody's turn to do the facial cleanser based on labradorite includes that mass ratio is
The facial cleanser matrix and elongation stone powder of 100:3, elongates stone powder and is prepared by labradorite；
Elongating stone powder is that labradorite includes powder, and it is to be included labradorite extract powder with polyvinyl resin that labradorite, which includes powder,
It is made, the average particle size distribution that labradorite includes powder is 120 μm, 150 μm and 200 μm each 1g；
Facial cleanser matrix includes 3g octanoic acid/Kui acid glyceryl ester, 2g hexadecanol, 2g acetylated lanolin, 58g white oil, 3g
Jojoba oil, 4g polyethylene glycol (400) stearate, 4g Tween 80,4g Macrogol 600,0.05g preservative, 0.05g antioxygen
Agent, 0.9g essence, 19g deionized water；
Wherein, labradorite inclusion powder preparation method the following steps are included:
A. it takes polyvinyl resin to be placed in extruder, is heated to 225 DEG C, keep the temperature 25min, the poly- second of molten condition is made
Olefine resin；
B. labradorite extract powder is added in extruder again, the mass ratio of labradorite extract powder and polyvinyl resin is 1:
1.5,35min is stirred under conditions of temperature is 225 DEG C, mixing speed is 280prm, polyvinyl resin mixture is made；
C. polyvinyl resin mixture made from step B is squeezed out diameter in the ratio of 1:1:1 is respectively 120 μm, 150 μm
It is rodlike with 200 μm, it is cut to length after being water-cooled it is 120 μm, 150 μm and 200 μm and includes powder to get labradorite；
Wherein, facial cleanser preparation method the following steps are included:
S1: the hexadecanol of definite quality ratio, Tween 80, octanoic acid/Kui acid glyceryl ester are heated to 70 DEG C, 220prm's
Under the conditions of stir 6min, be made the first mixed liquor；
S2: the glycerol of definite quality ratio is heated to 60 DEG C, jojoba oil is added, is stirred under conditions of 520prm
The second mixed liquor is made in 16min；
S3: by the acetylated lanolin of definite quality ratio, polyethylene glycol (400) stearate, deionized water, polyethylene glycol
600 are heated to 70 DEG C, stir 7min under conditions of 230prm, and third mixed liquor is made；
S4: the first mixed liquor, the second mixed liquor being added in third mixed liquor, stirred evenly, and are cooled to 38 DEG C, are added
Elongation stone powder, essence, preservative and the antioxidant of definite quality ratio, are sufficiently mixed uniformly to get facial cleanser.
Embodiment 8
A kind of facial cleanser based on labradorite is present embodiments provided, being somebody's turn to do the facial cleanser based on labradorite includes that 116g washes one's face
Milk matrix and 4g elongate stone powder, elongate stone powder and are prepared by labradorite；
Labradorite powder includes that mass ratio is that 3g labradorite includes powder and 1g labradorite extract powder, labradorite extract powder be by
It grinds and is made after labradorite boiling, the average grain diameter of labradorite extract powder is 75 μm, and it is to use polyvinyl resin that labradorite, which includes powder,
Labradorite extract powder inclusion is made, the average particle size distribution that labradorite includes powder is 120 μm, 150 μm and 200 μm each 1g；
Facial cleanser matrix includes 4g octanoic acid/Kui acid glyceryl ester, 3g hexadecanol, 4g acetylated lanolin, 62g white oil, 4g
Jojoba oil, 5g polyethylene glycol (400) stearate, 5g Tween 80,6g Macrogol 600,0.15g preservative, 0.15g antioxygen
Agent, 1.7g essence, 20g deionized water and 1g arbutin；
Wherein, labradorite extract powder preparation method the following steps are included:
(1) pre-process: taking average diameter is the labradorite pearl of 15cm, is cleaned；
(2) boiling: it will be placed in reaction kettle and mix by pretreated labradorite pearl, and add boiling to boil, wherein labradorite
Pearl and water volume ratio are 1:6, and adjustment pressure is 250KPa, primary every 15min stirring, stir 30min every time, mixing speed is
300prm, boiling 5h, is down to room temperature altogether, takes out labradorite pearl, and being crushed to average grain diameter is 75 μm to get labradorite extract powder；
Wherein, labradorite inclusion powder preparation method the following steps are included:
A. it takes polyvinyl resin to be placed in extruder, is heated to 230 DEG C, keep the temperature 30min, the poly- second of molten condition is made
Olefine resin；
B. labradorite extract powder is added in extruder again, the mass ratio of labradorite extract powder and polyvinyl resin is 1:2,
40min is stirred under conditions of temperature is 230 DEG C, mixing speed is 300prm, polyvinyl resin mixture is made；
C. polyvinyl resin mixture made from step B is squeezed out diameter in the ratio of 1:1:1 is respectively 120 μm, 150 μm
It is rodlike with 200 μm, it is cut to length after being water-cooled it is 120 μm, 150 μm and 200 μm and includes powder to get labradorite；
Wherein, facial cleanser preparation method the following steps are included:
S1: the hexadecanol of definite quality ratio, Tween 80, octanoic acid/Kui acid glyceryl ester are heated to 70 DEG C, 250prm's
Under the conditions of stir 8min, be made the first mixed liquor；
S2: the glycerol of definite quality ratio is heated to 60 DEG C, jojoba oil is added, is stirred under conditions of 550prm
The second mixed liquor is made in 18min；
S3: by the acetylated lanolin of definite quality ratio, polyethylene glycol (400) stearate, deionized water, polyethylene glycol
600 are heated to 70 DEG C, stir 7min under conditions of 250prm, and third mixed liquor is made；
S4: the first mixed liquor, the second mixed liquor being added in third mixed liquor, stirred evenly, and are cooled to 39 DEG C, are added
The arbutin of definite quality ratio elongates stone powder, essence, preservative and antioxidant, is sufficiently mixed uniformly to get facial cleanser.
Embodiment 9
A kind of facial cleanser based on labradorite is present embodiments provided, being somebody's turn to do the facial cleanser based on labradorite includes that 116g washes one's face
Milk matrix and 4g elongate stone powder, elongate stone powder and are prepared by labradorite；
Labradorite powder includes that mass ratio is that 3g labradorite includes powder and 1g labradorite extract powder, labradorite extract powder be by
It grinds and is made after labradorite boiling, the average grain diameter of labradorite extract powder is 75 μm, and it is to use polyvinyl resin that labradorite, which includes powder,
Labradorite extract powder inclusion is made, the average particle size distribution that labradorite includes powder is 120 μm, 150 μm and 200 μm each 1g；
Facial cleanser matrix includes 4g octanoic acid/Kui acid glyceryl ester, 3g hexadecanol, 4g acetylated lanolin, 62g white oil, 4g
Jojoba oil, 5g polyethylene glycol (400) stearate, 5g Tween 80,6g Macrogol 600,0.15g preservative, 0.15g antioxygen
Agent, 1.7g essence, 20g deionized water and 1g Cortex Moutan extract；
Cortex Moutan extract can be made by conventional aqueous extraction step；The application is not specifically limited；
Wherein, labradorite extract powder preparation method the following steps are included:
(1) pre-process: taking average diameter is the labradorite pearl of 15cm, is cleaned；
(2) boiling: it will be placed in reaction kettle and mix by pretreated labradorite pearl, and add boiling to boil, wherein labradorite
Pearl and water volume ratio are 1:6, and adjustment pressure is 250KPa, primary every 15min stirring, stir 30min every time, mixing speed is
300prm, boiling 5h, is down to room temperature altogether, takes out labradorite pearl, and being crushed to average grain diameter is 75 μm to get labradorite extract powder；
Wherein, labradorite inclusion powder preparation method the following steps are included:
A. it takes polyvinyl resin to be placed in extruder, is heated to 230 DEG C, keep the temperature 30min, the poly- second of molten condition is made
Olefine resin；
B. labradorite extract powder is added in extruder again, the mass ratio of labradorite extract powder and polyvinyl resin is 1:2,
40min is stirred under conditions of temperature is 230 DEG C, mixing speed is 300prm, polyvinyl resin mixture is made；
C. polyvinyl resin mixture made from step B is squeezed out diameter in the ratio of 1:1:1 is respectively 120 μm, 150 μm
It is rodlike with 200 μm, it is cut to length after being water-cooled it is 120 μm, 150 μm and 200 μm and includes powder to get labradorite；
Wherein, facial cleanser preparation method the following steps are included:
S1: the hexadecanol of definite quality ratio, Tween 80, octanoic acid/Kui acid glyceryl ester are heated to 70 DEG C, 250prm's
Under the conditions of stir 8min, be made the first mixed liquor；
S2: the glycerol of definite quality ratio is heated to 60 DEG C, jojoba oil is added, is stirred under conditions of 550prm
The second mixed liquor is made in 18min；
S3: by the acetylated lanolin of definite quality ratio, polyethylene glycol (400) stearate, deionized water, polyethylene glycol
600 are heated to 70 DEG C, stir 7min under conditions of 250prm, and third mixed liquor is made；
S4: the first mixed liquor, the second mixed liquor being added in third mixed liquor, stirred evenly, and are cooled to 39 DEG C, are added
The arbutin of definite quality ratio elongates stone powder, essence, preservative and antioxidant, is sufficiently mixed uniformly to get facial cleanser.
Reference examples 1
A kind of facial cleanser is present embodiments provided, which includes the facial cleanser matrix and almond that mass ratio is 100:3
Shell powder；
Facial cleanser matrix includes 3g octanoic acid/Kui acid glyceryl ester, 2g hexadecanol, 2g acetylated lanolin, 58g white oil, 3g
Jojoba oil, 4g polyethylene glycol (400) stearate, 4g Tween 80,4g Macrogol 600,0.05g preservative, 0.05g antioxygen
Agent, 0.9g essence, 19g deionized water；
Wherein, facial cleanser preparation method the following steps are included:
S1: the hexadecanol of definite quality ratio, Tween 80, octanoic acid/Kui acid glyceryl ester are heated to 70 DEG C, 300prm's
Under the conditions of stir 10min, be made the first mixed liquor；
S2: the glycerol of definite quality ratio is heated to 60 DEG C, jojoba oil is added, is stirred under conditions of 600prm
The second mixed liquor is made in 20min；
S3: by the acetylated lanolin of definite quality ratio, polyethylene glycol (400) stearate, deionized water, polyethylene glycol
600 are heated to 70 DEG C, stir 8min under conditions of 300prm, and third mixed liquor is made；
S4: the first mixed liquor, the second mixed liquor being added in third mixed liquor, stirred evenly, and are cooled to 40 DEG C, are added
Apricot shell powder, essence, preservative and the antioxidant of definite quality ratio, are sufficiently mixed uniformly to get facial cleanser.
Reference examples 2
A kind of facial cleanser is present embodiments provided, which includes the facial cleanser matrix and walnut that mass ratio is 100:3
Shell powder；
Facial cleanser matrix includes 3g octanoic acid/Kui acid glyceryl ester, 2g hexadecanol, 2g acetylated lanolin, 58g white oil, 3g
Jojoba oil, 4g polyethylene glycol (400) stearate, 4g Tween 80,4g Macrogol 600,0.05g preservative, 0.05g antioxygen
Agent, 0.9g essence, 19g deionized water；
Wherein, facial cleanser preparation method the following steps are included:
S1: the hexadecanol of definite quality ratio, Tween 80, octanoic acid/Kui acid glyceryl ester are heated to 70 DEG C, 300prm's
Under the conditions of stir 10min, be made the first mixed liquor；
S2: the glycerol of definite quality ratio is heated to 60 DEG C, jojoba oil is added, is stirred under conditions of 600prm
The second mixed liquor is made in 20min；
S3: by the acetylated lanolin of definite quality ratio, polyethylene glycol (400) stearate, deionized water, polyethylene glycol
600 are heated to 70 DEG C, stir 8min under conditions of 300prm, and third mixed liquor is made；
S4: the first mixed liquor, the second mixed liquor being added in third mixed liquor, stirred evenly, and are cooled to 40 DEG C, are added
Walnut shell powder, essence, preservative and the antioxidant of definite quality ratio, are sufficiently mixed uniformly to get facial cleanser.
Reference examples 3
A kind of facial cleanser is present embodiments provided, which includes the facial cleanser matrix and dioxy that mass ratio is 100:3
Change titanium valve；
Facial cleanser matrix includes 3g octanoic acid/Kui acid glyceryl ester, 2g hexadecanol, 2g acetylated lanolin, 58g white oil, 3g
Jojoba oil, 4g polyethylene glycol (400) stearate, 4g Tween 80,4g Macrogol 600,0.05g preservative, 0.05g antioxygen
Agent, 0.9g essence, 19g deionized water；
Wherein, facial cleanser preparation method the following steps are included:
S1: the hexadecanol of definite quality ratio, Tween 80, octanoic acid/Kui acid glyceryl ester are heated to 70 DEG C, 300prm's
Under the conditions of stir 10min, be made the first mixed liquor；
S2: the glycerol of definite quality ratio is heated to 60 DEG C, jojoba oil is added, is stirred under conditions of 600prm
The second mixed liquor is made in 20min；
S3: by the acetylated lanolin of definite quality ratio, polyethylene glycol (400) stearate, deionized water, polyethylene glycol
600 are heated to 70 DEG C, stir 8min under conditions of 300prm, and third mixed liquor is made；
S4: the first mixed liquor, the second mixed liquor being added in third mixed liquor, stirred evenly, and are cooled to 40 DEG C, are added
Titanium dioxide powder, essence, preservative and the antioxidant of definite quality ratio, are sufficiently mixed uniformly to get facial cleanser.
Reference examples 4
A kind of facial cleanser is present embodiments provided, which includes the facial cleanser matrix and silica that mass ratio is 100:3
Powder；
Facial cleanser matrix includes 3g octanoic acid/Kui acid glyceryl ester, 2g hexadecanol, 2g acetylated lanolin, 58g white oil, 3g
Jojoba oil, 4g polyethylene glycol (400) stearate, 4g Tween 80,4g Macrogol 600,0.05g preservative, 0.05g antioxygen
Agent, 0.9g essence, 19g deionized water；
Wherein, facial cleanser preparation method the following steps are included:
S1: the hexadecanol of definite quality ratio, Tween 80, octanoic acid/Kui acid glyceryl ester are heated to 70 DEG C, 300prm's
Under the conditions of stir 10min, be made the first mixed liquor；
S2: the glycerol of definite quality ratio is heated to 60 DEG C, jojoba oil is added, is stirred under conditions of 600prm
The second mixed liquor is made in 20min；
S3: by the acetylated lanolin of definite quality ratio, polyethylene glycol (400) stearate, deionized water, polyethylene glycol
600 are heated to 70 DEG C, stir 8min under conditions of 300prm, and third mixed liquor is made；
S4: the first mixed liquor, the second mixed liquor being added in third mixed liquor, stirred evenly, and are cooled to 40 DEG C, are added
Cab-O-sil, essence, preservative and the antioxidant of definite quality ratio, are sufficiently mixed uniformly to get facial cleanser.
Reference examples 5
A kind of facial cleanser is present embodiments provided, which includes the facial cleanser matrix and poly- second that mass ratio is 100:3
Alkene abrasive particle；
Facial cleanser matrix includes 3g octanoic acid/Kui acid glyceryl ester, 2g hexadecanol, 2g acetylated lanolin, 58g white oil, 3g
Jojoba oil, 4g polyethylene glycol (400) stearate, 4g Tween 80,4g Macrogol 600,0.05g preservative, 0.05g antioxygen
Agent, 0.9g essence, 19g deionized water；
Wherein, facial cleanser preparation method the following steps are included:
S1: the hexadecanol of definite quality ratio, Tween 80, octanoic acid/Kui acid glyceryl ester are heated to 70 DEG C, 300prm's
Under the conditions of stir 10min, be made the first mixed liquor；
S2: the glycerol of definite quality ratio is heated to 60 DEG C, jojoba oil is added, is stirred under conditions of 600prm
The second mixed liquor is made in 20min；
S3: by the acetylated lanolin of definite quality ratio, polyethylene glycol (400) stearate, deionized water, polyethylene glycol
600 are heated to 70 DEG C, stir 8min under conditions of 300prm, and third mixed liquor is made；
S4: the first mixed liquor, the second mixed liquor being added in third mixed liquor, stirred evenly, and are cooled to 40 DEG C, are added
Polyethylene abrasive particle, essence, preservative and the antioxidant of definite quality ratio, are sufficiently mixed uniformly to get facial cleanser.
Reference examples 6
A kind of facial cleanser is present embodiments provided, which includes the facial cleanser matrix and polyphenyl that mass ratio is 100:3
Ethylene abrasive particle；
Facial cleanser matrix includes 3g octanoic acid/Kui acid glyceryl ester, 2g hexadecanol, 2g acetylated lanolin, 58g white oil, 3g
Jojoba oil, 4g polyethylene glycol (400) stearate, 4g Tween 80,4g Macrogol 600,0.05g preservative, 0.05g antioxygen
Agent, 0.9g essence, 19g deionized water；
Wherein, facial cleanser preparation method the following steps are included:
S1: the hexadecanol of definite quality ratio, Tween 80, octanoic acid/Kui acid glyceryl ester are heated to 70 DEG C, 300prm's
Under the conditions of stir 10min, be made the first mixed liquor；
S2: the glycerol of definite quality ratio is heated to 60 DEG C, jojoba oil is added, is stirred under conditions of 600prm
The second mixed liquor is made in 20min；
S3: by the acetylated lanolin of definite quality ratio, polyethylene glycol (400) stearate, deionized water, polyethylene glycol
600 are heated to 70 DEG C, stir 8min under conditions of 300prm, and third mixed liquor is made；
S4: the first mixed liquor, the second mixed liquor being added in third mixed liquor, stirred evenly, and are cooled to 40 DEG C, are added
Polystyrene abrasive particle, essence, preservative and the antioxidant of definite quality ratio, are sufficiently mixed uniformly to get facial cleanser.
Reference examples 7
A kind of facial cleanser is present embodiments provided, which includes the facial cleanser matrix and nylon that mass ratio is 100:3
Particle；
Facial cleanser matrix includes 3g octanoic acid/Kui acid glyceryl ester, 2g hexadecanol, 2g acetylated lanolin, 58g white oil, 3g
Jojoba oil, 4g polyethylene glycol (400) stearate, 4g Tween 80,4g Macrogol 600,0.05g preservative, 0.05g antioxygen
Agent, 0.9g essence, 19g deionized water；
Wherein, facial cleanser preparation method the following steps are included:
S1: the hexadecanol of definite quality ratio, Tween 80, octanoic acid/Kui acid glyceryl ester are heated to 70 DEG C, 300prm's
Under the conditions of stir 10min, be made the first mixed liquor；
S2: the glycerol of definite quality ratio is heated to 60 DEG C, jojoba oil is added, is stirred under conditions of 600prm
The second mixed liquor is made in 20min；
S3: by the acetylated lanolin of definite quality ratio, polyethylene glycol (400) stearate, deionized water, polyethylene glycol
600 are heated to 70 DEG C, stir 8min under conditions of 300prm, and third mixed liquor is made；
S4: the first mixed liquor, the second mixed liquor being added in third mixed liquor, stirred evenly, and are cooled to 40 DEG C, are added
Nylon particles, essence, preservative and the antioxidant of definite quality ratio, are sufficiently mixed uniformly to get facial cleanser.
1 facial cleanser of test example is heat-resisting, low temperature resistant test
Heat resistant test: respectively Example 4-9 and reference examples 1-7 each 50g of facial cleanser according to GB5296.3 regulation into
Row packaging, the temperature of regulating thermostatic incubator are 40 DEG C ± 1 DEG C, and the facial cleanser that packaging finishes is placed in constant incubator,
It takes out afterwards for 24 hours, the form and record of facial cleanser, heat-resisting to the results are shown in Table 1, low temperature resistant test: by refrigerator tune is observed after restoring to room temperature
- 8 DEG C ± 1 DEG C is saved, the facial cleanser that packaging finishes is placed in refrigerator, is taken out afterwards for 24 hours, restores to room temperature to observe facial cleanser
Form and record, it is cold-resistant to the results are shown in Table 1.
Heat-resisting, the cold-resistant effect of 1. each group facial cleanser of table
It infuses and refers to that no any lamination, slight lamination refer to the precipitation capacity of insoluble matter without lamination
Less than the 1/20 of insoluble matter total amount, moderate layering refer to the precipitation capacity of insoluble matter be located at insoluble matter total amount 1/20-1/10 it
Between, severe layering refers to that the precipitation capacity of insoluble matter is greater than the 1/10 of insoluble matter total amount.
As shown in Table 1, the facial cleanser of embodiment 4-9 provided by the present application under high temperature and cryogenic conditions without it is coarse, point
The case where layer and discoloration, heat-resisting and cold tolerance is good, and reference examples 1-7 has different degrees of layering or coarse phenomenon, it was demonstrated that
Facial cleanser provided by the present application is more stable, when replacing elongation stone powder of the invention with apricot shell powder, walnut shell powder etc.,
The stability of facial cleanser can be reduced.
The test of 2 oil stain removing rate of test example
It is measured using oil stain removing rate of the universally acknowledged SEBUMETER method to facial cleanser, the specific method is as follows: will
84 volunteers are divided into 14 groups, and every group of 6 volunteers, men and women is fifty-fifty, in the forehead of volunteer, nose two sides, cheek and chin four
It is 2cm that a size is drawn at a position respectively2Fixed area as test zone, with the special delustring adhesive tape with a thickness of 0.1mm
Absorb volunteer's nose two sides skin on grease, every group of volunteer use respectively embodiment 4-9, reference examples 1-7 facial cleanser and
Paris L'Oreal frosted facial washing milk is washed one's face with identical dosage and method, wherein Paris L'Oreal frosted that man uses is washed one's face
The goods number of milk is 28591881172, and the goods number for Paris L'Oreal frosted facial washing milk that Ms uses is
28760938018, in the same way measure four forehead of volunteer, nose two sides, cheek and chin site tests regions
Fat content calculates the oil stain removing rate of each group facial cleanser, and test result is shown in Table 2, and every group of facial cleanser, which passes through 6 volunteers, to be done
6 parallel tests, results are averaged.(skin oil and fat contains oil stain removing rate %=after skin oil and fat content-face cleaning before face cleaning
Amount) skin oil and fat content × 100% before/face cleaning.
2. facial cleanser oil stain removing rate measurement result of table
As shown in Table 2, the facial cleanser that 4-9 of the embodiment of the present invention is provided ground significant to the oil stain removing rate of human facial skin is high
In reference examples 1-7 and Paris L'Oreal facial cleanser, it was demonstrated that facial cleanser provided by the invention has good cleaning capacity.
To sum up, only the preferred embodiments of the invention, is not limited the scope of protection of the present invention with this, all according to the invention patent
Equivalent changes and modifications made by range and description are all within the scope of the invention patent covers.
Claims (10)
1. a kind of facial cleanser based on labradorite, which is characterized in that the facial cleanser based on labradorite includes that mass ratio is 95-
The facial cleanser matrix and elongation stone powder, the elongation stone powder of 116:2-10 is prepared by labradorite, the elongation mountain flour
The average grain diameter at end is 75 μm -200 μm.
2. as described in claim 1 based on the facial cleanser of labradorite, which is characterized in that the labradorite powder includes raw elongates
One of mountain flour, labradorite extract powder and labradorite inclusion powder are a variety of, and the raw mountain flour that elongates is directly to grind labradorite
It grinds, the raw average grain diameter for elongating mountain flour is 80 μm, and the labradorite extract powder is that system will be ground after labradorite boiling
, the average grain diameter of the labradorite extract powder is 75 μm, and the labradorite inclusion powder is to be mentioned labradorite with polyvinyl resin
Powder inclusion is taken to be made, the average particle size distribution of the labradorite inclusion powder is 120 μm, 150 μm and 200 μm and respectively accounts for 1/3.
3. as claimed in claim 2 based on the facial cleanser of labradorite, which is characterized in that the preparation side of the labradorite extract powder
Method the following steps are included:
(1) pre-process: taking average diameter is the labradorite pearl of 10cm-20cm, is cleaned；
(2) boiling: will be placed in reaction kettle and mix by pretreated labradorite pearl, boiling is added to boil, wherein labradorite pearl with
Water volume ratio is 1:5-1:7, and adjustment pressure is 200KPa-300KPa, primary every 10min-20min stirring, is stirred every time
20min-40min, mixing speed 200prm-400prm, boiling 4h-6h, is down to room temperature altogether, takes out labradorite pearl, is crushed to
Average grain diameter is 75 μm to get labradorite extract powder.
4. as claimed in claim 2 based on the facial cleanser of labradorite, which is characterized in that the preparation side of the labradorite inclusion powder
Method the following steps are included:
A. it takes polyvinyl resin to be placed in extruder, is heated to 220 DEG C -230 DEG C, keep the temperature 20-30min, molten condition is made
Polyvinyl resin；
B. labradorite extract powder is added in extruder again, the mass ratio of the labradorite extract powder and polyvinyl resin is 1:1-
1:2 stirs 30min-40min under conditions of temperature is 220 DEG C -230 DEG C, mixing speed is 250prm-300prm, is made poly-
Vinyl mixture；
C. by polyvinyl resin mixture made from step B in 1:1:1 ratio squeeze out diameter be respectively 120 μm, 150 μm and
200 μm rodlike, is cut to length and is 120 μm, 150 μm and 200 μm and include powder to get labradorite after being water-cooled.
5. as described in claim 1 based on the facial cleanser of labradorite, which is characterized in that the facial cleanser matrix include octanoic acid/
Kui acid glyceryl ester, hexadecanol, acetylated lanolin, white oil, jojoba oil, polyethylene glycol (400) stearate, Tween 80,
Macrogol 600, preservative, antioxidant, essence, deionized water, the octanoic acid/Kui acid glyceryl ester, hexadecanol, acetylation sheep
Hair alcohol, white oil, jojoba oil, polyethylene glycol (400) stearate, Tween 80, Macrogol 600, preservative, antioxidant, perfume (or spice)
Smart, deionized water mass ratio is 2-4:1-3:2-4:58-62:2-4:3-5:3-5:4-6:0.05-0.15:0.05-0.15:
0.9-1.7:19-21。
6. as described in claim 1 based on the facial cleanser of labradorite, which is characterized in that the elongation stone powder is made a living labradorite
Powder.
7. as described in claim 1 based on the facial cleanser of labradorite, which is characterized in that the labradorite powder includes mass ratio
Raw for 3:1 elongates mountain flour and labradorite extract powder.
8. as described in claim 1 based on the facial cleanser of labradorite, which is characterized in that the elongation stone powder is labradorite packet
Close powder.
9. as claimed in claim 5 based on the facial cleanser of labradorite, which is characterized in that the preparation method of the facial cleanser includes
Following steps:
S1: the hexadecanol of definite quality ratio, Tween 80, octanoic acid/Kui acid glyceryl ester are heated to 70 DEG C, in 200prm-
5min-10min is stirred under conditions of 300prm, and the first mixed liquor is made；
S2: the glycerol of definite quality ratio is heated to 60 DEG C, jojoba oil is added, is stirred under conditions of 500prm-600prm
The second mixed liquor is made in 15min-20min；
S3: by the acetylated lanolin of definite quality ratio, polyethylene glycol (400) stearate, deionized water, Macrogol 600
70 DEG C are heated to, stirs 6min-8min under conditions of 200prm-300prm, third mixed liquor is made；
S4: the first mixed liquor, the second mixed liquor are added in third mixed liquor, stirred evenly, 38 DEG C -40 DEG C is cooled to, adds
Elongation stone powder, essence, preservative and the antioxidant for entering definite quality ratio, are sufficiently mixed uniformly to get facial cleanser.
10. of any of claims 1 or 2 have grease superfluous in removal skin pore in preparation based on the facial cleanser of labradorite
Application in the cosmetics of effect.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910214166.6A CN109771309A (en) | 2019-03-20 | 2019-03-20 | A kind of facial cleanser and application thereof based on labradorite |
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| CN201910214166.6A CN109771309A (en) | 2019-03-20 | 2019-03-20 | A kind of facial cleanser and application thereof based on labradorite |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103565654A (en) * | 2013-10-15 | 2014-02-12 | 昆山威胜干燥剂研发中心有限公司 | Montmorillonite facial cleanser |
| US20170079891A1 (en) * | 2013-12-23 | 2017-03-23 | Imerys Minerals Limited | Cleansing compositions |
| CN108498354A (en) * | 2018-05-23 | 2018-09-07 | 佛山市汇汾化妆品科技有限公司 | A kind of sepiolite absorption facial cleanser and preparation method thereof |
| CN109199888A (en) * | 2018-11-15 | 2019-01-15 | 七道水（厦门）环保科技有限公司 | A kind of novel U.S. face and the water of makeup removing function and preparation method thereof |
-
2019
- 2019-03-20 CN CN201910214166.6A patent/CN109771309A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103565654A (en) * | 2013-10-15 | 2014-02-12 | 昆山威胜干燥剂研发中心有限公司 | Montmorillonite facial cleanser |
| US20170079891A1 (en) * | 2013-12-23 | 2017-03-23 | Imerys Minerals Limited | Cleansing compositions |
| CN108498354A (en) * | 2018-05-23 | 2018-09-07 | 佛山市汇汾化妆品科技有限公司 | A kind of sepiolite absorption facial cleanser and preparation method thereof |
| CN109199888A (en) * | 2018-11-15 | 2019-01-15 | 七道水（厦门）环保科技有限公司 | A kind of novel U.S. face and the water of makeup removing function and preparation method thereof |
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Application publication date: 20190521 |