CN1158991C - Natural rectorite mud face mask and its preparing method - Google Patents
Natural rectorite mud face mask and its preparing method Download PDFInfo
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- CN1158991C CN1158991C CNB021387192A CN02138719A CN1158991C CN 1158991 C CN1158991 C CN 1158991C CN B021387192 A CNB021387192 A CN B021387192A CN 02138719 A CN02138719 A CN 02138719A CN 1158991 C CN1158991 C CN 1158991C
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- rectorite
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Abstract
The present invention relates to a natural rectorite mud masque and a preparation method thereof, which belongs to the field of beautification and skin care. The natural rectorite mud masque is prepared by sterilizing the purified natural ore concentrate of calcium-based rectorite, adding fine zinc oxide, sorbitol, glycerol, span-60, deionized water and essence and proportionally mixing and stirring the mixture. The mud masque has an easy preparation method and low cost; the mud masque has the characteristics of fine and smooth texture, no toxic or side effect, etc., has the functions of stimulating blood circulation to end stasis, improving skin elasticity, delaying senescence and regulating the metabolism of human bodies, and also possesses the functions of wrinkle resistance, whitening, inflammation alleviation, sterilization and ultraviolet radiation resistance, and the mud masque is applicable to people of all ages and different skin qualities, particularly to people with hypersensitive skin.
Description
Technical field
The present invention relates to a kind of natural accumulation supporting stone mud facial film and compound method thereof, belong to the cosmetics and skincare product field.
Background technology
Returning Piao on the beauty industry both at home and abroad returns very, it is the effect that the cosmetics and skincare product of primary raw material reaches beauty treatment and nourishes rough skin that attention is sought with the natural materials, some adverse consequencess of avoiding the pure chemistry material that skin is caused, natural resources such as Sargassum mud, deep-sea mud, mineral mud have become the important source material of various facial films.Before the present invention, the various mud facial films that have Israel and Jordan to utilize Dead Sea mud to make abroad are in great demand all over the world; The useful volcanic rock mineral in domestic Hainan Province and Heilongjiang Province, the useful green stone mud in Beijing is primary raw material, is mixed with products such as mineral mud facial film and beautifying skincare slime paste., Lu Mingxia application number favourable as city road, nineteen ninety-five Harbin City, Heilongjiang Province is " pack cream made of volcano cold spring mineral mud " patent of 95105278.0; Haikou City, Hainan Province Wang Yi unit application number in 1998 is " a kind of volcanic rock mineral mud facial film " patent of 98123922.6; The real natural cosmetics company limited application number in east, Heilongjiang Province in 1999 is " volcano and spring mineral mask " patent of 99112682.3.The sludge essential mineral composition of above-mentioned patent mostly is clay minerals such as hydromica, bentonite, Kaolin, chlorite, calcite, dolomite, quartz, Anhydrite, and its weak point is that fineness, caking property, film property and the slip of above-mentioned sludge are all not as good as the rectorite clay.
It is the abundant pure natural mineral of content of mineral substances on the earth that the present invention selects the rectorite of natural output for use, finds first and called after " Rectorite " by E.W.Rector that transliteration was a rectorite in 1891.Nineteen fifty, S.Caillere etc. have reported a kind of new clay mineral of French Allevard, and called after " Allevardite " is translated into rectorite, and the two is real to be a kind of mineral.Rectorite becomes the ore deposit in the geochronic Permian System, apart from modern existing 2.7 hundred million years, is commonly called as two folded mud.The now existing bigger rectorite industrial mineral deposit of reserves is exploited in China, but still find no the rectorite mineral deposit that commercial mining is worth abroad, so always it as a kind of rare rare material, do not see of the application of domestic and international useful rectorite clay so far as the health and beauty aspect yet.
Summary of the invention
The object of the present invention is to provide a kind of natural accumulation supporting stone mud facial film and compound method thereof, a kind of skin protection mud facial film new varieties that are primary raw material with natural calcio rectorite concentrate are provided, and the compound method that a kind of production technology is simple, cost is low is provided.
The present invention in order to achieve the above object, a kind of natural accumulation supporting stone mud facial film is provided, the composition that it is characterized in that compositions is by mass percentage: rectorite powder 20～50, meticulous zinc oxide 1～2, sorbitol 12～20, glycerol 15～22, this dish-601～2, deionized water 20～35, essence 0.01～0.02.
The natural calcio rectorite of the present invention is silver gray, and silk oil gloss is arranged, and water-swellable is dissociated into cement paste, hardness＜1; Under polarizing microscope, observe, be colourless or faint yellow fibrous, needle-like; Under ultramicroscope, observe, be irregular flakey, lath-shaped and enveloped band shape; Its main chemical compositions is by mass percentage: SiO
240～46, TiO
21～3, Al
2O
330～36, FeO
30.5～1.5, CaO 2.5～4.5, MgO 0.1～0.5, Na
2O 1～1.5, K
2O 0.5～1.5, and S 0.5～0.7, and surplus is loss on ignition and trace element.The trace element that contained human body skin is required is as tens kinds of selenium (Se), cobalt (Co), strontium (Sr), lanthanums (La) etc.; Limiting the quantity of that hazardous trace elements hydrargyrum (Hg), plumbous (Pb), arsenic (As) require in the State Standard of the People's Republic of China UDC.58:613.49 hygienic standards for cosmetics GB791687 sees Table 1.
Noxious substance content (10 in table 1 hygienic standards for cosmetics and the rectorite powder
-6)
| Noxious substance | Limit the quantity of in the cosmetic standard | Content in the rectorite powder |
| Hydrargyrum | 1 | 0.28-0.31 |
| Plumbous | 40 | 7.2-7.8 |
| Arsenic | 10 | 0.53-0.59 |
The natural calcio rectorite of the present invention mineral have some characteristic of Muscovitum and montmorillonite mineral concurrently, electronegative between montmorillonite layer, be adsorbed with aquation cationes such as calcium, magnesium, potassium, sodium, wherein based on calcium ion, account for more than 50% of cation exchange total amount, so be called the calcio rectorite.In water, can be distributed to below the 1 μ m, the general character that not only has other clay minerals, as dispersibility, dilatancy, thixotropy, suspension, caking property, plasticity, adsorptivity and cation exchange etc., its dispersibility, caking property, film property and slip are better than other clay minerals greatly, but also have good performances such as anti-ultraviolet.
In the production method of natural accumulation supporting stone mud facial film of the present invention, at first be the preparation of calcio rectorite concentrate: adopt the wet method gravity treatment to separate, the rectorite raw ore is purified to the concentrate that contains rectorite 70%～80%, filter pressing makes water content≤35%, under 105～110 ℃ of temperature, be dried to moisture content≤10% again, with disintegrating machine the bulk filter cake is crushed to granularity＜5mm, levigate with Raymond machine to＜74 μ m, be calcio rectorite fine ore; The reuse ultra-fine grinding mill is calcio rectorite concentrate micropowder with its levigate extremely＜5 μ m, packages spare.Remaining raw material is all commercially available to be got.
The compound method of natural accumulation supporting stone mud facial film of the present invention is characterized in that the step of preparing is:
(1) prepares the rectorite powder earlier: adopt the wet method gravity treatment to separate, the rectorite raw ore is purified to the concentrate that contains rectorite 70%～80%, filter pressing makes water content≤35%, under 105～110 ℃ of temperature, be dried to moisture content≤10% again, with disintegrating machine the bulk filter cake is crushed to granularity＜5mm, levigate with Raymond machine to＜74 μ m, be calcio rectorite fine ore; The reuse ultra-fine grinding mill is levigate to＜5 μ m with it, is ultra-fine calcio rectorite powder;
(2) with ultra-fine calcio rectorite powder sterilization 30～60 minutes under 110～120 ℃ of temperature;
(3) by mass percentage 20～35 deionized water is joined in the blender, add 12～20 sorbitol, 15～22 glycerol, 1～2 this dish-60 and 0.01～0.02 essence again, stirred 2～8 minutes, add 1～2 meticulous zinc oxide and 20～50 rectorite powder of sterilization more respectively, restir 20-30 minute, natural accumulation supporting stone mud facial film.
The present invention has following outstanding advantage:
1. the raw material of the present invention's employing is based on natural calcio rectorite concentrate, and production cost is low, and production method is simple.
2. the granularity after the calcio rectorite concentrate of the present invention's employing disperses in water less than 1 μ m (other clay minerals are then greater than 3 μ m), does not have oarse-grained hard mineral, as quartz, Anhydrite etc. more than 90%.
3. the present invention adopts the mud facial film exquisite quality, smooth of calcio rectorite concentrate preparation, screening characteristics is good, good film-forming property, excellent adsorption, moisture retention are good, PH6-7, Acidity of Aikalinity are moderate, have activating blood circulation to dissipate blood stasis, increase skin elasticity, delaying decrepitude of skin and the metabolic effect of conditioning human body, crease-resistant in addition, whiten, the function of antiinflammatory, sterilization and anti-ultraviolet.
4. calcio rectorite provided by the invention is a pure natural substance, and is without any side effects to the skin nonirritant, and any age of mud facial film of preparation, the crowd of skin matter can use, and the people who especially is fit to allergic skin uses.
The specific embodiment
Embodiment 1: produce a collection of natural accumulation supporting stone mud facial film with calcio rectorite fine ore.The calcio rectorite concentrate of at first purifying, making rectorite content is 73.3%, the Montmorillonitum interlayer cation accounts for 70.8% of cation exchange total amount based on calcium ion in the mineral structure.
Get 50kg calcio rectorite fine ore sterilization 45 minutes under 115 ± 5 ℃ of temperature, be cooled to room temperature.The 22.48kg deionized water is joined in the blender, add 15kg sorbitol, 16kg glycerol, 1kg Si dish-60 and 0.02kg essence respectively, stirred 5 minutes, add meticulous oxide powder and zinc of 1.5kg and the 44kg rectorite fine ore of sterilization more respectively, continue to stir 30 minutes, promptly get natural accumulation supporting stone mud facial film, emit bottling.
Embodiment 2: produce a collection of natural accumulation supporting stone mud facial film with calcio rectorite concentrate micropowder.The calcio rectorite concentrate of at first purifying, making rectorite content is 76.7%, the Montmorillonitum interlayer cation accounts for 71.3% of cation exchange total amount based on calcium ion in the mineral structure.
Get 40kg calcio rectorite concentrate micropowder sterilization 50 minutes under 115 ± 5 ℃ of temperature, be cooled to room temperature.The 30.19kg deionized water is joined in the blender, add 15.5kg sorbitol, 16.5kg glycerol, 1.2kg Si dish-60 and 0.01kg essence respectively, stirred 5 minutes, add meticulous oxide powder and zinc of 1.6kg and the 35kg concentrate micropowder of sterilization calcio rectorite more respectively, continue to stir 25 minutes, promptly get natural accumulation supporting stone mud facial film, emit bottling.
Production method of the present invention is simple, and cost is low.The mud facial film has exquisite quality, smooth, screening characteristics is good, good film-forming property, excellent adsorption, moisture retention is good, Acidity of Aikalinity is moderate, characteristics such as without any side effects have activating blood circulation to dissipate blood stasis, increase skin elasticity, delaying decrepitude of skin and the metabolic effect of conditioning human body, crease-resistant in addition, whiten, the function of antiinflammatory, sterilization and anti-ultraviolet, the crowd who is suitable for any age, skin matter uses, and the people who is particularly suitable for allergic skin uses.
Claims (2)
1. a natural accumulation supporting stone mud facial film is characterized in that the compositions composition by mass percent is: rectorite powder 20～50, meticulous zinc oxide 1～2, sorbitol 12～20, glycerol 15～22, this dish-601～2, deionized water 20～35, essence 0.01～0.02.
2. the compound method of a natural accumulation supporting stone mud facial film is characterized in that the step of preparing is:
(1) prepares the rectorite powder earlier: adopt the wet method gravity treatment to separate, the rectorite raw ore is purified to the concentrate that contains rectorite 70%～80%, filter pressing makes water content≤35%, under 105～110 ℃ of temperature, be dried to moisture content≤10% again, with disintegrating machine the bulk filter cake is crushed to granularity＜5mm, levigate with Raymond machine to＜74 μ m, be calcio rectorite fine ore; The reuse ultra-fine grinding mill is levigate to＜5 μ m with it, is ultra-fine calcio rectorite powder;
(2) with ultra-fine calcio rectorite powder sterilization 30～60 minutes under 110～120 ℃ of temperature;
(3) by mass percentage 20～35 deionized water is joined in the blender, add 12～20 sorbitol, 15～22 glycerol, 1～2 this dish-60 and 0.01～0.02 essence again, stirred 2～8 minutes, add 1～2 meticulous zinc oxide and 20～50 rectorite powder of sterilization more respectively, restir 20-30 minute, natural accumulation supporting stone mud facial film.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB021387192A CN1158991C (en) | 2002-06-27 | 2002-06-27 | Natural rectorite mud face mask and its preparing method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB021387192A CN1158991C (en) | 2002-06-27 | 2002-06-27 | Natural rectorite mud face mask and its preparing method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1391885A CN1391885A (en) | 2003-01-22 |
| CN1158991C true CN1158991C (en) | 2004-07-28 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB021387192A Expired - Fee Related CN1158991C (en) | 2002-06-27 | 2002-06-27 | Natural rectorite mud face mask and its preparing method |
Country Status (1)
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|---|---|
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Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100377700C (en) * | 2006-03-07 | 2008-04-02 | 许盛英 | Embossed-rod health-cave bathing-mud powder |
| CN101199469B (en) * | 2006-12-12 | 2011-04-13 | 广东海洋大学 | Process for preparing lava pearl beauty mask |
| CN107951732B (en) * | 2017-12-26 | 2020-10-30 | 湖南御家化妆品制造有限公司 | Rectorite tearing slurry mask |
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2002
- 2002-06-27 CN CNB021387192A patent/CN1158991C/en not_active Expired - Fee Related
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| Publication number | Publication date |
|---|---|
| CN1391885A (en) | 2003-01-22 |
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