KR100368914B1 - Method for preparing multi-function bath soap - Google Patents

Method for preparing multi-function bath soap Download PDF

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KR100368914B1
KR100368914B1 KR10-2000-0054526A KR20000054526A KR100368914B1 KR 100368914 B1 KR100368914 B1 KR 100368914B1 KR 20000054526 A KR20000054526 A KR 20000054526A KR 100368914 B1 KR100368914 B1 KR 100368914B1
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raw material
mica
material powder
sodium carbonate
powder
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KR20020021765A (en
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김정자
정종인
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정종인
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/87Application Devices; Containers; Packaging

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Birds (AREA)
  • Inorganic Chemistry (AREA)
  • Epidemiology (AREA)
  • Chemical & Material Sciences (AREA)
  • Dermatology (AREA)
  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)
  • Cosmetics (AREA)

Abstract

각각 수비공정을 거치면서 인체에 해로운 철등의 중금속을 걸러내고, 분말로한다음 건조한 규석(차돌)30-40%, 운모 40-50%, 옥 10-20%, 게르마늄10-15%로 혼합하여, 원료물질파우다를 제조하고, 이 원료물질파우다 70-80%와 무수탄산나트륨20-30% 혼합, 300-650℃에서 연수물에 용해시킨 후 액상화한다.During the defensive process, the heavy metals such as iron that are harmful to the human body are filtered out, powdered, and then mixed with dry silica (calcite) 30-40%, mica 40-50%, jade 10-20%, and germanium 10-15%. A raw material powder is prepared, and 70-80% of this raw material powder and 20-30% of anhydrous sodium carbonate are mixed, dissolved in soft water at 300-650 ° C, and then liquefied.

상기 액상화물6ℓ에, 상기 원료물질파우다 55-65%, 무수탄산나트륨 25-30%,야자유지방산 5-7%, 키토산 3-4%, 무수피로인산나트륨 1-2%, 향료1-2% 혼합하여 반죽을 한 후 하트형 금형기에 부어 -5℃내지 -30℃로 급냉한 후 자연건조상태로 5-15시간 숙성하여 가공한 것으로, 일정형태의 고체 덩어리나 파우다로 만들어 입욕시 일정량을 넣어 사용할 경우 피부미용등에 탁월한 효과를 나타낸다.To 6 liters of the liquefied product, 55-65% of the raw material powder, 25-30% of anhydrous sodium carbonate, 5-7% of palm oil fatty acid, 3-4% of chitosan, 1-2% of anhydrous pyrophosphate, flavor 1-2% After kneading, it is poured into a heart mold and quenched at -5 ℃ to -30 ℃ and then aged for 5-15 hours in a natural dry state. It shows an excellent effect on skin beauty.

Description

다기능 목욕용재의 제조방법{METHOD FOR PREPARING MULTI-FUNCTION BATH SOAP}Manufacturing method of multifunctional bath material {METHOD FOR PREPARING MULTI-FUNCTION BATH SOAP}

본 발명은 원적외선 방사 목욕용 제품의 제조에 관한 것이며, 보다 상세하게는 운모,규석,게르마늄,옥.키토산을 일정량 혼합하여 다량의 음이온과 원적외선을 방출할 뿐만 아니라 탈취, 항균 , 중금속 흡착기능이 우수한 다기능 목욕용재를 제조하는 방법에 관한 것이다.The present invention relates to the manufacture of products for far-infrared radiation bath, and more specifically, by mixing a certain amount of mica, quartz, germanium, ox chitosan to release a large amount of anions and far infrared rays, as well as deodorizing, antibacterial, heavy metal adsorption It relates to a method for producing a bath material.

오늘날 목욕용재는 거의 계면활성제를 사용하여 제조하기 때문에 하천 등의 환경적 피해가 적지 않았다.Today, bathing materials are manufactured using almost no surfactants, so there is little environmental damage such as rivers.

이러한 환경적 피해를 줄이기 위해 근래에 인삼 등의 식물성원료, 맥반석 등의 광물성원료등을 이용하여 환경친화적인 목욕용재를 만들기 위해 부단히 노력하고 있으나 역시 근본적인 문제를 해결할 수 없었다.In order to reduce such environmental damage, we have made great efforts to make environmentally friendly bath materials using vegetable raw materials such as ginseng and mineral raw materials such as elvan, but could not solve the fundamental problems.

한국공개특허 제99-9259호(1999.2.05)에서는 견운모를 파쇄하여 정제하고, 그 정제된 원료를 황산용액과 섞어 용기내에서 가열,교반하여 증류수를 추출하는 공정 등을 걸쳐 미네랄원액를 제조하는 방법이 있으나, 황산용액을 사용하여 화학적으로 견운모를 추출 하기 때문에 환경친화적인 제품을 만들 수 없는 결점이 있었다.In Korean Patent Publication No. 99-9259 (1999.2.05), a method of preparing a mineral stock solution is performed by crushing and refining the sorghum, and mixing the purified raw material with sulfuric acid solution and heating and stirring it in a container to extract distilled water. However, there was a drawback that the environment-friendly product could not be made because chemically extracted biotite using sulfuric acid solution.

한국공개특허 제97-033047(1998.03.26)에서도 운모를 파쇄, 분쇄한 다음 부유 선별기에서 운모정광을 부유, 회수, 광액의 수소이온농도를 조절하기 위해 황산을 첨가하는 방법이 있으나, 이 방법 역시 황산을 이용하여 추출된 운모로 건강분야,정밀분야 등에 사용하기 때문에 환경적으로 원하는 제품을 만들 수 없었다.In Korean Patent Publication No. 97-033047 (1998.03.26), there is also a method of crushing and crushing mica, and then adding sulfuric acid to float, recover, and control the hydrogen ion concentration of the mineral liquid in the flotation sorter. Mica extracted with sulfuric acid was used for health, precision, etc. and thus could not produce environmentally desired products.

이하 같은 목적을 달성하는 본 발명의 방법은, 각각 수비공정을 거치면서 인체에 해로운 철등의 중금속을 걸러내고, 분말로 한다음 건조한 규석(차돌)30-40%,운모 40-50%, 옥 10-20%, 게르마늄10-15%로 혼합하여, 원료물질 파우다를 제조하고, 이 원료물질파우다 70-80%와 무수탄산나트륨 20-30% 혼합, 300-650℃에서 연수물에 용해시킨 후 액상화한다.The method of the present invention to achieve the following objects, respectively, through the defensive process to filter out heavy metals, such as iron harmful to the human body, and then to powder, and then to dry silica (marble) 30-40%, mica 40-50%, jade 10 -20% mixed with germanium 10-15% to prepare a raw material powder, 70-80% of this raw material powder and 20-30% of anhydrous sodium carbonate are dissolved in soft water at 300-650 ° C, and then liquefied. .

상기 액상화물6ℓ에, 상기 원료물질파우다 55-65%, 무수탄산나트륨 25-30%,야자유지방산 5-7%, 키토산 3-4%, 무수피로인산나트륨 1-2%, 향료1-2% 혼합하여 반죽을 한 후 하트형 금형기에 부어 -5℃내지 -30℃로 급냉한 후 자연건조상태로 5-15시간 숙성하여, 소비자의 취향에 따라 일정 형태의 고체 덩어리나 파우다로 가공한다.바람직한 급냉온도는 -24℃이다.To 6 liters of the liquefied product, 55-65% of the raw material powder, 25-30% of anhydrous sodium carbonate, 5-7% of palm oil fatty acid, 3-4% of chitosan, 1-2% of anhydrous pyrophosphate, flavor 1-2% After kneading, it is poured into a heart mold and quenched at -5 ℃ to -30 ℃, then aged in natural dry state for 5-15 hours, and processed into a solid lump or powder according to customer's preference. The temperature is -24 ° C.

이하, 본 발명에 대하여 상세히 설명한다.EMBODIMENT OF THE INVENTION Hereinafter, this invention is demonstrated in detail.

이미 알려진 바와 같이 운모석은 백운모, 흑운모, 견운모, 일라이트운모 등 그 종류가 매우 다양하며, 원적외선을 방사하여 체내의 혈액순환 작용에 도움을 주고, 탁월한 항균 및 살균력을 보유하고 있어, 피부미용, 노화방지등에 유용한 효과를 나타내는 것으로 되어 있고. 특히 예로부터 중국의 본초강목,동의보감 등에 약석으로 알려져 있어 현재 건강제품등의 다양한 분야에 적용되어 널리 사용되고 있으며,환경오염 독소제거에도 탁월한 효과가 있는 것으로 나타나고 있다.As already known, the mica stones are very diverse in type such as dolomite, biotite, biotite, illite mica, and emit far infrared rays to help blood circulation in the body, and have excellent antibacterial and bactericidal power. It is supposed to show effect that is useful for prevention. In particular, since it is known as a herbal medicine for Chinese herbal wood, Dongbobom, etc., it is widely used in various fields such as health products, and has been shown to have an excellent effect in removing toxins of environmental pollution.

키토산은 다량의 음이온을 발생시키는 물질로서, 음이온은 인체내에서 과량의 세로토닌이나 히스타민을 분비하게 하여 건강을 해치면 허파의 산소흡수 능력을 저하시키는 양이온과는 달리, 혈액중의 미넬랄 성분등의 이온화율을 상승시켜 알카리화 함으로써 혈액을 정화시키고, 세포막에서의 전기적 물질 교류를 촉진시켜 신진대사를 왕성하게 하여 체내의 노폐물을 신속히 배출시키는 한편, 혈청속의 면역성분인 감마 -글로부린의 양을 증가시켜 저항력을 증대시키고 자율신경계통, 혈액 및 임파액을 활성화시키는 것으로 나타나고 있다.Chitosan is a substance that generates a large amount of negative ions.Anions, like cations that cause the lungs to release excess serotonin or histamine, reduce the oxygen absorption ability of lungs when they hurt your health. By increasing the ionization rate and alkalizing the blood, it purifies the blood, promotes the exchange of electrical substances in the cell membrane, activates the metabolism, releases the waste products in the body quickly, and increases the amount of gamma-globurin, an immune component in the serum. It has been shown to increase resistance and activate the autonomic nervous system, blood and lymphatic fluid.

본 발명에서는 규석, 운모, 옥, 게르마늄의 입경을 200-450메쉬 분말로 하는데 이 입경의 범위에서 상호 물질간에 혼합이 잘 이루어 지면, 바람직하게는 325메쉬가 가장 좋다.In the present invention, the particle size of silica, mica, jade, and germanium is 200-450 mesh powder. If the material is well mixed between the materials in the range of the particle size, 325 mesh is preferable.

규석(차돌)규석(차돌)30-40%, 운모 40-50%, 옥 10-20%, 게르마늄10-15%로 혼합하여 이 범위의 것이 상호간의 조성 성분이 잘 조화됨은 물론, 이온화작용, 흡수, 흡착작용 등이 원활히 이루어 질수 있어, 본 발명의 목적을 달성 할 수 있다. 여기서 운모는 수비과정을 걸쳐 제조된 운모를 사용하게 되는데 즉 참나무멧돌에 필터에 의해 중금석이 제거된 연수물과 함께 운모분체를 넣고, 갈아서 반죽 상태로 하고 난 다음, 미세한 스크린으로 연수물과 함께 걸러서 침전 시킨다. 침전된 운모를 탈수하여 열풍기로 말려서 다시 마이크로밀탱크로 미세하게 분쇄한 것을 사용한다. 다시 말하면 불순물이 거의 없는 99.9%이상 순수한 운모를 사용한다. 원료물질파우다 55-65%, 무수탄산나트륨 25-30%, 야자유지방산 5-7%, 키토산 3-4%, 무수피로인산나트륨 1-2%, 향료 1-2%로 범위를 한정한 이유는 이 범위에서 가상 활발히 활성화 작용을 일으켜 신진대사를 촉진시킬 수 있을 뿐만 아니라 미네랄의 용출을 증대시켜 생체기능을 활성화 시킬 수 있다.이 범위를 벗어나면 미네랄의 용출이 어려워져 활성화기능이 저하된다.Quartzite (stone) Quartzite (stone) 30-40%, mica 40-50%, jade 10-20%, germanium 10-15% mixed in this range of the composition of the composition well, the ionization, Absorption, adsorption, etc. can be made smoothly, to achieve the object of the present invention. Here, the mica is used for the mica produced through the defensive process, that is, put the mica powder together with the soft water from which the lapis lazuli was removed by the filter on the oak metstone, grind it into a dough state, and then filter it with the soft water with a fine screen. Precipitate. Dehydrated mica is dehydrated, dried in a hot air and finely ground in a micromill tank. In other words, use more than 99.9% pure mica with almost no impurities. Raw materials powder 55-65%, anhydrous sodium carbonate 25-30%, palm oil fatty acid 5-7%, chitosan 3-4%, sodium pyrophosphate 1-2%, fragrance 1-2% In this range, it is possible to stimulate the metabolism by actively activating the metabolic activity, and to increase the dissolution of minerals to activate the biological function. Outside this range, the dissolution of minerals becomes difficult and the activation function is reduced.

액상화온도를 300-650℃의 범위로 한 것은 이 온도범위에서 액상화가 활발히 진행되며, 가장 바람직한 온도는 425℃이다. 또한, 반죽된 것을 하트형 금형기에 넣어 -5℃ 내지 -30℃에서 냉각을 해야만 제품의 수분함량이 높아져 사용시 잘 용해될 뿐 아니라 풍해성을 방지할 수 있다. 만일 여기에서 자연건조를 하게되면 제품의 자체가 딱딱하게 굳어 지면서 용해성 늦어지게 되고 풍해성이 생긴다. 바람직하게는 -24℃에서 냉각을 할 경우 수분함량을 적당히 포함하고 있어 물에 잘 용해되며, 풍해성을 효율적으로 방지 할 수 있다.The liquefaction temperature is in the range of 300-650 ° C, and liquefaction proceeds actively in this temperature range, and the most preferable temperature is 425 ° C. In addition, the dough is put into the heart-shaped mold machine and cooled at -5 ℃ to -30 ℃ only to increase the water content of the product can not only dissolve well in use, but also to prevent wind disintegration. If the product is naturally dried here, the product itself hardens, solubility is slowed down, and solubility is generated. Preferably, when cooled at -24 ℃ it contains a suitable water content so that it is well soluble in water, it can effectively prevent wind dispersibility.

이하 본 발명의 실시예를 들어 설명 한다.Hereinafter, an embodiment of the present invention will be described.

<실시예><Example>

제1공정1st process

필터로 걸려진 연수된 물에 운모분체를 넣고 멧돌에 넣어 서서히 갈면서 반죽상태로 한 다음, 연수물을 다시 첨가하여 운모를 침전시키고, 침전된 운모를 수분을 빼고 탈수, 열풍건조 한다.Put mica powder into soft water hung by filter and put it in a millstone to grind it gradually. Then, add soft water again to precipitate mica, dehydrate mica, dehydrate and dry with hot air.

제2공정2nd process

제1공정과 같이 각각수비공정을 걸친 순도 99.9%이상, 입경 325메쉬인 규석30%. 운모 35%, 옥 20%, 게르마늄 15%를 각각 혼합, 연수물에 넣고, 교반한 다음 건조하여 원료물질 파우다를 제조한다.30% of silica with a purity of 99.9% or more and a particle size of 325 mesh. 35% mica, 20% jade and 15% germanium are mixed, put in soft water, stirred and dried to prepare raw material powder.

제3공정3rd process

제2공정에서 제조된 파우다 75%와 무수탄산나트륨 25%를 혼합하고, 450℃의 연수물에 서서히 넣어 저으면서 교반하면 처음에는 반죽상태로 되고, 계속 저으면서 교반하면 파우다가 용해되어 액상화 된다.75% of the powder prepared in the second step and 25% of anhydrous sodium carbonate are mixed, and the mixture is gradually stirred into the soft water at 450 ° C. and stirred to become a dough state at first, and stirring is continued to stir and the powder is dissolved and liquefied.

제4공정4th process

제3공정에서 제조된 액상화물6ℓ, 원료물질파우다 60%, 무수탄산나트륨 28%,야자유지방산 6%, 키토산 4%, 무수피로인산나트륨 1%, 향료 1%로 조성하여 혼합, 반죽, 급냉한 후 냉 자연건조상태로 8시간 숙성하여 고체나 파우다로 공한다.After mixing, kneading and quenching, 6L of liquid liquefaction prepared in the 3rd step, raw material powder 60%, sodium carbonate anhydrous 28%, palm oil fatty acid 6%, chitosan 4%, sodium pyrophosphate 1%, fragrance 1% It is aged for 8 hours in cold and dry condition and is vacant in solid or powder.

본 발명에 의해 제조된 목욕용재는 흡착, 탈취효과가 우수할 뿐만 아니라 유효 미네랄이 용출되어 이온화 작용에 의한 세포 활성화기능이 탁월하여 노화방지 특히 피부비용에 좋은 것으로 나타나고 있다.The bath material prepared by the present invention is not only excellent in adsorption and deodorizing effect, but also shows that the effective minerals are eluted and excellent in cell activation by ionization, which is good for anti-aging, especially skin cost.

Claims (4)

각각 수비공정을 거치면서 인체에 해로운 철등의 중금속을 걸러내고, 분말로 한다음 건조한 규석(차돌)30-40%, 운모 40-50%, 옥 10-20%, 게르마늄10-15%로 혼합하여, 원료물질파우다를 제조하고, 원료물질파우다 70-80%와 무수탄산나트륨 20-30% 혼합, 300-650℃에서 연수물에 용해시킨 후 액상화한다.During the defensive process, filter out heavy metals such as iron, which are harmful to the human body, and make them into powder, and then mix them with dry silica (calcite) 30-40%, mica 40-50%, jade 10-20%, and germanium 10-15%. Prepare raw material powder, mix 70-80% raw material powder with 20-30% anhydrous sodium carbonate, dissolve in soft water at 300-650 ℃ and liquefy. 상기 액상화물6ℓ에, 상기 원료물질파우다 55-65%, 무수탄산나트륨 25-30%,야자유지방산 5-7%, 키토산 3-4%, 무수피로인산나트륨 1-2%, 향료 1-2% 혼합하여 반죽을 한 후 하트형 금형기에 부어 급냉한 후 자연건조상태로 5-15시간 숙성하여 가공하여 활성화 기능이 우수한 다기능 목욕용재를 제조하는 방법.To 6 liters of the liquefied product, 55-65% of the raw material powder, 25-30% of anhydrous sodium carbonate, 5-7% of palm oil fatty acid, 3-4% of chitosan, 1-2% of anhydrous pyrophosphate, 1-2% of fragrance Method of producing multifunctional bath material with excellent activation function by kneading the dough, pouring it into a heart mold and quenching it, and then aging it for 5-15 hours in a natural dry state. 제1항에 있어서 규석, 운모, 옥, 게르마늄의 입경은 200-450메쉬인 것을 특징으로 하는 다기능 목욕용재의 제조방법The method for producing a multifunctional bath material according to claim 1, wherein the silica, mica, jade and germanium have a particle diameter of 200-450 mesh. 제1항에 있어서 급냉온도는 -5℃ 내지 -30℃ 급냉하는 것을 특징으로 하는 다기능 목욕용재의 제조방법The method of claim 1, wherein the quenching temperature is -5 ° C to -30 ° C. 제1항, 제2항에 있어서 액상화온도는 300-650℃인 것을 특징으로 하는 다기능 목욕용재의 제조방법The method for producing a multifunctional bath material according to claim 1 or 2, wherein the liquefaction temperature is 300-650 ° C.
KR10-2000-0054526A 2000-09-16 2000-09-16 Method for preparing multi-function bath soap KR100368914B1 (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR200453121Y1 (en) 2008-07-17 2011-04-13 (주)아모레퍼시픽 A lump type powder
KR101684869B1 (en) 2016-09-19 2016-12-09 한상선 Bath agent containing ceriporia lacerata extract
KR101708721B1 (en) 2016-05-18 2017-02-21 김성현 Method for manufacturing bath agent improving far-infrared emission and antibiotic and the bath agent made therefrom

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KR20020088864A (en) * 2001-05-22 2002-11-29 도영수 Functional bath additive composition made of chitosan and processing therefore
DE102007057662B4 (en) * 2007-11-28 2010-01-14 Stefan Kolumbuchi Basic shoe cleaning powder for the neutralization of foot sweat when worn

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JPS6416714A (en) * 1987-07-08 1989-01-20 Nanyo Kasei Kk Bathing agent
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JPS61129112A (en) * 1984-11-27 1986-06-17 Miyazawa Kogyo Kk Warm bathing agent of germanium
JPS6416714A (en) * 1987-07-08 1989-01-20 Nanyo Kasei Kk Bathing agent
KR0163501B1 (en) * 1994-12-30 1998-12-01 성재갑 Bathing composition
JPH08291048A (en) * 1995-04-25 1996-11-05 Nippon Fine Chem Co Ltd Bathing agent
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR200453121Y1 (en) 2008-07-17 2011-04-13 (주)아모레퍼시픽 A lump type powder
KR101708721B1 (en) 2016-05-18 2017-02-21 김성현 Method for manufacturing bath agent improving far-infrared emission and antibiotic and the bath agent made therefrom
KR101684869B1 (en) 2016-09-19 2016-12-09 한상선 Bath agent containing ceriporia lacerata extract

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