CN110897938A - Quick-foaming antibacterial anti-wrinkle cleansing foam and preparation method thereof - Google Patents
Quick-foaming antibacterial anti-wrinkle cleansing foam and preparation method thereof Download PDFInfo
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- CN110897938A CN110897938A CN201911338901.0A CN201911338901A CN110897938A CN 110897938 A CN110897938 A CN 110897938A CN 201911338901 A CN201911338901 A CN 201911338901A CN 110897938 A CN110897938 A CN 110897938A
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- wrinkle
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- 239000006260 foam Substances 0.000 title claims abstract description 78
- 238000005187 foaming Methods 0.000 title claims abstract description 74
- 230000001153 anti-wrinkle effect Effects 0.000 title claims abstract description 73
- 230000000844 anti-bacterial effect Effects 0.000 title claims description 34
- 238000002360 preparation method Methods 0.000 title abstract description 13
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 54
- 230000003385 bacteriostatic effect Effects 0.000 claims abstract description 40
- 230000003078 antioxidant effect Effects 0.000 claims abstract description 38
- 239000004088 foaming agent Substances 0.000 claims abstract description 37
- 230000001815 facial effect Effects 0.000 claims abstract description 36
- 239000003963 antioxidant agent Substances 0.000 claims abstract description 35
- 239000003755 preservative agent Substances 0.000 claims abstract description 23
- 230000002335 preservative effect Effects 0.000 claims abstract description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 23
- 239000004166 Lanolin Substances 0.000 claims abstract description 19
- 229940039717 lanolin Drugs 0.000 claims abstract description 19
- 235000019388 lanolin Nutrition 0.000 claims abstract description 19
- 239000008367 deionised water Substances 0.000 claims abstract description 17
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 17
- 239000004094 surface-active agent Substances 0.000 claims abstract description 17
- 239000003242 anti bacterial agent Substances 0.000 claims abstract description 5
- 239000000203 mixture Substances 0.000 claims description 32
- 238000003756 stirring Methods 0.000 claims description 24
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 22
- 229920001661 Chitosan Polymers 0.000 claims description 19
- 235000010469 Glycine max Nutrition 0.000 claims description 18
- 108010046377 Whey Proteins Proteins 0.000 claims description 18
- 102000007544 Whey Proteins Human genes 0.000 claims description 18
- 235000011187 glycerol Nutrition 0.000 claims description 18
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 18
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 18
- ZUFONQSOSYEWCN-UHFFFAOYSA-M sodium;2-(methylamino)acetate Chemical group [Na+].CNCC([O-])=O ZUFONQSOSYEWCN-UHFFFAOYSA-M 0.000 claims description 18
- 235000021119 whey protein Nutrition 0.000 claims description 18
- 239000000341 volatile oil Substances 0.000 claims description 17
- 244000068988 Glycine max Species 0.000 claims description 16
- 229940110456 cocoa butter Drugs 0.000 claims description 16
- 235000019868 cocoa butter Nutrition 0.000 claims description 16
- FBPFZTCFMRRESA-KVTDHHQDSA-N D-Mannitol Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-KVTDHHQDSA-N 0.000 claims description 15
- 229930195725 Mannitol Natural products 0.000 claims description 15
- 239000000594 mannitol Substances 0.000 claims description 15
- 235000010355 mannitol Nutrition 0.000 claims description 15
- 229910019142 PO4 Inorganic materials 0.000 claims description 14
- 239000010452 phosphate Substances 0.000 claims description 14
- 229910052700 potassium Inorganic materials 0.000 claims description 14
- 239000011591 potassium Substances 0.000 claims description 14
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 12
- 238000004140 cleaning Methods 0.000 claims description 12
- 238000001816 cooling Methods 0.000 claims description 12
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims description 12
- LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical compound CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 claims description 10
- 239000007788 liquid Substances 0.000 claims description 10
- 238000000034 method Methods 0.000 claims description 7
- 230000037303 wrinkles Effects 0.000 claims description 7
- 238000001914 filtration Methods 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 6
- SFNALCNOMXIBKG-UHFFFAOYSA-N ethylene glycol monododecyl ether Chemical compound CCCCCCCCCCCCOCCO SFNALCNOMXIBKG-UHFFFAOYSA-N 0.000 claims description 5
- 239000003906 humectant Substances 0.000 claims description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical group C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 2
- 230000002421 anti-septic effect Effects 0.000 claims description 2
- 239000011734 sodium Substances 0.000 claims description 2
- 229910052708 sodium Inorganic materials 0.000 claims description 2
- 238000004945 emulsification Methods 0.000 claims 2
- 239000004909 Moisturizer Substances 0.000 claims 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims 1
- 230000001333 moisturizer Effects 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 8
- 241000894006 Bacteria Species 0.000 abstract description 3
- 231100000331 toxic Toxicity 0.000 abstract description 3
- 230000002588 toxic effect Effects 0.000 abstract description 3
- 239000002537 cosmetic Substances 0.000 abstract description 2
- 235000006708 antioxidants Nutrition 0.000 description 31
- 230000000052 comparative effect Effects 0.000 description 25
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 17
- 229910052938 sodium sulfate Inorganic materials 0.000 description 17
- 235000011152 sodium sulphate Nutrition 0.000 description 17
- 238000012360 testing method Methods 0.000 description 12
- 230000001804 emulsifying effect Effects 0.000 description 10
- LWIHDJKSTIGBAC-UHFFFAOYSA-K tripotassium phosphate Chemical compound [K+].[K+].[K+].[O-]P([O-])([O-])=O LWIHDJKSTIGBAC-UHFFFAOYSA-K 0.000 description 6
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- -1 polyoxyethylene Polymers 0.000 description 4
- 230000006872 improvement Effects 0.000 description 3
- 229910000160 potassium phosphate Inorganic materials 0.000 description 3
- 235000011009 potassium phosphates Nutrition 0.000 description 3
- 238000010998 test method Methods 0.000 description 3
- TXFPEBPIARQUIG-UHFFFAOYSA-N 4'-hydroxyacetophenone Chemical compound CC(=O)C1=CC=C(O)C=C1 TXFPEBPIARQUIG-UHFFFAOYSA-N 0.000 description 2
- 229930003427 Vitamin E Natural products 0.000 description 2
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 2
- 230000002045 lasting effect Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000011056 performance test Methods 0.000 description 2
- 239000012488 sample solution Substances 0.000 description 2
- 235000019165 vitamin E Nutrition 0.000 description 2
- 229940046009 vitamin E Drugs 0.000 description 2
- 239000011709 vitamin E Substances 0.000 description 2
- KWIUHFFTVRNATP-UHFFFAOYSA-N Betaine Natural products C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 description 1
- KWIUHFFTVRNATP-UHFFFAOYSA-O N,N,N-trimethylglycinium Chemical compound C[N+](C)(C)CC(O)=O KWIUHFFTVRNATP-UHFFFAOYSA-O 0.000 description 1
- 244000046052 Phaseolus vulgaris Species 0.000 description 1
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 1
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical group [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 1
- 108010073771 Soybean Proteins Proteins 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 230000002730 additional effect Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000003254 anti-foaming effect Effects 0.000 description 1
- 229960003237 betaine Drugs 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000002738 chelating agent Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 150000002191 fatty alcohols Chemical group 0.000 description 1
- 229940087068 glyceryl caprylate Drugs 0.000 description 1
- 239000008233 hard water Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- RGUVUPQQFXCJFC-UHFFFAOYSA-N n-hydroxyoctanamide Chemical compound CCCCCCCC(=O)NO RGUVUPQQFXCJFC-UHFFFAOYSA-N 0.000 description 1
- 239000002504 physiological saline solution Substances 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 235000018102 proteins Nutrition 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- GHBFNMLVSPCDGN-UHFFFAOYSA-N rac-1-monooctanoylglycerol Chemical compound CCCCCCCC(=O)OCC(O)CO GHBFNMLVSPCDGN-UHFFFAOYSA-N 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 235000019710 soybean protein Nutrition 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/55—Phosphorus compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/645—Proteins of vegetable origin; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/736—Chitin; Chitosan; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Dermatology (AREA)
- Emergency Medicine (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Cosmetics (AREA)
- Detergent Compositions (AREA)
Abstract
The invention belongs to the field of cosmetics, and particularly relates to a quick-foaming bacteriostatic anti-wrinkle cleansing foam and a preparation method thereof. The quick-foaming bacteriostatic anti-wrinkle facial cleansing foam provided by the invention comprises the following components in percentage by weight: 58-74% of deionized water, 8-12% of surfactant, 12-17% of quick-acting foaming agent, 0.4-1.6% of antioxidant, 3-5% of auxiliary surfactant, 0.4-2% of water-soluble lanolin, 0.2-1% of antibacterial agent, 1.5-2.5% of glycerol and 0.45-0.8% of preservative. The facial cleansing bubble provided by the invention can quickly bubble, can directly beat fine and firm foam from a bottle, can mildly clean the face, has an obvious antioxidant effect, can effectively inhibit bacteria and preserve moisture, and has no toxic or side effect.
Description
Technical Field
The invention belongs to the field of cosmetics, and particularly relates to a quick-foaming bacteriostatic anti-wrinkle cleansing foam and a preparation method thereof.
Background
Along with the development of economy and the improvement of the economic level of people, people demand materials for convenience and functionality, and the function of the facial cleanser as an indispensable daily necessity in modern life of people is more and more important. The facial cleanser is an important daily product for women, the requirement on the facial cleanser is not as simple as that of a face, and the facial cleanser needs to be endowed with new additional effects. The abundant foam can remove dirt on the skin more easily, and the use is more comfortable, so that the bubble facial cleanser meets the favor of people on the foam, people do not need to rub out the foam by hands any more, but can obtain enough foam by pressing the bottle body directly, and the bubble facial cleanser is more and more popular.
Chinese patent application CN107260579A discloses a mild cleansing bubble which comprises the following components: 0.05-0.1% of chelating agent, 9-21% of polyalcohol, 1.5-6% of fatty acid, 0.5-1.5% of alkali, 10-23% of surfactant, 8-15% of betaine, 0.05-0.2% of cellulose, 0.5-2% of conditioner, 0.1-0.4% of preservative, 0.01-0.03% of essence and the balance of water. The cleansing bubble provided by the invention can effectively clean the skin, and the generated foam is fine, rich, lasting and thick, has low odor and low pigment degree, is strong in foamability, soft and rich in foam, and is very mild to the skin and eyes. However, the cleansing bubbles contain alkaline components, and are not friendly to the acidic skin of the human body; the generated foam is soft, and the comfortable feeling of the foam cleaning face cannot be improved; moreover, the cleansing bubble has a single function and cannot meet the increasing product requirements of people.
Most of the existing bubble facial cleansers have the problems of unsatisfactory foaming effect, excessively soft generated foam, poor facial cleansing effect and comfort, single effect and the like.
Disclosure of Invention
Aiming at the defects of the prior art, the invention aims to provide a quick-foaming bacteriostatic anti-wrinkle cleansing bubble and a preparation method thereof. The quick-foaming antibacterial anti-wrinkle cleansing foam provided by the invention can quickly foam, can directly beat fine and firm foam from a bottle, has lasting foam, can mildly clean the face, has an obvious antioxidant effect, can effectively inhibit bacteria and preserve moisture, and has no toxic or side effect.
A quick-foaming antibacterial anti-wrinkle cleansing foam comprises the following components in percentage by weight: 8-12% of surfactant, 12-17% of quick-acting foaming agent and 3-5% of auxiliary surfactant, wherein the quick-acting foaming agent comprises potassium lauryl alcohol ether phosphate and/or soybean whey protein and the balance of water.
Further, the potassium laureth phosphate and the soybean whey protein are in a weight ratio of (12-15): (1-3).
Further, the quick-foaming antibacterial anti-wrinkle facial cleansing foam comprises the following components in percentage by weight: 65.83% of water, 10% of surfactant, 15% of quick-acting foaming agent and 4% of auxiliary surfactant.
Further, the quick-foaming antibacterial anti-wrinkle facial cleansing bubble further comprises 1% of antioxidant, wherein the antioxidant is prepared from cocoa butter essential oil and mannitol in a weight ratio of 5-9: 1-3.
Further, the quick-foaming antibacterial anti-wrinkle facial cleansing foam also comprises 0.45-0.8% of preservative, 1.9-4.5% of humectant and 0.2-1% of antibacterial agent.
Further, the preservative is GC-04 preservative, the humectant comprises 0.4% -2% of water-soluble lanolin and 1.5% -2.5% of glycerin, and the antibacterial agent is chitosan.
Further, the surfactant is fatty alcohol-polyoxyethylene ether sodium sulfate.
Further, the auxiliary surfactant is sodium cocoyl sarcosinate.
The invention also aims to provide a preparation method of the quick-foaming bacteriostatic anti-wrinkle facial cleansing bubble, which comprises the following steps:
further, S1 adding deionized water and surfactant into the cleaned emulsifying cylinder, adjusting the heater of the emulsifying cylinder to 70-90 ℃ for heating, and stirring for 12-17 minutes at 30-50r/min to obtain a mixture A;
s2, adding a quick-acting foaming agent, an antioxidant, sodium cocoyl sarcosinate, water-soluble lanolin, chitosan and glycerol into the mixture A obtained in the step S1, stirring for 15-30 minutes at 30-50r/min until the mixture is transparent, and continuing stirring for 15-25 minutes at the temperature of 70-90 ℃ to obtain a mixture B;
s3 opening cooling system, cooling mixture B to 40-50 deg.C, adding dissolved essence and antiseptic, adjusting pH, stirring at 30-50r/min for 4-6 min, and filtering the face cleaning liquid with filter screen.
Further, in the step S3, the pH is adjusted to 5.5 to 6.5, and the size of the filter screen is 200 meshes.
Compared with the prior art, the invention has the following advantages:
(1) the quick-foaming antibacterial anti-wrinkle cleansing foam provided by the invention contains a quick-acting foaming agent consisting of the potassium lauryl alcohol ether phosphate and the soybean whey protein, so that the cleansing foam can foam quickly and can generate firm and rich foam quickly.
(2) The quick-foaming antibacterial anti-wrinkle cleansing foam provided by the invention contains the antioxidant consisting of the cocoa butter essential oil and the mannitol, so that the cleansing foam has an obvious antioxidant effect and has an anti-wrinkle effect.
(3) The quick-foaming antibacterial anti-wrinkle cleansing foam provided by the invention contains chitosan, can inhibit bacteria and preserve moisture, and has the effect of deep cleaning.
(4) The quick-foaming antibacterial anti-wrinkle cleansing foam provided by the invention is simple in preparation process, and the prepared cleansing foam is safe and has no toxic or side effect.
Detailed Description
The present invention is further described in the following description of the specific embodiments, which is not intended to limit the invention, but various modifications and improvements can be made by those skilled in the art according to the basic idea of the invention, within the scope of the invention, as long as they do not depart from the basic idea of the invention.
Cocoa butter essential oil, which is an essential oil extracted from natural plant cocoa beans and can be purchased from Qingdao diwatson chemical Co., Ltd; the soybean whey protein is acid-soluble protein when the acid is adjusted to the isoelectric point pH of 415-418 in the process of extracting the soybean protein by water, and can be purchased from Guangzhou MinSong chemical products, Inc.; sodium polyoxyethylene fatty alcohol sulfate is available from Guangzhou Xing Cheng Shang Shu Co., Ltd;
GC-04 preservative, the active ingredients of which are glyceryl caprylate, caprylhydroxamic acid and p-hydroxyacetophenone, is available from Qin Ying refining chemical Co., Ltd, Guangzhou city.
Example 1A quick-foaming, bacteriostatic and anti-wrinkle facial cleanser bubble
A quick-foaming antibacterial anti-wrinkle cleansing foam comprises the following components in percentage by weight: 58% of deionized water, 12% of fatty alcohol-polyoxyethylene ether sodium sulfate, 17% of quick-acting foaming agent, 1.6% of antioxidant, 5% of sodium cocoyl sarcosinate, 2% of water-soluble lanolin, 1% of chitosan, 2.5% of glycerol and 0.8% of GC-04 preservative; wherein the quick-acting foaming agent is composed of lauryl alcohol ether potassium phosphate and soybean whey protein according to the weight ratio of 12: 1, preparing a composition; the antioxidant is prepared from cocoa butter essential oil and mannitol in a weight ratio of 9: 1.
The quick-foaming antibacterial anti-wrinkle cleansing foam is prepared by the following method:
s1, adding deionized water and fatty alcohol-polyoxyethylene ether sodium sulfate into the cleaned emulsifying cylinder, adjusting a heater of the emulsifying cylinder to 80 ℃ for heating, and stirring for 17 minutes at the same time at 30r/min to obtain a mixture A;
s2, adding a quick-acting foaming agent, an antioxidant, sodium cocoyl sarcosinate, water-soluble lanolin, chitosan and glycerol into the mixture A obtained in the step S1, stirring at 30r/min for 30 minutes until the mixture is transparent, and continuing stirring for 20 minutes at the temperature of 80 ℃ to obtain a mixture B;
s3, opening a cooling system, cooling the mixture B to 45 ℃, adding dissolved GC-04 preservative, adjusting the pH to 5.5, stirring at 30r/min for 6 minutes, and filtering the face cleaning liquid through a 200-mesh filter screen to obtain the face cleaning liquid.
Example 2 quick-foaming bacteriostatic anti-wrinkle cleansing foam
A quick-foaming antibacterial anti-wrinkle cleansing foam comprises the following components in percentage by weight: 74% of deionized water, 8% of fatty alcohol-polyoxyethylene ether sodium sulfate, 12% of quick-acting foaming agent, 0.4% of antioxidant, 3% of sodium cocoyl sarcosinate, 0.4% of water-soluble lanolin, 0.2% of chitosan, 1.5% of glycerol and 0.45% of GC-04 preservative; wherein the quick-acting foaming agent is composed of lauryl alcohol ether potassium phosphate and soybean whey protein according to a weight ratio of 15: 3, preparing a composition; the antioxidant is prepared from cocoa butter essential oil and mannitol in a weight ratio of 5: 3, and (3).
The quick-foaming antibacterial anti-wrinkle cleansing foam is prepared by the following method:
s1, adding deionized water and fatty alcohol-polyoxyethylene ether sodium sulfate into the cleaned emulsifying cylinder, adjusting a heater of the emulsifying cylinder to 80 ℃ for heating, and stirring for 12 minutes at the same time at 50r/min to obtain a mixture A;
s2, adding a quick-acting foaming agent, an antioxidant, sodium cocoyl sarcosinate, water-soluble lanolin, chitosan and glycerol into the mixture A obtained in the step S1, stirring at 50r/min for 15 minutes until the mixture is transparent, and continuing to stir for 20 minutes at the temperature of 80 ℃ to obtain a mixture B;
s3, opening a cooling system, cooling the mixture B to 45 ℃, adding the dissolved GC-04 preservative, adjusting the pH value to 6.5, stirring at 50r/min for 4 minutes, and filtering the face cleaning liquid through a 200-mesh filter screen to obtain the face cleaning liquid.
Example 3A quick-foaming, bacteriostatic and anti-wrinkle facial cleanser bubble
A quick-foaming antibacterial anti-wrinkle cleansing foam comprises the following components in percentage by weight: 65.83% of deionized water, 10% of fatty alcohol-polyoxyethylene ether sodium sulfate, 15% of quick-acting foaming agent, 1% of antioxidant, 4% of sodium cocoyl sarcosinate, 1% of water-soluble lanolin, 0.5% of chitosan, 2% of glycerol and 0.6% of GC-04 preservative, wherein the quick-acting foaming agent is composed of lauryl alcohol ether potassium phosphate and soybean whey protein according to the weight ratio of 13: 2; the antioxidant consists of cocoa butter essential oil and mannitol in a weight ratio of 7: 2.
The quick-foaming antibacterial anti-wrinkle cleansing foam is prepared by the following method:
s1, adding deionized water and fatty alcohol-polyoxyethylene ether sodium sulfate into the cleaned emulsifying tank, adjusting a heater of the emulsifying tank to 80 ℃ for heating, and stirring for 15 minutes at the same time at 40r/min to obtain a mixture A;
s2, adding a quick-acting foaming agent, an antioxidant, sodium cocoyl sarcosinate, water-soluble lanolin, chitosan and glycerol into the mixture A obtained in the step S1, stirring at 40r/min for 20 minutes until the mixture is transparent, and continuing stirring for 20 minutes at the temperature of 80 ℃ to obtain a mixture B;
s3, opening a cooling system, cooling the mixture B to 45 ℃, adding the dissolved GC-04 preservative, adjusting the pH to 6.0, stirring for 4-6 minutes at 40r/min, and filtering the face cleaning liquid through a 200-mesh filter screen to obtain the face cleaning liquid.
Example 4A quick-foaming, bacteriostatic and anti-wrinkle facial cleanser bubble
A quick-foaming antibacterial anti-wrinkle cleansing foam comprises the following components in percentage by weight: 67.6% of deionized water, 9% of fatty alcohol-polyoxyethylene ether sodium sulfate, 14% of quick-acting foaming agent, 0.7% of antioxidant, 4% of sodium cocoyl sarcosinate, 1.5% of water-soluble lanolin, 0.8% of chitosan, 1.8% of glycerin and 0.53% of GC-04 preservative; wherein the quick-acting foaming agent is composed of potassium laureth phosphate and soybean whey protein according to a weight ratio of 14: 3; the antioxidant is prepared from cocoa butter essential oil and mannitol in a weight ratio of 8: 3, and (3).
The quick-foaming antibacterial anti-wrinkle cleansing foam is prepared by the following method:
s1, adding deionized water and fatty alcohol-polyoxyethylene ether sodium sulfate into the cleaned emulsifying cylinder, adjusting a heater of the emulsifying cylinder to 80 ℃ for heating, and stirring for 13 minutes at the same time at 50r/min to obtain a mixture A;
s2, adding a quick-acting foaming agent, an antioxidant, sodium cocoyl sarcosinate, water-soluble lanolin, chitosan and glycerol into the mixture A obtained in the step S1, stirring at 50r/min for 25 minutes until the mixture is transparent, and continuing stirring for 20 minutes at the temperature of 80 ℃ to obtain a mixture B;
s3, opening a cooling system, cooling the mixture B to 45 ℃, adding the dissolved GC-04 preservative, adjusting the pH value to 6.0, stirring at 50r/min for 6 minutes, and filtering the face cleaning liquid through a 200-mesh filter screen to obtain the face cleaning liquid.
Comparative example 1 quick-foaming bacteriostatic anti-wrinkle cleansing foam
A quick-foaming antibacterial anti-wrinkle cleansing foam comprises the following components in percentage by weight: 65.83% of deionized water, 10% of fatty alcohol-polyoxyethylene ether sodium sulfate, 15% of quick-acting foaming agent, 1% of antioxidant, 4% of sodium cocoyl sarcosinate, 1% of water-soluble lanolin, 0.5% of chitosan, 2% of glycerol and 0.6% of GC-04 preservative, wherein the quick-acting foaming agent is composed of potassium lauryl alcohol ether phosphate and soybean whey protein according to the weight ratio of 13:2, and the antioxidant is cocoa butter essential oil.
The preparation method of the quick-foaming bacteriostatic anti-wrinkle facial cleanser bubble is similar to that in example 3, and is different from that in example 3 in that the antioxidant is cocoa butter essential oil and does not contain mannitol.
Comparative example 2 quick-foaming bacteriostatic anti-wrinkle cleansing foam
A quick-foaming antibacterial anti-wrinkle cleansing foam comprises the following components in percentage by weight: 65.83% of deionized water, 10% of fatty alcohol-polyoxyethylene ether sodium sulfate, 15% of a quick-acting foaming agent, 1% of an antioxidant, 4% of sodium cocoyl sarcosinate, 1% of water-soluble lanolin, 0.5% of chitosan, 2% of glycerol and 0.6% of a GC-04 preservative, wherein the quick-acting foaming agent is composed of potassium lauryl alcohol ether phosphate and soybean whey protein according to a weight ratio of 13:2, and the antioxidant is mannitol.
The preparation method of the quick-foaming bacteriostatic anti-wrinkle facial cleanser bubble is similar to that of example 3, and is different from that of example 3 in that the antioxidant is mannitol and does not contain cocoa butter essential oil.
Comparative example 3 quick-foaming bacteriostatic anti-wrinkle cleansing foam
A quick-foaming antibacterial anti-wrinkle cleansing foam comprises the following components in percentage by weight: 65.83% of deionized water, 10% of fatty alcohol-polyoxyethylene ether sodium sulfate, 15% of a quick-acting foaming agent, 1% of an antioxidant, 4% of sodium cocoyl sarcosinate, 1% of water-soluble lanolin, 0.5% of chitosan, 2% of glycerol and 0.6% of a GC-04 preservative, wherein the quick-acting foaming agent is composed of potassium lauryl alcohol ether phosphate and soybean whey protein according to a weight ratio of 13:2, and the antioxidant is vitamin E.
The preparation method of the quick-foaming bacteriostatic anti-wrinkle facial cleansing bubble is similar to that of example 3, and is different from that of example 3 in that the antioxidant is vitamin E and does not contain mannitol and cocoa butter essential oil.
Comparative example 4 quick-foaming bacteriostatic anti-wrinkle cleansing foam
A quick-foaming antibacterial anti-wrinkle cleansing foam comprises the following components in percentage by weight: 65.83% of deionized water, 10% of fatty alcohol-polyoxyethylene ether sodium sulfate, 15% of quick-acting foaming agent, 1% of antioxidant, 4% of sodium cocoyl sarcosinate, 1% of water-soluble lanolin, 0.5% of chitosan, 2% of glycerol and 0.6% of GC-04 preservative, wherein the quick-acting foaming agent is potassium lauryl alcohol ether phosphate, and the antioxidant consists of cocoa butter essential oil and mannitol in a weight ratio of 7: 2.
The preparation method of the quick-foaming bacteriostatic anti-wrinkle facial cleanser bubble is similar to that of example 3, and is different from that of example 3 in that the quick-acting foaming agent is potassium laureth phosphate and does not contain soybean whey protein.
Comparative example 5 quick-foaming bacteriostatic anti-wrinkle cleansing foam
A quick-foaming antibacterial anti-wrinkle cleansing foam comprises the following components in percentage by weight: 65.83% of deionized water, 10% of fatty alcohol-polyoxyethylene ether sodium sulfate, 15% of quick-acting foaming agent, 1% of antioxidant, 4% of sodium cocoyl sarcosinate, 1% of water-soluble lanolin, 0.5% of chitosan, 2% of glycerol and 0.6% of GC-04 preservative, wherein the quick-acting foaming agent is soybean whey protein, and the antioxidant consists of cocoa butter essential oil and mannitol in a weight ratio of 7: 2.
The preparation method of the quick-foaming bacteriostatic anti-wrinkle facial cleansing foam is similar to that of example 3, and the quick-foaming agent is soybean whey protein and does not contain potassium lauryl alcohol ether phosphate ester, and is different from example 3.
Comparative example 6 quick-foaming bacteriostatic anti-wrinkle cleansing foam
A quick-foaming antibacterial anti-wrinkle cleansing foam comprises the following components in percentage by weight: 65.83% of deionized water, 10% of fatty alcohol-polyoxyethylene ether sodium sulfate, 15% of quick-acting foaming agent, 1% of antioxidant, 4% of sodium cocoyl sarcosinate, 1% of water-soluble lanolin, 0.5% of chitosan, 2% of glycerol and 0.6% of GC-04 preservative, wherein the quick-acting foaming agent is fatty alcohol-polyoxyethylene ether sodium sulfate, and the antioxidant is composed of cocoa butter essential oil and mannitol in a weight ratio of 7: 2.
The preparation method of the quick-foaming antibacterial anti-wrinkle cleansing foam is similar to that in example 3, and the quick-foaming agent is fatty alcohol polyoxyethylene ether sodium sulfate and does not contain soybean whey protein and potassium lauryl alcohol ether phosphate ester as the difference from example 3.
Experimental example 1 quick-foaming antibacterial anti-wrinkle cleansing foam anti-wrinkle performance test
1. Test materials: the quick-foaming bacteriostatic anti-wrinkle facial cleansing foam prepared in the following steps of example 1, example 2, example 3, example 4, comparative example 1, comparative example 2 and comparative example 3.
2. The test method comprises the following steps:
70 volunteers were collected and randomly divided into 7 groups of 10 persons, and the quick-foaming bacteriostatic anti-wrinkle cleansing foam prepared in example 1, example 2, example 3, example 4, comparative example 1, comparative example 2 and comparative example 3 was used for 30 days, and the skin wrinkle condition of each volunteer was analyzed by detecting the skin wrinkle condition of each volunteer using a skin analyzer.
3. And (3) test results: the test results are shown in table 1.
TABLE 1 anti-wrinkle test result of quick-foaming antibacterial anti-wrinkle cleansing foam
As can be seen from table 1, the wrinkle ratio of examples 1 to 4 is lower than that of comparative examples 1 to 3 in each of the groups of examples, and the addition of the cocoa butter essential oil and mannitol, which are single components, does not significantly improve the anti-wrinkle effect of the cleansing foam, but significantly improves the fine line improvement and anti-wrinkle effect of the cleansing foam when the two are used in combination. Compared with example 1, example 2 and example 4, example 3 is significantly superior to other example groups in terms of each performance, and is the best embodiment of the present invention.
Experimental example 2 foaming Performance test of quick-foaming, antibacterial and anti-wrinkle cleansing foam
1. Test materials: the quick-foaming bacteriostatic anti-wrinkle facial cleansing foam prepared in the following steps of example 1, example 2, example 3, example 4, comparative example 5 and comparative example 6.
2. The test method comprises the following steps:
the quick-foaming bacteriostatic anti-wrinkle facial cleansing bubbles prepared in example 1, example 2, example 3, example 4, comparative example 5 and comparative example 6 were taken to be 6mL each, added with 150ppm of hard water to the mark in a 1L volumetric flask, and shaken up gently. The sample solution was heated to 40 ℃ for measurement. Using a Roche foam meter, about 50ml of sample solution was injected from the bottom of the graduated tube, the piston of the graduated tube was closed, and all measurements in which the difference between the flow-out time and the arithmetic mean of the observed flow-out times was greater than 5% were ignored, and abnormally long periods indicated the presence of air bubbles in the metering tube or stopcock. The foam volume (foam only) was measured at 0.5min, 2min, 4min after the flow had stopped.
2. And (3) test results: the test results are shown in table 2.
TABLE 2 quick-foaming antibacterial anti-wrinkle cleansing foam test results
| Item | Example 1 | Example 2 | Example 3 | Example 4 | Comparative example 4 | Comparative example 5 | Comparative example 6 |
| 0.5min | 30mL | 31mL | 35mL | 31mL | 22mL | 19mL | 16mL |
| 2min | 82mL | 84mL | 90mL | 83mL | 46mL | 41mL | 35mL |
| 4min | 145mL | 147mL | 161mL | 143mL | 86mL | 81mL | 75mL |
As can be seen from table 2, the wrinkle ratio of examples 1 to 4 compared to comparative examples 4 to 6, the foam production amount of each set of examples was higher than each comparative example, and the addition of the soy whey protein and the potassium laureth phosphate, which are single ingredients, did not significantly improve the foaming effect of the cleansing bubbles, but significantly improved the foam production amount of the cleansing bubbles when the two were used in combination. Compared with example 1, example 2 and example 4, the foam generation amount of example 3 is the fastest, and is the best embodiment of the invention.
Experimental example 3 bacteriostatic property test of quick-foaming bacteriostatic anti-wrinkle cleansing foam
1. Test materials: the quick-foaming bacteriostatic anti-wrinkle facial cleansing foam prepared in the following steps of example 1, example 2, example 3, example 4, comparative example 1 and comparative example 4.
2. The test method comprises the following steps: dripping 0.5mL of the 6 groups of quick-foaming antibacterial anti-wrinkle facial cleansing bubbles on a culture dish after ultraviolet irradiation sterilization, setting 0.5mL of physiological saline, and respectively inoculating with 9.0 × 104CFU/mL mold 0.5mL, 30min later test mold number.
3. And (3) test results: the results are shown in Table 3.
TABLE 3 results of bacteriostatic and anti-wrinkle quick-foaming cleansing foam
As can be seen from Table 3, compared with the normal saline group, the amount of the mold is significantly reduced in each example or comparative example group, which shows that the quick-foaming bacteriostatic anti-wrinkle cleansing foam prepared by the invention has a good bacteriostatic effect, and the bacteriostatic effect of example 3 is the best.
From the above results, it can be seen that the instant foaming bacteriostatic anti-wrinkle facial cleanser prepared by the present invention has excellent anti-wrinkle, foaming and bacteriostatic properties, and the best performance of example 3 is the best example of the present invention.
The foregoing embodiments are merely illustrative of the principles and utilities of the present invention and are not intended to limit the invention. Any person skilled in the art can modify or change the above-mentioned embodiments without departing from the spirit and scope of the present invention. Accordingly, it is intended that all equivalent modifications or changes which can be made by those skilled in the art without departing from the spirit and technical spirit of the present invention be covered by the claims of the present invention.
Claims (10)
1. The quick-foaming antibacterial anti-wrinkle facial cleansing foam is characterized by comprising the following components in percentage by weight: 8-12% of surfactant, 12-17% of quick-acting foaming agent and 3-5% of auxiliary surfactant, wherein the quick-acting foaming agent comprises potassium lauryl alcohol ether phosphate and/or soybean whey protein and the balance of water.
2. The quick-foaming, antibacterial and anti-wrinkle facial cleansing foam according to claim 1, wherein the potassium laureth phosphate and the soy whey protein are in a weight ratio of (12-15): (1-3).
3. The quick-foaming bacteriostatic anti-wrinkle facial cleanser bubble of claim 1, which is characterized by comprising the following components in percentage by weight: 65.83% of water, 10% of surfactant, 15% of quick-acting foaming agent and 4% of auxiliary surfactant.
4. The quick-foaming bacteriostatic wrinkle-resistant cleansing foam according to claim 1, further comprising 1% of an antioxidant, wherein the antioxidant is prepared from cocoa butter essential oil and mannitol in a weight ratio of 5-9: 1-3.
5. The quick-foaming bacteriostatic wrinkle-resistant facial cleansing bubble according to claim 1, further comprising 0.45% -0.8% of a preservative, 1.9% -4.5% of a humectant and 0.2% -1% of an antibacterial agent.
6. The quick-foaming bacteriostatic anti-wrinkle facial cleanser bubble according to claim 5, wherein the preservative is GC-04 preservative, the moisturizer comprises 0.4% -2% of water-soluble lanolin and 1.5% -2.5% of glycerin, and the antibacterial agent is chitosan.
7. The quick-foaming bacteriostatic wrinkle-resistant cleansing foam according to claim 1 or 2, wherein the surfactant is sodium fatty alcohol-polyoxyethylene ether sulfate.
8. The quick-foaming bacteriostatic anti-wrinkle facial cleansing bubble according to claim 1 or 2, wherein the auxiliary surfactant is sodium cocoyl sarcosinate.
9. The method for preparing instant-foaming bacteriostatic anti-wrinkle facial cleansing bubbles according to any one of claims 1 to 8, comprising the following steps:
s1 adding deionized water and a surfactant into the cleaned emulsification cylinder, adjusting a heater of the emulsification cylinder to 70-90 ℃ for heating, and stirring for 12-17 minutes at 30-50r/min to obtain a mixture A;
s2, adding a quick-acting foaming agent, an antioxidant, sodium cocoyl sarcosinate, water-soluble lanolin, chitosan and glycerol into the mixture A obtained in the step S1, stirring for 15-30 minutes at 30-50r/min until the mixture is transparent, and continuing stirring for 15-25 minutes at the temperature of 70-90 ℃ to obtain a mixture B;
s3 opening cooling system, cooling mixture B to 40-50 deg.C, adding dissolved essence and antiseptic, adjusting pH, stirring at 30-50r/min for 4-6 min, and filtering the face cleaning liquid with filter screen.
10. The method for preparing quick-foaming, anti-bacteria and anti-wrinkle facial cleansing foam according to claim 9, wherein the pH is adjusted to 5.5-6.5 in step S3, and the size of the filter screen is 200 meshes.
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