CN106890128A - A kind of Huoshan rice dry measure used in former times Essence - Google Patents
A kind of Huoshan rice dry measure used in former times Essence Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/99—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/66—Enzymes
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/676—Ascorbic acid, i.e. vitamin C
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/81—Preparation or application process involves irradiation
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/92—Oral administration
Abstract
The invention mainly relates to skin care item processing technique field, a kind of Huoshan rice dry measure used in former times Essence is disclosed, be made up of the raw material of following weight portion：Raw material A：Huoshan meter dry measure used in former times 32 ~ 34, Artemisia stelleriana 8 ~ 10, rice chaff 8 ~ 10, Shorthairy Antenoron 5 ~ 7, Chinese pholidota pseudobulb or herb 5 ~ 7, pekoe 5 ~ 7, Chinese mugwort 5 ~ 7；Raw material B：Hippophae rhamnoides fruit oil 0.15 ~ 0.17, vitamin C 0.06 ~ 0.08, vitamin E 0.05 ~ 0.07, glycyrrhizic acid 0.04 ~ 0.05；Raw material C：Mixed Microbes 3 ~ 5, complex enzyme 0.02 ~ 0.04；Abundant raw material, nutrition is balanced, it is easy to absorb, can be anti-oxidant, anti-aging reduces allergy, red blood silk is reduced, desalinates color spot, strengthen skin resistance, enhance metabolism, the skin injury for avoiding traditional removal cuticula from bringing, quick reparation damages skin, accelerates wound and acne print desalination, water and oil balance is kept, keeps skin delicate salubrious.
Description
Technical field
The invention mainly relates to skin care item processing technique field, more particularly to a kind of Huoshan rice dry measure used in former times Essence.
Background technology
Huoshan rice dry measure used in former times, i.e. Dendrobidium huoshanness, are the superfine product in the stem of noble dendrobium, are the endangered rare medicinal materials of China national.Dry measure used in former times suddenly
Rich in more than the ten kinds of alkaloid such as polysaccharide, amino acid and dendrobine, stem of noble dendrobium amine base.It is identified：Polyoses content is 18.974%, total raw
Alkaloids content is 0.030%, can effectively improve body's immunity, to the organs such as human body eye, pharynx, lung, stomach, intestines, kidney and blood,
The diseases such as angiocarpy have special efficacy, can physical fitness, anti-cataract, beauty and skin care, anti-aging, anti-mutation is antitumor,
Prevent and treat diabetes.
At present, for eating after the application method of Huoshan rice dry measure used in former times is also mainly directly soaked or decocted, at other
Seldom, but also there is not Huoshan rice dry measure used in former times Essence in the application in field.
The content of the invention
In order to make up the defect of prior art, it is an object of the invention to provide a kind of Huoshan rice dry measure used in former times Essence.
A kind of Huoshan rice dry measure used in former times Essence, is made up of the raw material of following weight portion：
Raw material A：Huoshan meter dry measure used in former times 32 ~ 34, Artemisia stelleriana 8 ~ 10, rice chaff 8 ~ 10, Shorthairy Antenoron 5 ~ 7, Chinese pholidota pseudobulb or herb 5 ~ 7, pekoe 5 ~ 7, Chinese mugwort 5 ~
7；
Raw material B：Hippophae rhamnoides fruit oil 0.15 ~ 0.17, vitamin C 0.06 ~ 0.08, vitamin E 0.05 ~ 0.07, glycyrrhizic acid 0.04 ~
0.05；
Raw material C：Mixed Microbes 3 ~ 5, complex enzyme 0.02 ~ 0.04；
Described Huoshan rice dry measure used in former times, is fresh Huoshan rice dry measure used in former times, increases fresh fragrance and viscosity.
Described hippophae rhamnoides fruit oil, is that physical squeezing method is obtained, purity >=98%.
Described Mixed Microbes, are made up of the raw material of following weight portion：It is wine yeast 18 ~ 20, Bifidobacterium 16 ~ 18, thermophilic
Lactobacillus lactis 13 ~ 15, acetic acid bacteria 13 ~ 15, lactobacillus paracasei 6 ~ 8, aspergillus niger 6 ~ 8.
Described complex enzyme, is made up of the raw material of following weight portion：Cellulase 15 ~ 17, hemicellulase 10 ~ 12, α-
Amylase 7 ~ 9, pectase 7 ~ 9.
A kind of preparation method of Huoshan rice dry measure used in former times Essence, comprises the following steps：
（1）Raw material A is cleaned, 80 ~ 100 mesh are crushed to, blanching 40 ~ 60 seconds in steam are placed in, crushed material is obtained；
（2）To 5 ~ 7 times of water of amount of raw material A weight are added in crushed material, it is well mixed, adds complex enzyme, is heated to 40 ~ 42 DEG C,
Stirring enzymolysis 180 ~ 200 minutes, is heated to 80 ~ 85 DEG C, is incubated 10 ~ 12 minutes, decomposes plant structure, promotes active ingredient leaching
Go out, material must be digested；
（3）To Mixed Microbes are added in enzymolysis material, stir, fermented 16 ~ 18 hours in 32 ~ 34 DEG C, be cooled to 19 ~ 21 DEG C, stir
Mix uniform, continue to ferment 8 ~ 9 days, then reduce temperature to 2 ~ 4 DEG C, stand 10 ~ 12 hours, decompose the macromolecular nutrition in raw material
Composition, and the metabolite of various small molecules is produced, make the pH of Essence be 5.6 ~ 5.8, it is adapted to skin acid-base value, it is easy to flesh
Skin absorbs, and improves the utilization rate of Essence, obtains fermentation material；
（4）Fermentation material is filtered, is retained filtrate and filter residue, to adding alcoholic solution in filter residue, in 46 ~ 48 DEG C, 28 ~
30kHz ultrasonic extractions, filtering merges all filtrates, is concentrated under reduced pressure into alcohol-free, 0.1 μm excessively of supermicro filtration membrane, improves recovery rate
And raw material availability, production cost is saved, obtain extract solution；
（5）Extract solution is heated to 72 ~ 74 DEG C, raw material B is added, is well mixed, through two sections of homogeneous, through 0.08 ~ 0.1 μm of sheet frame
Hyperfiltration, reduces the molecular weight of nutritional ingredient, promotes absorption of the skin to Essence, obtains Huoshan rice dry measure used in former times Essence；
（6）Packing, radiation sterilization obtains finished product.
The step（4）Ultrasonic extraction, be repeatedly ultrasound 3 times, for the first time add volume fraction for 61 ~ 63% alcohol
Solution, ultrasound 40 ~ 45 minutes adds the alcoholic solution that volume fraction is 72 ~ 74%, ultrasound 30 ~ 35 minutes, third time for the second time
The alcoholic solution that volume fraction is 81 ~ 83% is added, ultrasound 25 ~ 30 minutes is filtered after ultrasound every time.
The step（4）It is concentrated under reduced pressure, temperature is 46 ~ 48 DEG C, and pressure is 0 ~ 0.1MPa, and rotating speed is 60 ~ 65 revs/min
Clock.
The step（5）Two sections of homogeneous, first paragraph homogeneous：Temperature is 71 ~ 73 DEG C, pressure is 26.6 ~ 28.4MPa, the
Two sections of homogeneous：Temperature is 56 ~ 58 DEG C, pressure is 14.2 ~ 16.8Mpa.
The application method of the Huoshan rice dry measure used in former times Essence, after evening cleaning face, after having smeared smoothing toner or toner, takes
2 ~ 3 drop Huoshan rice dry measure used in former times Essences are applied to face, massage 13 ~ 15 minutes, and cleaning face carries out normal skin care, and 2 are used weekly
~ 3 times, also can at night sleep in first 3 hours, take 2 ~ 3 drop Huoshan rice dry measure used in former times Essences and drunk in 40 ~ 80 DEG C of warm water,
1 times a week；The applicable crowd of Huoshan rice dry measure used in former times Essence, it is adaptable to any skin quality, the age at 23 years old and after, containing being conducive to
The medicinal herb componentses of development of fetus are prevented miscarriage and promote, pregnant woman and the women of nursing period can also be used.
It is an advantage of the invention that：A kind of Huoshan rice dry measure used in former times Essence that the present invention is provided, abundant raw material, nutrition is balanced, it is easy to
Absorb, can be anti-oxidant, anti-aging reduces allergy, reduces red blood silk, desalinates color spot, strengthens skin resistance, promotes new old generation
Thank, the defencive function of enhancing skin and mucous membrane, it is to avoid the skin injury that traditional removal cuticula brings, quick reparation damages flesh
Skin, accelerates wound and acne print desalination, keeps water and oil balance, keeps skin delicate salubrious；Raw material A decomposes plant knot after enzymolysis
Structure, promotes active ingredient to leach, and increased the further technological processing way of rice chaff, turns waste into wealth, and improves the income of peasant；It is former
Fermented repeatedly through Mixed Microbes after material enzymolysis and low temperature immersion, decompose the macromolecular nutritional ingredient in raw material, and produce various small
The metabolite of molecule, makes the pH of Essence be 5.6 ~ 5.8, is adapted to skin acid-base value, it is easy to percutaneous absorption, improves Essence
Utilization rate；Through extracting repeatedly after fermentation, recovery rate is improved 12.4%, improve raw material availability, save production cost 8.9%；Institute
Have raw material carries out homogeneous repeatedly and filtering after mixing, and reduces the molecular weight of nutritional ingredient, promotes absorption of the skin to Essence；It is pure
Plant extract, without any chemical formula composition, to skin and human-body safety health, can not only be smeared with external application, can also be taken orally,
Age can use in the crowd of 23 years old and the above, containing the medicinal herb componentses for being conducive to preventing miscarriage and promoting development of fetus, pregnant woman
Applied widely and the women of nursing period can equally be used, income improves 17.2%.
Specific embodiment
Below the present invention is illustrated with specific embodiment.
Embodiment 1
A kind of Huoshan rice dry measure used in former times Essence, is made up of the raw material of following weight portion：
Raw material A：Huoshan meter dry measure used in former times 32, Artemisia stelleriana 8, rice chaff 8, Shorthairy Antenoron 5, Chinese pholidota pseudobulb or herb 5, pekoe 5, Chinese mugwort 5；Raw material B：Hippophae rhamnoides fruit oil
0.15th, vitamin C 0.06, vitamin E 0.05, glycyrrhizic acid 0.04；Raw material C：Mixed Microbes 3, complex enzyme 0.02；Described Huoshan
Rice dry measure used in former times, is fresh Huoshan rice dry measure used in former times, increases fresh fragrance and viscosity.
Described hippophae rhamnoides fruit oil, is that physical squeezing method is obtained, purity >=98%.
Described Mixed Microbes, are made up of the raw material of following weight portion：Wine yeast 18, Bifidobacterium 16, acidophilus breast bar
Bacterium 13, acetic acid bacteria 13, lactobacillus paracasei 6, aspergillus niger 6.
Described complex enzyme, is made up of the raw material of following weight portion：Cellulase 15, hemicellulase 10, AMS
7th, pectase 7.
A kind of preparation method of Huoshan rice dry measure used in former times Essence, comprises the following steps：
（1）Raw material A is cleaned, 100 mesh are crushed to, blanching 40 seconds in steam are placed in, crushed material is obtained；
（2）To 5 times of water of amount of raw material A weight are added in crushed material, it is well mixed, adds complex enzyme, be heated to 42 DEG C, stirs enzyme
Solution 200 minutes, is heated to 85 DEG C, is incubated 12 minutes, decomposes plant structure, promotes active ingredient to leach, and must digest material；
（3）To Mixed Microbes are added in enzymolysis material, stir, fermented 16 hours in 32 DEG C, be cooled to 19 DEG C, stir, after
Supervention ferment 9 days, then reduces temperature to 4 DEG C, stands 10 hours, decomposes the macromolecular nutritional ingredient in raw material, and produce many
The metabolite of small molecule is planted, makes the pH of Essence be 5.6 ~ 5.8, be adapted to skin acid-base value, it is easy to percutaneous absorption, improve elite
The utilization rate of liquid, obtains fermentation material；
（4）Fermentation material is filtered, is retained filtrate and filter residue, to alcoholic solution is added in filter residue, in 46 DEG C, 30kHz ultrasounds
Extract, filtering merges all filtrates, be concentrated under reduced pressure into alcohol-free, cross 0.1 μm of supermicro filtration membrane, improve recovery rate and raw material profit
With rate, production cost is saved, obtain extract solution；
（5）Extract solution is heated to 73 DEG C, raw material B is added, is well mixed, it is super through 0.08 ~ 0.1 μm of sheet frame through two sections of homogeneous
Microfiltration, reduces the molecular weight of nutritional ingredient, promotes absorption of the skin to Essence, obtains Huoshan rice dry measure used in former times Essence；
（6）Packing, radiation sterilization obtains finished product.
The step（4）Ultrasonic extraction, be repeatedly ultrasound 3 times, for the first time add volume fraction be 62% alcohol it is molten
Liquid, ultrasound 45 minutes adds the alcoholic solution that volume fraction is 73% for the second time, and ultrasound 30 minutes, third time adds volume fraction
It is 82% alcoholic solution, ultrasound 25 minutes is filtered after ultrasound every time.
The step（4）It is concentrated under reduced pressure, temperature is 46 DEG C, and pressure is 0 ~ 0.1MPa, and rotating speed is 65 revs/min.
The step（5）Two sections of homogeneous, first paragraph homogeneous：Temperature is 73 DEG C, pressure is 27.4MPa, second segment homogeneous：
Temperature is 57 DEG C, pressure is 15.8Mpa.
The application method of the Huoshan rice dry measure used in former times Essence, after evening cleaning face, after having smeared smoothing toner or toner, takes
2 ~ 3 drop Huoshan rice dry measure used in former times Essences are applied to face, massage 13 ~ 15 minutes, and cleaning face carries out normal skin care, and 2 are used weekly
~ 3 times, also can at night sleep in first 3 hours, take 2 ~ 3 drop Huoshan rice dry measure used in former times Essences and drunk in 40 ~ 80 DEG C of warm water,
1 times a week；The applicable crowd of Huoshan rice dry measure used in former times Essence, it is adaptable to any skin quality, the age at 23 years old and after, containing being conducive to
The medicinal herb componentses of development of fetus are prevented miscarriage and promote, pregnant woman and the women of nursing period can also be used.
Embodiment 2
A kind of Huoshan rice dry measure used in former times Essence, is made up of the raw material of following weight portion：
Raw material A：Huoshan meter dry measure used in former times 33, Artemisia stelleriana 9, rice chaff 9, Shorthairy Antenoron 6, Chinese pholidota pseudobulb or herb 6, pekoe 6, Chinese mugwort 6；Raw material B：Hippophae rhamnoides fruit oil
0.16th, vitamin C 0.07, vitamin E 0.06, glycyrrhizic acid 0.04；Raw material C：Mixed Microbes 4, complex enzyme 0.03；Described Huoshan
Rice dry measure used in former times, is fresh Huoshan rice dry measure used in former times, increases fresh fragrance and viscosity.
Described hippophae rhamnoides fruit oil, is that physical squeezing method is obtained, purity >=98%.
Described Mixed Microbes, are made up of the raw material of following weight portion：Wine yeast 19, Bifidobacterium 17, acidophilus breast bar
Bacterium 14, acetic acid bacteria 14, lactobacillus paracasei 7, aspergillus niger 7.
Described complex enzyme, is made up of the raw material of following weight portion：Cellulase 16, hemicellulase 11, AMS
8th, pectase 8.
Preparation and application, with embodiment 1.
Embodiment 3
A kind of Huoshan rice dry measure used in former times Essence, is made up of the raw material of following weight portion：
Raw material A：Huoshan meter dry measure used in former times 34, Artemisia stelleriana 10, rice chaff 10, Shorthairy Antenoron 7, Chinese pholidota pseudobulb or herb 7, pekoe 7, Chinese mugwort 7；Raw material B：Hippophae rhamnoides fruit oil
0.17th, vitamin C 0.08, vitamin E 0.07, glycyrrhizic acid 0.05；Raw material C：Mixed Microbes 5, complex enzyme 0.04；Described Huoshan
Rice dry measure used in former times, is fresh Huoshan rice dry measure used in former times, increases fresh fragrance and viscosity.
Described hippophae rhamnoides fruit oil, is that physical squeezing method is obtained, purity >=98%.
Described Mixed Microbes, are made up of the raw material of following weight portion：Wine yeast 20, Bifidobacterium 18, acidophilus breast bar
Bacterium 15, acetic acid bacteria 15, lactobacillus paracasei 8, aspergillus niger 8.
Described complex enzyme, is made up of the raw material of following weight portion：Cellulase 17, hemicellulase 12, AMS
9th, pectase 9.
Preparation and application, with embodiment 1.
Comparative example 1
Huoshan rice dry measure used in former times is changed to drying Huoshan rice dry measure used in former times, remaining preparation and application, with embodiment 1.
Comparative example 2
Removal Artemisia stelleriana, rice chaff, Shorthairy Antenoron, Chinese pholidota pseudobulb or herb, pekoe, Chinese mugwort, remaining preparation and application, with embodiment 1.
Comparative example 3
Removal hippophae rhamnoides fruit oil and glycyrrhizic acid, remaining preparation and application, with embodiment 1.
Comparative example 4
Removal Mixed Microbes and step（3）, remaining preparation and application, with embodiment 1.
Comparative example 5
Removal complex enzyme and step（2）, remaining preparation and application, with embodiment 1.
Comparative example 6
Removal step（4）In alcoholic solution ultrasonic extraction, remaining preparation and application, with embodiment 1.
Comparative example 7
Removal step（5）In two sections of homogeneous, remaining preparation and application, with embodiment 1.
Comparative example 8
Removal step（5）In sheet frame hyperfiltration, remaining preparation and application, with embodiment 1.
The sanitary index of rice dry measure used in former times Essence in Huoshan of the present invention：
The standard of the toner according to QB/T2660-2004, detects, the present invention to Huoshan of the invention rice dry measure used in former times Essence
The sanitary index of Huoshan rice dry measure used in former times Essence is shown in Table 1.
Table 1：The sanitary index of rice dry measure used in former times Essence in Huoshan of the present invention
| Project | The present invention | Standard |
| Total number of bacteria/（CFU/g） | 315 | ≤1000 |
| Excrement colibacillus group | Do not detect | Must not detect |
| Staphylococcus aureus | Do not detect | Must not detect |
| Pseudomonas aeruginosa | Do not detect | Must not detect |
| Lead/（mg/kg） | 2.2 | ≤40 |
| Mercury/（mg/kg） | 0.06 | ≤1 |
| Arsenic/（mg/kg） | 1.2 | ≤10 |
| Methyl alcohol/（mg/kg） | 398 | ≤2000 |
| Outward appearance | Uniform liquid, free from admixture | Uniform liquid, free from admixture |
| pH | 5.6~5.8 | 4.0~8.5 |
From the results shown in Table 1, the Huoshan rice dry measure used in former times Essence of the application meets the mark of the toner of QB/T2660-2004
Standard, safety and Health.
The skin effect of embodiment and comparative example Huoshan rice dry measure used in former times Essence：
（One）, test crowd
（1）, the age is between 25-40 Sui；
（2）, healthy, rule of life；
（3）, without skin disease and allergies.
According to mentioned above principle, the people of testing crew 180 being determined, being divided into 9 groups, the present invention and comparative example 1 ~ 8 are corresponded to respectively, it is left
Arm smears the Huoshan rice dry measure used in former times Essence of the present invention and comparative example, and right arm does not smear any Essence as blank control group right arm,
Every group of 20 people；
（Two）, test method
（1）, skin moisture content assay method：
Test environment temperature be 25 DEG C, relative humidity be 60 ~ 90%, measure tested position was exposed in first 10 minutes, while allow by
Inspection person keeps tranquil.2 square Experimental Areas of 4cm × 4cm are respectively marked on the forearm of left and right, left arm is smeared of the invention and right
The Huoshan rice dry measure used in former times Essence of ratio, right arm does not smear any Essence as blank control group right arm.Determined using moisture of skin
Instrument difference determination test region 5 times, records result, calculates average value；Consumption according to 1ml/cm smears this money Essence gently
After being massaged into absorption, measured respectively using moisture of skin tester at 0 and 240 minute, test out keratoderma water
Point content value (being represented with a.u.), and record test result.In order to preferably evaluate the data obtained, skin moisture-keeping is introduced
The concept of increase rate, will every time detect the difference with blank control group moisture content value using the moisture content value measured after product
Value, then divided by the moisture content value of blank control group, the result for obtaining as skin moisture-keeping increase rate.By calculating using this
Different time points moisture of skin percentage change after money Essence, can be very good to evaluate whether product has moistening effect,
Skin test the results are shown in Table 2.
（2）, skin elasticity assay method：
2 square Experimental Areas of 4cm × 4cm are respectively marked on the forearm of left and right, left arm smears the present invention and comparative example suddenly
Mountain rice dry measure used in former times Essence, right arm does not smear any Essence as blank control group right arm.Consumption according to 1ml/cm smears this money
After Essence is gently massaged into absorption, test section and check plot were entered respectively using skin elasticity tester at 0 and 240 minute
Row measurement.In order to preferably evaluate the data of gained, the concept of skin elasticity increase rate is introduced, will every time detect and use product
The difference of skin elasticity value when the skin elasticity value and blank control group that measure afterwards, then divided by the skin elasticity value of blank control group,
Acquired results are skin elasticity value increase rate.By calculating using this money Essence in different time points skin skin elasticity value
Percentage, can well evaluate product and whether have and keep skin elasticity effect, skin test the results are shown in Table 2.
Table 2：Skin test result
| Project | Moisture/（%） | Moisturizing increase rate/（%） | Elasticity/（%） | Elastic increase rate/（%） |
| The present invention | 68.3 | 99.7 | 1.8 | 50.0 |
| Comparative example 1 | 56.4 | 65.0 | 1.6 | 33.3 |
| Comparative example 2 | 51.6 | 50.9 | 1.5 | 25.0 |
| Comparative example 3 | 52.5 | 53.5 | 1.5 | 25.0 |
| Comparative example 4 | 50.3 | 47.1 | 1.5 | 25.0 |
| Comparative example 5 | 51.8 | 51.5 | 1.6 | 33.3 |
| Comparative example 6 | 52.7 | 54.1 | 1.5 | 25.0 |
| Comparative example 7 | 60.3 | 76.3 | 1.7 | 41.7 |
| Comparative example 8 | 62.5 | 82.7 | 1.6 | 33.3 |
| Blank control group | 34.2 | — | 1.2 | — |
Show from the result of table 2, embodiment Huoshan rice dry measure used in former times Essence, subject can be significantly improved after skin and water content and
Elasticity, illustrating the Huoshan rice dry measure used in former times Essence of present invention offer has obvious moisturizing and anti-wrinkle effect.
Claims (9)
1. a kind of Huoshan rice dry measure used in former times Essence, it is characterised in that be made up of the raw material of following weight portion：
Raw material A：Huoshan meter dry measure used in former times 32 ~ 34, Artemisia stelleriana 8 ~ 10, rice chaff 8 ~ 10, Shorthairy Antenoron 5 ~ 7, Chinese pholidota pseudobulb or herb 5 ~ 7, pekoe 5 ~ 7, Chinese mugwort 5 ~
7；
Raw material B：Hippophae rhamnoides fruit oil 0.15 ~ 0.17, vitamin C 0.06 ~ 0.08, vitamin E 0.05 ~ 0.07, glycyrrhizic acid 0.04 ~
0.05；
Raw material C：Mixed Microbes 3 ~ 5, complex enzyme 0.02 ~ 0.04；
Described Huoshan rice dry measure used in former times, is fresh Huoshan rice dry measure used in former times, increases fresh fragrance and viscosity.
2. according to claim 1 Huoshan rice dry measure used in former times Essence, it is characterised in that described hippophae rhamnoides fruit oil, is physical squeezing method
It is obtained, purity >=98%.
3. according to claim 1 Huoshan rice dry measure used in former times Essence, it is characterised in that described Mixed Microbes, by following weight portion
Raw material is constituted：Wine yeast 18 ~ 20, Bifidobacterium 16 ~ 18, lactobacillus acidophilus 13 ~ 15, acetic acid bacteria 13 ~ 15, secondary cheese breast bar
Bacterium 6 ~ 8, aspergillus niger 6 ~ 8.
4. according to claim 1 Huoshan rice dry measure used in former times Essence, it is characterised in that described complex enzyme, by following weight portion
Raw material is constituted：Cellulase 15 ~ 17, hemicellulase 10 ~ 12, AMS 7 ~ 9, pectase 7 ~ 9.
5. the preparation method of a kind of Huoshan according to claim 1 rice dry measure used in former times Essence, it is characterised in that comprise the following steps：
（1）Raw material A is cleaned, 80 ~ 100 mesh are crushed to, blanching 40 ~ 60 seconds in steam are placed in, crushed material is obtained；
（2）To 5 ~ 7 times of water of amount of raw material A weight are added in crushed material, it is well mixed, adds complex enzyme, is heated to 40 ~ 42 DEG C,
Stirring enzymolysis 180 ~ 200 minutes, is heated to 80 ~ 85 DEG C, is incubated 10 ~ 12 minutes, must digest material；
（3）To Mixed Microbes are added in enzymolysis material, stir, fermented 16 ~ 18 hours in 32 ~ 34 DEG C, be cooled to 19 ~ 21 DEG C, stir
Mix uniform, continue to ferment 8 ~ 9 days, then reduce temperature to 2 ~ 4 DEG C, stand 10 ~ 12 hours, obtain fermentation material；
（4）Fermentation material is filtered, is retained filtrate and filter residue, to adding alcoholic solution in filter residue, in 46 ~ 48 DEG C, 28 ~
30kHz ultrasonic extractions, filtering merges all filtrates, is concentrated under reduced pressure into alcohol-free, 0.1 μm excessively of supermicro filtration membrane, obtains extract solution；
（5）Extract solution is heated to 72 ~ 74 DEG C, raw material B is added, is well mixed, through two sections of homogeneous, through 0.08 ~ 0.1 μm of sheet frame
Hyperfiltration, obtains Huoshan rice dry measure used in former times Essence；
（6）Packing, radiation sterilization obtains finished product.
6. according to claim 5 Huoshan rice dry measure used in former times Essence preparation method, it is characterised in that the step（4）Ultrasound
Extract, be ultrasound 3 times repeatedly, the alcoholic solution that volume fraction is 61 ~ 63%, ultrasound 40 ~ 45 minutes, second are added for the first time
Addition volume fraction is 72 ~ 74% alcoholic solution, and ultrasound 30 ~ 35 minutes, third time adds the alcohol that volume fraction is 81 ~ 83%
Solution, ultrasound 25 ~ 30 minutes is filtered after ultrasound every time.
7. according to claim 5 Huoshan rice dry measure used in former times Essence preparation method, it is characterised in that the step（4）Decompression
Concentration, temperature is 46 ~ 48 DEG C, and pressure is 0 ~ 0.1MPa, and rotating speed is 60 ~ 65 revs/min.
8. according to claim 5 Huoshan rice dry measure used in former times Essence preparation method, it is characterised in that the step（5）Two sections
Homogeneous, first paragraph homogeneous：Temperature is 71 ~ 73 DEG C, pressure is 26.6 ~ 28.4MPa, second segment homogeneous：Temperature is 56 ~ 58 DEG C, pressure
Power is 14.2 ~ 16.8Mpa.
9. according to any one of claim 1 ~ 7 Huoshan rice dry measure used in former times Essence application method, Huoshan rice dry measure used in former times Essence
Application method, after evening cleaning face, after having smeared smoothing toner or toner, takes 2 ~ 3 drop Huoshan rice dry measure used in former times Essences and is applied to face
Portion, massages 13 ~ 15 minutes, cleaning face, carries out normal skin care, weekly using 2 ~ 3 times, can also sleep at night first 3 hours
It is interior, take 2 ~ 3 drop Huoshan rice dry measure used in former times Essences and drunk in 40 ~ 80 DEG C of warm water, 1 times a week；The Huoshan rice dry measure used in former times Essence
Applicable crowd, it is adaptable to any skin quality, the age at 23 years old and after, containing the Chinese herbal medicine for being conducive to preventing miscarriage and promoting development of fetus
The women of composition, pregnant woman and nursing period can also be used.
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|---|---|---|---|---|
| CN103957885A (en) * | 2011-09-14 | 2014-07-30 | 奈夫利公司 | Herbal skin care composition |
| CN105963206A (en) * | 2016-06-24 | 2016-09-28 | 霍山县众康堂中药材开发有限公司 | Facial mask with dendrobium huoshanense and method for preparing facial mask |
| CN105997689A (en) * | 2016-06-30 | 2016-10-12 | 广西健宝石斛有限责任公司 | Dendrobium officinale cream and preparation method thereof |
| CN106344478A (en) * | 2016-11-11 | 2017-01-25 | 福建师范大学 | Preparation method of dendrobium officinale extractive used for cosmetics |
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2017
- 2017-03-09 CN CN201710138804.1A patent/CN106890128A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103957885A (en) * | 2011-09-14 | 2014-07-30 | 奈夫利公司 | Herbal skin care composition |
| CN105963206A (en) * | 2016-06-24 | 2016-09-28 | 霍山县众康堂中药材开发有限公司 | Facial mask with dendrobium huoshanense and method for preparing facial mask |
| CN105997689A (en) * | 2016-06-30 | 2016-10-12 | 广西健宝石斛有限责任公司 | Dendrobium officinale cream and preparation method thereof |
| CN106344478A (en) * | 2016-11-11 | 2017-01-25 | 福建师范大学 | Preparation method of dendrobium officinale extractive used for cosmetics |
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Application publication date: 20170627 |