CN106239664A - A kind of high temperature resistant aging resistance straw treatment fluid and preparation method thereof - Google Patents
A kind of high temperature resistant aging resistance straw treatment fluid and preparation method thereof Download PDFInfo
- Publication number
- CN106239664A CN106239664A CN201610723628.3A CN201610723628A CN106239664A CN 106239664 A CN106239664 A CN 106239664A CN 201610723628 A CN201610723628 A CN 201610723628A CN 106239664 A CN106239664 A CN 106239664A
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- CN
- China
- Prior art keywords
- high temperature
- treatment fluid
- temperature resistant
- water
- aging resistance
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/52—Impregnating agents containing mixtures of inorganic and organic compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/007—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process employing compositions comprising nanoparticles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K9/00—Chemical or physical treatment of reed, straw, or similar material
- B27K9/007—Straw
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K2240/00—Purpose of the treatment
- B27K2240/20—Removing fungi, molds or insects
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K2240/00—Purpose of the treatment
- B27K2240/50—Ageing
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K2240/00—Purpose of the treatment
- B27K2240/70—Hydrophobation treatment
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Forests & Forestry (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Nanotechnology (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The invention discloses a kind of high temperature resistant aging resistance straw treatment fluid, it is to be prepared by the raw material of following weight parts: Tissuemat E 35, nano aluminium oxide 35, dimethicone 12, peregal o 10 0.4 0.6, rosin glyceride 0.3 0.5, Butylated hydroxyanisole 0.01 0.02, modified polyvinyl chloride emulsion 10 15, triethanolamine borate 0.3 0.5, tetramethylolmethane 0.3 0.5, water 40 50.The straw treatment fluid of the present invention can form the coating of clear homogeneous on straw surface, and it is water-fast, water vapour permeability is excellent, and stalk material plays good protective action, is difficult to make moist, go mouldy.There is high temperature resistant age inhibiting feature simultaneously, can protect stalk material under higher temperature conditions life-time service, storage and do not affect its performance, contribute to expansive approach scope.
Description
Technical field
The present invention relates to straw technical field of surface, particularly relate to a kind of high temperature resistant aging resistance straw treatment fluid and
Preparation method.
Background technology
China is large agricultural country, and stalk resource is the abundantest, and distribution is wide, and kind is many and yield is huge.At present, crops straw
The processing mode of the stalk overwhelming majority is to process at direct open incineration, and this not only causes the great wasting of resources, and causes big
Gas pollutes, and affects atmosphere quality.Straw has the advantages that quality is pliable and tough, cheap, is suitable for weaving industry, makes grass
Kinds of processes product and the article of everyday use such as cap, straw mat, hand basket, extension picture, can make full use of existing resource, alleviates ambient pressure, again can
Develop the value of straw substantially, meet consumer's market demand to baskets craft.But straw is as one
Vegetable material, its resistance to water is poor, is susceptible to go rotten, deliquescence, it is difficult to long-term preserve and uses, and resistance to elevated temperatures is poor, height
Being susceptible to aging under the conditions of temperature, serviceability declines, and have impact on the using value of straw baskets craft.
Summary of the invention
The object of the invention is contemplated to make up the defect of prior art, it is provided that a kind of high temperature resistant aging resistance straw treatment fluid and
Its preparation method.
The present invention is achieved by the following technical solutions:
A kind of high temperature resistant aging resistance straw treatment fluid, it is to be prepared by the raw material of following weight parts:
Tissuemat E 3-5, nano aluminium oxide 3-5, dimethicone 1-2, peregal o-10 0.4-0.6, rosin glyceride 0.3-
0.5, Butylated hydroxyanisole 0.01-0.02, modified polyvinyl chloride emulsion 10-15, triethanolamine borate 0.3-0.5, season penta
Tetrol 0.3-0.5, water 40-50；
Wherein modified polyvinyl chloride emulsion is prepared by the raw materials in: vinyl chloride 10-15, acrylic acid 3-5, and carboxymethyl is fine
Dimension element 0.5-1, trifluoro propyl methyl cyclotrisiloxane 0.3-0.5, potassium peroxydisulfate 0.01-0.02, nano titanium oxide 1-2, ten
Sodium dialkyl sulfate 0.05-0.1, water 20-30；The preparation method of modified polyvinyl chloride emulsion be first by sodium lauryl sulphate and
Carboxymethyl cellulose be added to the water stirring until being completely dissolved, be subsequently adding vinyl chloride, acrylic acid, nano titanium oxide and trifluoro
Hydroxypropyl methyl cyclotrisiloxane 800-1000r/min stirs 0.5-1h, is eventually adding remaining raw material 70-80 DEG C reaction 2-4h, cold
The most afterwards and get final product.
The preparation method of a kind of high temperature resistant aging resistance straw treatment fluid, comprises the following steps:
(1) by Tissuemat E, nano aluminium oxide, dimethicone, Butylated hydroxyanisole, peregal o-10 and rosin glyceride
Common addition adds 90-95 DEG C, 800-1000r/min stirring in the water that 1/2-2/3 measures after 110-120 DEG C of melting mixing in container
0.5-1h, adds modified polyvinyl chloride emulsion and stirs, obtain complex emulsions after cooling；
(2) 400-600r/min, 60-80 DEG C of stirring 0.5-1h after being mixed by remaining raw material, adds the Composite Milk in (1) after cooling
Liquid 1000-1500r/min stirs 5-10min, obtains high temperature resistant aging resistance straw treatment fluid.
The invention have the advantage that
The present invention improves poisture-penetrability by acrylic acid and Modified by Carboxymethyl Cellulose, is changed by trifluoro propyl methyl cyclotrisiloxane
Property improve resistance to water, by compound ageing resistance and the mechanical property of improving of nano titanium oxide, prepared modified polyvinyl chloride breast
Obtaining straw treatment fluid after liquid is compounding with remaining raw material, can form the coating of clear homogeneous on straw surface, it is water-fast, poisture-penetrability
Can be excellent, stalk material is played good protective action, is difficult to make moist, go mouldy.There is high temperature resistant age inhibiting feature simultaneously,
Can protect stalk material under higher temperature conditions life-time service, storage and do not affect its performance, contribute to expansive approach scope.
Detailed description of the invention
A kind of high temperature resistant aging resistance straw treatment fluid, it is to be prepared by the raw material of following weight parts:
Tissuemat E 3, nano aluminium oxide 3, dimethicone 1, peregal o-10 0.4, rosin glyceride 0.3, butylhydroxy fennel
Fragrant ether 0.01, modified polyvinyl chloride emulsion 10, triethanolamine borate 0.3, tetramethylolmethane 0.3, water 40；
Wherein modified polyvinyl chloride emulsion is prepared by the raw materials in: vinyl chloride 10, acrylic acid 3, carboxymethyl cellulose
0.5, trifluoro propyl methyl cyclotrisiloxane 0.3, potassium peroxydisulfate 0.01, nano titanium oxide 1, sodium lauryl sulphate 0.05,
Water 20；The preparation method of modified polyvinyl chloride emulsion is first sodium lauryl sulphate and carboxymethyl cellulose to be added to the water stirring
Until being completely dissolved, it is subsequently adding vinyl chloride, acrylic acid, nano titanium oxide and trifluoro propyl methyl cyclotrisiloxane 800r/
Min stirs 0.5h, is eventually adding remaining raw material 70 DEG C reaction 2h, after cooling and get final product.
The preparation method of a kind of high temperature resistant aging resistance straw treatment fluid, comprises the following steps:
(1) by Tissuemat E, nano aluminium oxide, dimethicone, Butylated hydroxyanisole, peregal o-10 and rosin glyceride
Common add in the water adding 1/2 amount in container after 110 DEG C of melting mixing 90 DEG C, 800r/min stir 0.5h, addition after cooling
Modified polyvinyl chloride emulsion stirs, and obtains complex emulsions；
(2) after being mixed by remaining raw material, 400r/min, 60 DEG C of stirring 0.5h, add the complex emulsions 1000r/ in (1) after cooling
Min stirs 5min, obtains high temperature resistant aging resistance straw treatment fluid.
Above-mentioned prepared straw treatment fluid is carried out performance test, and result is as follows:
| Project | Testing result |
| Appearance of film | Normally |
| Transparency | Excellent |
| Fineness (μm) | ≤10 |
| Bin stability (50 DEG C) | Without exception |
| Resistance to water (24h) | Without exception |
| Boiling water resistance (15min) | Without exception |
Claims (2)
1. a high temperature resistant aging resistance straw treatment fluid, it is characterised in that it is to be prepared by the raw material of following weight parts:
Tissuemat E 3-5, nano aluminium oxide 3-5, dimethicone 1-2, peregal o-10 0.4-0.6, rosin glyceride 0.3-
0.5, Butylated hydroxyanisole 0.01-0.02, modified polyvinyl chloride emulsion 10-15, triethanolamine borate 0.3-0.5, season penta
Tetrol 0.3-0.5, water 40-50；
Described modified polyvinyl chloride emulsion is prepared by the raw materials in: vinyl chloride 10-15, acrylic acid 3-5, and carboxymethyl is fine
Dimension element 0.5-1, trifluoro propyl methyl cyclotrisiloxane 0.3-0.5, potassium peroxydisulfate 0.01-0.02, nano titanium oxide 1-2, ten
Sodium dialkyl sulfate 0.05-0.1, water 20-30；The preparation method of modified polyvinyl chloride emulsion be first by sodium lauryl sulphate and
Carboxymethyl cellulose be added to the water stirring until being completely dissolved, be subsequently adding vinyl chloride, acrylic acid, nano titanium oxide and trifluoro
Hydroxypropyl methyl cyclotrisiloxane 800-1000r/min stirs 0.5-1h, is eventually adding remaining raw material 70-80 DEG C reaction 2-4h, cold
The most afterwards and get final product.
The preparation method of a kind of high temperature resistant aging resistance straw treatment fluid the most according to claim 1, it is characterised in that include
Following steps:
(1) by Tissuemat E, nano aluminium oxide, dimethicone, Butylated hydroxyanisole, peregal o-10 and rosin glyceride
Common addition adds 90-95 DEG C, 800-1000r/min stirring in the water that 1/2-2/3 measures after 110-120 DEG C of melting mixing in container
0.5-1h, adds modified polyvinyl chloride emulsion and stirs, obtain complex emulsions after cooling；
(2) 400-600r/min, 60-80 DEG C of stirring 0.5-1h after being mixed by remaining raw material, adds the Composite Milk in (1) after cooling
Liquid 1000-1500r/min stirs 5-10min, obtains high temperature resistant aging resistance straw treatment fluid.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610723628.3A CN106239664A (en) | 2016-08-25 | 2016-08-25 | A kind of high temperature resistant aging resistance straw treatment fluid and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610723628.3A CN106239664A (en) | 2016-08-25 | 2016-08-25 | A kind of high temperature resistant aging resistance straw treatment fluid and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106239664A true CN106239664A (en) | 2016-12-21 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610723628.3A Pending CN106239664A (en) | 2016-08-25 | 2016-08-25 | A kind of high temperature resistant aging resistance straw treatment fluid and preparation method thereof |
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| CN (1) | CN106239664A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107139294A (en) * | 2017-05-10 | 2017-09-08 | 安徽持家汉家居工艺品有限公司 | A kind of renovation method of outmoded modeling rattan cradle |
| CN108313984A (en) * | 2018-01-09 | 2018-07-24 | 朱勇 | A kind of small space elevator slow-release oxygenate |
| CN108328579A (en) * | 2018-01-09 | 2018-07-27 | 朱勇 | A kind of preparation method of small space elevator slow-release oxygenate |
| CN108394352A (en) * | 2018-03-20 | 2018-08-14 | 安徽三联学院 | Car surface protecting film and its spray coating liquor used |
| CN108504101A (en) * | 2018-03-28 | 2018-09-07 | 天长市蓝天复合材料有限公司 | A kind of high Anti-corrosion glass steel grating and preparation method |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1618866A (en) * | 2004-10-11 | 2005-05-25 | 华东理工大学 | Preparation method of polyvinyl chloride/inorganic rigid particle composite resin |
| CN103254797A (en) * | 2013-04-18 | 2013-08-21 | 东莞大宝化工制品有限公司 | Photocatalyst water wax and preparation method thereof |
-
2016
- 2016-08-25 CN CN201610723628.3A patent/CN106239664A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1618866A (en) * | 2004-10-11 | 2005-05-25 | 华东理工大学 | Preparation method of polyvinyl chloride/inorganic rigid particle composite resin |
| CN103254797A (en) * | 2013-04-18 | 2013-08-21 | 东莞大宝化工制品有限公司 | Photocatalyst water wax and preparation method thereof |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107139294A (en) * | 2017-05-10 | 2017-09-08 | 安徽持家汉家居工艺品有限公司 | A kind of renovation method of outmoded modeling rattan cradle |
| CN108313984A (en) * | 2018-01-09 | 2018-07-24 | 朱勇 | A kind of small space elevator slow-release oxygenate |
| CN108328579A (en) * | 2018-01-09 | 2018-07-27 | 朱勇 | A kind of preparation method of small space elevator slow-release oxygenate |
| CN108394352A (en) * | 2018-03-20 | 2018-08-14 | 安徽三联学院 | Car surface protecting film and its spray coating liquor used |
| CN108394352B (en) * | 2018-03-20 | 2019-09-13 | 安徽三联学院 | Car surface protecting film and its spray coating liquor used |
| CN108504101A (en) * | 2018-03-28 | 2018-09-07 | 天长市蓝天复合材料有限公司 | A kind of high Anti-corrosion glass steel grating and preparation method |
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Application publication date: 20161221 |
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