CN106182279A - A kind of antibacterial deodouring straw treatment fluid and preparation method thereof - Google Patents

A kind of antibacterial deodouring straw treatment fluid and preparation method thereof Download PDF

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Publication number
CN106182279A
CN106182279A CN201610723728.6A CN201610723728A CN106182279A CN 106182279 A CN106182279 A CN 106182279A CN 201610723728 A CN201610723728 A CN 201610723728A CN 106182279 A CN106182279 A CN 106182279A
Authority
CN
China
Prior art keywords
treatment fluid
water
polyvinyl chloride
modified polyvinyl
straw treatment
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610723728.6A
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Chinese (zh)
Inventor
李永兴
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
FU'NAN YONGXING ARTS & CRAFTS Co Ltd
Original Assignee
FU'NAN YONGXING ARTS & CRAFTS Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by FU'NAN YONGXING ARTS & CRAFTS Co Ltd filed Critical FU'NAN YONGXING ARTS & CRAFTS Co Ltd
Priority to CN201610723728.6A priority Critical patent/CN106182279A/en
Publication of CN106182279A publication Critical patent/CN106182279A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/52Impregnating agents containing mixtures of inorganic and organic compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K9/00Chemical or physical treatment of reed, straw, or similar material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K2240/00Purpose of the treatment
    • B27K2240/20Removing fungi, molds or insects

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  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Forests & Forestry (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a kind of antibacterial deodouring straw treatment fluid, it is to be prepared by the raw material of following weight parts: nanometer jade powder 24, nano medical stone powder 24, Tissuemat E 35, peregal o 10 0.4 0.6, glycerol monolaurate 0.3 0.5, decanoyl/octanoyl glycerides 0.3 0.5, modified polyvinyl chloride emulsion 10 15, sodium gluconate 12, carboxymethyl chitosan 0.2 0.4, water 40 50.The straw treatment fluid of the present invention can form the coating of clear homogeneous on straw surface, and it is water-fast, water vapour permeability is excellent, and stalk material plays good protective action, is difficult to make moist, go mouldy.There is effect of antibacterial deodorizing, beneficially environmental health and health simultaneously, practical.

Description

A kind of antibacterial deodouring straw treatment fluid and preparation method thereof
Technical field
The present invention relates to straw technical field of surface, particularly relate to a kind of antibacterial deodouring straw treatment fluid and preparation thereof Method.
Background technology
China is large agricultural country, and stalk resource is the abundantest, and distribution is wide, and kind is many and yield is huge.At present, crops straw The processing mode of the stalk overwhelming majority is to process at direct open incineration, and this not only causes the great wasting of resources, and causes big Gas pollutes, and affects atmosphere quality.Straw has the advantages that quality is pliable and tough, cheap, is suitable for weaving industry, makes grass Kinds of processes product and the article of everyday use such as cap, straw mat, hand basket, extension picture, can make full use of existing resource, alleviates ambient pressure, again can Develop the value of straw substantially, meet consumer's market demand to baskets craft.But straw is as one Vegetable material, its resistance to water is poor, is susceptible to go rotten, deliquescence, it is difficult to long-term preserve and uses, and the microorganisms such as antibacterial are held Easily grow on surface, produce abnormal flavour, be unfavorable for the health of user, have impact on the using value of straw baskets craft.
Summary of the invention
The object of the invention is contemplated to make up the defect of prior art, it is provided that a kind of antibacterial deodouring straw treatment fluid and system thereof Preparation Method.
The present invention is achieved by the following technical solutions:
A kind of antibacterial deodouring straw treatment fluid, it is to be prepared by the raw material of following weight parts:
Nanometer jade powder 2-4, nano medical stone powder 2-4, Tissuemat E 3-5, peregal o-10 0.4-0.6, lauric monoglyceride Ester 0.3-0.5, decanoyl/octanoyl glycerides 0.3-0.5, modified polyvinyl chloride emulsion 10-15, sodium gluconate 1-2, carboxymethyl chitosan Sugar 0.2-0.4, water 40-50;
Wherein modified polyvinyl chloride emulsion is prepared by the raw materials in: vinyl chloride 10-15, acrylic acid 3-5, and carboxymethyl is fine Dimension element 0.5-1, trifluoro propyl methyl cyclotrisiloxane 0.3-0.5, potassium peroxydisulfate 0.01-0.02, nano titanium oxide 1-2, ten Sodium dialkyl sulfate 0.05-0.1, water 20-30;The preparation method of modified polyvinyl chloride emulsion be first by sodium lauryl sulphate and Carboxymethyl cellulose be added to the water stirring until being completely dissolved, be subsequently adding vinyl chloride, acrylic acid, nano titanium oxide and trifluoro Hydroxypropyl methyl cyclotrisiloxane 800-1000r/min stirs 0.5-1h, is eventually adding remaining raw material 70-80 DEG C reaction 2-4h, cold The most afterwards and get final product.
The preparation method of a kind of antibacterial deodouring straw treatment fluid, comprises the following steps:
(1) by sweet to Tissuemat E, nanometer jade powder, nano medical stone powder, peregal o-10, decanoyl/octanoyl glycerides and lauric acid list Grease adds 90-95 DEG C, 800-1000r/min in the water adding 1/2-2/3 amount in container after 110-120 DEG C of melting mixing jointly Stirring 0.5-1h, adds modified polyvinyl chloride emulsion and stirs, obtain complex emulsions after cooling;
(2) 400-600r/min, 60-80 DEG C of stirring 0.5-1h after being mixed by remaining raw material, adds the Composite Milk in (1) after cooling Liquid 1000-1500r/min stirs 5-10min, obtains antibacterial deodouring straw treatment fluid.
The invention have the advantage that
The present invention improves poisture-penetrability by acrylic acid and Modified by Carboxymethyl Cellulose, is changed by trifluoro propyl methyl cyclotrisiloxane Property improve resistance to water, by compound ageing resistance and the mechanical property of improving of nano titanium oxide, prepared modified polyvinyl chloride breast Obtaining straw treatment fluid after liquid is compounding with remaining raw material, can form the coating of clear homogeneous on straw surface, it is water-fast, poisture-penetrability Can be excellent, stalk material is played good protective action, is difficult to make moist, go mouldy.There is effect of antibacterial deodorizing simultaneously, have It is beneficial to environmental health and health, practical.
Detailed description of the invention
A kind of antibacterial deodouring straw treatment fluid, it is to be prepared by the raw material of following weight parts:
Nanometer jade powder 2, nano medical stone powder 2, Tissuemat E 3, peregal o-10 0.4, glycerol monolaurate 0.3, the pungent last of the ten Heavenly stems Acid glyceride 0.3, modified polyvinyl chloride emulsion 10, sodium gluconate 1, carboxymethyl chitosan 0.2, water 40;
Wherein modified polyvinyl chloride emulsion is prepared by the raw materials in: vinyl chloride 10, acrylic acid 3, carboxymethyl cellulose 0.5, trifluoro propyl methyl cyclotrisiloxane 0.3, potassium peroxydisulfate 0.01, nano titanium oxide 1, sodium lauryl sulphate 0.05, Water 20;The preparation method of modified polyvinyl chloride emulsion is first sodium lauryl sulphate and carboxymethyl cellulose to be added to the water stirring Until being completely dissolved, it is subsequently adding vinyl chloride, acrylic acid, nano titanium oxide and trifluoro propyl methyl cyclotrisiloxane 800r/ Min stirs 0.5h, is eventually adding remaining raw material 70 DEG C reaction 2h, after cooling and get final product.
The preparation method of a kind of antibacterial deodouring straw treatment fluid, comprises the following steps:
(1) by sweet to Tissuemat E, nanometer jade powder, nano medical stone powder, peregal o-10, decanoyl/octanoyl glycerides and lauric acid list Grease jointly add in container in the water adding 1/2 amount after 110 DEG C of melting mixing 90 DEG C, 800r/min stir 0.5h, after cooling Add modified polyvinyl chloride emulsion to stir, obtain complex emulsions;
(2) after being mixed by remaining raw material, 400r/min, 60 DEG C of stirring 0.5h, add the complex emulsions 1000r/ in (1) after cooling Min stirs 5min, obtains antibacterial deodouring straw treatment fluid.
Above-mentioned prepared straw treatment fluid is carried out performance test, and result is as follows:
Project Testing result
Appearance of film Normally
Transparency Excellent
Fineness (μm) ≤10
Bin stability (50 DEG C) Without exception
Resistance to water (24h) Without exception

Claims (2)

1. an antibacterial deodouring straw treatment fluid, it is characterised in that it is to be prepared by the raw material of following weight parts:
Nanometer jade powder 2-4, nano medical stone powder 2-4, Tissuemat E 3-5, peregal o-10 0.4-0.6, lauric monoglyceride Ester 0.3-0.5, decanoyl/octanoyl glycerides 0.3-0.5, modified polyvinyl chloride emulsion 10-15, sodium gluconate 1-2, carboxymethyl chitosan Sugar 0.2-0.4, water 40-50;
Described modified polyvinyl chloride emulsion is prepared by the raw materials in: vinyl chloride 10-15, acrylic acid 3-5, and carboxymethyl is fine Dimension element 0.5-1, trifluoro propyl methyl cyclotrisiloxane 0.3-0.5, potassium peroxydisulfate 0.01-0.02, nano titanium oxide 1-2, ten Sodium dialkyl sulfate 0.05-0.1, water 20-30;The preparation method of modified polyvinyl chloride emulsion be first by sodium lauryl sulphate and Carboxymethyl cellulose be added to the water stirring until being completely dissolved, be subsequently adding vinyl chloride, acrylic acid, nano titanium oxide and trifluoro Hydroxypropyl methyl cyclotrisiloxane 800-1000r/min stirs 0.5-1h, is eventually adding remaining raw material 70-80 DEG C reaction 2-4h, cold The most afterwards and get final product.
The preparation method of a kind of antibacterial deodouring straw treatment fluid the most according to claim 1, it is characterised in that include following Step:
(1) by sweet to Tissuemat E, nanometer jade powder, nano medical stone powder, peregal o-10, decanoyl/octanoyl glycerides and lauric acid list Grease adds 90-95 DEG C, 800-1000r/min in the water adding 1/2-2/3 amount in container after 110-120 DEG C of melting mixing jointly Stirring 0.5-1h, adds modified polyvinyl chloride emulsion and stirs, obtain complex emulsions after cooling;
(2) 400-600r/min, 60-80 DEG C of stirring 0.5-1h after being mixed by remaining raw material, adds the Composite Milk in (1) after cooling Liquid 1000-1500r/min stirs 5-10min, obtains antibacterial deodouring straw treatment fluid.
CN201610723728.6A 2016-08-25 2016-08-25 A kind of antibacterial deodouring straw treatment fluid and preparation method thereof Pending CN106182279A (en)

Priority Applications (1)

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CN201610723728.6A CN106182279A (en) 2016-08-25 2016-08-25 A kind of antibacterial deodouring straw treatment fluid and preparation method thereof

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Application Number Priority Date Filing Date Title
CN201610723728.6A CN106182279A (en) 2016-08-25 2016-08-25 A kind of antibacterial deodouring straw treatment fluid and preparation method thereof

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CN106182279A true CN106182279A (en) 2016-12-07

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107805976A (en) * 2017-10-27 2018-03-16 六安市九十里山水画廊有限公司 The preparation method of calligraphy and painting protection against the tide rice paper
CN107828258A (en) * 2017-10-27 2018-03-23 六安市九十里山水画廊有限公司 A kind of calligraphy and painting mounting anti-blushing agent
CN108556101A (en) * 2018-05-22 2018-09-21 天长市双丰文化用品有限公司 A kind of timber pretreating process for easel
CN114748668A (en) * 2022-05-13 2022-07-15 广州市康洁明环保科技有限公司 Preparation method of long-acting bacteriostatic aldehyde-removing deodorizing treatment fluid

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1618866A (en) * 2004-10-11 2005-05-25 华东理工大学 Preparation method of polyvinyl chloride/inorganic rigid particle composite resin
CN101284386A (en) * 2008-06-03 2008-10-15 浙江林学院 Nano wood antiseptics and manufacturing method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1618866A (en) * 2004-10-11 2005-05-25 华东理工大学 Preparation method of polyvinyl chloride/inorganic rigid particle composite resin
CN101284386A (en) * 2008-06-03 2008-10-15 浙江林学院 Nano wood antiseptics and manufacturing method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
李东光: "《装饰装修材料和建筑涂料配方与制备》", 30 November 2010, 中国纺织出版社 *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107805976A (en) * 2017-10-27 2018-03-16 六安市九十里山水画廊有限公司 The preparation method of calligraphy and painting protection against the tide rice paper
CN107828258A (en) * 2017-10-27 2018-03-23 六安市九十里山水画廊有限公司 A kind of calligraphy and painting mounting anti-blushing agent
CN108556101A (en) * 2018-05-22 2018-09-21 天长市双丰文化用品有限公司 A kind of timber pretreating process for easel
CN114748668A (en) * 2022-05-13 2022-07-15 广州市康洁明环保科技有限公司 Preparation method of long-acting bacteriostatic aldehyde-removing deodorizing treatment fluid

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Application publication date: 20161207