CN106346576A - High-weather-resistance straw treatment fluid and preparation method thereof - Google Patents
High-weather-resistance straw treatment fluid and preparation method thereof Download PDFInfo
- Publication number
- CN106346576A CN106346576A CN201610723714.4A CN201610723714A CN106346576A CN 106346576 A CN106346576 A CN 106346576A CN 201610723714 A CN201610723714 A CN 201610723714A CN 106346576 A CN106346576 A CN 106346576A
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- CN
- China
- Prior art keywords
- treatment fluid
- parts
- water
- straw
- emulsion
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/52—Impregnating agents containing mixtures of inorganic and organic compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/007—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process employing compositions comprising nanoparticles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K9/00—Chemical or physical treatment of reed, straw, or similar material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K2240/00—Purpose of the treatment
- B27K2240/20—Removing fungi, molds or insects
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K2240/00—Purpose of the treatment
- B27K2240/70—Hydrophobation treatment
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Forests & Forestry (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Nanotechnology (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a high-weather-resistance straw treatment fluid which is prepared from the following raw materials in parts by weight: 3-5 parts of polyethylene wax, 0.4-0.6 part of Peregal O-10, 1-2 parts of epoxy soybean oil, 0.1-0.2 part of pentalyn, 10-15 parts of modified polyvinyl chloride emulsion, 0.5-1 part of 2-hydroxy-4-methoxy diphenyl ketone, 3-5 parts of silicone-acrylic emulsion, 0.1-0.2 part of antioxidant BHT, 0.1-0.2 part of polyvinyl alcohol, 0.1-0.2 part of nonylphenol polyethenoxy ether and 40-50 parts of water. The straw treatment fluid can form a transparent uniform coating on the straw surface, has favorable water resistance and water vapor permeability, performs favorable protective functions on the straw material, and can not easily become damp or mildewy. The treatment fluid has favorable weather resistance, is applicable to different climate conditions, effectively resists aging and has long service life.
Description
Technical field
The present invention relates to straw technical field of surface, more particularly, to a kind of high-weatherability straw treatment fluid and its preparation
Method.
Background technology
China is large agricultural country, stalk resource very abundant, and distribution is wide, and species is many and yield is huge.At present, crops straw
The processing mode of the stalk overwhelming majority is to process in direct open incineration, and this not only causes the great wasting of resources, and leads to big
Gas pollutes, and affects atmosphere quality.Straw has the characteristics that quality is pliable and tough, cheap, is suitable for weaving industry, makes grass
Kinds of processes product and the article of everyday use such as cap, straw mat, hand basket, extension picture, can make full use of existing resource, alleviate ambient pressure, and energy
Substantially develop the value of straw, meet the market demand to baskets craft for the consumer.But straw is as one kind
Vegetable material, its resistance to water is poor, is susceptible to go rotten, deliquescence, and weatherability difference, it is difficult to long-term preserve and use, have impact on
The using value of straw baskets craft.
Content of the invention
The object of the invention is exactly the defect in order to make up prior art, provides a kind of high-weatherability straw treatment fluid and its system
Preparation Method.
The present invention is achieved by the following technical solutions:
A kind of high-weatherability straw treatment fluid, it is to be obtained by the raw material of following weight parts:
Tissuemat E 3-5, peregal o-10 0.4-0.6, epoxy soybean oil 1-2, pentalyn 0.1-0.2, modified poly-
Vinyl chloride emulsion 10-15, ESCALOL 567 0.5-1, silicone acrylic emulsion 3-5, antioxidant bht 0.1-0.2, gathers
Vinyl alcohol 0.1-0.2, NPE 0.1-0.2, water 40-50；
Wherein modified polyvinyl chloride emulsion is prepared by the raw materials in: vinyl chloride 10-15, acrylic acid 3-5, and carboxymethyl is fine
The plain 0.5-1 of dimension, trifluoro propyl methyl cyclotrisiloxane 0.3-0.5, potassium peroxydisulfate 0.01-0.02, nano titanium oxide 1-2, ten
Sodium dialkyl sulfate 0.05-0.1, water 20-30；The preparation method of modified polyvinyl chloride emulsion be first by sodium lauryl sulphate and
Carboxymethyl cellulose is added to the water stirring until being completely dissolved, and is subsequently adding vinyl chloride, acrylic acid, nano titanium oxide and trifluoro
Hydroxypropyl methyl cyclotrisiloxane 800-1000r/min stirs 0.5-1h, is eventually adding 70-80 DEG C of reaction 2-4h of remaining raw material, cold
But obtain final product afterwards.
A kind of preparation method of high-weatherability straw treatment fluid, comprises the following steps:
(1) Tissuemat E, epoxy soybean oil, antioxidant bht, peregal o-10 and pentalyn are added container jointly
Add 90-95 DEG C in the water of 1/2-2/3 amount after middle 110-120 DEG C of melting mixing, 800-1000r/min stirs 0.5-1h, cooling
Add modified polyvinyl chloride emulsion and silicone acrylic emulsion to stir afterwards, obtain complex emulsions；
(2) by 400-600r/min, 80-90 DEG C of stirring 0.5-1h after the mixing of remaining raw material, after cooling, add the Composite Milk in (1)
Liquid 1000-1500r/min stirs 5-10min, obtains final product high-weatherability straw treatment fluid.
The invention has the advantage that
The present invention passes through acrylic acid and Modified by Carboxymethyl Cellulose improves poisture-penetrability, is changed by trifluoro propyl methyl cyclotrisiloxane
Property improve resistance to water, be combined by nano titanium oxide and improve ageing resistance and mechanical property, prepared modified polyvinyl chloride breast
Liquid obtains straw treatment fluid after compounding with remaining raw material, can form the coating of clear homogeneous on straw surface, it is water-fast, poisture-penetrability
Can excellent, stalk material is played with good protective action, not moisture-sensitive, go mouldy.Weather resistance is good simultaneously, adapts to different gas
Use under the conditions of time, effective anti-aging, long service life.
Specific embodiment
A kind of high-weatherability straw treatment fluid, it is to be obtained by the raw material of following weight parts:
Tissuemat E 3, peregal o-10 0.4, epoxy soybean oil 1, pentalyn 0.1, modified polyvinyl chloride emulsion
10, ESCALOL 567 0.5, silicone acrylic emulsion 3, antioxidant bht 0.1, polyvinyl alcohol 0.1, polyoxyethylene nonyl phenyl
Vinyl Ether 0.1, water 40；
Wherein modified polyvinyl chloride emulsion is prepared by the raw materials in: vinyl chloride 10, acrylic acid 3, carboxymethyl cellulose
0.5, trifluoro propyl methyl cyclotrisiloxane 0.3, potassium peroxydisulfate 0.01, nano titanium oxide 1, sodium lauryl sulphate 0.05,
Water 20；The preparation method of modified polyvinyl chloride emulsion is first sodium lauryl sulphate and carboxymethyl cellulose to be added to the water stirring
Until being completely dissolved, it is subsequently adding vinyl chloride, acrylic acid, nano titanium oxide and trifluoro propyl methyl cyclotrisiloxane 800r/
Min stirs 0.5h, is eventually adding 70 DEG C of reaction 2h of remaining raw material, obtains final product after cooling.
A kind of preparation method of high-weatherability straw treatment fluid, comprises the following steps:
(1) Tissuemat E, epoxy soybean oil, antioxidant bht, peregal o-10 and pentalyn are added container jointly
In add 90 DEG C, 800r/min stirring 0.5h in the water of 1/2 amount, addition modified polyvinyl chloride after cooling after 110 DEG C of melting mixing
Emulsion and silicone acrylic emulsion stir, and obtain complex emulsions；
(2) by 400r/min, 80 DEG C of stirring 0.5h after the mixing of remaining raw material, after cooling, add the complex emulsions 1000r/ in (1)
Min stirs 5min, obtains final product high-weatherability straw treatment fluid.
Performance test is carried out to above-mentioned prepared straw treatment fluid, result is as follows:
| Project | Testing result |
| Appearance of film | Normally |
| Transparency | Excellent |
| Fineness (μm) | ≤10 |
| Bin stability (50 DEG C) | Without exception |
| Resistance to water (24h) | Without exception |
Claims (2)
1. a kind of high-weatherability straw treatment fluid is it is characterised in that it is to be obtained by the raw material of following weight parts:
Tissuemat E 3-5, peregal o-10 0.4-0.6, epoxy soybean oil 1-2, pentalyn 0.1-0.2, modified poly-
Vinyl chloride emulsion 10-15, ESCALOL 567 0.5-1, silicone acrylic emulsion 3-5, antioxidant bht 0.1-0.2, gathers
Vinyl alcohol 0.1-0.2, NPE 0.1-0.2, water 40-50；
Described modified polyvinyl chloride emulsion is prepared by the raw materials in: vinyl chloride 10-15, acrylic acid 3-5, and carboxymethyl is fine
The plain 0.5-1 of dimension, trifluoro propyl methyl cyclotrisiloxane 0.3-0.5, potassium peroxydisulfate 0.01-0.02, nano titanium oxide 1-2, ten
Sodium dialkyl sulfate 0.05-0.1, water 20-30；The preparation method of modified polyvinyl chloride emulsion be first by sodium lauryl sulphate and
Carboxymethyl cellulose is added to the water stirring until being completely dissolved, and is subsequently adding vinyl chloride, acrylic acid, nano titanium oxide and trifluoro
Hydroxypropyl methyl cyclotrisiloxane 800-1000r/min stirs 0.5-1h, is eventually adding 70-80 DEG C of reaction 2-4h of remaining raw material, cold
But obtain final product afterwards.
2. a kind of preparation method of high-weatherability straw treatment fluid according to claim 1 is it is characterised in that include following
Step:
(1) Tissuemat E, epoxy soybean oil, antioxidant bht, peregal o-10 and pentalyn are added container jointly
Add 90-95 DEG C in the water of 1/2-2/3 amount after middle 110-120 DEG C of melting mixing, 800-1000r/min stirs 0.5-1h, cooling
Add modified polyvinyl chloride emulsion and silicone acrylic emulsion to stir afterwards, obtain complex emulsions；
(2) by 400-600r/min, 80-90 DEG C of stirring 0.5-1h after the mixing of remaining raw material, after cooling, add the Composite Milk in (1)
Liquid 1000-1500r/min stirs 5-10min, obtains final product high-weatherability straw treatment fluid.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610723714.4A CN106346576A (en) | 2016-08-25 | 2016-08-25 | High-weather-resistance straw treatment fluid and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610723714.4A CN106346576A (en) | 2016-08-25 | 2016-08-25 | High-weather-resistance straw treatment fluid and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106346576A true CN106346576A (en) | 2017-01-25 |
Family
ID=57856164
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610723714.4A Pending CN106346576A (en) | 2016-08-25 | 2016-08-25 | High-weather-resistance straw treatment fluid and preparation method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN106346576A (en) |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104341914A (en) * | 2014-10-14 | 2015-02-11 | 凤阳徽亨商贸有限公司 | Dirt-resistant mold-resistant paint for glass doors and preparation method thereof |
-
2016
- 2016-08-25 CN CN201610723714.4A patent/CN106346576A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104341914A (en) * | 2014-10-14 | 2015-02-11 | 凤阳徽亨商贸有限公司 | Dirt-resistant mold-resistant paint for glass doors and preparation method thereof |
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| C06 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
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| RJ01 | Rejection of invention patent application after publication | ||
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Application publication date: 20170125 |