CN106235393A - Chinese medicine extract additive and the application in Nicotiana tabacum L. thereof - Google Patents
Chinese medicine extract additive and the application in Nicotiana tabacum L. thereof Download PDFInfo
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- CN106235393A CN106235393A CN201610871475.7A CN201610871475A CN106235393A CN 106235393 A CN106235393 A CN 106235393A CN 201610871475 A CN201610871475 A CN 201610871475A CN 106235393 A CN106235393 A CN 106235393A
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
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Abstract
The invention provides a kind of cigarette Chinese medicine extract additive, each taste Chinese medicines such as Flos Eriocauli in formula, Semen Fagopyri Esculenti, Folium Mori, Fructus Cannabis, Flos Sophorae, Semen Oroxyli, Herba Eupatorii, Radix Asteris with the use of, can reduce ammonia in main flume, phenol, carbon monoxide and the content of these harmful substances of nitrosamine, reduce the impact on health during cigarette smoking.Use production technology of the present invention can improve the fall evil effect of prepared Chinese medicine extract additive, reduce ammonia, phenol, carbon monoxide and the content of nitrosamines in flue gas further.The Chinese medicine extract additive that the present invention prepares does not interferes with the original suction quality of Medicated cigarette, also can significantly reduce the harmful substance in main flume, contrast with blank sample, ammonia in flue gas reduces more than 15%, phenol reduces more than 38%, CO reduces more than 8%, and nitrosamine reduces more than 25%.
Description
Technical field
The present invention relates to Field of Tobacco, particularly relate to a kind of Chinese medicine extract additive and the application in Nicotiana tabacum L. thereof.
Background technology
Along with becoming increasingly conspicuous of smoking and health problem and going deep into further of Harm reduction techniques fall Jiao's research application, Chinese herbal medicine
Cause the research in terms of disease achieved with breakthrough progress reducing cigarette smoke harmful substance with attenuating smoking.Medium-height grass
Medicine adds in cigarette products, makes Medicated cigarette have special function and can realize completely.China is the native place of Chinese herbal medicine, in
Chinese herbal medicine additive agent application in Chinese-style cigarette is the peculiar advantage of Chinese Tobacco Industry.
Ammonia is a kind of natural component in Nicotiana tabacum L..Owing to the Nicotiana tabacum L. in Medicated cigarette is in acid, so in Nicotiana tabacum L.
Ammonia is to exist with proton form, i.e. exists with the ammonium salts of natural carboxylic acid in Nicotiana tabacum L., otherwise can volatilize and escape.After result of combustion of tobacco
Although main flume in ammonia content far below in solid tobacco shred, but because it directly acts on human body, thus its hazardness is the most not
Hold and ignore.Not only affecting the jealous of Medicated cigarette due to ammonia, also can stimulate vision and the respiratory system of human body, long-term suction can be to human body
Cause serious harm, a kind of main harmful components in main flume after therefore ammonia is also considered as result of combustion of tobacco.
Summary of the invention
It is an object of the invention to provide a kind of Chinese medicine extract additive reducing harmful substance in Nicotiana tabacum L., and it is provided
Application process in Medicated cigarette.
The present invention uses following technical scheme:
A kind of Chinese medicine extract additive, its formula is: Flos Eriocauli 40-60 part, Semen Fagopyri Esculenti 75-85 part, Folium Mori 15-20 part,
Fructus Cannabis 10-20 part, Flos Sophorae 80-100 part, Semen Oroxyli 25-33 part, Herba Eupatorii 40-52 part, Radix Asteris 3-8 part, Radix Sophorae Tonkinensis 0.5-1.0
Part, Semen zanthoxyli 1-3 part, Folium Pini 1-5 part；
Its preparation method is:
1) Flos Eriocauli, Semen Fagopyri Esculenti, Folium Mori, Fructus Cannabis, Flos Sophorae, Semen Oroxyli, Herba Eupatorii are ground into coarse powder, add coarse powder weight 5-10
92% ethanol again, 80 DEG C of reflux, extract, 2h of constant temperature, leach extracting solution, filtering residue is permanent with 60% ethanol of coarse powder weight 3-5 times again
82 DEG C of reflux, extract, 1.5h of temperature, leach extracting solution, and gained filtering residue is again by 100 DEG C of reflux, extract, of water termostat of coarse powder weight 6-8 times
2h, leaches extracting solution, is merged by the extracting solution of three gained, obtains mixed extract；
2) Radix Asteris, Radix Sophorae Tonkinensis, Semen zanthoxyli, the Folium Pini water of 50-70 part impregnate 10-15h at 40-60 DEG C, filter, obtain filtrate；
3) by step 1) mixed extract and step 2) filtrate mix, stand 20-24h, re-evaporation is condensed into paste,
Obtain.
Number of the present invention is weight portion, and percentage ratio is mass percent.
The 0.1-1% that addition is tobacco shred weight, preferably 0.1-0.5% of described Chinese medicine extract additive.Specifically
, by above-mentioned additive ethanol dilution so that additive concentration in ethanol is 10%, then add cigarette with spray pattern
In Si, then according to common process produces Medicated cigarette, do not affect normal production process.
Each taste Chinese medicines such as Flos Eriocauli in inventive formulation, Semen Fagopyri Esculenti, Folium Mori, Fructus Cannabis, Flos Sophorae, Semen Oroxyli, Herba Eupatorii, Radix Asteris
With the use of, it is possible to decrease ammonia, phenol, carbon monoxide and the content of these harmful substances of nitrosamine in main flume, reduce Medicated cigarette
Impact on health in aspiration procedure.Use production technology of the present invention can improve prepared Chinese medicine extract to add
The fall evil effect of agent, reduces ammonia, phenol, carbon monoxide and the content of nitrosamines in flue gas further.
The Chinese medicine extract additive that the present invention prepares does not interferes with the original suction quality of Medicated cigarette, also can significantly reduce master
Stream flue gas in harmful substance, with blank sample contrast, the ammonia in flue gas reduces more than 15%, phenol reduce 38% with
On, CO reduces more than 8%, and nitrosamine reduces more than 25%.
Specific embodiment
Embodiment 1: a kind of Chinese medicine extract additive, its formula is: Flos Eriocauli 50 parts, 78 parts of Semen Fagopyri Esculenti, 16 parts of Folium Mori, fire
Fructus Cannabis 15 parts, 90 parts of Flos Sophorae, Semen Oroxyli 29 parts, Herba Eupatorii 48 parts, Radix Asteris 4 parts, Radix Sophorae Tonkinensis 0.6 part, Semen zanthoxyli 2 parts, 3 parts of Folium Pini；
Its preparation method is:
1) Flos Eriocauli, Semen Fagopyri Esculenti, Folium Mori, Fructus Cannabis, Flos Sophorae, Semen Oroxyli, Herba Eupatorii are ground into coarse powder, add coarse powder weight 8 times
92% ethanol, 80 DEG C of reflux, extract, 2h of constant temperature, leach extracting solution, filtering residue is again with 60% ethanol constant temperature 82 of coarse powder weight 4 times
DEG C reflux, extract, 1.5h, leaches extracting solution, and gained filtering residue by 100 DEG C of reflux, extract, 2h of water termostat of coarse powder weight 8 times, leaches again
Extracting solution, merges the extracting solution of three gained, obtains mixed extract；
2) Radix Asteris, Radix Sophorae Tonkinensis, Semen zanthoxyli, Folium Pini impregnate 12h with the water of 60 parts at 50 DEG C, filter, obtain filtrate；
3) by step 1) mixed extract and step 2) filtrate mix, stand 24h, re-evaporation is condensed into paste, i.e.
?.
Embodiment 2: a kind of Chinese medicine extract additive, its formula with embodiment 1, its preparation method is: Flos Eriocauli, buckwheat
Wheat, Folium Mori, Fructus Cannabis, Flos Sophorae, Semen Oroxyli, Herba Eupatorii, Radix Asteris, Radix Sophorae Tonkinensis, Semen zanthoxyli, Folium Pini with the water of 1200 parts at 50 DEG C of dippings
12h, filters, obtains filtrate, and filtrate evaporation and concentration becomes paste, to obtain final product.
Embodiment 3: a kind of Chinese medicine extract additive, its formula is: Flos Eriocauli 40 parts, 75 parts of Semen Fagopyri Esculenti, 15 parts of Folium Mori, fire
Fructus Cannabis 10 parts, 80 parts of Flos Sophorae, Semen Oroxyli 25 parts, Herba Eupatorii 40 parts, Radix Asteris 3 parts, Radix Sophorae Tonkinensis 0.5 part, Semen zanthoxyli 1 part, 1 part of Folium Pini；
Its preparation method is:
1) Flos Eriocauli, Semen Fagopyri Esculenti, Folium Mori, Fructus Cannabis, Flos Sophorae, Semen Oroxyli, Herba Eupatorii are ground into coarse powder, add coarse powder weight 5 times
92% ethanol, 80 DEG C of reflux, extract, 2h of constant temperature, leach extracting solution, filtering residue is again with 60% ethanol constant temperature 82 of coarse powder weight 3 times
DEG C reflux, extract, 1.5h, leaches extracting solution, and gained filtering residue by 100 DEG C of reflux, extract, 2h of water termostat of coarse powder weight 6 times, leaches again
Extracting solution, merges the extracting solution of three gained, obtains mixed extract；
2) Radix Asteris, Radix Sophorae Tonkinensis, Semen zanthoxyli, Folium Pini impregnate 10h with the water of 50 parts at 40 DEG C, filter, obtain filtrate；
3) by step 1) mixed extract and step 2) filtrate mix, stand 20h, re-evaporation is condensed into paste, i.e.
?.
Embodiment 4: a kind of Chinese medicine extract additive, its formula is: Flos Eriocauli 60 parts, 85 parts of Semen Fagopyri Esculenti, 20 parts of Folium Mori, fire
Fructus Cannabis 20 parts, 100 parts of Flos Sophorae, Semen Oroxyli 33 parts, Herba Eupatorii 52 parts, Radix Asteris 8 parts, Radix Sophorae Tonkinensis 1.0 parts, Semen zanthoxyli 3 parts, 5 parts of Folium Pini；
Its preparation method is:
1) Flos Eriocauli, Semen Fagopyri Esculenti, Folium Mori, Fructus Cannabis, Flos Sophorae, Semen Oroxyli, Herba Eupatorii are ground into coarse powder, add coarse powder weight 10 times
92% ethanol, 80 DEG C of reflux, extract, 2h of constant temperature, leach extracting solution, filtering residue is again with 60% ethanol constant temperature 82 of coarse powder weight 5 times
DEG C reflux, extract, 1.5h, leaches extracting solution, and gained filtering residue by 100 DEG C of reflux, extract, 2h of water termostat of coarse powder weight 8 times, leaches again
Extracting solution, merges the extracting solution of three gained, obtains mixed extract；
2) Radix Asteris, Radix Sophorae Tonkinensis, Semen zanthoxyli, Folium Pini impregnate 15h with the water of 70 parts at 60 DEG C, filter, obtain filtrate；
3) by step 1) mixed extract and step 2) filtrate mix, stand 24h, re-evaporation is condensed into paste, i.e.
?.
Experiment 1: add, in the ratio of the 0.3% of tobacco shred weight, the Chinese medicine extract additive that embodiment 1 prepares to cigarette
In Si, technique makes Medicated cigarette the most routinely.Through sensory evaluating smoking, the original style of sucking of Medicated cigarette is basically unchanged, and flue gas is surveyed
Test result shows: compared with the Medicated cigarette being not added with described Chinese medicine extract additive, the ammonia in its main flume reduces
20.6%, phenol reduces 48.2%, and CO reduces 12.8%, and nitrosamine reduces 37%, and harm reduction effect is obvious.
Experiment 2: add, in the ratio of the 0.1% of tobacco shred weight, the Chinese medicine extract additive that embodiment 2 prepares to cigarette
In Si, technique makes Medicated cigarette the most routinely.Through sensory evaluating smoking, the original style of sucking of Medicated cigarette is basically unchanged, and flue gas is surveyed
Test result shows: compared with the Medicated cigarette being not added with described Chinese medicine extract additive, the ammonia in its main flume reduces
8.3%, phenol reduces 23.9%, and CO reduces 3.4%, and nitrosamine reduces 14%, and harm reduction effect is obvious.
Experiment 3: add, in the ratio of the 0.5% of tobacco shred weight, the Chinese medicine extract additive that embodiment 3 prepares to cigarette
In Si, technique makes Medicated cigarette the most routinely.Through sensory evaluating smoking, the original style of sucking of Medicated cigarette is basically unchanged, and flue gas is surveyed
Test result shows: compared with the Medicated cigarette being not added with described Chinese medicine extract additive, the ammonia in its main flume reduces
15.2%, phenol reduces 41.5%, and CO reduces 11.5%, and nitrosamine reduces 28%, and harm reduction effect is obvious.
Experiment 4: add, in the ratio of the 0.5% of tobacco shred weight, the Chinese medicine extract additive that embodiment 4 prepares to cigarette
In Si, technique makes Medicated cigarette the most routinely.Through sensory evaluating smoking, the original style of sucking of Medicated cigarette is basically unchanged, and flue gas is surveyed
Test result shows: compared with the Medicated cigarette being not added with described Chinese medicine extract additive, the ammonia in its main flume reduces
17.8%, phenol reduces 38.3%, and CO reduces 8.7%, and nitrosamine reduces 26%, and harm reduction effect is obvious.
Further, by above-mentioned experimental data it can be seen that the Chinese medicine extract additive application for preparing of the present invention is in volume
In cigarette, on the premise of keeping smoking property of cigarette style to be basically unchanged, it is possible to effectively reduce in cigarette mainstream flue gas and side-stream smoke
The burst size of harmful substance, has the biggest Social benefit and economic benefit.
Last it is noted that above example is only in order to illustrate technical scheme, it is not intended to limit；Although
With reference to previous embodiment, the present invention is described in detail, it will be understood by those within the art that: it still may be used
So that the technical scheme described in foregoing embodiments to be modified, or wherein portion of techniques feature is carried out equivalent.
Claims (3)
1. a Chinese medicine extract additive, it is characterised in that: formula is made up of the raw material of following weight parts: Flos Eriocauli 40-60
Part, Semen Fagopyri Esculenti 75-85 part, Folium Mori 15-20 part, Fructus Cannabis 10-20 part, Flos Sophorae 80-100 part, Semen Oroxyli 25-33 part, Herba Eupatorii 40-52
Part, Radix Asteris 3-8 part, Radix Sophorae Tonkinensis 0.5-1.0 part, Semen zanthoxyli 1-3 part, Folium Pini 1-5 part；
Its preparation method is:
1) Flos Eriocauli, Semen Fagopyri Esculenti, Folium Mori, Fructus Cannabis, Flos Sophorae, Semen Oroxyli, Herba Eupatorii are ground into coarse powder, add coarse powder weight 5-10 times
92% ethanol, 80 DEG C of reflux, extract, 2h of constant temperature, leach extracting solution, filtering residue is again with 60% ethanol constant temperature 82 of coarse powder weight 3-5 times
DEG C reflux, extract, 1.5h, leaches extracting solution, and gained filtering residue by 100 DEG C of reflux, extract, 2h of water termostat of coarse powder weight 6-8 times, is filtered again
Go out extracting solution, the extracting solution of three gained is merged, obtains mixed extract；
2) Radix Asteris, Radix Sophorae Tonkinensis, Semen zanthoxyli, the Folium Pini water of 50-70 part impregnate 10-15h at 40-60 DEG C, filter, obtain filtrate；
3) by step 1) mixed extract and step 2) filtrate mix, stand 20-24h, re-evaporation is condensed into paste, i.e.
?.
2. a kind of Chinese medicine extract additive as claimed in claim 1, it is characterised in that: formula is by the raw material of following weight parts
Composition: Flos Eriocauli 50 parts, 78 parts of Semen Fagopyri Esculenti, 16 parts of Folium Mori, Fructus Cannabis 15 parts, 90 parts of Flos Sophorae, Semen Oroxyli 29 parts, Herba Eupatorii 48 parts, purple
Aster 4 parts, Radix Sophorae Tonkinensis 0.6 part, Semen zanthoxyli 2 parts, 3 parts of Folium Pini；
Its preparation method is:
1) Flos Eriocauli, Semen Fagopyri Esculenti, Folium Mori, Fructus Cannabis, Flos Sophorae, Semen Oroxyli, Herba Eupatorii are ground into coarse powder, add coarse powder weight 8 times
92% ethanol, 80 DEG C of reflux, extract, 2h of constant temperature, leach extracting solution, filtering residue is again with the 60% ethanol constant temperature 82 DEG C of coarse powder weight 4 times
Reflux, extract, 1.5h, leaches extracting solution, and gained filtering residue by 100 DEG C of reflux, extract, 2h of water termostat of coarse powder weight 8 times, leaches and carries again
Take liquid, the extracting solution of three gained is merged, obtains mixed extract；
2) Radix Asteris, Radix Sophorae Tonkinensis, Semen zanthoxyli, Folium Pini impregnate 12h with the water of 60 parts at 50 DEG C, filter, obtain filtrate；
3) by step 1) mixed extract and step 2) filtrate mix, stand 24h, re-evaporation is condensed into paste, to obtain final product.
3. a Chinese medicine extract additive, it is characterised in that: formula is: Flos Eriocauli, Semen Fagopyri Esculenti, Folium Mori, Fructus Cannabis, Flos Sophorae, wood
Butterfly, Herba Eupatorii, Radix Asteris, Radix Sophorae Tonkinensis, Semen zanthoxyli, Folium Pini.
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| CN201610871475.7A CN106235393B (en) | 2016-09-30 | 2016-09-30 | Traditional Chinese medicine extract additive and application thereof in tobacco |
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| CN201610871475.7A CN106235393B (en) | 2016-09-30 | 2016-09-30 | Traditional Chinese medicine extract additive and application thereof in tobacco |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108095185A (en) * | 2017-12-14 | 2018-06-01 | 江西中烟工业有限责任公司 | A kind of pipe tobacco pretreating process |
| CN109355156A (en) * | 2018-12-04 | 2019-02-19 | 赵为兴 | A kind of formula and preparation method thereof of fructus cannabis alcoholic drink mixed with fruit juice |
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| CN109355156A (en) * | 2018-12-04 | 2019-02-19 | 赵为兴 | A kind of formula and preparation method thereof of fructus cannabis alcoholic drink mixed with fruit juice |
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| CN106235393B (en) | 2021-07-27 |
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