CN102796204A - Extraction method of tremella polysaccharide and application of tremella polysaccharide in tobaccos - Google Patents
Extraction method of tremella polysaccharide and application of tremella polysaccharide in tobaccos Download PDFInfo
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- CN102796204A CN102796204A CN2012103093649A CN201210309364A CN102796204A CN 102796204 A CN102796204 A CN 102796204A CN 2012103093649 A CN2012103093649 A CN 2012103093649A CN 201210309364 A CN201210309364 A CN 201210309364A CN 102796204 A CN102796204 A CN 102796204A
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Abstract
The invention discloses an extraction method of tremella polysaccharide and an application of the tremella polysaccharide in tobaccos. The method comprises the following steps of: a. after pre-processing tremella, drying the tremella at 30-80 DEG C and then grinding the tremella to 40-100 meshes; b. soaking the tremella powder in 80-100% ethanol for 1-24 hours; c. extracting the tremella powder with water for 1-4 hours at 50-100 DEG C; d. concentrating the filtrate obtained after filtration; and e. adding the concentrate to absolute ethyl alcohol to a scale, carrying out static precipitation for more than 24 hours and obtaining the tremella polysaccharide after filtration. The extraction method has the following beneficial effects that the tremella polysaccharide is added to cut tobaccos as feed liquid for tobaccos, so when the cigarettes burn, the smoking quality of the cigarettes can be obviously improved, the aroma quantity is increased, the irritation and the dry sensation are reduced and the taste is improved; the tremella polysaccharide also has a certain moisture preserving function and can reduce the contents of such harmful components in the main stream smoke of the cigarettes as free radicals; and the tremella polysaccharide does not change the original performances of the cigarettes or the existing processing techniques of the cigarettes, so the tremella polysaccharide further has practical production significance and value.
Description
Technical field
The present invention relates to the white fungus Crude polysaccharides and in Application in Tobacco.This The Application of Technology does not change the existing complete processing of cigarette, the aesthetic quality that can improve cigarette, the hazardness of reduction cigarette.
Background technology
Along with smoking and healthy problem more and more receive publicity, the objectionable constituent of sucking security, increase nourishing function, reducing in the cigarette smoke that improve cigarette are the inevitable development trend of cigarette.Therefore one occurred on the market, promptly in pipe tobacco, added the material that genseng, peppermint etc. have unique nourishing function or taste like kinds such as ginseng cigarette, peppermint cigarettes.
White fungus is in the existing long medicinal and edible history of China, and the white fungus Crude polysaccharides can be extracted by white fungus and obtain.White fungus has the increase body's immunity, and the enhancing body hypoxia-bearing capability is removed radical, reaches effects such as suppressing tumour.Domestic relevant research is mainly at the chemical constituents determination of white fungus, aspect such as medical.Do not see that the white fungus Crude polysaccharides reports in Application in Tobacco.
Summary of the invention
To the weak point that present technology exists, the present invention provides a kind of process for extracting of white fungus Crude polysaccharides and in Application in Tobacco.The cigarette that makes props up the quality quality that when burning and sucking, can obviously improve cigarette, increases perfume quantity and improves mouthfeel etc., has certain humectation performance again, and can reduce the content of objectionable constituent such as radical in the cigarette mainstream flue gas.The present invention does not change original performance of cigarette, does not change the existing complete processing of cigarette, therefore has more the meaning and the value of actual production.
In order to solve the problems of the technologies described above, the present invention adopts following technical scheme:
The process for extracting of white fungus Crude polysaccharides and in Application in Tobacco, it is characterized in that: it is to be made by following method:
A. white fungus is crushed to 40～100 orders after the oven dry down at 30～80 ℃ after pre-treatment;
B. the white fungus powder is with 80～100% alcohol immersion, 1～24h;
C. under 50～100 ℃ of conditions, water extraction white fungus powder 1～4h;
D. the tremella extract filtrate filtered concentrates;
E. with liquid concentrator, add absolute ethyl alcohol by a certain percentage, static precipitating after the filtration, both obtained white fungus Crude polysaccharides of the present invention more than 24 hours.
Further, processing in the early stage of white fungus comprises washing, rejects impurity, baking.
Further, in the d step, the concentration that contains dry-matter in the filtering and concentrating liquid is 1～10%.
Further, in step e, by liquid concentrator: absolute ethyl alcohol is that the volume ratio of 1:4 adds absolute ethyl alcohol.
Further, the white fungus Crude polysaccharides is after water dissolution, and white fungus Crude polysaccharides consumption is 0.001～0.5% of a pipe tobacco weight, joins on the cigarette shreds with feed liquid as cigarette.
The usefulness of technique scheme is:
The present invention is based on the situation of above-mentioned prior art and study and then develop the white fungus Crude polysaccharides and in Application in Tobacco to white fungus specially; White fungus Crude polysaccharides extraction separation is come out, join on the cigarette shreds, can improve the sucking quality of cigarette, and can reduce the content of objectionable constituent such as radical in the cigarette mainstream flue gas.And this The Application of Technology does not change the existing complete processing of cigarette, can improve the quality of cigarette, reduces the hazardness of cigarette.
The present invention compares prior art and has the following advantages:
1, can improve the sucking quality of cigarette;
2, can reduce some objectionable constituent in the cigarette mainstream flue gas;
3, do not change the original performance and the cigarette complete processing of cigarette;
4, has certain humectation effect;
5, have the increase perfume quantity, reduce pungency and improve effect such as mouthfeel;
6, cost is not high, has practicality;
7, without any side effects.
Through testing: compared with the contrast cigarette by the obtained cigarette of the present invention, the content of some objectionable constituent obviously reduces in the cigarette mainstream flue gas, and like tobacco-specific nitrosamine, smoke gaseous phase free radical etc., the reduction amplitude is between 5%～20%; When burning and sucking cigarette, flue gas, the flue gas free from extraneous odour can improve the sucking quality of cigarette.
Description of drawings
Do not have
Embodiment
Further set forth the present invention below in conjunction with specific embodiment.These embodiment only be used to the present invention is described and be not used in the restriction scope of the present invention.
Embodiment one:
The process for extracting of white fungus Crude polysaccharides and in Application in Tobacco, wherein the white fungus Crude polysaccharides is obtained by following method among the present invention:
A. white fungus is through pre-treatment: get white fungus, with the fresh water washes clean, reject impurity, dry or dry;
B. oven dry is pulverized: the white fungus of pre-treatment after oven dry under 50 ℃ of temperature, is crushed to 40 orders;
C. under the alcohol reflux condition, with absolute ethyl alcohol lixiviate white fungus 2h;
D. filter vat liquor, again to white fungus under 70 ℃ of conditions, with water extraction white fungus 3h;
After the content that the tremella extract filtrate filtered is concentrated to dry-matter was 5%, with the filtrating after concentrating, by filtrating: absolute ethyl alcohol was that the volume ratio of 1:4 adds, mix more than the static 48h in back, after the filtration, both white fungus Crude polysaccharides of the present invention.The white fungus Crude polysaccharides is a white solid, water soluble.
The white fungus Crude polysaccharides joins on the cigarette shreds with feed liquid through processing cigarette after the water dissolution, and the ratio that specifically applies is: the consumption of white fungus Crude polysaccharides is 0.05% of a pipe tobacco weight, adds on the pipe tobacco through spray pattern behind the dilute with water.
Through smokeing panel test, the flue gas free from extraneous odour, perfume quantity increases, and reduces pungency, reduces dry sensation and improves mouthfeel.
Embodiment two
The process for extracting of white fungus Crude polysaccharides and in Application in Tobacco, wherein the white fungus Crude polysaccharides is obtained by following method among the present invention:
A. white fungus is through pre-treatment: get white fungus, with the fresh water washes clean, reject impurity, dry or dry;
B. oven dry is pulverized: the white fungus of pre-treatment after oven dry under 60 ℃ of temperature, is crushed to 80 orders;
C. under the alcohol reflux condition, with absolute ethyl alcohol lixiviate white fungus 24h;
D. filter vat liquor, again to white fungus under 100 ℃ of conditions, with water extraction white fungus 4h;
After the content that the tremella extract filtrate filtered is concentrated to dry-matter was 5%, with the filtrating after concentrating, by filtrating: absolute ethyl alcohol was that the volume ratio of 1:4 adds, mix more than the static 48h in back, after the filtration, both white fungus Crude polysaccharides of the present invention.The white fungus Crude polysaccharides is a white solid, water soluble.
The white fungus Crude polysaccharides joins on the cigarette shreds with feed liquid through processing cigarette after the water dissolution, and the ratio that specifically applies is: the consumption of white fungus Crude polysaccharides is 0.05% of a pipe tobacco weight, adds on the pipe tobacco through spray pattern behind the dilute with water.
Through smokeing panel test, the flue gas free from extraneous odour, perfume quantity increases, and reduces pungency, reduces dry sensation and improves mouthfeel.
Embodiment three
The process for extracting of white fungus Crude polysaccharides and in Application in Tobacco, wherein the white fungus Crude polysaccharides is obtained by following method among the present invention:
A. white fungus is through pre-treatment: get white fungus, with the fresh water washes clean, reject impurity, dry or dry;
B. oven dry is pulverized: the white fungus of pre-treatment after oven dry under 40 ℃ of temperature, is crushed to 60 orders;
C. under the alcohol reflux condition, with absolute ethyl alcohol lixiviate white fungus 12h;
D. filter vat liquor, again to white fungus under 90 ℃ of conditions, with water extraction white fungus 3h;
After the content that the tremella extract filtrate filtered is concentrated to dry-matter was 5%, with the filtrating after concentrating, by filtrating: absolute ethyl alcohol was that the volume ratio of 1:4 adds, mix more than the static 48h in back, after the filtration, both white fungus Crude polysaccharides of the present invention.The white fungus Crude polysaccharides is a white solid, water soluble.
The white fungus Crude polysaccharides joins on the cigarette shreds with feed liquid through processing cigarette after the water dissolution, and the ratio that specifically applies is: the consumption of white fungus Crude polysaccharides is 0.05% of a pipe tobacco weight, adds on the pipe tobacco through spray pattern behind the dilute with water.
Above-mentionedly be merely two specific embodiments of the present invention, but design concept of the present invention is not limited thereto, allly utilizes this design that the present invention is carried out the change of unsubstantiality, all should belong to the behavior of invading protection domain of the present invention.
Claims (9)
1. the process for extracting of white fungus Crude polysaccharides and in Application in Tobacco, it is characterized in that: it is to be made by following method:
A. white fungus is crushed to 40～100 orders after the oven dry down at 30～80 ℃ after pre-treatment;
B. the white fungus powder is with 80～100% alcohol immersion, 1～24h;
C. under 50～100 ℃ of conditions, water extraction white fungus powder 1～4h;
D. the tremella extract filtrate filtered concentrates;
E. with liquid concentrator, add absolute ethyl alcohol by a certain percentage, static precipitating after the filtration, both obtained white fungus Crude polysaccharides of the present invention more than 24 hours.
2. the process for extracting of white fungus Crude polysaccharides according to claim 1 and in Application in Tobacco is characterized in that: handle the early stage of white fungus and comprise washing, rejecting impurity, baking.
3. the process for extracting of white fungus Crude polysaccharides according to claim 1 and 2 and in Application in Tobacco, it is characterized in that: in the d step, the concentration that contains dry-matter in the filtering and concentrating liquid is 1～10%.
4. the process for extracting of white fungus Crude polysaccharides according to claim 1 and 2 and in Application in Tobacco is characterized in that: in step e, by liquid concentrator: by liquid concentrator: absolute ethyl alcohol is that the volume ratio of 1:4 adds absolute ethyl alcohol.
5. the process for extracting of white fungus Crude polysaccharides according to claim 3 and in Application in Tobacco is characterized in that: by liquid concentrator: absolute ethyl alcohol is that the volume ratio of 1:4 adds absolute ethyl alcohol.
6. the process for extracting of white fungus Crude polysaccharides according to claim 1 and 2 and in Application in Tobacco; It is characterized in that: the white fungus Crude polysaccharides is after water dissolution; White fungus Crude polysaccharides consumption is 0.001～0.5% of a pipe tobacco weight, joins on the cigarette shreds with feed liquid as cigarette.
7. the process for extracting of white fungus Crude polysaccharides according to claim 3 and in Application in Tobacco; It is characterized in that: the white fungus Crude polysaccharides is after water dissolution; White fungus Crude polysaccharides consumption is 0.001～0.5% of a pipe tobacco weight, joins on the cigarette shreds with feed liquid as cigarette.
8. the process for extracting of white fungus Crude polysaccharides according to claim 4 and in Application in Tobacco; It is characterized in that: the white fungus Crude polysaccharides is after water dissolution; White fungus Crude polysaccharides consumption is 0.001～0.5% of a pipe tobacco weight, joins on the cigarette shreds with feed liquid as cigarette.
9. the process for extracting of white fungus Crude polysaccharides according to claim 5 and in Application in Tobacco; It is characterized in that: the white fungus Crude polysaccharides is after water dissolution; White fungus Crude polysaccharides consumption is 0.001～0.5% of a pipe tobacco weight, joins on the cigarette shreds with feed liquid as cigarette.
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103504463A (en) * | 2013-09-27 | 2014-01-15 | 广东中烟工业有限责任公司 | Application of shaddock ped polysaccharide to tobacco leaf moisturizing |
| CN103859582A (en) * | 2014-04-02 | 2014-06-18 | 甘肃烟草工业有限责任公司 | Application of potentilla anserine polysaccharide to cigarettes and preparation method of tobacco material liquid thereof |
| CN103923222A (en) * | 2014-04-29 | 2014-07-16 | 中华全国供销合作总社昆明食用菌研究所 | Method for extracting and separating low viscosity tremella aurantialba polysaccharide |
| CN104031166A (en) * | 2014-06-26 | 2014-09-10 | 河南中烟工业有限责任公司 | Tremella polysaccharide, extraction and purification method and application of tremella polysaccharide as tobacco humectant |
| CN107586349A (en) * | 2017-10-27 | 2018-01-16 | 福州大学 | The method that neutral buffer extracts tremella polysaccharides |
| CN107602721A (en) * | 2017-10-27 | 2018-01-19 | 福州大学 | The method that acidic buffer solution extracts tremella polysaccharides |
| CN112442136A (en) * | 2019-09-03 | 2021-03-05 | 广东乐尔康生物科技股份有限公司 | Method for extracting functional components from tremella |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103504463A (en) * | 2013-09-27 | 2014-01-15 | 广东中烟工业有限责任公司 | Application of shaddock ped polysaccharide to tobacco leaf moisturizing |
| CN103504463B (en) * | 2013-09-27 | 2015-09-30 | 广东中烟工业有限责任公司 | The application of a kind of shaddock ped polysaccharide in tobacco leaf humectation |
| CN103859582A (en) * | 2014-04-02 | 2014-06-18 | 甘肃烟草工业有限责任公司 | Application of potentilla anserine polysaccharide to cigarettes and preparation method of tobacco material liquid thereof |
| CN103859582B (en) * | 2014-04-02 | 2016-04-06 | 甘肃烟草工业有限责任公司 | The preparation method of fern amylose cigarette feed liquid |
| CN103923222A (en) * | 2014-04-29 | 2014-07-16 | 中华全国供销合作总社昆明食用菌研究所 | Method for extracting and separating low viscosity tremella aurantialba polysaccharide |
| CN103923222B (en) * | 2014-04-29 | 2016-04-13 | 中华全国供销合作总社昆明食用菌研究所 | A kind of low viscosity golden fungus polysaccharides extraction and separation method |
| CN104031166A (en) * | 2014-06-26 | 2014-09-10 | 河南中烟工业有限责任公司 | Tremella polysaccharide, extraction and purification method and application of tremella polysaccharide as tobacco humectant |
| CN107586349A (en) * | 2017-10-27 | 2018-01-16 | 福州大学 | The method that neutral buffer extracts tremella polysaccharides |
| CN107602721A (en) * | 2017-10-27 | 2018-01-19 | 福州大学 | The method that acidic buffer solution extracts tremella polysaccharides |
| CN112442136A (en) * | 2019-09-03 | 2021-03-05 | 广东乐尔康生物科技股份有限公司 | Method for extracting functional components from tremella |
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Application publication date: 20121128 |