CN109355156A - A kind of formula and preparation method thereof of fructus cannabis alcoholic drink mixed with fruit juice - Google Patents
A kind of formula and preparation method thereof of fructus cannabis alcoholic drink mixed with fruit juice Download PDFInfo
- Publication number
- CN109355156A CN109355156A CN201811473030.9A CN201811473030A CN109355156A CN 109355156 A CN109355156 A CN 109355156A CN 201811473030 A CN201811473030 A CN 201811473030A CN 109355156 A CN109355156 A CN 109355156A
- Authority
- CN
- China
- Prior art keywords
- fructus cannabis
- filter residue
- filtrate
- fruit juice
- solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12G—WINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
- C12G3/00—Preparation of other alcoholic beverages
- C12G3/04—Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs
- C12G3/06—Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs with flavouring ingredients
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Medicines Containing Plant Substances (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention discloses a kind of formulas of fructus cannabis alcoholic drink mixed with fruit juice, are mainly prepared by fructus cannabis, betadex, edible alcohol, further include the angelica extract for seasoning and seasoning, capejasmine extract, lemon extract, granulated sugar.The present invention first carries out immersion extraction to fructus cannabis powder with edible alcohol, that is, ethyl alcohol, after the filter residue drying obtained after filtering, immersion extraction is carried out with petroleum ether again, first inorganic compound, small-molecule substance are extracted with ethyl alcohol, the organic compound in petroleum ether extraction raw material is used again, so that the inorganic compound and organic compound in raw material are fully extracted out；The wrapped of betadex is recycled, extract ingredient is wrapped up, adjustable mouthfeel increases solubility, especially increase bioavilability, while keeping fructus cannabis alcoholic drink mixed with fruit juice color beautiful.
Description
Technical field
The present invention relates to alcoholic drink mixed with fruit juice production technical field, the formula and preparation method thereof of specifically a kind of fructus cannabis alcoholic drink mixed with fruit juice.
Background technique
In the prior art, rarely have and fructus cannabis is fabricated to finished product alcoholic drink mixed with fruit juice by alcoholic drink mixed with fruit juice GB/T27588-2011 standard.
Summary of the invention
The present invention provides a kind of formula and preparation method thereof of fructus cannabis alcoholic drink mixed with fruit juice.
A kind of formula of fructus cannabis alcoholic drink mixed with fruit juice, is mainly prepared by fructus cannabis, betadex, edible alcohol, further includes
For the angelica extract of seasoning and seasoning, capejasmine extract, lemon extract, granulated sugar.
A kind of preparation method of fructus cannabis alcoholic drink mixed with fruit juice, which comprises the following steps:
Step 1: full grains, the fructus cannabis without moldy metamorphism, free from insect pests are selected in screening；
Step 2: baking more than the fructus cannabis raw material grind to 5 mesh after screening, is laid on drip pan, is put into oven braking,
Moisture is dried to lower than 8%；
Step 3: extraction is impregnated, immersion extraction first is carried out to fructus cannabis powder with edible alcohol, after the filter residue drying obtained after filtering,
Immersion extraction is carried out with petroleum ether again, specifically includes the following steps:
Step 3.1: fructus cannabis powder and edible alcohol being mixed into solution A according to the mass ratio of 1:5, stirs, are impregnated for 24 hours at room temperature
After filter, obtain filtrate A, filter residue A；
Step 3.2: filter residue A and edible alcohol being mixed into solution B according to the mass ratio of 1:3, after stirring, being impregnated for 24 hours at room temperature
Filtering, obtains liquor B, filter residue B;
Step 3.3: filter residue B being put into oven baking, its moisture content is dried to 3-5%；
Step 3.4: according to the mass ratio of 1:1, petroleum ether is added into the filter residue B of drying, obtains solution C, solution C water bath sonicator
30min is stirred at room temperature, is impregnated 2h, and filtering obtains liquor C, filter residue C；
Step 3.5: according to the mass ratio of 1:1, petroleum ether is added into filter residue C, obtains solution D, solution D water bath sonicator 30min, room
2h is impregnated in the lower stirring of temperature, and filtering obtains filtrate D, filter residue D, and stirring, soaking temperature are no more than 50 DEG C；
Step 3.6: by the paste after liquor C, filtrate D steaming petroleum ether, edible alcohol, reflux is added by the mass ratio of 1:5
It is filtered after 2h, obtains filtrate E, filter residue E;
Step 3.7: edible alcohol is added by the mass ratio of 1:5 in filter residue E, filters after the 2h that flows back, obtains filtrate F, filter residue F;
Step 4: being filtered after filtrate A, liquor B, filtrate E, filtrate F are mixed, obtain filtrate P；
Step 5: weighing food grade betadex according to the 8% of fructus cannabis material quality ratio, be added according to the mass ratio of 1:5 pure
Water purification is stirred at 50 °C, after betadex is completely dissolved, is slowly added to filtrate P, is continued after stirring 30min,
Stop heating, continues after stirring 8h, filter to get filtrate Q；
Step 6: the alcoholic strength of alcoholic drink mixed with fruit juice is adjusted by addition pure water or edible alcohol.
Further, the solution A in the step 3.1, solution B in the step 3.2, molten in the step 3.4
Liquid C water bath sonicator 30min before stirring, immersion.
Further, 130-160 DEG C of baking temperature in the step 3.3, duration 15-35min.
Further, appropriate angelica extract, capejasmine extract, lemon extract and granulated sugar is added into the filtrate Q.
The present invention first carries out immersion extraction to fructus cannabis powder with edible alcohol, that is, ethyl alcohol, the filter residue drying obtained after filtering
Afterwards, then with petroleum ether immersion extraction is carried out, first inorganic compound, small-molecule substance is extracted with ethyl alcohol, then use petroleum ether
Organic compound in extraction feed, so that the inorganic compound and organic compound in raw material are extracted as far as possible；Again
Using the wrapped of betadex, extract ingredient is wrapped up, adjustable mouthfeel increases solubility, especially increases
Add bioavilability, while keeping fructus cannabis alcoholic drink mixed with fruit juice color bright beautiful.
Specific embodiment
The present invention will be further described in detail with reference to the specific embodiments.The embodiment of the present invention is to show
It is provided for the sake of example and description, and is not exhaustively or to limit the invention to disclosed form.Many modifications and
Variation is obvious for the ordinary skill in the art.Selection and description embodiment are to more preferably illustrate this
The principle and practical application of invention, and make those skilled in the art it will be appreciated that the present invention is to which design is suitable for specific
The various embodiments with various modifications of purposes.
Embodiment 1
A kind of formula of fructus cannabis alcoholic drink mixed with fruit juice, is mainly prepared by fructus cannabis, betadex, edible alcohol, further includes being used for
Angelica extract, capejasmine extract, lemon extract, the granulated sugar of seasoning and seasoning, preparation method includes the following steps:
Step 1: full grains, the fructus cannabis without moldy metamorphism, free from insect pests are selected in screening；
Step 2: baking more than the fructus cannabis raw material grind to 5 mesh after screening, is laid on drip pan, is put into oven braking,
160 DEG C of baking temperature, duration 30min, moisture is dried to lower than 8%；
Step 3: extraction is impregnated, immersion extraction first is carried out to fructus cannabis powder with edible alcohol, after the filter residue drying obtained after filtering,
Immersion extraction is carried out with petroleum ether again, specifically includes the following steps:
Step 3.1: fructus cannabis powder and edible alcohol being mixed into solution A according to the mass ratio of 1:5, stirs, are impregnated for 24 hours at room temperature
After filter, obtain filtrate A, filter residue A；
Step 3.2: filter residue A and edible alcohol being mixed into solution B according to the mass ratio of 1:3, after stirring, being impregnated for 24 hours at room temperature
Filtering, obtains liquor B, filter residue B;
Step 3.3: filter residue B being put into oven baking, its moisture content is dried to 3-5%；
Step 3.4: according to the mass ratio of 1:1, petroleum ether is added into the filter residue B of drying, obtains solution C, solution C water bath sonicator
30min is stirred at room temperature, is impregnated 2h, and filtering obtains liquor C, filter residue C；
Step 3.5: according to the mass ratio of 1:1, petroleum ether is added into filter residue C, obtains solution D, solution D water bath sonicator 30min, room
2h is impregnated in the lower stirring of temperature, and filtering obtains filtrate D, filter residue D, and stirring, soaking temperature are no more than 50 DEG C；
Step 3.6: by the paste after liquor C, filtrate D steaming petroleum ether, edible alcohol, reflux is added by the mass ratio of 1:5
It is filtered after 2h, obtains filtrate E, filter residue E;
Step 3.7: edible alcohol is added by the mass ratio of 1:5 in filter residue E, filters after the 2h that flows back, obtains filtrate F, filter residue F;
Step 4: being filtered after filtrate A, liquor B, filtrate E, filtrate F are mixed, obtain filtrate P；
Step 5: weighing food grade betadex according to the 8% of fructus cannabis material quality ratio, be added according to the mass ratio of 1:5 pure
Water purification is stirred at 50 °C, after betadex is completely dissolved, is slowly added to filtrate P, is continued after stirring 30min,
Stop heating, continues after stirring 8h, filter to get filtrate Q；
Step 6: appropriate angelica extract, capejasmine extract, lemon extract and granulated sugar is added into the filtrate Q, Radix Angelicae Sinensis mentions
The additive amount of object, capejasmine extract, lemon extract and granulated sugar is taken to be adjusted according to taste；
Step 7: the alcoholic strength of alcoholic drink mixed with fruit juice is adjusted by addition pure water or edible alcohol.
The edible alcohol that the present embodiment refers to is 95%vol or more, because of some ingredient indissolubles or insoluble in fructus cannabis
Yu Shui, but it is dissolved in organic solvent alcohol, and alcoholic strength is higher, ingredient therein is just easy to leach.The present invention first uses edible alcohol
I.e. ethyl alcohol carries out immersion extraction to fructus cannabis powder, after the drying of the filter residue that obtains after filtering, then with petroleum ether carries out immersion extraction, first
Inorganic compound, small-molecule substance are extracted with ethyl alcohol, then with the organic compound in petroleum ether extraction raw material, so that former
Inorganic compound and organic compound in material are fully extracted out；The wrapped of betadex is recycled, by extract
Ingredient is wrapped up, and adjustable mouthfeel increases solubility, especially increase bioavilability, while making fructus cannabis alcoholic drink mixed with fruit juice color
Pool is bright orange.
The main component of fructus cannabis is wrapped in its histocyte, and cell periphery is one layer of cellulose, hemicellulose and fruit
The cell wall of the material compositions such as glue is plasm in cell wall.It is molten in solution A, the step 3.2 in the step 3.1
Solution C in liquid B, the step 3.4 can destroy plasmic physiology function in stirring, the preceding water bath sonicator 30min of immersion
Can, so that the effective component and other solable matters in fructus cannabis histocyte penetrate into outside cell, improve recovery rate.
130-160 DEG C of baking temperature in the step 3.3, duration 15-35min, being mainly used for will be in fructus cannabis powder
Moisture content is baked between 3-5%, reduces the water content in filter residue B, improves extraction of the fructus cannabis internal component in petroleum ether
Rate, and promote cannabidiol this ingredient maturation in fructus cannabis, making it, there is no bioactivity, to will not be converted into
Four phenol of hemp of poison.
Obviously, described embodiment is only a part of the embodiments of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, this field and those of ordinary skill in the related art institute without creative labor
The every other embodiment obtained, all should belong to the scope of protection of the invention.
Claims (6)
1. a kind of formula of fructus cannabis alcoholic drink mixed with fruit juice, which is characterized in that mainly by fructus cannabis, betadex, edible alcohol preparation and
At.
2. the formula of fructus cannabis alcoholic drink mixed with fruit juice according to claim 1, which is characterized in that further include the Radix Angelicae Sinensis for seasoning and seasoning
Extract, capejasmine extract, lemon extract, granulated sugar.
3. a kind of preparation method of fructus cannabis alcoholic drink mixed with fruit juice, which comprises the following steps:
Step 1: full grains, the fructus cannabis without moldy metamorphism, free from insect pests are selected in screening；
Step 2: baking more than the fructus cannabis raw material grind to 5 mesh after screening, is laid on drip pan, is put into oven braking,
Moisture is dried to lower than 8%；
Step 3: extraction is impregnated, immersion extraction first is carried out to fructus cannabis powder with edible alcohol, after the filter residue drying obtained after filtering,
Immersion extraction is carried out with petroleum ether again, specifically includes the following steps:
Step 3.1: fructus cannabis powder and edible alcohol being mixed into solution A according to the mass ratio of 1:5, stirs, are impregnated for 24 hours at room temperature
After filter, obtain filtrate A, filter residue A；
Step 3.2: filter residue A and edible alcohol being mixed into solution B according to the mass ratio of 1:3, after stirring, being impregnated for 24 hours at room temperature
Filtering, obtains liquor B, filter residue B;
Step 3.3: filter residue B being put into oven baking, its moisture content is dried to 3-5%；
Step 3.4: according to the mass ratio of 1:1, petroleum ether is added into the filter residue B of drying, obtains solution C, solution C water bath sonicator
30min is stirred at room temperature, is impregnated 2h, and filtering obtains liquor C, filter residue C；
Step 3.5: according to the mass ratio of 1:1, petroleum ether is added into filter residue C, obtains solution D, solution D water bath sonicator 30min, room
2h is impregnated in the lower stirring of temperature, and filtering obtains filtrate D, filter residue D, and stirring, soaking temperature are no more than 50 DEG C；
Step 3.6: by the paste after liquor C, filtrate D steaming petroleum ether, edible alcohol, reflux is added by the mass ratio of 1:5
It is filtered after 2h, obtains filtrate E, filter residue E;
Step 3.7: edible alcohol is added by the mass ratio of 1:5 in filter residue E, filters after the 2h that flows back, obtains filtrate F, filter residue F;
Step 4: being filtered after filtrate A, liquor B, filtrate E, filtrate F are mixed, obtain filtrate P；
Step 5: weighing food grade betadex according to the 8% of fructus cannabis material quality ratio, be added according to the mass ratio of 1:5 pure
Water purification is stirred at 50 °C, after betadex is completely dissolved, is slowly added to filtrate P, is continued after stirring 30min,
Stop heating, continues after stirring 8h, filter to get filtrate Q；
Step 6: the alcoholic strength of alcoholic drink mixed with fruit juice is adjusted by addition pure water or edible alcohol.
4. the preparation method of fructus cannabis alcoholic drink mixed with fruit juice according to claim 3, which is characterized in that the solution in the step 3.1
A, the solution B in the step 3.2, the solution C in the step 3.4, the solution D in the step 3.5 in stirring, are impregnated
Preceding equal water bath sonicator 30min.
5. the preparation method of fructus cannabis alcoholic drink mixed with fruit juice according to claim 3, which is characterized in that the baking in the step 3.3
130-160 DEG C of temperature, duration 15-35min.
6. the preparation method of fructus cannabis alcoholic drink mixed with fruit juice according to claim 3, which is characterized in that be added into the filtrate Q suitable
Measure angelica extract, capejasmine extract, lemon extract and granulated sugar.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811473030.9A CN109355156A (en) | 2018-12-04 | 2018-12-04 | A kind of formula and preparation method thereof of fructus cannabis alcoholic drink mixed with fruit juice |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811473030.9A CN109355156A (en) | 2018-12-04 | 2018-12-04 | A kind of formula and preparation method thereof of fructus cannabis alcoholic drink mixed with fruit juice |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109355156A true CN109355156A (en) | 2019-02-19 |
Family
ID=65331264
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811473030.9A Pending CN109355156A (en) | 2018-12-04 | 2018-12-04 | A kind of formula and preparation method thereof of fructus cannabis alcoholic drink mixed with fruit juice |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109355156A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110305759A (en) * | 2019-01-18 | 2019-10-08 | 赵为兴 | A kind of formula and preparation method thereof of fructus cannabis egg alcoholic drink mixed with fruit juice |
| CN110903937A (en) * | 2019-12-18 | 2020-03-24 | 黑龙江国麻汉麻科技有限公司 | Hemp seed extract, liqueur and preparation method and application of liqueur |
| CN115232699A (en) * | 2022-03-31 | 2022-10-25 | 赵为兴 | Fructus cannabis beverage and preparation method thereof |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1552839A (en) * | 2003-06-01 | 2004-12-08 | 高景曦 | Nano modified red common stonecrop health-care wine |
| CN103243007A (en) * | 2013-04-03 | 2013-08-14 | 邢海明 | Alcoholic beverage and preparation method of alcoholic beverage |
| CN105296275A (en) * | 2015-09-23 | 2016-02-03 | 黑龙江省科学院 | Fructus cannabis health care baijiu and brewing method thereof |
| CN106235393A (en) * | 2016-09-30 | 2016-12-21 | 江西中烟工业有限责任公司 | Chinese medicine extract additive and the application in Nicotiana tabacum L. thereof |
| CN106860492A (en) * | 2017-01-05 | 2017-06-20 | 杭州福斯特光伏材料股份有限公司 | A kind of preparation method of cannabinol compounds |
| CN107586682A (en) * | 2017-10-23 | 2018-01-16 | 广西巴马响泉食品有限公司 | A kind of brew method of alcoholic drink mixed with fruit juice |
| CN107898826A (en) * | 2017-11-01 | 2018-04-13 | 云南谷益美农业开发有限公司 | The preparation method of the numb medicinal extract of fire containing cannabidiol |
-
2018
- 2018-12-04 CN CN201811473030.9A patent/CN109355156A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1552839A (en) * | 2003-06-01 | 2004-12-08 | 高景曦 | Nano modified red common stonecrop health-care wine |
| CN103243007A (en) * | 2013-04-03 | 2013-08-14 | 邢海明 | Alcoholic beverage and preparation method of alcoholic beverage |
| CN105296275A (en) * | 2015-09-23 | 2016-02-03 | 黑龙江省科学院 | Fructus cannabis health care baijiu and brewing method thereof |
| CN106235393A (en) * | 2016-09-30 | 2016-12-21 | 江西中烟工业有限责任公司 | Chinese medicine extract additive and the application in Nicotiana tabacum L. thereof |
| CN106860492A (en) * | 2017-01-05 | 2017-06-20 | 杭州福斯特光伏材料股份有限公司 | A kind of preparation method of cannabinol compounds |
| CN107586682A (en) * | 2017-10-23 | 2018-01-16 | 广西巴马响泉食品有限公司 | A kind of brew method of alcoholic drink mixed with fruit juice |
| CN107898826A (en) * | 2017-11-01 | 2018-04-13 | 云南谷益美农业开发有限公司 | The preparation method of the numb medicinal extract of fire containing cannabidiol |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110305759A (en) * | 2019-01-18 | 2019-10-08 | 赵为兴 | A kind of formula and preparation method thereof of fructus cannabis egg alcoholic drink mixed with fruit juice |
| CN110903937A (en) * | 2019-12-18 | 2020-03-24 | 黑龙江国麻汉麻科技有限公司 | Hemp seed extract, liqueur and preparation method and application of liqueur |
| CN115232699A (en) * | 2022-03-31 | 2022-10-25 | 赵为兴 | Fructus cannabis beverage and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN109355156A (en) | A kind of formula and preparation method thereof of fructus cannabis alcoholic drink mixed with fruit juice | |
| CN104543913B (en) | Manufacture craft for the spice juice of cooking wine | |
| CN102342472B (en) | Five-spice powder and preparation method thereof | |
| CN103750257B (en) | Prepared cooking wine and preparation method thereof | |
| CN107007662B (en) | Processing method of traditional Chinese medicine monkshood | |
| CN104222324A (en) | Vine pepper wind-expelling and cold-removing tea oil | |
| RU2009118941A (en) | HIGH POLYPHENOL CONTENT OF VEGETABLE RAW MATERIALS | |
| CN103834529B (en) | A kind of making method of Wild Buckwheat Rhizome yellow rice wine | |
| CN105017055B (en) | A kind of method of the separation capsicum red pigment of the rapid extraction from pimiento and capsaicine | |
| CN103131591B (en) | Method for producing dried persimmon wine | |
| CN102618413B (en) | Production method of traditional Chinese medicine alcoholic drink | |
| CN104351329B (en) | Composite leaching vegetable fresh-keeping agent for tragus berteronianus and preparation method of fresh-keeping agent | |
| CN111518613A (en) | Blending production process of zanthoxylum oil | |
| CN103820214A (en) | Tea oil squeezing method | |
| CN109280595A (en) | A kind of formula and preparation method thereof of coffee alcoholic drink mixed with fruit juice | |
| CN105379869B (en) | A kind of Rosa roxburghii Tratt black tea and preparation method thereof | |
| CN105623839B (en) | A method of extracting Silybum Marianum Gaertn Seed Oil | |
| CN104450170A (en) | Nutrition and health anticancer rapeseed oil | |
| CN109266500A (en) | A kind of formula of tea wine and preparation method thereof | |
| CN110898104A (en) | Hemp seed extract, preparation method and application thereof, and hemp seed wine | |
| KR101315005B1 (en) | Method for manufacturing grain syrup using ginkgo leaves | |
| CN107474946A (en) | A kind of processing method of brain-nourishing intelligence-benefiting tea oil | |
| CN103992928A (en) | Rambutan/Thamnolia vermicularia tea wine and preparation method thereof | |
| CN109805346A (en) | A kind of preparation method of bottom stuff of red soup of fire pot | |
| CN110305759A (en) | A kind of formula and preparation method thereof of fructus cannabis egg alcoholic drink mixed with fruit juice |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20190219 |