CN106232231B - 支链氟化乳化剂的回收 - Google Patents

支链氟化乳化剂的回收 Download PDF

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Publication number
CN106232231B
CN106232231B CN201580020259.5A CN201580020259A CN106232231B CN 106232231 B CN106232231 B CN 106232231B CN 201580020259 A CN201580020259 A CN 201580020259A CN 106232231 B CN106232231 B CN 106232231B
Authority
CN
China
Prior art keywords
emulsifier
fluorinated
water
anion exchange
recovery
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201580020259.5A
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English (en)
Chinese (zh)
Other versions
CN106232231A (zh
Inventor
克劳斯·辛策
埃贡·奥伯迈尔
阿尔内·塔勒
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
3M Innovative Properties Co
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3M Innovative Properties Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 3M Innovative Properties Co filed Critical 3M Innovative Properties Co
Publication of CN106232231A publication Critical patent/CN106232231A/zh
Application granted granted Critical
Publication of CN106232231B publication Critical patent/CN106232231B/zh
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K23/00—Use of substances as emulsifying, wetting, dispersing, or foam-producing agents
    • C09K23/007—Organic compounds containing halogen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J49/00—Regeneration or reactivation of ion-exchangers; Apparatus therefor
    • B01J49/05—Regeneration or reactivation of ion-exchangers; Apparatus therefor of fixed beds
    • B01J49/07—Regeneration or reactivation of ion-exchangers; Apparatus therefor of fixed beds containing anionic exchangers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J41/00—Anion exchange; Use of material as anion exchangers; Treatment of material for improving the anion exchange properties
    • B01J41/04—Processes using organic exchangers
    • B01J41/05—Processes using organic exchangers in the strongly basic form
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J41/00—Anion exchange; Use of material as anion exchangers; Treatment of material for improving the anion exchange properties
    • B01J41/08—Use of material as anion exchangers; Treatment of material for improving the anion exchange properties
    • B01J41/12—Macromolecular compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J49/00—Regeneration or reactivation of ion-exchangers; Apparatus therefor
    • B01J49/50—Regeneration or reactivation of ion-exchangers; Apparatus therefor characterised by the regeneration reagents
    • B01J49/57—Regeneration or reactivation of ion-exchangers; Apparatus therefor characterised by the regeneration reagents for anionic exchangers
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/47—Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Emulsifying, Dispersing, Foam-Producing Or Wetting Agents (AREA)
CN201580020259.5A 2014-04-18 2015-04-15 支链氟化乳化剂的回收 Expired - Fee Related CN106232231B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201461981237P 2014-04-18 2014-04-18
US61/981,237 2014-04-18
PCT/US2015/025937 WO2015160926A1 (en) 2014-04-18 2015-04-15 Recovery of branched fluorinated emulsifiers

Publications (2)

Publication Number Publication Date
CN106232231A CN106232231A (zh) 2016-12-14
CN106232231B true CN106232231B (zh) 2020-11-20

Family

ID=54324530

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201580020259.5A Expired - Fee Related CN106232231B (zh) 2014-04-18 2015-04-15 支链氟化乳化剂的回收

Country Status (5)

Country Link
US (1) US9694333B2 (enExample)
EP (1) EP3131675B1 (enExample)
JP (1) JP6532524B2 (enExample)
CN (1) CN106232231B (enExample)
WO (1) WO2015160926A1 (enExample)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP4026808B1 (en) * 2016-04-13 2024-07-24 Emerging Compounds Treatment Technologies, Inc. System for removing and concentrating per-and polyfluoroalkyl substances (pfas) from water
WO2020260702A1 (en) 2019-06-28 2020-12-30 Katholieke Universiteit Leuven Adsorptive removal of perfluorinated or partially fluorinated surfactants
CN113248699B (zh) * 2021-05-20 2022-11-04 甘肃华隆芯材料科技有限公司 一种除去全氟聚醚羧酸中金属离子杂质的方法

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1446181A (zh) * 2000-08-11 2003-10-01 大金工业株式会社 含氟阴离子表面活性剂的分离方法

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4213154C1 (enExample) 1992-04-22 1993-06-17 Hoechst Ag, 6230 Frankfurt, De
US5763552A (en) * 1996-07-26 1998-06-09 E. I. Du Pont De Nemours And Company Hydrogen-containing flourosurfacant and its use in polymerization
DE19932771A1 (de) * 1999-07-14 2001-01-18 Dyneon Gmbh Verfahren zur Eluierung fluorierter Emulgatoren
DE19953285A1 (de) * 1999-11-05 2001-05-10 Dyneon Gmbh Verfahren zur Rückgewinnung fluorierter Emulgatoren
EP1561742B1 (en) 2004-02-05 2012-11-21 3M Innovative Properties Company Method of recovering fluorinated acid surfactants from adsorbent particles loaded therewith
EP1700869A1 (en) * 2005-03-11 2006-09-13 3M Innovative Properties Company Recovery of fluorinated surfactants from a basic anion exchange resin having quaternary ammonium groups
GB0514387D0 (en) * 2005-07-15 2005-08-17 3M Innovative Properties Co Aqueous emulsion polymerization of fluorinated monomers using a perfluoropolyether surfactant
US20070015937A1 (en) 2005-07-15 2007-01-18 3M Innovative Properties Company Process for recovery of fluorinated carboxylic acid surfactants from exhaust gas
WO2007043278A1 (ja) * 2005-10-14 2007-04-19 Asahi Glass Company, Limited 塩基性陰イオン交換樹脂の再生方法
US20070276103A1 (en) * 2006-05-25 2007-11-29 3M Innovative Properties Company Fluorinated Surfactants
US20090281261A1 (en) 2008-05-09 2009-11-12 E. I. Du Pont De Nemours And Company Abatement of Fluoroether Carboxylic Acids or Salts Employed in Fluoropolymer Resin Manufacture
EP3385249A1 (en) * 2008-06-24 2018-10-10 AGC Inc. Method for purifying fluorinated compound
CN102740974A (zh) * 2010-02-03 2012-10-17 旭硝子株式会社 阴离子性含氟乳化剂的回收方法

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1446181A (zh) * 2000-08-11 2003-10-01 大金工业株式会社 含氟阴离子表面活性剂的分离方法

Also Published As

Publication number Publication date
US9694333B2 (en) 2017-07-04
JP2017516843A (ja) 2017-06-22
JP6532524B2 (ja) 2019-06-19
US20170028370A1 (en) 2017-02-02
EP3131675B1 (en) 2019-01-09
WO2015160926A1 (en) 2015-10-22
EP3131675A1 (en) 2017-02-22
CN106232231A (zh) 2016-12-14
EP3131675A4 (en) 2017-12-20

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Granted publication date: 20201120