CN106083307A - A kind of solubility compound fertilizer - Google Patents
A kind of solubility compound fertilizer Download PDFInfo
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- CN106083307A CN106083307A CN201610396904.XA CN201610396904A CN106083307A CN 106083307 A CN106083307 A CN 106083307A CN 201610396904 A CN201610396904 A CN 201610396904A CN 106083307 A CN106083307 A CN 106083307A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
Abstract
nullThe invention discloses a kind of solubility compound fertilizer，Raw material including following weight portion: 10 60 parts of potash fertilizer、10 60 parts of phosphate fertilizer、Calcareous fertilisers 10 30 parts、2 20 parts of carbamide、Trace element 28 parts、Humic acid 15 25 parts、Bacillus subtilis microbial agent 2 10 parts、Chinese medicinal components 24 parts、Metal ion amino acid complex concentrated solution 20 40 parts、Rare-earth Aminoacid Complexes concentrated solution 20 40 parts，Described Chinese medicinal components includes the raw material of following weight portion: Jerusalem artichoke 5 15 parts、48 parts of Pericarpium Zanthoxyli、5 15 parts of Ramulus Et Folium Picrasmae tree、Folium Artemisiae Argyi 24 parts、Dittany 13 parts、Radix Platycodonis 24 parts、Flos Daturae 26 parts、Radix Rhapontici 15 parts、Rhizoma et radix veratri (Radix Rhizoma Veratri) 13 parts、Cortex Meliae 6 10 parts、Ramulus et Folium Pcrasmae (Cortex Picrasmae) 15 parts、Semen Arecae 12 parts、Cortex ulmi pumilae 5 15 parts、Cortex Ailanthi 28 parts.The present invention can guarantee that the steady of trace element is imitated and long-acting, activating soil, and total nutrient content is high, and solubility property is good；Chinese medicinal components has the effect of parasite killing, sterilization, can prevent and treat fusarium root rot of maize, eliminates the corn yield caused because of root rot and reduces.
Description
Technical field
The present invention relates to a kind of compound fertilizer, specifically a kind of solubility compound fertilizer.
Background technology
China is one of minimum country in per capita arable land, preserves the ecological environment, and increasing soil fertility, it is the heaviest to have
The strategic importance wanted.China currently puts forth effort to implement fertile soil engineering project, and applying organic manure material and fertilizer are emphasized in this plan
With chemical fertilizer compounding application, the blindness reducing chemical fertilizer puts into, improves nutrientuse efficiency.
Semen Maydis is important cereal crops and industrial crops, has statistics display, and its yield and cultivated area are only second to Oryza sativa L.
And Semen Tritici aestivi, occupy third place in the world, occupy an important position in the people's livelihood and national economy.Effectively utilize limited land resource,
The yield and quality improving Semen Maydis is the direction made great efforts of people and eternal problem.Scientific and reasonable fertilising is high-quality, highly efficient and productive
The importance of development Maize Production, after common fertilizer is manured into soil, fertilizer efficiency period is short, and effect is poor.
There is no the solubility compound fertilizer containing Chinese medicinal components that Semen Maydis is special at present, therefore in the urgent need to a kind of fertilizer, a side
Face meets the needs of high-yield fertilization, on the other hand can improve again the physicochemical property of In Soils of Northeastern, reaches to improve the mesh of soil
, at the same time it can also be preventing and treating fusarium root rot of maize.
Summary of the invention
It is an object of the invention to provide a kind of solubility compound fertilizer, with asking of solving to propose in above-mentioned background technology
Topic.
For achieving the above object, the present invention provides following technical scheme:
A kind of solubility compound fertilizer, including the raw material of following weight portion: potash fertilizer 10-60 part, phosphate fertilizer 10-60 part, calcareous fertilisers
10-30 part, carbamide 2-20 part, trace element 2-8 part, humic acid 15-25 part, bacillus subtilis microbial agent 2-10 part, Chinese drug-treated group
Divide 2-4 part, metal ion amino acid complex concentrated solution 20-40 part, Rare-earth Aminoacid Complexes concentrated solution 20-40 part.
As the further scheme of the present invention: include the raw material of following weight portion: 35 parts of potash fertilizer, 35 parts of phosphate fertilizer, calcareous fertilisers 20
Part, 11 parts of carbamide, trace element 5 parts, humic acid 20 parts, bacillus subtilis microbial agent 6 parts, Chinese medicinal components 3 parts, metal ion ammonia
Base acid complex concentrated solution 30 parts, Rare-earth Aminoacid Complexes concentrated solution 30 parts.
As the present invention further scheme: described Chinese medicinal components includes the raw material of following weight portion: Jerusalem artichoke 5-15 part,
Pericarpium Zanthoxyli 4-8 part, Ramulus Et Folium Picrasmae tree 5-15 part, Folium Artemisiae Argyi 2-4 part, dittany 1-3 part, Radix Platycodonis 2-4 part, Flos Daturae 2-6 part, Radix Rhapontici 1-5 part, Herba chenopodii
Reed 1-3 part, Cortex Meliae 6-10 part, Ramulus et Folium Pcrasmae (Cortex Picrasmae) 1-5 part, Semen Arecae 1-2 part, Cortex ulmi pumilae 5-15 part, Cortex Ailanthi 2-8 part, Ramulus Sambuci Williamsii 1-3
Part, decomposite leaf common violet 1-3 part, Salix babylonica L. leaf 5-9 part.
As the present invention further scheme: described Chinese medicinal components includes the raw material of following weight portion: Jerusalem artichoke 10 parts, flower
Green pepper 6 parts, 10 parts of Ramulus Et Folium Picrasmae tree, Folium Artemisiae Argyi 3 parts, dittany 2 parts, Radix Platycodonis 3 parts, Flos Daturae 4 parts, Radix Rhapontici 3 parts, Rhizoma et radix veratri (Radix Rhizoma Veratri) 2 parts, Cortex Meliae 8 parts,
Ramulus et Folium Pcrasmae (Cortex Picrasmae) 3 parts, Semen Arecae 1 part, Cortex ulmi pumilae 10 parts, Cortex Ailanthi 5 parts, Ramulus Sambuci Williamsii 2 parts, decomposite leaf common violet 2 parts, 7 parts of Salix babylonica L. leaf.
As the present invention further scheme: described calcareous fertilisers are in calcium oxide, calcium nitrate, calcium ammonium nitrate or calcium chloride
One or more；Described phosphate fertilizer is one or more in MAP, Diammonium phosphate (DAP), urea phosphate, phosphoric acid or APP；Institute
Stating potash fertilizer is one or more in potassium chloride, potassium nitrate, potassium sulfate, potassium dihydrogen phosphate, potassium metaphosphate or dipotassium hydrogen phosphate.
As the present invention further scheme: described Rare-earth Aminoacid Complexes concentrated solution includes the former of following weight portion
Material: leather waste 20-60 part, cerine 20-40 part, concentration are sulfuric acid solution 80-100 part, perchloric acid 30-50 part of 40%.
As the present invention further scheme: described metal ion amino acid complex concentrated solution includes following weight portion
Raw material: bean cake 30-60 part, concentration are hydrochloric acid solution 60-100 part, smithsonite 30-50 part of 40%.
As the present invention further scheme: the preparation method of described solubility compound fertilizer, comprise the following steps:
(1) by the Chinese medicinal components Jerusalem artichoke weighed, Pericarpium Zanthoxyli, Ramulus Et Folium Picrasmae tree, Folium Artemisiae Argyi, dittany, Radix Platycodonis, Flos Daturae, Radix Rhapontici, Herba chenopodii
Reed, Cortex Meliae, Ramulus et Folium Pcrasmae (Cortex Picrasmae), Semen Arecae, Cortex ulmi pumilae, Cortex Ailanthi, Ramulus Sambuci Williamsii, decomposite leaf common violet, Salix babylonica L. leaf are put in container, add 3-8
Times water soaking 2-5 hour, then heating 1-2 hour, leaches filtrate, for filtrate one, is placed back in by filtering residue in container, add 2-3
Times water, heats 1 hour, filters filtrate, obtain filtrate two, merging filtrate one and filtrate two, obtain herb liquid, and filtering residue is standby；
(2) by the most mixed to described metal ion amino acid complex concentrated solution and Rare-earth Aminoacid Complexes concentrated solution
Close, be sufficiently stirred for 15 minutes, regulate pH value 8-9, obtain mixed concentrated liquid；
(3) by potash fertilizer, phosphate fertilizer, carbamide, humic acid mix homogeneously, it is then slowly added into calcareous fertilisers, stirring while adding, keep anti-
Answering system temperature is 50～80 DEG C, reacts complete, cooling, obtains mixture；
(4) by the herb liquid of step (1), the mixed concentrated liquid of step (2) and the mixture of step (3), bacillus subtilis
Bacteria agent and trace element mixing and stirring, pack and get final product.
As the present invention further scheme: the preparation method of described Rare-earth Aminoacid Complexes concentrated solution includes following
Step: the leather waste of described weight portion is crushed to fineness is 200, places it in autoclave, adds described
The concentration of weight portion is the sulfuric acid solution of 40%, is 110-125 DEG C in temperature, and pressure is to hydrolyze 8 hours under conditions of 20MP, warp
Animal protein factor digest is obtained after filtration, standby；At normal temperatures the cerine powder of described weight portion is dissolved in in perchloric acid,
React 1 hour under the conditions of 100 DEG C, filter out the impurity in solution, obtain rare earth ion settled solution；Gained rare earth ion is clarified
Liquid mixes with animal protein factor digest, stirs in one direction, reacts 1 hour, obtain Rare Earth Amino-Acid complexation under the conditions of 90 DEG C
Thing solution, being shifted bleeds in vaporizer is concentrated into the 1/4 of original volume, obtains Rare-earth Aminoacid Complexes concentrated solution.
As the present invention further scheme: the preparation method of described metal ion amino acid complex concentrated solution includes
Following steps: it is 200 mesh that the bean cake powder of described weight portion is broken to fineness, throw to described weight portion hydrochloric acid solution in, boil to
Add smithsonite, in one direction stirring 1 hour after boiling, obtain metal ion amino acid complex after filtering, be transferred to steam
Sending out bleeds in device is concentrated into original volume 1/4, obtains metal ion amino acid complex concentrated solution.
Compared with prior art, the invention has the beneficial effects as follows: metal ion amino acid complex and Rare Earth Amino-Acid network
Compound, can keep slowly discharging and making full use of of rare earth element and metal ion, also can guarantee that trace element steady effect and
Long-acting, the rare earth element of the present invention and the ratio of metallic element can make corn yield increasing 18%；Activating soil, total nutrient content is high,
Physics and chemical properties are stable, and without phenomenons such as caking, precipitation, flatulence under high temperature, low temperature and normal temperature condition, solubility property is good；
Chinese medicinal components has the effect of parasite killing, sterilization, with the addition of the Chinese medicinal components of parasite killing class so that it is while having fertilizer function, also
The growth of pythium spp, rhizoctonia, Fusarium spp. etc. can be suppressed, thus prevent and treat fusarium root rot of maize, eliminate the jade caused because of root rot
Rice yield reduces.
Detailed description of the invention
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described,
Obviously, described embodiment is only a part of embodiment of the present invention rather than whole embodiments.Based in the present invention
Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under not making creative work premise, all
Belong to the scope of protection of the invention.
Embodiment 1
In the embodiment of the present invention, a kind of solubility compound fertilizer, including the raw material of following weight portion: 10 parts of potash fertilizer, phosphate fertilizer
10 parts, calcareous fertilisers 10 parts, 2 parts of carbamide, trace element 2 parts, humic acid 15 parts, bacillus subtilis microbial agent 2 parts, Chinese medicinal components 2 parts,
Metal ion amino acid complex concentrated solution 20 parts, Rare-earth Aminoacid Complexes concentrated solution 20 parts.
Described Chinese medicinal components includes the raw material of following weight portion: Jerusalem artichoke 5 parts, 4 parts of Pericarpium Zanthoxyli, 5 parts of Ramulus Et Folium Picrasmae tree, Folium Artemisiae Argyi 2 parts, white
Moss 1 part, Radix Platycodonis 2 parts, Flos Daturae 2 parts, Radix Rhapontici 1 part, Rhizoma et radix veratri (Radix Rhizoma Veratri) 1 part, Cortex Meliae 6 parts, Ramulus et Folium Pcrasmae (Cortex Picrasmae) 1 part, Semen Arecae 1 part, Cortex ulmi pumilae 5
Part, Cortex Ailanthi 2 parts, Ramulus Sambuci Williamsii 1 part, decomposite leaf common violet 1 part, 5 parts of Salix babylonica L. leaf.
Described calcareous fertilisers are calcium oxide；Described phosphate fertilizer is MAP and Diammonium phosphate (DAP)；Described potash fertilizer is potassium chloride.
Described Rare-earth Aminoacid Complexes concentrated solution includes the raw material of following weight portion: leather waste 20 parts, cerine 20
Part, concentration are sulfuric acid solution 80 parts, 30 parts of the perchloric acid of 40%.
Described metal ion amino acid complex concentrated solution includes the raw material of following weight portion: bean cake 30 parts, concentration are
The hydrochloric acid solution of 40% 60 parts, 30 parts of smithsonite.
The preparation method of described solubility compound fertilizer, comprises the following steps:
(1) by the Chinese medicinal components Jerusalem artichoke weighed, Pericarpium Zanthoxyli, Ramulus Et Folium Picrasmae tree, Folium Artemisiae Argyi, dittany, Radix Platycodonis, Flos Daturae, Radix Rhapontici, Herba chenopodii
Reed, Cortex Meliae, Ramulus et Folium Pcrasmae (Cortex Picrasmae), Semen Arecae, Cortex ulmi pumilae, Cortex Ailanthi, Ramulus Sambuci Williamsii, decomposite leaf common violet, Salix babylonica L. leaf are put in container, add 3 times
Water soaking 2 hours, then heating 1 hour, leaches filtrate, for filtrate one, is placed back in by filtering residue in container, add 2 times of water, heating
1 hour, filtering filtrate, obtain filtrate two, merging filtrate one and filtrate two, obtain herb liquid, filtering residue is standby；
(2) Rare-earth Aminoacid Complexes concentrated solution is prepared: it is 200 that the leather waste of described weight portion is crushed to fineness
Day, place it in autoclave, add the sulfuric acid solution that concentration is 40% of described weight portion, be 110 DEG C in temperature,
Pressure is to hydrolyze 8 hours under conditions of 20MP, after filtering animal protein factor digest, standby；At normal temperatures by described weight
Part cerine powder be dissolved in in perchloric acid, react 1 hour under the conditions of 100 DEG C, filter out the impurity in solution, obtain rare earth from
Sub-settled solution；Gained rare earth ion clear liquor is mixed with animal protein factor digest, stirs in one direction, 90 DEG C of conditions
Lower reaction 1 hour, obtains Rare-earth Aminoacid Complexes solution, and being shifted bleeds in vaporizer is concentrated into the 1/4 of original volume,
To Rare-earth Aminoacid Complexes concentrated solution；
Prepare metal ion amino acid complex concentrated solution: it is 200 mesh that the bean cake powder of described weight portion is broken to fineness, throw
To the hydrochloric acid solution of described weight portion, boil to boiling and add smithsonite, in one direction stirring 1 hour, after filtering
Metal ion amino acid complex, being transferred in vaporizer bleeds is concentrated into original volume 1/4, obtains metal ion amino acid complex
Concentrated solution；
Described metal ion amino acid complex concentrated solution and Rare-earth Aminoacid Complexes concentrated solution are mixed by weight,
It is sufficiently stirred for 15 minutes, regulates pH value 8, obtain mixed concentrated liquid；
(3) by potash fertilizer, phosphate fertilizer, carbamide, humic acid mix homogeneously, it is then slowly added into calcareous fertilisers, stirring while adding, keep anti-
Answering system temperature is 50 DEG C, reacts complete, cooling, obtains mixture；
(4) by the herb liquid of step (1), the mixed concentrated liquid of step (2) and the mixture of step (3), bacillus subtilis
Bacteria agent and trace element mixing and stirring, pack and get final product.
Embodiment 2
In the embodiment of the present invention, a kind of solubility compound fertilizer, including the raw material of following weight portion: 35 parts of potash fertilizer, phosphate fertilizer
35 parts, calcareous fertilisers 20 parts, 11 parts of carbamide, trace element 5 parts, humic acid 20 parts, bacillus subtilis microbial agent 6 parts, Chinese medicinal components 3
Part, metal ion amino acid complex concentrated solution 30 parts, Rare-earth Aminoacid Complexes concentrated solution 30 parts.
Described Chinese medicinal components includes the raw material of following weight portion: Jerusalem artichoke 10 parts, 6 parts of Pericarpium Zanthoxyli, 10 parts of Ramulus Et Folium Picrasmae tree, Folium Artemisiae Argyi 3 parts,
Dittany 2 parts, Radix Platycodonis 3 parts, Flos Daturae 4 parts, Radix Rhapontici 3 parts, Rhizoma et radix veratri (Radix Rhizoma Veratri) 2 parts, Cortex Meliae 8 parts, Ramulus et Folium Pcrasmae (Cortex Picrasmae) 3 parts, Semen Arecae 1 part, Cortex ulmi pumilae
10 parts, Cortex Ailanthi 5 parts, Ramulus Sambuci Williamsii 2 parts, decomposite leaf common violet 2 parts, 7 parts of Salix babylonica L. leaf.
Described calcareous fertilisers are calcium oxide and calcium chloride；Described phosphate fertilizer is urea phosphate, phosphoric acid and APP；Described potash fertilizer is nitre
Acid potassium and potassium sulfate.
Described Rare-earth Aminoacid Complexes concentrated solution includes the raw material of following weight portion: leather waste 40 parts, cerine 30
Part, concentration are sulfuric acid solution 90 parts, 40 parts of the perchloric acid of 40%.
Described metal ion amino acid complex concentrated solution includes the raw material of following weight portion: bean cake 45 parts, concentration are
The hydrochloric acid solution of 40% 80 parts, 40 parts of smithsonite.
The preparation method of described solubility compound fertilizer, comprises the following steps:
(1) by the Chinese medicinal components Jerusalem artichoke weighed, Pericarpium Zanthoxyli, Ramulus Et Folium Picrasmae tree, Folium Artemisiae Argyi, dittany, Radix Platycodonis, Flos Daturae, Radix Rhapontici, Herba chenopodii
Reed, Cortex Meliae, Ramulus et Folium Pcrasmae (Cortex Picrasmae), Semen Arecae, Cortex ulmi pumilae, Cortex Ailanthi, Ramulus Sambuci Williamsii, decomposite leaf common violet, Salix babylonica L. leaf are put in container, add 5 times
Water soaking 3 hours, then heating 1.5 hours, leach filtrate, for filtrate one, are placed back in by filtering residue in container, add 2 times of water, add
Heat 1 hour, filters filtrate, obtains filtrate two, merging filtrate one and filtrate two, obtain herb liquid, and filtering residue is standby；
(2) Rare-earth Aminoacid Complexes concentrated solution is prepared: it is 200 that the leather waste of described weight portion is crushed to fineness
Day, place it in autoclave, add the sulfuric acid solution that concentration is 40% of described weight portion, be 120 DEG C in temperature,
Pressure is to hydrolyze 8 hours under conditions of 20MP, after filtering animal protein factor digest, standby；At normal temperatures by described weight
Part cerine powder be dissolved in in perchloric acid, react 1 hour under the conditions of 100 DEG C, filter out the impurity in solution, obtain rare earth from
Sub-settled solution；Gained rare earth ion clear liquor is mixed with animal protein factor digest, stirs in one direction, 90 DEG C of conditions
Lower reaction 1 hour, obtains Rare-earth Aminoacid Complexes solution, and being shifted bleeds in vaporizer is concentrated into the 1/4 of original volume,
To Rare-earth Aminoacid Complexes concentrated solution；
Prepare metal ion amino acid complex concentrated solution: it is 200 mesh that the bean cake powder of described weight portion is broken to fineness, throw
To the hydrochloric acid solution of described weight portion, boil to boiling and add smithsonite, in one direction stirring 1 hour, after filtering
Metal ion amino acid complex, being transferred in vaporizer bleeds is concentrated into original volume 1/4, obtains metal ion amino acid complex
Concentrated solution；
Described metal ion amino acid complex concentrated solution and Rare-earth Aminoacid Complexes concentrated solution are mixed by weight,
It is sufficiently stirred for 15 minutes, regulates pH value 8.5, obtain mixed concentrated liquid；
(3) by potash fertilizer, phosphate fertilizer, carbamide, humic acid mix homogeneously, it is then slowly added into calcareous fertilisers, stirring while adding, keep anti-
Answering system temperature is 65 DEG C, reacts complete, cooling, obtains mixture；
(4) by the herb liquid of step (1), the mixed concentrated liquid of step (2) and the mixture of step (3), bacillus subtilis
Bacteria agent and trace element mixing and stirring, pack and get final product.
Embodiment 3
In the embodiment of the present invention, a kind of solubility compound fertilizer, including the raw material of following weight portion: 60 parts of potash fertilizer, phosphate fertilizer
60 parts, calcareous fertilisers 30 parts, 20 parts of carbamide, trace element 8 parts, humic acid 25 parts, bacillus subtilis microbial agent 10 parts, Chinese medicinal components 4
Part, metal ion amino acid complex concentrated solution 40 parts, Rare-earth Aminoacid Complexes concentrated solution 40 parts.
As the present invention further scheme: described Chinese medicinal components includes the raw material of following weight portion: Jerusalem artichoke 15 parts, flower
Green pepper 8 parts, 15 parts of Ramulus Et Folium Picrasmae tree, Folium Artemisiae Argyi 4 parts, dittany 3 parts, Radix Platycodonis 4 parts, Flos Daturae 6 parts, Radix Rhapontici 5 parts, Rhizoma et radix veratri (Radix Rhizoma Veratri) 3 parts, Cortex Meliae 10
Part, Ramulus et Folium Pcrasmae (Cortex Picrasmae) 5 parts, Semen Arecae 2 parts, Cortex ulmi pumilae 15 parts, Cortex Ailanthi 8 parts, Ramulus Sambuci Williamsii 3 parts, decomposite leaf common violet 3 parts, 9 parts of Salix babylonica L. leaf.
Described calcareous fertilisers are calcium chloride；Described phosphate fertilizer is phosphoric acid and APP；Described potash fertilizer is potassium sulfate, biphosphate
Potassium and potassium metaphosphate.
Described Rare-earth Aminoacid Complexes concentrated solution includes the raw material of following weight portion: leather waste 60 parts, cerine 40
Part, concentration are sulfuric acid solution 100 parts, 50 parts of the perchloric acid of 40%.
Described metal ion amino acid complex concentrated solution includes the raw material of following weight portion: bean cake 60 parts, concentration are
The hydrochloric acid solution of 40% 100 parts, 50 parts of smithsonite.
The preparation method of described solubility compound fertilizer, comprises the following steps:
(1) by the Chinese medicinal components Jerusalem artichoke weighed, Pericarpium Zanthoxyli, Ramulus Et Folium Picrasmae tree, Folium Artemisiae Argyi, dittany, Radix Platycodonis, Flos Daturae, Radix Rhapontici, Herba chenopodii
Reed, Cortex Meliae, Ramulus et Folium Pcrasmae (Cortex Picrasmae), Semen Arecae, Cortex ulmi pumilae, Cortex Ailanthi, Ramulus Sambuci Williamsii, decomposite leaf common violet, Salix babylonica L. leaf are put in container, add 8 times
Water soaking 5 hours, then heating 2 hours, leach filtrate, for filtrate one, are placed back in by filtering residue in container, add 3 times of water, heating
1 hour, filtering filtrate, obtain filtrate two, merging filtrate one and filtrate two, obtain herb liquid, filtering residue is standby；
(2) Rare-earth Aminoacid Complexes concentrated solution is prepared: it is 200 that the leather waste of described weight portion is crushed to fineness
Day, place it in autoclave, add the sulfuric acid solution that concentration is 40% of described weight portion, be 125 DEG C in temperature,
Pressure is to hydrolyze 8 hours under conditions of 20MP, after filtering animal protein factor digest, standby；At normal temperatures by described weight
Part cerine powder be dissolved in in perchloric acid, react 1 hour under the conditions of 100 DEG C, filter out the impurity in solution, obtain rare earth from
Sub-settled solution；Gained rare earth ion clear liquor is mixed with animal protein factor digest, stirs in one direction, 90 DEG C of conditions
Lower reaction 1 hour, obtains Rare-earth Aminoacid Complexes solution, and being shifted bleeds in vaporizer is concentrated into the 1/4 of original volume,
To Rare-earth Aminoacid Complexes concentrated solution；
Prepare metal ion amino acid complex concentrated solution: it is 200 mesh that the bean cake powder of described weight portion is broken to fineness, throw
To the hydrochloric acid solution of described weight portion, boil to boiling and add smithsonite, in one direction stirring 1 hour, after filtering
Metal ion amino acid complex, being transferred in vaporizer bleeds is concentrated into original volume 1/4, obtains metal ion amino acid complex
Concentrated solution；
Described metal ion amino acid complex concentrated solution and Rare-earth Aminoacid Complexes concentrated solution are mixed by weight,
It is sufficiently stirred for 15 minutes, regulates pH value 9, obtain mixed concentrated liquid；
(3) by potash fertilizer, phosphate fertilizer, carbamide, humic acid mix homogeneously, it is then slowly added into calcareous fertilisers, stirring while adding, keep anti-
Answering system temperature is 80 DEG C, reacts complete, cooling, obtains mixture；
(4) by the herb liquid of step (1), the mixed concentrated liquid of step (2) and the mixture of step (3), bacillus subtilis
Bacteria agent and trace element mixing and stirring, pack and get final product.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie
In the case of the spirit or essential attributes of the present invention, it is possible to realize the present invention in other specific forms.Therefore, no matter
From the point of view of which point, all should regard embodiment as exemplary, and be nonrestrictive, the scope of the present invention is by appended power
Profit requires rather than described above limits, it is intended that all by fall in the implication of equivalency and scope of claim
Change is included in the present invention.
Although moreover, it will be appreciated that this specification is been described by according to embodiment, but the most each embodiment only wraps
Containing an independent technical scheme, this narrating mode of description is only that for clarity sake those skilled in the art should
Description can also be formed those skilled in the art through appropriately combined as an entirety, the technical scheme in each embodiment
May be appreciated other embodiments.
Claims (10)
1. a solubility compound fertilizer, it is characterised in that include the raw material of following weight portion: potash fertilizer 10-60 part, phosphate fertilizer 10-
60 parts, calcareous fertilisers 10-30 part, carbamide 2-20 part, trace element 2-8 part, humic acid 15-25 part, bacillus subtilis microbial agent 2-10
Part, Chinese medicinal components 2-4 part, metal ion amino acid complex concentrated solution 20-40 part, Rare-earth Aminoacid Complexes concentrated solution 20-
40 parts.
Solubility compound fertilizer the most according to claim 1, it is characterised in that include the raw material of following weight portion: potash fertilizer
35 parts, 35 parts of phosphate fertilizer, calcareous fertilisers 20 parts, 11 parts of carbamide, trace element 5 parts, humic acid 20 parts, bacillus subtilis microbial agent 6 parts, in
Medicine component 3 parts, metal ion amino acid complex concentrated solution 30 parts, Rare-earth Aminoacid Complexes concentrated solution 30 parts.
Solubility compound fertilizer the most according to claim 1, it is characterised in that described Chinese medicinal components includes following weight portion
Raw material: Jerusalem artichoke 5-15 part, Pericarpium Zanthoxyli 4-8 part, Ramulus Et Folium Picrasmae tree 5-15 part, Folium Artemisiae Argyi 2-4 part, dittany 1-3 part, Radix Platycodonis 2-4 part, Flos Daturae
2-6 part, Radix Rhapontici 1-5 part, Rhizoma et radix veratri (Radix Rhizoma Veratri) 1-3 part, Cortex Meliae 6-10 part, Ramulus et Folium Pcrasmae (Cortex Picrasmae) 1-5 part, Semen Arecae 1-2 part, Cortex ulmi pumilae 5-15 part, the tree of heaven
Rhizoma Euonymus 2-8 part, Ramulus Sambuci Williamsii 1-3 part, decomposite leaf common violet 1-3 part, Salix babylonica L. leaf 5-9 part.
Solubility compound fertilizer the most according to claim 3, it is characterised in that described Chinese medicinal components includes following weight portion
Raw material: Jerusalem artichoke 10 parts, 6 parts of Pericarpium Zanthoxyli, 10 parts of Ramulus Et Folium Picrasmae tree, Folium Artemisiae Argyi 3 parts, dittany 2 parts, Radix Platycodonis 3 parts, Flos Daturae 4 parts, Radix Rhapontici 3 parts,
Rhizoma et radix veratri (Radix Rhizoma Veratri) 2 parts, Cortex Meliae 8 parts, Ramulus et Folium Pcrasmae (Cortex Picrasmae) 3 parts, Semen Arecae 1 part, Cortex ulmi pumilae 10 parts, Cortex Ailanthi 5 parts, Ramulus Sambuci Williamsii 2 parts, decomposite leaf common violet 2
Part, 7 parts of Salix babylonica L. leaf.
Solubility compound fertilizer the most according to claim 1, it is characterised in that described calcareous fertilisers are calcium oxide, calcium nitrate, nitre
One or more in acid ammonium calcium or calcium chloride；Described phosphate fertilizer is MAP, Diammonium phosphate (DAP), urea phosphate, phosphoric acid or polyphosphoric acid
One or more in ammonium；Described potash fertilizer is potassium chloride, potassium nitrate, potassium sulfate, potassium dihydrogen phosphate, potassium metaphosphate or phosphoric acid hydrogen two
One or more in potassium.
Solubility compound fertilizer the most according to claim 1, it is characterised in that described Rare-earth Aminoacid Complexes concentrated solution
Raw material including following weight portion: leather waste 20-60 part, cerine 20-40 part, concentration are the sulfuric acid solution 80-100 of 40%
Part, perchloric acid 30-50 part.
Solubility compound fertilizer the most according to claim 1, it is characterised in that described metal ion amino acid complex is dense
Contracting liquid includes the raw material of following weight portion: bean cake 30-60 part, concentration are hydrochloric acid solution 60-100 part, the smithsonite 30-50 of 40%
Part.
8. the preparation method of the solubility compound fertilizer as described in claim 1-7 is arbitrary, it is characterised in that include following
Step:
(1) by the Chinese medicinal components Jerusalem artichoke weighed, Pericarpium Zanthoxyli, Ramulus Et Folium Picrasmae tree, Folium Artemisiae Argyi, dittany, Radix Platycodonis, Flos Daturae, Radix Rhapontici, Rhizoma et radix veratri (Radix Rhizoma Veratri), hardship
Chinaberry skin, Ramulus et Folium Pcrasmae (Cortex Picrasmae), Semen Arecae, Cortex ulmi pumilae, Cortex Ailanthi, Ramulus Sambuci Williamsii, decomposite leaf common violet, Salix babylonica L. leaf are put in container, add 3-8 times of water logging
Steeping 2-5 hour, then heating 1-2 hour, leaches filtrate, for filtrate one, is placed back in by filtering residue in container, add 2-3 times of water, add
Heat 1 hour, filters filtrate, obtains filtrate two, merging filtrate one and filtrate two, obtain herb liquid, and filtering residue is standby；
(2) described metal ion amino acid complex concentrated solution and Rare-earth Aminoacid Complexes concentrated solution are mixed by weight,
It is sufficiently stirred for 15 minutes, regulates pH value 8-9, obtain mixed concentrated liquid；
(3) by potash fertilizer, phosphate fertilizer, carbamide, humic acid mix homogeneously, it is then slowly added into calcareous fertilisers, stirring while adding, keep reactant
Be temperature be 50～80 DEG C, react complete, cooling, obtain mixture；
(4) by the herb liquid of step (1), the mixed concentrated liquid of step (2) and the mixture of step (3), bacillus subtilis bacterium
Agent and trace element mixing and stirring, pack and get final product.
The preparation method of solubility compound fertilizer the most according to claim 8, it is characterised in that described Rare Earth Amino-Acid network
The preparation method of compound concentrated solution comprises the following steps: the leather waste of described weight portion is crushed to fineness is 200, by it
It is placed in autoclave, adds the sulfuric acid solution that concentration is 40% of described weight portion, be 110-125 ° of C in temperature, pressure
Strong be to hydrolyze 8 hours under conditions of 20MP, obtains animal protein factor digest after filtering, standby；At normal temperatures by described weight portion
Cerine powder be dissolved in in perchloric acid, react 1 hour under the conditions of 100 DEG C, filter out the impurity in solution, obtain rare earth ion
Settled solution；Gained rare earth ion clear liquor is mixed with animal protein factor digest, stirs in one direction, under the conditions of 90 DEG C
Reacting 1 hour, obtain Rare-earth Aminoacid Complexes solution, being shifted bleeds in vaporizer is concentrated into the 1/4 of original volume, obtains
Rare-earth Aminoacid Complexes concentrated solution.
The preparation method of solubility compound fertilizer the most according to claim 8, it is characterised in that described metal ion ammonia
The preparation method of base acid complex concentrated solution comprises the following steps: it is 200 mesh that the bean cake powder of described weight portion is broken to fineness, throws
To the hydrochloric acid solution of described weight portion, boil to boiling and add smithsonite, in one direction stirring 1 hour, after filtering
Metal ion amino acid complex, being transferred in vaporizer bleeds is concentrated into original volume 1/4, obtains metal ion amino acid complex
Concentrated solution.
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| CN106883060A (en) * | 2016-12-28 | 2017-06-23 | 赵永明 | A kind of pesticide-germicide growth promoting composition for promoting crop growth |
| CN107400016A (en) * | 2017-09-01 | 2017-11-28 | 临泉县生产力促进中心 | A kind of garden soil improvement organic fertilizer and preparation method thereof |
| CN107573189A (en) * | 2017-09-01 | 2018-01-12 | 临泉县生产力促进中心 | A kind of gardens specific complex chemical fertilizer |
| CN107573184A (en) * | 2017-09-01 | 2018-01-12 | 临泉县生产力促进中心 | A kind of gardens nutritious fertilizer and preparation method thereof |
| CN109336680A (en) * | 2018-11-07 | 2019-02-15 | 郑州启汇果品有限公司 | A kind of bio-feritlizer and preparation method thereof for preventing and treating root-rot |
| CN109942343A (en) * | 2019-03-11 | 2019-06-28 | 安徽泓森高科林业股份有限公司 | A kind of composite microbe fertilizer |
| CN109988006A (en) * | 2017-12-30 | 2019-07-09 | 程艳青 | A kind of processing method of the micro- fertilizer of fulvic acid base biological pesticide |
| CN110862284A (en) * | 2019-12-20 | 2020-03-06 | 河南浩创生物科技有限公司 | Crop yield increasing complexing agent and preparation method thereof |
| CN111763116A (en) * | 2020-07-13 | 2020-10-13 | 广西南宁华夏农业科技有限公司 | Organic-inorganic compound fertilizer capable of adjusting acid, supplementing magnesium and preventing plant yellowing and preparation method thereof |
| CN112919962A (en) * | 2021-02-03 | 2021-06-08 | 吉林省农业科学院 | Tobacco high-potassium soluble fertilizer and preparation method thereof |
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| CN106883060A (en) * | 2016-12-28 | 2017-06-23 | 赵永明 | A kind of pesticide-germicide growth promoting composition for promoting crop growth |
| CN107400016A (en) * | 2017-09-01 | 2017-11-28 | 临泉县生产力促进中心 | A kind of garden soil improvement organic fertilizer and preparation method thereof |
| CN107573189A (en) * | 2017-09-01 | 2018-01-12 | 临泉县生产力促进中心 | A kind of gardens specific complex chemical fertilizer |
| CN107573184A (en) * | 2017-09-01 | 2018-01-12 | 临泉县生产力促进中心 | A kind of gardens nutritious fertilizer and preparation method thereof |
| CN109988006A (en) * | 2017-12-30 | 2019-07-09 | 程艳青 | A kind of processing method of the micro- fertilizer of fulvic acid base biological pesticide |
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| CN109942343A (en) * | 2019-03-11 | 2019-06-28 | 安徽泓森高科林业股份有限公司 | A kind of composite microbe fertilizer |
| CN110862284A (en) * | 2019-12-20 | 2020-03-06 | 河南浩创生物科技有限公司 | Crop yield increasing complexing agent and preparation method thereof |
| CN111763116A (en) * | 2020-07-13 | 2020-10-13 | 广西南宁华夏农业科技有限公司 | Organic-inorganic compound fertilizer capable of adjusting acid, supplementing magnesium and preventing plant yellowing and preparation method thereof |
| CN112919962A (en) * | 2021-02-03 | 2021-06-08 | 吉林省农业科学院 | Tobacco high-potassium soluble fertilizer and preparation method thereof |
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