CN106061934B - 用于生产丙烯酸的方法和系统 - Google Patents
用于生产丙烯酸的方法和系统 Download PDFInfo
- Publication number
- CN106061934B CN106061934B CN201580009720.7A CN201580009720A CN106061934B CN 106061934 B CN106061934 B CN 106061934B CN 201580009720 A CN201580009720 A CN 201580009720A CN 106061934 B CN106061934 B CN 106061934B
- Authority
- CN
- China
- Prior art keywords
- column
- stream
- final process
- process column
- acrylic acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
- C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/10—Vacuum distillation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
- B01D5/0027—Condensation of vapours; Recovering volatile solvents by condensation by direct contact between vapours or gases and the cooling medium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
- B01D5/0057—Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes
- B01D5/006—Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes with evaporation or distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/50—Use of additives, e.g. for stabilisation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C57/00—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms
- C07C57/02—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms with only carbon-to-carbon double bonds as unsaturation
- C07C57/03—Monocarboxylic acids
- C07C57/04—Acrylic acid; Methacrylic acid
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201461942261P | 2014-02-20 | 2014-02-20 | |
US61/942,261 | 2014-02-20 | ||
PCT/US2015/015520 WO2015126704A1 (en) | 2014-02-20 | 2015-02-12 | Process and system for producing acrylic acid |
Publications (2)
Publication Number | Publication Date |
---|---|
CN106061934A CN106061934A (zh) | 2016-10-26 |
CN106061934B true CN106061934B (zh) | 2019-05-03 |
Family
ID=53878832
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201580009720.7A Active CN106061934B (zh) | 2014-02-20 | 2015-02-12 | 用于生产丙烯酸的方法和系统 |
Country Status (11)
Country | Link |
---|---|
US (1) | US10112885B2 (ko) |
EP (1) | EP3110786B1 (ko) |
JP (1) | JP6703950B2 (ko) |
KR (1) | KR102327728B1 (ko) |
CN (1) | CN106061934B (ko) |
BR (1) | BR112016019248B1 (ko) |
MX (1) | MX2016010692A (ko) |
SA (1) | SA516371688B1 (ko) |
SG (1) | SG11201606743PA (ko) |
TW (1) | TWI658035B (ko) |
WO (1) | WO2015126704A1 (ko) |
Families Citing this family (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR3041958B1 (fr) * | 2015-10-06 | 2019-06-14 | Arkema France | Procede ameliore de production d’acide (meth)acrylique de grade polymere |
DE202015106097U1 (de) * | 2015-11-11 | 2016-02-01 | Holger Blum | Fördereinrichtung für eine Vakuumdestillationsanlage |
FR3049601B1 (fr) * | 2016-03-29 | 2018-03-09 | Arkema France | Procede ameliore de production d'acide (meth)acrylique |
JP6522213B1 (ja) * | 2018-08-03 | 2019-05-29 | 住友化学株式会社 | メタクロレイン及び/又はメタクリル酸の製造方法 |
FR3094716B1 (fr) * | 2019-04-02 | 2021-06-04 | Arkema France | Production d’acide acrylique de grade polymere |
FR3108906B1 (fr) | 2020-04-06 | 2022-03-04 | Arkema France | Procede de purification d’acide (meth)acrylique |
KR20230054198A (ko) * | 2021-10-15 | 2023-04-24 | 주식회사 엘지화학 | 아크릴산 제조방법 |
KR20230054201A (ko) * | 2021-10-15 | 2023-04-24 | 주식회사 엘지화학 | 아크릴산 제조방법 |
CN114632343B (zh) * | 2022-05-18 | 2022-12-02 | 北京化工大学 | 一种mvr热泵精馏系统及方法 |
KR20240037081A (ko) * | 2022-09-14 | 2024-03-21 | 주식회사 엘지화학 | 아크릴산 제조방법 |
KR20240037093A (ko) * | 2022-09-14 | 2024-03-21 | 주식회사 엘지화학 | 아크릴산 제조방법 |
CN115738328B (zh) * | 2022-11-28 | 2024-07-19 | 东营市赫邦化工有限公司 | 一种节能的循环式甘油蒸馏蒸发器 |
WO2024215008A1 (ko) * | 2023-04-12 | 2024-10-17 | 주식회사 엘지화학 | 젖산 탈수 반응을 통한 아크릴산 제조 방법 및 이의 제조 장치 |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6525216B1 (en) * | 1999-06-10 | 2003-02-25 | Nippon Shokubai Co., Ltd. | Method of manufacturing (meth)acrylic acid |
WO2010027732A1 (en) * | 2008-09-04 | 2010-03-11 | Dow Global Technologies Inc. | Process for producing acrolein and/or acrylic acid from propane |
Family Cites Families (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3168136A (en) * | 1955-03-17 | 1965-02-02 | Babcock & Wilcox Co | Shell and tube-type heat exchanger |
FR1357332A (fr) | 1962-05-18 | 1964-04-03 | Shell Int Research | Procédé d'amélioration de la résistance au choc des pièces moulées en polypropylène |
US3301871A (en) | 1964-06-15 | 1967-01-31 | Upjohn Co | Novel 1, 4-dialkylprolines, derivatives thereof and process |
US3314220A (en) * | 1965-03-22 | 1967-04-18 | Foster Wheeler Corp | Multiannular centrifugal separator |
EP0557790B1 (en) * | 1992-02-28 | 1998-08-19 | Sumitomo Chemical Company Limited | Process for producing isobutylene by oxidative dehydrogenation of isobutane |
JP3411280B2 (ja) * | 1992-09-21 | 2003-05-26 | 協和醗酵工業株式会社 | 血小板減少症治療剤 |
JPH10204030A (ja) * | 1997-01-24 | 1998-08-04 | Toagosei Co Ltd | (メタ)アクリル酸エステルの精製方法及び製造方法並びにその製造装置 |
US6019820A (en) | 1997-05-07 | 2000-02-01 | E. I. Du Pont De Nemours And Company | Liquid jet compressor |
DE19740253A1 (de) | 1997-09-12 | 1999-03-18 | Basf Ag | Verfahren zur fraktionierten Kondensation eines heißen Gasgemisches mit einem hohen Anteil nicht kondensierbarer Komponenten |
DE19837519A1 (de) * | 1998-08-19 | 2000-02-24 | Basf Ag | Verfahren zur Herstellung von Acrolein und/oder Acrylsäure aus Propan |
JP4698778B2 (ja) * | 1999-06-03 | 2011-06-08 | 株式会社日本触媒 | (メタ)アクリル酸(エステル)の精製方法 |
JP2001131116A (ja) | 1999-11-08 | 2001-05-15 | Nippon Shokubai Co Ltd | 易重合性物質含有液の蒸留方法 |
CN1307145C (zh) | 2001-08-22 | 2007-03-28 | 三菱化学株式会社 | 容易聚合化合物用蒸馏装置 |
JP2005179352A (ja) * | 2003-11-28 | 2005-07-07 | Mitsubishi Chemicals Corp | (メタ)アクリル酸の精製方法 |
EP2502895B1 (en) * | 2006-09-15 | 2016-08-31 | Arkema Inc. | Process for producing acrylic acid |
WO2009123872A1 (en) | 2008-04-01 | 2009-10-08 | Dow Global Technologies Inc. | Procedure for the startup of a (meth)acrylic acid plant |
FR2935971B1 (fr) | 2008-09-16 | 2010-11-19 | Arkema France | Acide bio-acrylique de grade polymere et son procede de fabrication a partir de glycerol. |
US9745244B2 (en) | 2008-10-01 | 2017-08-29 | Arkeme Inc. | Control of a process for the purification of (meth)acrylic acid using on-line, near IR analysis |
EP2179981A1 (en) * | 2008-10-24 | 2010-04-28 | Arkema France | Process for manufacturing acrolein from glycerol |
-
2015
- 2015-02-12 EP EP15751390.4A patent/EP3110786B1/en active Active
- 2015-02-12 WO PCT/US2015/015520 patent/WO2015126704A1/en active Application Filing
- 2015-02-12 SG SG11201606743PA patent/SG11201606743PA/en unknown
- 2015-02-12 MX MX2016010692A patent/MX2016010692A/es unknown
- 2015-02-12 BR BR112016019248-6A patent/BR112016019248B1/pt active IP Right Grant
- 2015-02-12 JP JP2016553438A patent/JP6703950B2/ja active Active
- 2015-02-12 KR KR1020167023211A patent/KR102327728B1/ko active IP Right Grant
- 2015-02-12 CN CN201580009720.7A patent/CN106061934B/zh active Active
- 2015-02-12 US US15/118,126 patent/US10112885B2/en active Active
- 2015-02-17 TW TW104105708A patent/TWI658035B/zh not_active IP Right Cessation
-
2016
- 2016-08-18 SA SA516371688A patent/SA516371688B1/ar unknown
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6525216B1 (en) * | 1999-06-10 | 2003-02-25 | Nippon Shokubai Co., Ltd. | Method of manufacturing (meth)acrylic acid |
WO2010027732A1 (en) * | 2008-09-04 | 2010-03-11 | Dow Global Technologies Inc. | Process for producing acrolein and/or acrylic acid from propane |
Also Published As
Publication number | Publication date |
---|---|
EP3110786A4 (en) | 2017-09-06 |
EP3110786B1 (en) | 2021-08-25 |
WO2015126704A1 (en) | 2015-08-27 |
BR112016019248A2 (ko) | 2017-08-15 |
JP6703950B2 (ja) | 2020-06-03 |
SG11201606743PA (en) | 2016-09-29 |
US20170174604A1 (en) | 2017-06-22 |
TW201534581A (zh) | 2015-09-16 |
KR20160122749A (ko) | 2016-10-24 |
EP3110786A1 (en) | 2017-01-04 |
CN106061934A (zh) | 2016-10-26 |
US10112885B2 (en) | 2018-10-30 |
JP2017509613A (ja) | 2017-04-06 |
MX2016010692A (es) | 2017-05-09 |
BR112016019248B1 (pt) | 2022-03-15 |
KR102327728B1 (ko) | 2021-11-18 |
SA516371688B1 (ar) | 2019-04-16 |
TWI658035B (zh) | 2019-05-01 |
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GR01 | Patent grant |