CN105980346B - 生产碳酸酯的方法 - Google Patents

生产碳酸酯的方法 Download PDF

Info

Publication number
CN105980346B
CN105980346B CN201580007123.0A CN201580007123A CN105980346B CN 105980346 B CN105980346 B CN 105980346B CN 201580007123 A CN201580007123 A CN 201580007123A CN 105980346 B CN105980346 B CN 105980346B
Authority
CN
China
Prior art keywords
tube
catalyst
phosgene
reactor
diameter
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201580007123.0A
Other languages
English (en)
Chinese (zh)
Other versions
CN105980346A (zh
Inventor
潘卡杰·辛格·高塔姆
小威廉·E·霍拉
纳达尔 塞尔焦·费雷尔
约翰·约瑟夫·安德森
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SABIC Global Technologies BV
Original Assignee
SABIC Global Technologies BV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by SABIC Global Technologies BV filed Critical SABIC Global Technologies BV
Publication of CN105980346A publication Critical patent/CN105980346A/zh
Application granted granted Critical
Publication of CN105980346B publication Critical patent/CN105980346B/zh
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C68/00—Preparation of esters of carbonic or haloformic acids
    • C07C68/02—Preparation of esters of carbonic or haloformic acids from phosgene or haloformates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/245—Stationary reactors without moving elements inside placed in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/0285—Heating or cooling the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0403—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the fluid flow within the beds being predominantly horizontal
    • B01J8/0423—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the fluid flow within the beds being predominantly horizontal through two or more otherwise shaped beds
    • B01J8/0438—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the fluid flow within the beds being predominantly horizontal through two or more otherwise shaped beds the beds being placed next to each other
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0403—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the fluid flow within the beds being predominantly horizontal
    • B01J8/0423—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the fluid flow within the beds being predominantly horizontal through two or more otherwise shaped beds
    • B01J8/0442—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the fluid flow within the beds being predominantly horizontal through two or more otherwise shaped beds the beds being placed in separate reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B01J8/067—Heating or cooling the reactor
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/80—Phosgene
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/96—Esters of carbonic or haloformic acids
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28—HEAT EXCHANGE IN GENERAL
    • F28F—DETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
    • F28F1/00—Tubular elements; Assemblies of tubular elements
    • F28F1/02—Tubular elements of cross-section which is non-circular
    • F28F1/025—Tubular elements of cross-section which is non-circular with variable shape, e.g. with modified tube ends, with different geometrical features
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28—HEAT EXCHANGE IN GENERAL
    • F28F—DETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
    • F28F1/00—Tubular elements; Assemblies of tubular elements
    • F28F1/08—Tubular elements crimped or corrugated in longitudinal section
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28—HEAT EXCHANGE IN GENERAL
    • F28F—DETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
    • F28F1/00—Tubular elements; Assemblies of tubular elements
    • F28F1/10—Tubular elements and assemblies thereof with means for increasing heat-transfer area, e.g. with fins, with projections, with recesses
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28—HEAT EXCHANGE IN GENERAL
    • F28F—DETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
    • F28F1/00—Tubular elements; Assemblies of tubular elements
    • F28F1/10—Tubular elements and assemblies thereof with means for increasing heat-transfer area, e.g. with fins, with projections, with recesses
    • F28F1/12—Tubular elements and assemblies thereof with means for increasing heat-transfer area, e.g. with fins, with projections, with recesses the means being only outside the tubular element
    • F28F1/14—Tubular elements and assemblies thereof with means for increasing heat-transfer area, e.g. with fins, with projections, with recesses the means being only outside the tubular element and extending longitudinally
    • F28F1/16—Tubular elements and assemblies thereof with means for increasing heat-transfer area, e.g. with fins, with projections, with recesses the means being only outside the tubular element and extending longitudinally the means being integral with the element, e.g. formed by extrusion
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28—HEAT EXCHANGE IN GENERAL
    • F28F—DETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
    • F28F1/00—Tubular elements; Assemblies of tubular elements
    • F28F1/10—Tubular elements and assemblies thereof with means for increasing heat-transfer area, e.g. with fins, with projections, with recesses
    • F28F1/12—Tubular elements and assemblies thereof with means for increasing heat-transfer area, e.g. with fins, with projections, with recesses the means being only outside the tubular element
    • F28F1/24—Tubular elements and assemblies thereof with means for increasing heat-transfer area, e.g. with fins, with projections, with recesses the means being only outside the tubular element and extending transversely
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28—HEAT EXCHANGE IN GENERAL
    • F28F—DETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
    • F28F1/00—Tubular elements; Assemblies of tubular elements
    • F28F1/10—Tubular elements and assemblies thereof with means for increasing heat-transfer area, e.g. with fins, with projections, with recesses
    • F28F1/12—Tubular elements and assemblies thereof with means for increasing heat-transfer area, e.g. with fins, with projections, with recesses the means being only outside the tubular element
    • F28F1/34—Tubular elements and assemblies thereof with means for increasing heat-transfer area, e.g. with fins, with projections, with recesses the means being only outside the tubular element and extending obliquely
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28—HEAT EXCHANGE IN GENERAL
    • F28F—DETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
    • F28F1/00—Tubular elements; Assemblies of tubular elements
    • F28F1/10—Tubular elements and assemblies thereof with means for increasing heat-transfer area, e.g. with fins, with projections, with recesses
    • F28F1/12—Tubular elements and assemblies thereof with means for increasing heat-transfer area, e.g. with fins, with projections, with recesses the means being only outside the tubular element
    • F28F1/38—Tubular elements and assemblies thereof with means for increasing heat-transfer area, e.g. with fins, with projections, with recesses the means being only outside the tubular element and being staggered to form tortuous fluid passages
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28—HEAT EXCHANGE IN GENERAL
    • F28F—DETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
    • F28F1/00—Tubular elements; Assemblies of tubular elements
    • F28F1/10—Tubular elements and assemblies thereof with means for increasing heat-transfer area, e.g. with fins, with projections, with recesses
    • F28F1/40—Tubular elements and assemblies thereof with means for increasing heat-transfer area, e.g. with fins, with projections, with recesses the means being only inside the tubular element
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28—HEAT EXCHANGE IN GENERAL
    • F28F—DETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
    • F28F1/00—Tubular elements; Assemblies of tubular elements
    • F28F1/10—Tubular elements and assemblies thereof with means for increasing heat-transfer area, e.g. with fins, with projections, with recesses
    • F28F1/42—Tubular elements and assemblies thereof with means for increasing heat-transfer area, e.g. with fins, with projections, with recesses the means being both outside and inside the tubular element
    • F28F1/424—Means comprising outside portions integral with inside portions
    • F28F1/426—Means comprising outside portions integral with inside portions the outside portions and the inside portions forming parts of complementary shape, e.g. concave and convex
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28—HEAT EXCHANGE IN GENERAL
    • F28F—DETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
    • F28F13/00—Arrangements for modifying heat-transfer, e.g. increasing, decreasing
    • F28F13/06—Arrangements for modifying heat-transfer, e.g. increasing, decreasing by affecting the pattern of flow of the heat-exchange media
    • F28F13/08—Arrangements for modifying heat-transfer, e.g. increasing, decreasing by affecting the pattern of flow of the heat-exchange media by varying the cross-section of the flow channels
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00185—Fingers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00194—Tubes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00212—Plates; Jackets; Cylinders
    • B01J2208/00221—Plates; Jackets; Cylinders comprising baffles for guiding the flow of the heat exchange medium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00212—Plates; Jackets; Cylinders
    • B01J2208/00238—Adjusting the heat-exchange profile by adapting catalyst tubes or the distribution thereof, e.g. by using inserts in some of the tubes or adding external fins
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00513—Controlling the temperature using inert heat absorbing solids in the bed
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/02—Processes carried out in the presence of solid particles; Reactors therefor with stationary particles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/06—Details of tube reactors containing solid particles
    • B01J2208/065—Heating or cooling the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00004—Scale aspects
    • B01J2219/00015—Scale-up
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/19—Details relating to the geometry of the reactor
    • B01J2219/192—Details relating to the geometry of the reactor polygonal
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/19—Details relating to the geometry of the reactor
    • B01J2219/192—Details relating to the geometry of the reactor polygonal
    • B01J2219/1923—Details relating to the geometry of the reactor polygonal square or square-derived
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/19—Details relating to the geometry of the reactor
    • B01J2219/194—Details relating to the geometry of the reactor round
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/19—Details relating to the geometry of the reactor
    • B01J2219/194—Details relating to the geometry of the reactor round
    • B01J2219/1941—Details relating to the geometry of the reactor round circular or disk-shaped
    • B01J2219/1943—Details relating to the geometry of the reactor round circular or disk-shaped cylindrical
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/19—Details relating to the geometry of the reactor
    • B01J2219/194—Details relating to the geometry of the reactor round
    • B01J2219/1941—Details relating to the geometry of the reactor round circular or disk-shaped
    • B01J2219/1944—Details relating to the geometry of the reactor round circular or disk-shaped spiral
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/19—Details relating to the geometry of the reactor
    • B01J2219/194—Details relating to the geometry of the reactor round
    • B01J2219/1941—Details relating to the geometry of the reactor round circular or disk-shaped
    • B01J2219/1946—Details relating to the geometry of the reactor round circular or disk-shaped conical
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/19—Details relating to the geometry of the reactor
    • B01J2219/194—Details relating to the geometry of the reactor round
    • B01J2219/1947—Details relating to the geometry of the reactor round oval or ellipsoidal
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28—HEAT EXCHANGE IN GENERAL
    • F28F—DETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
    • F28F2210/00—Heat exchange conduits
    • F28F2210/02—Heat exchange conduits with particular branching, e.g. fractal conduit arrangements

Landscapes

  • Physics & Mathematics (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Thermal Sciences (AREA)
  • Geometry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Fluid Mechanics (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN201580007123.0A 2014-02-04 2015-02-04 生产碳酸酯的方法 Active CN105980346B (zh)

Applications Claiming Priority (9)

Application Number Priority Date Filing Date Title
EP14382039.7 2014-02-04
EP14382036.3 2014-02-04
EP14382036 2014-02-04
EP14382039 2014-02-04
EP14382037.1 2014-02-04
EP14382035.5 2014-02-04
EP14382037 2014-02-04
EP14382035 2014-02-04
PCT/US2015/014345 WO2015119981A2 (en) 2014-02-04 2015-02-04 Method for producing carbonates

Publications (2)

Publication Number Publication Date
CN105980346A CN105980346A (zh) 2016-09-28
CN105980346B true CN105980346B (zh) 2018-05-18

Family

ID=52469934

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201580007123.0A Active CN105980346B (zh) 2014-02-04 2015-02-04 生产碳酸酯的方法

Country Status (6)

Country Link
US (1) US9695106B2 (https=)
EP (1) EP3102558B1 (https=)
JP (1) JP6316446B2 (https=)
KR (1) KR101859207B1 (https=)
CN (1) CN105980346B (https=)
WO (1) WO2015119981A2 (https=)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU228612U1 (ru) * 2024-06-19 2024-09-05 Общество с ограниченной ответственностью "ФАСТ ИНЖИНИРИНГ" Каталитический реактор радиально-спирального типа

Families Citing this family (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3024782B1 (en) 2013-07-26 2019-06-12 SABIC Global Technologies B.V. Method and apparatus for producing high purity phosgene
WO2015013655A1 (en) 2013-07-26 2015-01-29 Sabic Innovative Plastics Ip B.V. Method and apparatus for producing high purity phosgene
EP3024813B1 (en) 2014-02-04 2017-03-29 SABIC Global Technologies B.V. Method for producing carbonates
JP1541388S (https=) * 2015-05-21 2016-01-12
JP1541387S (https=) * 2015-05-21 2016-01-12
DE102015113432A1 (de) * 2015-08-14 2017-02-16 Karlsruher Institut für Technologie Strömungsleitelemente in einem Kanal
US10889762B2 (en) * 2016-12-09 2021-01-12 Velocys Technologies Limited Process for operating a highly productive tubular reactor
JP6848456B2 (ja) * 2017-01-16 2021-03-24 株式会社Ihi 反応装置
US20180202724A1 (en) * 2017-01-19 2018-07-19 Dong Yong Hot Water System Inc. Conductive structure of heat exchange pipe
CN106679467B (zh) * 2017-02-28 2019-04-05 郑州大学 具有外接管箱的管壳式换热器
CN106855367B (zh) * 2017-02-28 2024-01-26 郑州大学 具有分布性出入口的管壳式换热器
CN111448237B (zh) * 2017-12-18 2022-12-23 科思创德国股份有限公司 使用基于氯代烃的有机溶剂制备聚碳酸酯的方法
EP3498752A1 (de) * 2017-12-18 2019-06-19 Covestro Deutschland AG Verfahren zur herstellung eines polycarbonats unter verwendung eines organischen lösungsmittels auf der grundlage von chlorkohlenwasserstoffen
US10563932B2 (en) 2017-12-21 2020-02-18 Uop Llc Process and apparatus for cooling catalyst
CN108355601A (zh) * 2018-03-16 2018-08-03 邱洪 顺-反螺纹管道与压凸管道交替的连续流反应器
WO2019202557A1 (en) * 2018-04-19 2019-10-24 Koch Heat Transfer Company, Lp Heat exchanging apparatus and method of supporting tube bundle within heat exchanger
FR3088994B1 (fr) * 2018-11-28 2020-12-25 Liebherr Aerospace Toulouse Sas Échangeur de chaleur et système de refroidissement d’un fluide comprenant un tel échangeur de chaleur
CN111760581B (zh) 2019-08-30 2021-07-23 万华化学（宁波）有限公司 制备光气的催化剂及其制备方法和光气制备与能源综合利用的方法
TWI744725B (zh) * 2019-09-27 2021-11-01 財團法人工業技術研究院 高溫分流組件及利用其之熱交換器與重組機構
US11656032B2 (en) * 2019-09-27 2023-05-23 Industrial Technology Research Institute High temperature flow splitting component and heat exchanger and reforming means using the same
KR102751369B1 (ko) * 2019-12-30 2025-01-06 에스케이이노베이션 주식회사 유동층 반응기 및 이를 이용한 리튬 이차 전지의 활성 금속 회수 방법
EP3855107B1 (en) 2020-01-24 2025-07-30 Hamilton Sundstrand Corporation Fractal heat exchanger

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6399823B1 (en) * 2001-04-30 2002-06-04 General Electric Company Method for producing phosgene
CN1638856A (zh) * 2002-02-27 2005-07-13 巴斯福股份公司 用于生产光气的反应器和方法
CN101027122A (zh) * 2004-09-27 2007-08-29 住友化学株式会社 接触气相反应用多管式反应装置

Family Cites Families (54)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1642959A1 (de) 1968-03-14 1971-06-03 Basf Ag Reaktor zur Ausfuehrung von endo- und exothermen Reaktionen
FR2113249A5 (https=) 1970-11-03 1972-06-23 Getters Spa
DE2509036C2 (de) 1975-03-01 1986-05-28 Bayer Ag, 5090 Leverkusen Verfahren zur Herstellung von symmetrischen Diarylcarbonaten
DE3327274A1 (de) * 1983-07-28 1985-02-07 Bayer Ag, 5090 Leverkusen Verfahren zur herstellung von phosgen unter gleichzeitiger erzeugung von dampf
US4792620A (en) * 1983-10-14 1988-12-20 Bp Chemicals Limited Carbonylation catalysts
GB2164438B (en) * 1984-09-14 1988-07-27 Aisin Seiki Heat exchangers
US4697034A (en) 1985-11-15 1987-09-29 General Electric Company Process for making diaryl carbonates
US4839458A (en) 1986-06-18 1989-06-13 Mitsubishi Chemical Industries Ltd. Preparation with controlled amounts of polycarbonate carbon tetrachloride
US5136077A (en) 1989-12-18 1992-08-04 The Dow Chemical Company Process for the preparation of diaryl carbonates
JP3100051B2 (ja) * 1990-02-19 2000-10-16 株式会社ノリタケカンパニーリミテド 熱交換用管体及び熱交換器
DE4034717A1 (de) 1990-11-01 1992-05-07 Bayer Ag Verfahren zur herstellung von arylcarbonaten
US5167946A (en) 1990-12-27 1992-12-01 The Dow Chemical Company Diaryl carbonate process
US5239105A (en) 1992-01-30 1993-08-24 The Dow Chemical Company Catalytic formation of diarylcarbonates
US5498319A (en) 1993-06-29 1996-03-12 General Electric Company Process for purifying diaryl carbonates
DE4324153A1 (de) 1993-07-19 1995-01-26 Bayer Ag Verfahren zur Herstellung von Arylcarbonaten
US5424473A (en) 1994-03-16 1995-06-13 The Dow Chemical Company Process for the preparation of aryl haloformates and diaryl carbonates
JP3124455B2 (ja) 1994-12-01 2001-01-15 出光石油化学株式会社 ホスゲンの製造方法
JPH08198816A (ja) 1995-01-23 1996-08-06 Mitsubishi Gas Chem Co Inc 炭酸ジフェニルの精製方法
DE19600631A1 (de) 1996-01-10 1997-07-17 Bayer Ag Verfahren zur Reinigung von Kohlensäurediarylestern
BR9612505A (pt) 1996-02-21 1999-07-20 Du Pont Plocesso para produção de fosgênio
DE19606384A1 (de) 1996-02-21 1997-08-28 Bayer Ag Verfahren zur kontinuierlichen Herstellung von Arylcarbonaten
EP0912443B1 (en) 1996-06-28 2001-09-19 E.I. Du Pont De Nemours And Company Phosgene manufacturing process
WO1998028227A1 (en) 1996-12-20 1998-07-02 E.I. Du Pont De Nemours And Company Phosgene manufacturing process
US6852667B2 (en) 1998-02-16 2005-02-08 Sumitomo Chemical Company Limited Process for producing chlorine
DE19848668A1 (de) 1998-10-22 2000-04-27 Bayer Ag Tetrachlorkohlenstoffarmes Phosgen
DE19909340A1 (de) 1999-03-03 2000-09-07 Basf Ag Rohrbündelreaktor mit gestuftem Innendurchmesser
DE19916856A1 (de) 1999-04-14 1999-09-23 Eckert Gmbh Dr Verfahren zur Herstellung von Carbonyldichlorid aus Chlor und Kohlenmonoxid
WO2001040352A1 (en) 1999-12-03 2001-06-07 Teijin Limited Aromatic polycarbonate, process for producing the same, and molded article
EP1112997B1 (en) 1999-12-28 2009-05-13 Mitsubishi Chemical Corporation Process for producing diaryl carbonate
DE10063297A1 (de) 2000-12-19 2002-06-20 Bayer Ag Kontinuierliches Verfahren zur Herstellung von Kohlensäurediarylester
DE10063296A1 (de) 2000-12-19 2002-06-20 Bayer Ag Verfahren zur Herstellung von Kohlensäurediarylester
DE10063869A1 (de) 2000-12-21 2002-06-27 Bayer Ag Kontinuierliches Verfahren zur Herstellung von Kohlensäurediarylester
EP1234845B1 (en) 2001-02-26 2008-11-12 Mitsubishi Chemical Corporation Process for producing diphenyl carbonate and process for producing aromatic polycarbonates
US7096931B2 (en) * 2001-06-08 2006-08-29 Exxonmobil Research And Engineering Company Increased heat exchange in two or three phase slurry
GB0306179D0 (en) 2003-03-18 2003-04-23 Imp College Innovations Ltd Piping
DE10332697A1 (de) 2003-07-18 2005-02-03 Bayer Materialscience Ag Methode zur Abtrennung von metallischen Katalysatorbestandteilen aus Reaktionsmischungen der Herstellung aromatischer Carbonate
US7250530B2 (en) 2003-07-30 2007-07-31 General Electric Company Processes and systems for making phosgene
BRPI0514564B1 (pt) 2004-08-25 2015-06-09 Asahi Kasei Chemicals Corp Processo industrial para produção de carbonato de difenila de pureza elevada e aparelho para produzir carbonato de difenila de pureza elevada
DE102004041777A1 (de) 2004-08-28 2006-03-02 Bayer Materialscience Ag Verfahren und Vorrichtung zur Herstellung von Phosgen
US7081597B2 (en) 2004-09-03 2006-07-25 The Esab Group, Inc. Electrode and electrode holder with threaded connection
JP4292214B2 (ja) 2004-10-14 2009-07-08 旭化成ケミカルズ株式会社 高純度ジアリールカーボネートの製造方法
DE102006022629A1 (de) 2006-05-12 2007-11-15 Spörl KG Wärmetauschvorrichtung für einen Wärmeaustausch zwischen Medien und Webstruktur
JP4765073B2 (ja) * 2006-07-05 2011-09-07 国立大学法人広島大学 リグノセルロースの水熱加水分解方法
DE102007057462A1 (de) 2007-11-29 2009-06-10 Bayer Materialscience Ag Verfahren zur Herstellung von Phosgen mit reduzierter CO-Emission
DE102007058701A1 (de) 2007-12-06 2009-06-10 Bayer Materialscience Ag Verfahren zur Herstellung von Diarylcarbonat
CN102348639A (zh) 2009-03-11 2012-02-08 巴斯夫欧洲公司 制备光气的方法
JP2011104507A (ja) * 2009-11-17 2011-06-02 Sumitomo Chemical Co Ltd 多管式反応器用伝熱管
JP2011106728A (ja) * 2009-11-17 2011-06-02 Sumitomo Chemical Co Ltd 多管式反応器用伝熱管
SG174715A1 (en) 2010-03-30 2011-10-28 Bayer Materialscience Ag Process for preparing diaryl carbonates and polycarbonates
WO2012076532A1 (en) 2010-12-08 2012-06-14 Shell Internationale Research Maatschappij B.V. Process for purifying aryl group containing carbonates
EP2591851A1 (en) * 2011-11-08 2013-05-15 Alfa Laval Corporate AB A tube module
WO2015013655A1 (en) 2013-07-26 2015-01-29 Sabic Innovative Plastics Ip B.V. Method and apparatus for producing high purity phosgene
EP3024782B1 (en) 2013-07-26 2019-06-12 SABIC Global Technologies B.V. Method and apparatus for producing high purity phosgene
EP3024813B1 (en) 2014-02-04 2017-03-29 SABIC Global Technologies B.V. Method for producing carbonates

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6399823B1 (en) * 2001-04-30 2002-06-04 General Electric Company Method for producing phosgene
CN1638856A (zh) * 2002-02-27 2005-07-13 巴斯福股份公司 用于生产光气的反应器和方法
CN101027122A (zh) * 2004-09-27 2007-08-29 住友化学株式会社 接触气相反应用多管式反应装置

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU228612U1 (ru) * 2024-06-19 2024-09-05 Общество с ограниченной ответственностью "ФАСТ ИНЖИНИРИНГ" Каталитический реактор радиально-спирального типа

Also Published As

Publication number Publication date
KR101859207B1 (ko) 2018-05-18
KR20160118228A (ko) 2016-10-11
US20170001943A1 (en) 2017-01-05
JP6316446B2 (ja) 2018-04-25
EP3102558A2 (en) 2016-12-14
US9695106B2 (en) 2017-07-04
EP3102558B1 (en) 2019-07-03
CN105980346A (zh) 2016-09-28
WO2015119981A3 (en) 2015-12-03
JP2017509598A (ja) 2017-04-06
WO2015119981A2 (en) 2015-08-13

Similar Documents

Publication Publication Date Title
CN105980346B (zh) 生产碳酸酯的方法
JP6286057B2 (ja) カーボネートを生成する方法
CN100335528C (zh) 通过熔融酯交换工艺连续生产聚碳酸酯的方法
EP3024782B1 (en) Method and apparatus for producing high purity phosgene
CN105408250B (zh) 用于生产高纯光气的方法和装置
JP5795975B2 (ja) ポリカーボネートの連続製造方法
WO2000058259A1 (en) Method and apparatus for preparing monofunctional aromatic haloformates
US6103855A (en) Batch process for the production of polycarbonate by interfacial polymerization
CN1309699C (zh) 用于制备碳酸二烷酯的方法和装置
CN119365515A (zh) 聚碳酸酯的制造方法、二羟基化合物的回收方法和聚碳酸酯的制造装置

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant