CN105961453A - Botanical mosquito repellent for repelling culex quinquefasciatus, preparation and application of botanical mosquito repellent - Google Patents
Botanical mosquito repellent for repelling culex quinquefasciatus, preparation and application of botanical mosquito repellent Download PDFInfo
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- CN105961453A CN105961453A CN201610361191.3A CN201610361191A CN105961453A CN 105961453 A CN105961453 A CN 105961453A CN 201610361191 A CN201610361191 A CN 201610361191A CN 105961453 A CN105961453 A CN 105961453A
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- anophelifuge
- vegetalitas
- repellent
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/36—Rutaceae [Rue family], e.g. lime, orange, lemon, corktree or pricklyash
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- Engineering & Computer Science (AREA)
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- Agronomy & Crop Science (AREA)
- Biotechnology (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Mycology (AREA)
- Plant Pathology (AREA)
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- Wood Science & Technology (AREA)
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Abstract
The invention relates to a botanical mosquito repellent for repelling culex quinquefasciatus, preparation and application of the botanical mosquito repellent. Main active substances of the mosquito repellent include a composition prepared from, by mass, 40-70 parts of zanthoxylum beecheyanum var. alatum essential oil, 15-30 parts of western red cedar essential oil and 10-30 parts of lantana camara essential oil. The preparing method of the botanical mosquito repellent includes the steps that all the raw materials are mixed evenly, emulsified and homogenized, and the botanical mosquito repellent is obtained. The botanical mosquito repellent has a remarkable repelling effect on culex quinquefasciatus inside a room, and is safe and nontoxic to human and livestock, and free of pollution to the environment.
Description
Technical field
The present invention relates to vegetalitas anophelifuge and the application thereof of a kind of repellent Culex quinquefasciatus, belong to botanical pesticide technology neck
Territory.
Background technology
Culex quinquefasciatus (Culex quinquefasciatus) it being distributed in south China each province and city, north and south has a common boundary
Jiangsu, Zhejiang, Anhui, Hubei, Shaanxi etc. save also distribution, typically in indoor activity, is indoor topmost mosquito of sucking blood.Remove
Outside the orthobiosis of the harassing and wrecking mankind, being also a kind of important viral vector, it can propagate multiple disease, such as Filaria philippinensis simultaneously
Mosquito matchmaker's infectious disease such as disease, dengue fever.
The main diethyltoluamide of mosquito component (DEET), pyrethroid etc. in the anophelifuge commonly used at present, these chemistry
Although repellant is effective, efficiency time is long, but exists human body toxic side effect, has the drawbacks such as pollution to environment.And plant
The anophelifuge of physical property has high-efficiency low-toxicity or feature nontoxic, environment amenable, and plants essential oil complex chemical composition, to mosquito
Mechanism of action is unique, and often the same plants essential oil repellent effect significant difference to different mosquitoes, therefore, filters out cause
Tired culex has the plants essential oil of notable repellent activity, develops the vegetalitas repellant of safety and environmental protection, to protection human health
And the environment tool of existence is of great significance.
Summary of the invention
It is an object of the invention to provide the vegetalitas anophelifuge of a kind of side effect environmentally safe non-toxic to humans, be used for
Repellent Culex quinquefasciatus, has significant repellent effect.
The technical scheme is that the vegetalitas anophelifuge of a kind of repellent Culex quinquefasciatus, the chief active of this anophelifuge
Thing is: touch essential oil, arborvitae quintessence oil and the compositions of Folium Lantanae Camarae quintessence oil containing one, the mass parts content of each component in said composition
It is to touch 40 ~ 70 parts of essential oil, arborvitae quintessence oil 15 ~ 30 parts and Folium Lantanae Camarae quintessence oil 10 ~ 30 parts.
Described one touch essential oil, arborvitae quintessence oil and Folium Lantanae Camarae quintessence oil be by steam distillation respectively from one touch Herba Pelargonii Graveolentis,
Arborvitae branch and leaf and the wounded in the battle branch and leaf of Folium Lantanae Camarae extract and obtains.
Further, described compositions also includes solvent, and solvent accounts for the 5 ~ 10% of described composition total weight.
In a specific embodiment, this anophelifuge is cream, and described compositions accounts for the mass percentage content of this cream
It is 60 ~ 85%.Mosquito-dispelling cream also includes emulsifying agent 1～4%, wetting agent 1～8%, moisturizing agent 10～20%, counter-stimulus 0.1～1%, pH
Regulator 0.1～0.5%, preservative 0.01～0.05% and odorant 0.1～0.5%, remaining is distilled water, adds up to 100%, to account for
The mass percent of this cream.
In a specific embodiment, this anophelifuge is spray, and described compositions accounts for the mass percent of this spray
Content is 45 ~ 65%.Spray also include emulsifying agent 1～5%, wetting agent 1～8%, moisturizing agent 1～4%, counter-stimulus 0.1～1%,
PH adjusting agent 0.1～0.6%, preservative 0.01～0.1% and odorant 0.1～0.5%, remaining is distilled water, adds up to 100%, with
Account for the mass percent of this spray.
Described emulsifying agent is the one in polyethenoxy ether class, carboxylate, sulfate, polyoxypropylene ethers and sulfonate
More than or, wetting agent is one or more in polyhydric alcohol, hyaluronic acid and aminoacid, described moisturizing agent be isomery dodecane,
One or more in higher alcohol, vegetable and animals oils and synthetic ester oil, described counter-stimulus is α-bisabolol, described pH adjusting agent
For triethanolamine or citric acid.
The preparation method of above-mentioned vegetalitas anophelifuge, is each raw material mix homogeneously, emulsifying, homogenizing to be made.
The vegetalitas repellant of the present invention, is touched, by one, the compositions that essential oil, arborvitae quintessence oil and Folium Lantanae Camarae quintessence oil form, joins
Enter auxiliary agent and make mosquito-dispelling cream, Mosquito-repellant spray, in indoor, Culex quinquefasciatus is had significant repellent effect, and to person poultry safety without
Poison, environment is not polluted.Up to now there is not yet by one touch essential oil, arborvitae quintessence oil and Folium Lantanae Camarae quintessence oil combination make
Vegetalitas anophelifuge.
Detailed description of the invention
The vegetalitas anophelifuge chief active thing of the present invention is: touch essential oil, arborvitae quintessence oil and Folium Lantanae Camarae quintessence oil containing one
Compositions (following " vegetalitas mosquito repellent composition "), in said composition, the mass parts content of each component is to touch essential oil
40 ~ 70 parts, arborvitae quintessence oil 15 ~ 30 parts and Folium Lantanae Camarae quintessence oil 10 ~ 30 parts.Touch one respectively with dehydrated alcohol during preparation essential oil,
Arborvitae quintessence oil and Folium Lantanae Camarae quintessence oil dissolve, and then mix and get final product, and wherein dehydrated alcohol accounts for the 5 ~ 10% of mosquito repellent composition weight.
Described one touch essential oil by Rutaceae (Rutaceae) touch perfume (or spice) (Zanthoxylum beecheyanum)
Leaf obtains through steam distillation.Described arborvitae quintessence oil by Cupressaceae (Cupressaceae) arborvitae (Thuja sutchuenensis) branch and leaf steam distillation and obtain.Described Folium Lantanae Camarae quintessence oil is by Verenaceae (Verbenaceae)
Plant Folium Lantanae Camarae (Lantana camara) wounded in the battle branch and leaf steam distillation and obtain.Described steam distillation often uses
The distilling with water of rule.
As required, vegetalitas anophelifuge can be made the form such as cream or spray.
In a detailed description of the invention, mosquito-dispelling cream includes following component, and (following mass percent is with mosquito-dispelling cream generally
Benchmark): vegetalitas mosquito repellent composition 60 ~ 85%, emulsifying agent 1～4%, wetting agent 1～8%, moisturizing agent 10～20%, counter-stimulus
0.1～1%, pH adjusting agent 0.1～0.5%, preservative 0.01～0.05%, odorant 0.1～0.5%.
During preparation, above-mentioned raw materials is mixed in proportion, add to 100% with distilled water, carry out emulsifying, then homogenizing 5～8
Minute, i.e. it is prepared as mosquito-dispelling cream.Then sample the stability to preparation to detect with outward appearance, qualified rear packaging, get product.
In a detailed description of the invention, Mosquito-repellant spray includes following component, and (following mass percent is whole with spray
On the basis of body): vegetalitas mosquito repellent composition 45 ~ 65% of the present invention, emulsifying agent 1～5%, wetting agent 1～8%, moisturizing agent 1～4%,
Counter-stimulus 0.1～1%, PH regulator 0.1～0.6%, preservative 0.01～0.1%, odorant 0.1～0.5%, remaining be distillation
Water.
During manufacture, above-mentioned raw materials is mixed in proportion, add to 100% with distilled water, carry out emulsifying, then homogenizing 3～5
Min, is i.e. prepared as Mosquito-repellant spray.Then sample the stability to preparation to detect with outward appearance, qualified rear packaging, must become
Product.
The present invention is described further rather than limits the scope of the invention for following example.
Embodiment 1, the preparation of mosquito-dispelling cream and indoor repellent Culex quinquefasciatus experiment
Mosquito-dispelling cream is prepared by following methods: take mass percent be vegetalitas mosquito repellent composition 70% of the present invention, emulsifying agent 2%,
Wetting agent 7%, moisturizing agent 15%, counter-stimulus 0.5%, pH adjusting agent 0.25%, preservative 0.05%, odorant 0.2%.By above-mentioned former
Material mixes in proportion, and adds to 100% with distilled water, and suction emulsifying pot carries out emulsifying, then homogenizing 5～8 minutes, i.e. prepares
Become mosquito-dispelling cream, then sample the stability to preparation and detect with outward appearance, qualified rear packaging, get product.
The above vegetalitas mosquito repellent composition is touched essential oil mass percent 55%, arborvitae quintessence oil 20%, the five colors by one
Prunus mume (sieb.) sieb.et zucc. quintessence oil 20%, the ethanol of addition 5% dissolves and mixes.The above emulsifying agent is polyethenoxy ether class, and described moisturizing agent is
Synthetic ester oil, described aminoacid, described counter-stimulus is α-bisabolol, and described pH adjusting agent is citric acid.
(laboratory room is 4 m × 4m × 3 m, and temperature is 25 ° of C ± 2 ° C, and humidity is in laboratory conditions
70% ± 5%), with reference to National Standard of the People's Republic of China's " indoor harmacological effect evaluation/repellent of agriculture chemical registration hygienic insecticide
Agent GB/T 13917.9-2009 ", test repellent effect.Test at the mosquito cage (30 equipped with 100 Culex quinquefasciatus sprouted wings latter 3 days
Cm × 25, cm × 30 cm) in carry out, 4 volunteers by put on after both hands wash clean have at the back of the hand position a 4cm ×
The medical latex glove of 4 cm breach, (number that stops falling is more than 20 and is considered as to put his hand into the attack of mosquito cage 2 min test mosquito
Qualified, this person and this mosquito cage can be used for repellent experiment).During experiment, one hands is blank, and another hands is directly naked at the back of the hand
Mosquito-dispelling cream is smeared at dew position, and dosage used is 3 mg/cm2.Put his hand into mosquito cage 2 min after natural air drying to test, every 0.5
H tests once, continues to observing that first mosquito stops falling or attempting to bite, is considered as complete shielding failure.Experiment repetition 3
Secondary, experimental result takes the meansigma methods of experiment every time.Recording mosquito-dispelling cream to the 100% complete guard time meansigma methods of volunteer is
6.56 ± 0.15 h。
Embodiment 2, the preparation of Mosquito-repellant spray and indoor repellent experiment
The Mosquito-repellant spray of experiment is prepared by following methods: taking mass percent is vegetalitas mosquito repellent composition of the present invention
58%, emulsifying agent 5%, wetting agent 5%, moisturizing agent 2%, counter-stimulus 0.25%, pH adjusting agent 0.6%, preservative 0.05%, odorant
0.1%, remaining is distilled water.During manufacture, above-mentioned raw materials is mixed in proportion, add to 100% with distilled water, suction emulsifying pot
Carrying out emulsifying, then homogenizing 3～5 min, is i.e. prepared as Mosquito-repellant spray.Then sample the stability to preparation to carry out with outward appearance
Detection, qualified rear packaging, get product.
The above vegetalitas mosquito repellent composition is touched essential oil mass percent 55%, arborvitae quintessence oil 20%, the five colors by one
Prunus mume (sieb.) sieb.et zucc. quintessence oil 20%, the ethanol of addition 5% dissolves and mixes.The above emulsifying agent is polyethenoxy ether class, and described moisturizing agent is
Synthetic ester oil, described aminoacid, described counter-stimulus is α-bisabolol, and described pH adjusting agent is citric acid.
(laboratory room is 4 m × 3, m × 4 m, and temperature is 25 ° of C ± 2 ° C, and humidity is in laboratory conditions
70% ± 5%), with reference to National Standard of the People's Republic of China's " indoor harmacological effect evaluation/repellent of agriculture chemical registration hygienic insecticide
Agent GB/T 13917.9-2009 ", test repellent effect.Test at the mosquito cage (30 equipped with 100 Culex quinquefasciatus sprouted wings latter 3 days
Cm × 25, cm × 30 cm) in carry out, 4 volunteers by put on after both hands wash clean have at the back of the hand position a 4cm ×
The medical latex glove of 4cm breach, (number that stops falling is more than 20 and is considered as to put his hand into the attack of mosquito cage 2 min test mosquito
Qualified, this person and this mosquito cage can be used for repellent experiment).During experiment, one hands is blank, and another hands is directly naked at the back of the hand
Mosquito-dispelling cream is smeared at dew position, and dosage used is 3 mg/cm2.Put his hand into mosquito cage 2 min after natural air drying to test, every 0.5
H tests once, continues to observing that first mosquito stops falling or attempting to bite, is considered as complete shielding failure.Experiment repetition 3
Secondary, experimental result takes the meansigma methods of experiment every time.Record the Mosquito-repellant spray 100% complete guard time meansigma methods to volunteer
It is 4.75 ± 0.70 h.
Embodiment 3
Prepare mosquito-dispelling cream as described in Example 1, and test repellent effect.Except that each constituent content: vegetalitas anophelifuge
Agent compositions 60%, emulsifying agent 3%, wetting agent 3%, moisturizing agent 15%, counter-stimulus 0.3%, pH adjusting agent 0.3%, preservative
0.05%, odorant 0.3%.Vegetalitas mosquito repellent composition: one touches essential oil mass percent 40%, arborvitae quintessence oil 25%, the five colors
Prunus mume (sieb.) sieb.et zucc. quintessence oil 30%, ethanol 5%.Test result: the 100% complete guard time meansigma methods to volunteer is 4.93 ± 0.37 h.
By the method for the present embodiment, respectively with one touching essential oil, arborvitae quintessence oil, Folium Lantanae Camarae quintessence oil replace the present embodiment formula
In vegetalitas mosquito repellent composition, prepare three kinds of single dose quintessence oil mosquito-dispelling creams, and test repelling effect.The test result obtained
It is: one touches fragrant mosquito-dispelling cream, arborvitae mosquito-dispelling cream, Folium Lantanae Camarae mosquito-dispelling cream to the 100% complete guard time meansigma methods of volunteer respectively
2.25 ± 0.19 h、 3.26 ± 0.19 h、3.03 ± 0.23 h。
Test result shows, vegetalitas mosquito repellent composition of the present invention the mosquito-dispelling cream prepared is than using in compositions respectively
Mosquito-dispelling cream prepared by any single quintessence oil, repellent effect is remarkably reinforced.
Embodiment 4
Prepare Mosquito-repellant spray as described in Example 2, and test repellent effect.Except that each constituent content: vegetalitas
Mosquito repellent composition 45%, emulsifying agent 3%, wetting agent 2%, moisturizing agent 3%, counter-stimulus 0.5%, pH adjusting agent 0.3%, preservative
0.05%, odorant 0.2%.Vegetalitas mosquito repellent composition: one touches essential oil mass percent 70%, arborvitae quintessence oil 15%, the five colors
Prunus mume (sieb.) sieb.et zucc. quintessence oil 10%, ethanol 5%.
Test result: the 100% complete guard time meansigma methods to volunteer is 3.87 ± 0.18 h.
By the method for the present embodiment, respectively with one touching essential oil, arborvitae quintessence oil, Folium Lantanae Camarae quintessence oil replace the present embodiment formula
In vegetalitas mosquito repellent composition, prepare three kinds of single dose quintessence oil Mosquito-repellant spray, and test repelling effect.The test obtained
Result is: one touch fragrant Mosquito-repellant spray, arborvitae Mosquito-repellant spray, Folium Lantanae Camarae Mosquito-repellant spray are protected completely to the 100% of volunteer
Time average is 2.19 ± 0.07 h, 3.06 ± 0.09 h, 2.33 ± 0.14 h.
Test result shows, vegetalitas mosquito repellent composition of the present invention the Mosquito-repellant spray prepared is than using in compositions respectively
Mosquito-repellant spray prepared by any single quintessence oil, repellent effect is remarkably reinforced.
The summary present invention:
Through the repetition test of inventor, find to touch essential oil, arborvitae quintessence oil and Folium Lantanae Camarae quintessence oil by one multiple according to a certain percentage
Join the compositions obtained, Culex quinquefasciatus is had significant repellent action.It is individually present in three vegetable oil that the present invention selects
Polytype repellency compounds, as one touches in essential oil containing limonene, myrcene, caryophyllene etc.；Arborvitae quintessence oil contains
There are elemene, cedrol, thujene, chamigrene etc.；Folium Lantanae Camarae quintessence oil contains alpha-terpineol, linalool, cineole, Isosorbide-5-Nitrae-Camphor tree
Alkene, myrcene etc.；Plants essential oil complex chemical composition, unique to the repellent action mechanism of housefly, these three plants essential oil
After mixture, pharmacologically mutually promote between active component.Vegetalitas mosquito repellent composition of the present invention is nontoxic degradable, uses simultaneously
Auxiliary agent be all environment-friend auxiliaries, safe to the human body nontoxic environmentally friendly, and preparation method is simple, is easy to implement.
Claims (10)
1. the vegetalitas anophelifuge of a repellent Culex quinquefasciatus, it is characterised in that the chief active thing of this anophelifuge is: containing
Touching essential oil, arborvitae quintessence oil and the compositions of Folium Lantanae Camarae quintessence oil, in said composition, the mass parts content of each component is to touch essence
Oil 40 ~ 70 parts, arborvitae quintessence oil 15 ~ 30 parts and Folium Lantanae Camarae quintessence oil 10 ~ 30 parts.
The vegetalitas anophelifuge of repellent Culex quinquefasciatus the most according to claim 1, it is characterised in that described one touch essential oil,
Arborvitae quintessence oil and Folium Lantanae Camarae quintessence oil are to touch, from one, the branch that Herba Pelargonii Graveolentis, arborvitae branch and leaf and Folium Lantanae Camarae are wounded in the battle respectively by steam distillation
Leaf extracts and obtains.
The vegetalitas anophelifuge of repellent Culex quinquefasciatus the most according to claim 1, it is characterised in that described compositions is also wrapped
Including solvent, solvent accounts for the 5 ~ 10% of described composition total weight.
4. according to the vegetalitas anophelifuge of the repellent Culex quinquefasciatus one of claim 1 ~ 3 Suo Shu, it is characterised in that this anophelifuge
For cream, it is 60 ~ 85% that described compositions accounts for the mass percentage content of this cream.
The vegetalitas anophelifuge of repellent Culex quinquefasciatus the most according to claim 4, it is characterised in that mosquito-dispelling cream also includes breast
Agent 1～4%, wetting agent 1～8%, moisturizing agent 10～20%, counter-stimulus 0.1～1%, pH adjusting agent 0.1～0.5%, preservative
0.01～0.05% and odorant 0.1～0.5%, remaining is distilled water, adds up to 100%, to account for the mass percent of this cream.
6. according to the vegetalitas anophelifuge of the repellent Culex quinquefasciatus one of claim 1 ~ 3 Suo Shu, it is characterised in that this anophelifuge
For spray, it is 45 ~ 65% that described compositions accounts for the mass percentage content of this spray.
The vegetalitas anophelifuge of repellent Culex quinquefasciatus the most according to claim 6, it is characterised in that spray also includes breast
Agent 1～5%, wetting agent 1～8%, moisturizing agent 1～4%, counter-stimulus 0.1～1%, pH adjusting agent 0.1～0.6%, preservative
0.01～0.1% and odorant 0.1～0.5%, remaining is distilled water, adds up to 100%, to account for the mass percent of this spray.
8. according to the vegetalitas anophelifuge of the repellent Culex quinquefasciatus described in claim 5 or 7, it is characterised in that described emulsifying agent
For one or more in polyethenoxy ether class, carboxylate, sulfate, polyoxypropylene ethers and sulfonate, wetting agent is polynary
One or more in alcohol, hyaluronic acid and aminoacid, described moisturizing agent is isomery dodecane, higher alcohol, vegetable and animals oils and conjunction
Become in oils and fats one or more, described counter-stimulus is α-bisabolol, and described pH adjusting agent is triethanolamine or citric acid.
9. the preparation method of vegetalitas anophelifuge described in a claim 1 ~ 8, it is characterised in that by each raw material mix homogeneously, breast
Change, homogenizing is made.
10. the application in indoor repellent Culex quinquefasciatus of the vegetalitas anophelifuge described in a claim 1 ~ 8.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610361191.3A CN105961453B (en) | 2016-05-27 | 2016-05-27 | A kind of vegetalitas culicifuge, preparation and its application of repellent Culex quinquefasciatus |
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| CN109090151A (en) * | 2018-08-17 | 2018-12-28 | 威宁县农景种植专业合作社 | A kind of Chinese prickly ash mosquito-repellent spray and preparation method thereof |
| CN111758723A (en) * | 2020-07-20 | 2020-10-13 | 成都彩虹电器（集团）股份有限公司 | Synergist for electric heating mosquito-repellent incense tablet and electric heating mosquito-repellent incense tablet |
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| CN101390525A (en) * | 2008-11-07 | 2009-03-25 | 中南林业科技大学 | Plant source mosquito driving and killing agent |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109090151A (en) * | 2018-08-17 | 2018-12-28 | 威宁县农景种植专业合作社 | A kind of Chinese prickly ash mosquito-repellent spray and preparation method thereof |
| CN111758723A (en) * | 2020-07-20 | 2020-10-13 | 成都彩虹电器（集团）股份有限公司 | Synergist for electric heating mosquito-repellent incense tablet and electric heating mosquito-repellent incense tablet |
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| CN105961453B (en) | 2018-07-24 |
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