CN108991032A - A kind of fly-killing agent and the preparation method and application thereof - Google Patents
A kind of fly-killing agent and the preparation method and application thereof Download PDFInfo
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- CN108991032A CN108991032A CN201811259092.XA CN201811259092A CN108991032A CN 108991032 A CN108991032 A CN 108991032A CN 201811259092 A CN201811259092 A CN 201811259092A CN 108991032 A CN108991032 A CN 108991032A
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- essential oil
- fly
- killing agent
- osmanthus
- hunan
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- 239000003139 biocide Substances 0.000 title claims abstract description 57
- 238000002360 preparation method Methods 0.000 title claims abstract description 24
- 239000000341 volatile oil Substances 0.000 claims abstract description 89
- 241000633855 Litsea pungens Species 0.000 claims abstract description 36
- 235000019082 Osmanthus Nutrition 0.000 claims abstract description 34
- 241000333181 Osmanthus Species 0.000 claims abstract description 34
- 239000000203 mixture Substances 0.000 claims abstract description 23
- 239000005871 repellent Substances 0.000 claims abstract description 17
- 230000002940 repellent Effects 0.000 claims abstract description 17
- 241000255925 Diptera Species 0.000 claims description 14
- 241000257159 Musca domestica Species 0.000 claims description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid group Chemical group C(CC(O)(C(=O)O)CC(=O)O)(=O)O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 9
- -1 sorbitan fatty acid ester Chemical class 0.000 claims description 9
- 238000001256 steam distillation Methods 0.000 claims description 9
- 239000004909 Moisturizer Substances 0.000 claims description 8
- 239000003963 antioxidant agent Substances 0.000 claims description 8
- 230000003078 antioxidant effect Effects 0.000 claims description 8
- 239000003995 emulsifying agent Substances 0.000 claims description 8
- 230000001333 moisturizer Effects 0.000 claims description 8
- 239000003755 preservative agent Substances 0.000 claims description 8
- 230000002335 preservative effect Effects 0.000 claims description 8
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 7
- 229930195729 fatty acid Natural products 0.000 claims description 7
- 239000000194 fatty acid Substances 0.000 claims description 7
- 239000003002 pH adjusting agent Substances 0.000 claims description 7
- 235000013399 edible fruits Nutrition 0.000 claims description 6
- OPLCSTZDXXUYDU-UHFFFAOYSA-N 2,4-dimethyl-6-tert-butylphenol Chemical compound CC1=CC(C)=C(O)C(C(C)(C)C)=C1 OPLCSTZDXXUYDU-UHFFFAOYSA-N 0.000 claims description 5
- 239000003795 chemical substances by application Substances 0.000 claims description 5
- BEFDCLMNVWHSGT-UHFFFAOYSA-N ethenylcyclopentane Chemical compound C=CC1CCCC1 BEFDCLMNVWHSGT-UHFFFAOYSA-N 0.000 claims description 5
- 239000004334 sorbic acid Substances 0.000 claims description 5
- 235000010199 sorbic acid Nutrition 0.000 claims description 5
- 229940075582 sorbic acid Drugs 0.000 claims description 5
- KIUKXJAPPMFGSW-DNGZLQJQSA-N (2S,3S,4S,5R,6R)-6-[(2S,3R,4R,5S,6R)-3-Acetamido-2-[(2S,3S,4R,5R,6R)-6-[(2R,3R,4R,5S,6R)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2-carboxylic acid Chemical compound CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 KIUKXJAPPMFGSW-DNGZLQJQSA-N 0.000 claims description 4
- 229920002674 hyaluronan Polymers 0.000 claims description 4
- 229960003160 hyaluronic acid Drugs 0.000 claims description 4
- 239000002904 solvent Substances 0.000 claims description 4
- 239000012153 distilled water Substances 0.000 claims description 3
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims description 2
- 150000001413 amino acids Chemical class 0.000 claims description 2
- 150000007942 carboxylates Chemical class 0.000 claims description 2
- OPGYRRGJRBEUFK-UHFFFAOYSA-L disodium;diacetate Chemical compound [Na+].[Na+].CC([O-])=O.CC([O-])=O OPGYRRGJRBEUFK-UHFFFAOYSA-L 0.000 claims description 2
- 150000002170 ethers Chemical class 0.000 claims description 2
- 239000006210 lotion Substances 0.000 claims description 2
- 239000003921 oil Substances 0.000 claims description 2
- 229920001451 polypropylene glycol Polymers 0.000 claims description 2
- 239000001632 sodium acetate Substances 0.000 claims description 2
- 235000017454 sodium diacetate Nutrition 0.000 claims description 2
- 150000005846 sugar alcohols Polymers 0.000 claims description 2
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims description 2
- JZODKRWQWUWGCD-UHFFFAOYSA-N 2,5-di-tert-butylbenzene-1,4-diol Chemical compound CC(C)(C)C1=CC(O)=C(C(C)(C)C)C=C1O JZODKRWQWUWGCD-UHFFFAOYSA-N 0.000 claims 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims 1
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims 1
- 239000011575 calcium Substances 0.000 claims 1
- 229910052791 calcium Inorganic materials 0.000 claims 1
- 235000001465 calcium Nutrition 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 19
- 241000196324 Embryophyta Species 0.000 abstract description 9
- 230000003000 nontoxic effect Effects 0.000 abstract description 9
- 231100000252 nontoxic Toxicity 0.000 abstract description 8
- 239000002994 raw material Substances 0.000 abstract description 3
- 230000008901 benefit Effects 0.000 abstract description 2
- 206010013663 drug dependence Diseases 0.000 abstract description 2
- 238000003912 environmental pollution Methods 0.000 abstract description 2
- 208000011117 substance-related disease Diseases 0.000 abstract description 2
- 230000000052 comparative effect Effects 0.000 description 9
- 239000002917 insecticide Substances 0.000 description 9
- 201000010099 disease Diseases 0.000 description 7
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 7
- 150000001875 compounds Chemical class 0.000 description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 5
- 229960000935 dehydrated alcohol Drugs 0.000 description 5
- 238000000034 method Methods 0.000 description 5
- 238000004945 emulsification Methods 0.000 description 4
- 235000013305 food Nutrition 0.000 description 4
- 238000002156 mixing Methods 0.000 description 4
- 239000000047 product Substances 0.000 description 4
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- 239000000839 emulsion Substances 0.000 description 3
- 206010008631 Cholera Diseases 0.000 description 2
- 244000131522 Citrus pyriformis Species 0.000 description 2
- 241001502121 Glossina brevipalpis Species 0.000 description 2
- 241000238631 Hexapoda Species 0.000 description 2
- 206010047700 Vomiting Diseases 0.000 description 2
- 239000011149 active material Substances 0.000 description 2
- 239000010692 aromatic oil Substances 0.000 description 2
- 230000005540 biological transmission Effects 0.000 description 2
- 238000004090 dissolution Methods 0.000 description 2
- 208000001848 dysentery Diseases 0.000 description 2
- 230000009347 mechanical transmission Effects 0.000 description 2
- DNIAPMSPPWPWGF-UHFFFAOYSA-N monopropylene glycol Natural products CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 2
- 244000052769 pathogen Species 0.000 description 2
- 239000002728 pyrethroid Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 230000002195 synergetic effect Effects 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- XRCRJFOGPCJKPF-UHFFFAOYSA-N 2-butylbenzene-1,4-diol Chemical compound CCCCC1=CC(O)=CC=C1O XRCRJFOGPCJKPF-UHFFFAOYSA-N 0.000 description 1
- 208000000230 African Trypanosomiasis Diseases 0.000 description 1
- 208000009079 Bronchial Spasm Diseases 0.000 description 1
- 206010006482 Bronchospasm Diseases 0.000 description 1
- BCZXFFBUYPCTSJ-UHFFFAOYSA-L Calcium propionate Chemical compound [Ca+2].CCC([O-])=O.CCC([O-])=O BCZXFFBUYPCTSJ-UHFFFAOYSA-L 0.000 description 1
- 241000837702 Cinnamomum pauciflorum Species 0.000 description 1
- 206010011224 Cough Diseases 0.000 description 1
- 206010059866 Drug resistance Diseases 0.000 description 1
- 208000000059 Dyspnea Diseases 0.000 description 1
- 206010013975 Dyspnoeas Diseases 0.000 description 1
- 241000104430 Elsholtzia rugulosa Species 0.000 description 1
- 241000588724 Escherichia coli Species 0.000 description 1
- 206010019233 Headaches Diseases 0.000 description 1
- 241000123728 Leptotrichia buccalis Species 0.000 description 1
- 241001081179 Litsea Species 0.000 description 1
- 235000012854 Litsea cubeba Nutrition 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 241000257226 Muscidae Species 0.000 description 1
- 241000187479 Mycobacterium tuberculosis Species 0.000 description 1
- LVDRREOUMKACNJ-BKMJKUGQSA-N N-[(2R,3S)-2-(4-chlorophenyl)-1-(1,4-dimethyl-2-oxoquinolin-7-yl)-6-oxopiperidin-3-yl]-2-methylpropane-1-sulfonamide Chemical compound CC(C)CS(=O)(=O)N[C@H]1CCC(=O)N([C@@H]1c1ccc(Cl)cc1)c1ccc2c(C)cc(=O)n(C)c2c1 LVDRREOUMKACNJ-BKMJKUGQSA-N 0.000 description 1
- 206010029350 Neurotoxicity Diseases 0.000 description 1
- 206010035664 Pneumonia Diseases 0.000 description 1
- 206010044221 Toxic encephalopathy Diseases 0.000 description 1
- 208000037386 Typhoid Diseases 0.000 description 1
- 244000273928 Zingiber officinale Species 0.000 description 1
- 235000006886 Zingiber officinale Nutrition 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 230000007059 acute toxicity Effects 0.000 description 1
- 231100000403 acute toxicity Toxicity 0.000 description 1
- 244000052616 bacterial pathogen Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- VEMKTZHHVJILDY-UXHICEINSA-N bioresmethrin Chemical compound CC1(C)[C@H](C=C(C)C)[C@H]1C(=O)OCC1=COC(CC=2C=CC=CC=2)=C1 VEMKTZHHVJILDY-UXHICEINSA-N 0.000 description 1
- 239000004330 calcium propionate Substances 0.000 description 1
- 235000010331 calcium propionate Nutrition 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- ZZVUWRFHKOJYTH-UHFFFAOYSA-N diphenhydramine Chemical compound C=1C=CC=CC=1C(OCCN(C)C)C1=CC=CC=C1 ZZVUWRFHKOJYTH-UHFFFAOYSA-N 0.000 description 1
- 238000005485 electric heating Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000029142 excretion Effects 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 210000001035 gastrointestinal tract Anatomy 0.000 description 1
- 231100000025 genetic toxicology Toxicity 0.000 description 1
- 230000001738 genotoxic effect Effects 0.000 description 1
- 235000008397 ginger Nutrition 0.000 description 1
- 231100000869 headache Toxicity 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 241000411851 herbal medicine Species 0.000 description 1
- 208000029080 human African trypanosomiasis Diseases 0.000 description 1
- 210000000987 immune system Anatomy 0.000 description 1
- 239000000077 insect repellent Substances 0.000 description 1
- 230000000749 insecticidal effect Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 244000144972 livestock Species 0.000 description 1
- 231100000053 low toxicity Toxicity 0.000 description 1
- 231100000189 neurotoxic Toxicity 0.000 description 1
- 230000002887 neurotoxic effect Effects 0.000 description 1
- 231100000228 neurotoxicity Toxicity 0.000 description 1
- 230000007135 neurotoxicity Effects 0.000 description 1
- 210000000056 organ Anatomy 0.000 description 1
- 230000003071 parasitic effect Effects 0.000 description 1
- 230000001717 pathogenic effect Effects 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- 230000001902 propagating effect Effects 0.000 description 1
- 230000005180 public health Effects 0.000 description 1
- 208000008128 pulmonary tuberculosis Diseases 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 208000023504 respiratory system disease Diseases 0.000 description 1
- 208000017520 skin disease Diseases 0.000 description 1
- 201000002612 sleeping sickness Diseases 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 201000002311 trypanosomiasis Diseases 0.000 description 1
- 201000008297 typhoid fever Diseases 0.000 description 1
- 230000008673 vomiting Effects 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/22—Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/24—Lauraceae [Laurel family], e.g. laurel, avocado, sassafras, cinnamon or camphor
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Agronomy & Crop Science (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of fly-killing agents and the preparation method and application thereof, its chief active object are as follows: sub- essential oil is pulled out containing Hunan Litsea pungens essential oil, open country and spends the composition of osmanthus essential oil less, the mass fraction of each component in the composition are as follows: 40~65 parts of Hunan Litsea pungens essential oil, open country pull out 20~35 parts of sub- essential oil and spend 15~30 parts of osmanthus essential oil less.Various plants source is used in the present invention and main active of the safe and non-toxic essential oil as fly-killing agent, make fly-killing agent obtained that there is advantage that is safe and non-toxic and being not likely to produce drug dependence.Single essential oil repellent effect is not significant, and the present invention is using Hunan Litsea pungens essential oil, the wild effect for pulling out sub- essential oil and spend the mutual synergy between the essential oil of osmanthus less, so that fly-killing agent obtained is more significant to the repellent effect of flies.And preparation process of the invention is simple, and primary raw material derives from plant, not can cause environmental pollution.
Description
Technical field
The invention belongs to botanical pesticide technology fields, and in particular to a kind of fly-killing agent and the preparation method and application thereof.
Background technique
Flies are insects relatively common during we live, can be mechanical since its body surface is with numerous hair on the neck and hair
It carries, transmitting multiple pathogens, has biggish harmfulness to our life.The harm of flies is in addition to harassing people, contaminated food
It outside, is more to propagate a variety of diseases and cause fly-blown.Flies spread the disease including mechanical transmission and biological transmission two
Kind mode, the disease of mechanical transmission are mainly that fly is expanded by stopping the activity such as falling, licking food, vomiting and excretion and propagating pathogen
Dissipate, the disease of propagation mainly include disease of digestive tract (such as dysentery, cholera), respiratory disease (such as pulmonary tuberculosis, pneumonia) and
Skin diseases；The disease of biological transmission mainly has tsetse fly (tsetse fly) that can propagate human body trypanosomiasis (sleeping sickness).And fly
Fly larvae can fly-blown caused by the tissue and organ of parasitic human body and animal.Housefly (Musca domestica L.) belongs to
In diptera: Muscidae, it is the most common flies during we live, is a kind of global public health insect, China various regions are extensive
Distribution, kitchen, food and drink, food processing factory etc. are its main playgrounds, it carries a large amount of pathogenic bacteria, as Escherichia coli,
Leptotrichia buccalis and mycobacterium tuberculosis etc. propagate a variety of diseases such as typhoid fever, dysentery, cholera, seriously threaten human health, harass
Human lives.
About flies control method there are many kinds of, the repellant and insecticide of flies are to use most effective side
Method.Currently, based on the chemical syntheses insecticide such as insecticidal pyrethroids of flies, but flies are to the anti-medicine of this insecticides
Property be in significant ascendant trend, and pyrethroid insectide is there are certain acute toxicity, can cause expiratory dyspnea, cough,
The symptoms such as bronchial spasm, nausea and vomiting, headache, more some researches show that pyrethroid insectide is neurotoxic substance, the mankind
Especially newborn, which is exposed to this insecticide, may generate Developmental neurotoxicity, genotoxicity and immune system toxicity.For solution
The certainly harm of chemical synthesis insecticides, researchers have developed the flies repellant and insecticide of plant source, compared to chemistry
Insecticides are synthesized, the repellant and insecticide of plant extracts preparation have certain repellent action to flies, and have
Have safety and low toxicity or it is nontoxic, be not easy the characteristics of making housefly develop drug resistance, but the repellant and insecticide kind of plant source at present
Class is less, and plant source is single, and the repellent effect of some plant sources is not significant.
Summary of the invention
The object of the present invention is to provide a kind of safe and non-toxic, significant fly-killing agent of repellent effect and preparation method thereof with answer
With.
The chief active object of this fly-killing agent of the present invention are as follows: pull out sub- essential oil containing Hunan Litsea pungens essential oil, open country and spend osmanthus less
The composition of essential oil, the mass fraction of each component in the composition are as follows: 40~65 parts of Hunan Litsea pungens essential oil, open country pull out sub- essential oil 20
~35 parts and less spend 15~30 parts of osmanthus essential oil.
Preferably, in the composition each component mass fraction are as follows: 50~60 parts of Hunan Litsea pungens essential oil, open country pull out sub- essence
25~30 parts of oil and less colored 20~25 parts of osmanthus essential oil.
It is by steam distillation respectively from lake that the Hunan Litsea pungens essential oil, open country, which pull out sub- essential oil and spend osmanthus essential oil less,
Southern Litsea pungens fruit, open country pull out sub- herb and spend to extract in the leaf of osmanthus less and obtain.
The composition be by each component by solvent dissolution be mixed to prepare, solvent account for composition gross mass 5~
10%.
The fly-killing agent, according to mass percent, including following component: composition 60~80%, emulsifier 1~5%,
Antioxidant 0.1~0.5%, preservative 0.1~1%, moisturizer 1~8%, pH adjusting agent 0.1~0.5%, remaining is distilled water,
Total 100%.
The fly-killing agent is lotion.
The emulsifier is sorbitan fatty acid ester, methyl glycol fatty acid ester, sulfonate, carboxylate, sulfate
With one of polyoxypropylene ethers or more；The antioxidant is bis- uncle of 2,4 dimethyl 6 tert butyl phenol and 2,5-
One or both of butylhydroquinone；The preservative is one of calcium propionate, sorbic acid and sodium Diacetate or more；
The moisturizer is one of hyaluronic acid, amino acid and polyalcohol or more；The pH adjusting agent is citric acid or three second
Hydramine.
A kind of preparation method of fly-killing agent, comprising the following steps: each component is uniformly mixed according to setting ratio, is emulsified,
After homogeneous, fly-killing agent is obtained.
The fly-killing agent is driving away the application in flies.
The application of repellant repellent housefly in various places.
The fruit of Litsea pungens can be used as medicine, thus the Litsea pungens essential oil as made from steam distillation is safe and non-toxic
Property.Open country is pulled out containing there are many aromatic oil in sub- complete stool, and branches and leaves can be used as Chinese herbal medicine, thus the open country as made from steam distillation
Pulling out sub- essential oil is also safety non-toxic.It spends aromatic-oil content in osmanthus high less, and its bark and root can also be used as medicine, thus passes through
Spending osmanthus essential oil made from steam distillation less is also safety non-toxic.
Beneficial effects of the present invention: using various plants source in the present invention and safe and non-toxic essential oil is as fly-killing agent
Main active makes fly-killing agent obtained have advantage that is safe and non-toxic and being not likely to produce drug dependence.Single essential oil repellent
Effect is not significant, and the present invention utilizes Hunan Litsea pungens essential oil, the wild mutual synergy pulled out between sub- essential oil and less colored osmanthus essential oil
Effect so that fly-killing agent obtained is more significant to the repellent effect of flies.And preparation process of the invention is simple, mainly
Raw material sources not can cause environmental pollution in plant.
Specific embodiment
Fly-killing agent chief active object of the invention are as follows: pull out sub- essential oil containing Hunan Litsea pungens essential oil, open country and spend osmanthus essential oil less
Composition (following " vegetalitas fly-killing agent compositions "), the mass parts content of each component in the composition are as follows: Hunan wood ginger
40~65 parts of sub- essential oil, open country pull out 20~35 parts of sub- essential oil and spend 15~30 parts of osmanthus essential oil less.It is right respectively with dehydrated alcohol when preparation
Hunan Litsea pungens essential oil, open country pull out sub- essential oil and spend the dissolution of osmanthus essential oil less, then mix to obtain the final product, wherein it is total to account for composition for dehydrated alcohol
The 5~10% of weight.
The Hunan Litsea pungens essential oil by Hunan Litsea pungens (Litsea hunanensis) fruit through steam distillation and
?.The open country pull out sub- essential oil by open country pull out son (Elsholtzia rugulosa) herb steam distillation and obtain.Described lacks
Flower osmanthus essential oil by less spend osmanthus (Cinnamomum pauciflorum) leaf steam distillation and obtain.The steam distillation is adopted
With conventional distilling with water.
In a specific embodiment, fly-killing agent include following components (following mass percents with fly-killing agent generally
Benchmark): composition 60~80%, emulsifier 1~5%, antioxidant 0.1~0.5%, preservative 0.1~1%, moisturizer 1~
8%, pH adjusting agent 0.1~0.5%, when preparation, mix in proportion above-mentioned raw materials, add to 100% with distilled water, carry out
Emulsification, then 5~8min of homogeneous, that is, be prepared into fly-killing agent.Then it samples and the stability of preparation is detected with appearance, it is qualified
After bottle to get finished product.
The present invention is described further for following embodiment, rather than limits the scope of the invention.
Embodiment 1
1) preparation of active compound
Hunan Litsea pungens fruit is obtained into Litsea pungens essential oil by distilling with water；It pulls out sub- herb and is obtained by distilling with water in open country
Pull out sub- essential oil in open country；Osmanthus leaf will be spent to obtain by distilling with water less and spend osmanthus essential oil less.
By Litsea pungens essential oil, open country pull out sub- essential oil, less spend osmanthus essential oil and dehydrated alcohol according to mass ratio be 50:25:20:5 into
Row mixing, after mixing to get active compound.
2) preparation of fly-killing agent
According to mass percent, by active compound 75%, emulsifier (methyl glycol fatty acid ester) 4%, antioxidant (2,4-
Dimethyl -6- tert-butyl phenol) 0.3%, preservative (sorbic acid) 0.4%, moisturizer (hyaluronic acid) 4%, pH adjusting agent (lemon
Lemon acid) 0.3% carry out it is uniformly mixed, then be pumped into emulsion pot in emulsified, after emulsification, to get drive after homogeneous 5min
Fly agent；It finally samples and the stability of preparation is detected with appearance, bottle after qualified to get fly-killing agent finished product.
3) the repellent effect test of fly-killing agent
Using Y-shaped olfactometer method, test under 3.0 μ L dosage, the repellent effect of above-mentioned fly-killing agent measures in 20min
The fly-killing agent is (92.5 ± 6.2) % to the scattering ratio of housefly.Referring to GB18418-2009 domestic sanitary desinsection articles electric heating liquid
Body mosquito-repellent incense standard, fumigates housefly with boxing method, measures the fly-killing agent to the killing time of 50(KT50) KT of housefly50Value for (13.7 ±
3.0) min, killing time of 50(KT50) is shorter, illustrates that the repellant is stronger to the stifling down effect of housefly.
Embodiment 2
1) preparation of active compound
Hunan Litsea pungens fruit is obtained into Litsea pungens essential oil by distilling with water；It pulls out sub- herb and is obtained by distilling with water in open country
Pull out sub- essential oil in open country；Osmanthus leaf will be spent to obtain by distilling with water less and spend osmanthus essential oil less.
By Litsea pungens essential oil, open country pull out sub- essential oil, less spend osmanthus essential oil and dehydrated alcohol according to mass ratio be 40:30:25:5 into
Row mixing, after mixing to get active compound.
2) preparation of fly-killing agent
According to mass percent, by active compound 60%, emulsifier (methyl glycol fatty acid ester) 4%, antioxidant (2,4-
Dimethyl -6- tert-butyl phenol) 0.3%, preservative (sorbic acid) 0.4%, moisturizer (hyaluronic acid) 4%, pH adjusting agent (lemon
Lemon acid) 0.3% carry out it is uniformly mixed, then be pumped into emulsion pot in emulsified, after emulsification, to get drive after homogeneous 5min
Fly agent；It finally samples and the stability of preparation is detected with appearance, bottle after qualified to get fly-killing agent finished product.
3) the repellent effect test of fly-killing agent
According to the test method of embodiment 1, repellent effect is tested are as follows: measure in 20min, fly-killing agent pair made from this implementation
The scattering ratio of housefly is (83.5 ± 3.4) %；Killing time of 50(KT50) KT50Value is (17.2 ± 2.1) min.
Comparative example 1
1) active material: Litsea pungens essential oil is that 95:5 is mixed according to mass percent with dehydrated alcohol, obtains activity
Substance.
2) preparation of fly-killing agent is compared: according to mass percent, by active material 60%, emulsifier (propylene glycol fatty acid
Ester) 4%, antioxidant (2,4 dimethyl 6 tert butyl phenol) 0.3%, preservative (sorbic acid) 0.4%, moisturizer (hyalomitome
Acid) 4%, pH adjusting agent (citric acid) 0.3% carry out it is uniformly mixed, then be pumped into emulsion pot in emulsified, after emulsification,
To get Litsea pungens essential oil fly-killing agent after homogeneous 5min；It finally samples and the stability of preparation is detected with appearance, filled after qualified
Bottle is to get Litsea pungens essential oil fly-killing agent finished product.
Comparative example 2
It changes the Litsea pungens essential oil in comparative example 1 into open country and pulls out sub- essential oil, other conditions are constant, obtain open country and pull out sub- essential oil drive fly
Agent.
Comparative example 3
Change the Litsea pungens essential oil in comparative example 1 into few colored osmanthus essential oil, other conditions are constant, obtain and spend osmanthus essential oil to drive fly less
Agent.
Sub- essential oil fly-killing agent is pulled out to the Litsea pungens essential oil fly-killing agent of comparative example 1, comparative example 2 and comparative example 3 preparation, open country respectively
It is tested with the repellent effect of few colored osmanthus essential oil fly-killing agent, test result is as follows:
Litsea pungens essential oil fly-killing agent in 20min is measured, sub- essential oil fly-killing agent is pulled out in open country and spends essential oil fly-killing agent in osmanthus to housefly less
Scattering ratio be respectively (56.5 ± 3.7) %, (45.5 ± 3.8) %, (28.5 ± 2.4) %.Litsea pungens essential oil fly-killing agent, open country
It pulls out sub- essential oil fly-killing agent and spends essential oil fly-killing agent in osmanthus to the killing time of 50(KT50) KT of housefly less50Value is respectively (24.2 ± 3.0)
min、(27.2±3.4)min、(30.5±4.0)min。
Compared with Example 2 compared with, its repellent of fly-killing agent and down effect of single essential oil preparation obviously weaken in comparative example,
Illustrate Hunan Litsea pungens, open country pull out it is sub, spend osmanthus essential oil mixture less after, synergistic effect is had between each other, so that its repellent
Significant effect increases.
Summarize the present invention:
By the repetition test of inventor, Hunan Litsea pungens essential oil, open country are pulled out sub- essential oil and spend osmanthus essential oil by one less by discovery
The composition that fixed ratio compounds has significant repellent and knockdown effect to housefly.After three kinds of plants essential oil mixtures, tool
There is significant synergistic function.For this vegetalitas housefly repellant to safety of human and livestock, preparation method is simple, is easy to implement.
Claims (10)
1. a kind of fly-killing agent, which is characterized in that its chief active object are as follows: pull out sub- essential oil containing Hunan Litsea pungens essential oil, open country and lack
The composition of osmanthus essential oil is spent, the mass fraction of each component in the composition are as follows: 40~65 parts of Hunan Litsea pungens essential oil, open country pull out sub- essence
20~35 parts of oil and less colored 15~30 parts of osmanthus essential oil.
2. fly-killing agent according to claim 1, which is characterized in that the mass fraction of each component in the composition are as follows: Hunan
50~60 parts of Litsea pungens essential oil, open country pull out 25~30 parts of sub- essential oil and spend 20~25 parts of osmanthus essential oil less.
3. fly-killing agent according to claim 1 or 2, which is characterized in that sub- essential oil is pulled out in the Hunan Litsea pungens essential oil, open country
It is to pull out sub- herb from Hunan Litsea pungens fruit, open country respectively by steam distillation and spend in the leaf of osmanthus less to extract with few colored osmanthus essential oil
It obtains.
4. fly-killing agent according to claim 1, which is characterized in that the composition is to be dissolved by each component by solvent
It is mixed to prepare, solvent accounts for the 5~10% of composition gross mass.
5. a kind of fly-killing agent according to claim 1, which is characterized in that according to mass percent, including following component: group
Object 60~80% is closed, emulsifier 1~5%, antioxidant 0.1~0.5%, preservative 0.1~1%, moisturizer 1~8%, pH are adjusted
Agent 0.1~0.5%, remaining is distilled water, adds up to 100%.
6. fly-killing agent according to claim 5, which is characterized in that the fly-killing agent is lotion.
7. fly-killing agent according to claim 5, which is characterized in that the emulsifier be sorbitan fatty acid ester,
One of methyl glycol fatty acid ester, sulfonate, carboxylate, sulfate and polyoxypropylene ethers or more；The antioxidant
For one or both of 2,4 dimethyl 6 tert butyl phenol and 2,5 di tert butyl hydroquinone；The preservative is third
One of sour calcium, sorbic acid and sodium Diacetate or more；The moisturizer is one in hyaluronic acid, amino acid and polyalcohol
Kind or more；The pH adjusting agent is citric acid or triethanolamine.
8. fly-killing agent according to claim 1 or 5, which is characterized in that a kind of preparation method of fly-killing agent, including following step
It is rapid: each component being uniformly mixed according to setting ratio, is emulsified, after homogeneous, fly-killing agent is obtained.
9. fly-killing agent is driving away the application in flies according to claim 1 or 5.
10. application of the repellant according to claim 9 in various places in repellent housefly.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201811259092.XA CN108991032B (en) | 2018-10-26 | 2018-10-26 | Fly repellent and preparation method and application thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109221281A (en) * | 2018-10-26 | 2019-01-18 | 中南林业科技大学 | A kind of Calliphoridae insect repellent and the preparation method and application thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109221281A (en) * | 2018-10-26 | 2019-01-18 | 中南林业科技大学 | A kind of Calliphoridae insect repellent and the preparation method and application thereof |
| CN109221281B (en) * | 2018-10-26 | 2020-08-04 | 中南林业科技大学 | Laricidae insect repellent as well as preparation method and application thereof |
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